KR20040013334A - Preparation and heating method of suicide using dried clay - Google Patents

Preparation and heating method of suicide using dried clay Download PDF

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KR20040013334A
KR20040013334A KR1020020046196A KR20020046196A KR20040013334A KR 20040013334 A KR20040013334 A KR 20040013334A KR 1020020046196 A KR1020020046196 A KR 1020020046196A KR 20020046196 A KR20020046196 A KR 20020046196A KR 20040013334 A KR20040013334 A KR 20040013334A
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salinity
salt
water
brine
clay
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KR1020020046196A
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Korean (ko)
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정낙추
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정낙추
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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D3/00Halides of sodium, potassium or alkali metals in general
    • C01D3/04Chlorides
    • C01D3/06Preparation by working up brines; seawater or spent lyes
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/40Table salts; Dietetic salt substitutes

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Fertilizers (AREA)
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Abstract

PURPOSE: A method for making boiled salt using dried mud is provided to obtain brine having high salinity and containing natural minerals regardless of season and weather and to save labor force. CONSTITUTION: The method for increasing the salinity of brine comprises the steps of introducing dried mud into filtering cloth and dipping it into brine having the salinity increased through three-step natural evaporating zones of mud flat. Then, the brine having the increased salinity is supplied to two-step heating containers. A high-quality boiled salt is precipitated from a first heating container at a high temperature, while the additional amount of the brine is introduced and the temperature is decreased. In addition, the brine is heated again in a second heating container at a low temperature so as to remove impurities and to discharge the precipitates.

Description

함토(말린 갯벌흙)을 이용한 자염(煮鹽)의 제조와 가열방법{omitted}Preparation and heating method of suicide using dried clay tidal soil

본 발명은 염도 10∼12% 함수에 조금(Neap tide) 때 5∼6일 동안 바닷물이 들어오지 않는 갯벌의 흙을 경운(耕耘)하여 수분을 증발시켜 만든 함토를, 증발지에서 염도를 높인 함수에 1차, 2차에 걸쳐 침적하여 갯벌에 함유된 각종 미네랄을 용출하는데 있으며, 또한 미네랄이 포함된 함수를 끓이는데 가마의 배치와 온도의 조절로 불순물 제거를 용이하게 하여 짠맛이 적고 감칠맛이 나는 전통소금 자염(煮鹽)의 맛을 살려내는데 있다.The present invention is a soil made by evaporating water by tilling soil of tidal-flat that does not enter seawater for 5-6 days when the salt is 10 ~ 12% hydride (Neap tide) It is used to elute various minerals contained in tidal flats by depositing it in the first and second stages.It also boils water containing minerals, and it is easy to remove impurities by adjusting the kiln's batch and controlling the temperature. It is to bring out the taste of salt salt.

종래의 소금 제조방법은 바닷물을 염전으로 유입하여 태양열에 의해 단계별로 수분을 증발시킨 후 소금을 만드는 천일제염법, 암염을 정제 가공하는 방법, 바닷물을 직접 끓여서 소금을 석출하는 방법, 바닷물을 전기 분해하여 염(NaCl)를 석출하는 이온교환막 정제염 등이 있다. 또한 말린 갯벌흙에 바닷물을 투과시켜 염도를 높인 함수를 끓이는 우리 선조들의 제염방법인 자염(煮鹽)이 있으나 생산이 중단된 상태이고 현재 국내 식염생산의 대부분은 천일제염법과 천일염을 재가공하는 방법이다.Conventional salt manufacturing method is a salt-washing method of making salt after evaporating water step by step by solar heat by introducing salt water into salt field, refining processing of salt salt, method of depositing salt by boiling sea water directly, electrolysis of sea water And an ion exchange membrane purified salt to precipitate a salt (NaCl). In addition, there is suicide, which is the decontamination method of our ancestors, which makes salt water to penetrate seawater through dried mud flat soil, but production is stopped, and most of the domestic salt production is reprocessing of sun salt and sun salt. .

위에 열거한 제염방법 중 자염과 천일염을 제외한 재가공염, 정제염 등은 NaCl농도는 90∼99% 이상 고순도이나 각종 미네랄 성분 함량이 미미하여 우수한 식염이라고는 할 수 없다.Among the decontamination methods listed above, reprocessing salts and purified salts except for salts and sun salts are not saline salts with a high NaCl concentration of 90-99% or more and a low content of various mineral components.

갯벌은 해양성 동,식물 사체(패류의 껍질 등)가 퇴적되어 생성된 각종미네랄(Ca. K. Ba. Mg 등)을 함유하고 있다. 이 미네랄은 함토와 함수를 만드는 과정에서 용해되어 소금과 같이 결정되기 때문에 자염을 섭취하였을 때 유용한 미네랄를 공급을 받을 수 있다. 또한 유용한 미네랄이 함유 된 저염도(低鹽度) 자염은 염분을 첨가하는 발효식품인 김치류, 장류를 만드는 과정에서 젓산균(乳酸醱酵菌)과 같은 발효미생물의 개체수(個體數)를 증가시키고 활발한 대사활동을 하게 하므로 발효식품의 맛을 높인다.Tidal-flats contain various minerals (Ca. K. Ba. Mg, etc.) produced by the deposition of marine animal and plant carcasses (shell shells, etc.). This mineral is dissolved in the process of making clay and hydride, so it is crystallized like salt, so you can get a useful mineral when you consume suicide. In addition, low-salt suicides containing useful minerals increase the number of fermented microorganisms such as lactic acid bacteria in the process of making kimchi, and fermented saline. Enhance the taste of fermented foods by active metabolic activity.

2001년 5월 20일에 충남 태안문화원에서는 50여년 만에 명맥이 끊어진 전통소금 자염의 제조방법 전 과정을 재현하는 행사를 갖었다. 삼국시대부터 1950년대 초까지 생산했던 자염은 우리나라의 전통소금이다. 서해안과 남해안 갯벌에서 생산한 자염의 제조방식은 지역마다 차이가 있지만 원리는 갯벌흙을 말려 함토를 만들고 그 함토에 바닷물을 투과시켜 염도를 높인 함수를 가마솥에 끓이는 방법이다. 이 소금의 특징은 염도가 낮으며 특히 갯벌에 함유된 각종 미네랄이 바닷물이 함토를 투과할 때 용출되어 함수에 용해되어 있다가 소금과 함께 결정되기 때문에 천일염보다 많은 미네랄 성분을 함유하고 있다.On May 20, 2001, Taean Cultural Center in Chungnam held an event to reproduce the entire process of manufacturing traditional salt suicide, which had been cut in 50 years. Suflame, which was produced from the Three Kingdoms to the early 1950s, is the traditional salt of Korea. The manufacturing method of suicide produced by the west and south coastal tidal flats varies from region to region, but the principle is to dry the mud flat soil to make a clay and permeate seawater through the clay to increase the salinity in the cauldron. This salt is characterized by low salinity and contains more minerals than natural salts, since various minerals contained in tidal-flat are eluted when dissolved in seawater and dissolved in water, and are determined together with salt.

위와 같은 특성을 간직한 양질의 자염을 만들기 위해서는 다음과 같은 문제점을 해결해야 한다The following problems must be solved in order to make high-quality suicide with these characteristics.

함수의 염도를 높이는 것은 매우 중요한 일이다. 바닷물의 염도는 평균 2.5% 정도이다. 조금 때 6∼7일 동안 만든 함토에 바닷물을 여과시켰을 때 함수의 염도는 7∼8% 정도 높아진다. 이는 본인이 주관했던 2001년∼2002년 태안문화원에서 재현한 전통소금 자염(煮鹽) 생산의 과정에서 얻은 결론이다. 함수의 염도와 소금의 생산량은 밀접한 관계가 있다.Increasing the salinity of a function is very important. The salinity of seawater averages about 2.5%. When the seawater is filtered through the soil made for 6-7 days, the salinity of hydride is increased by 7-8%. This is the conclusion obtained in the process of producing traditional salt suicide, which was reproduced at the Taean Cultural Center in 2001-2002. The salinity of hydride and the yield of salt are closely related.

갯벌에서 함토를 만드는데는 자연적인 조건을 극복하는 것과 어떻게 인력(人力)을 대체 하느냐가 관건이다. 함토는 양질의 갯벌에서 한 달(月)에 두 번인 조금(Necp tide) 동안(약 10∼12일) 만들어야 되는데 계절과 날씨에 의존하기 때문에 안정적인 함수 생산이 어렵다. 또한 갯벌은 조금 6∼7일(월2회) 동안을 제외하고는 하루에 2회 바닷물이 유입되어 무르기 때문에 대형기계를 이용한 쎄래질(경운耕耘)은 불가능한 일이다. 결국 인력이나 최소형 경운기를 이용해야 하는데 염도 7∼8%의 함수 1톤을 생산하려면 200톤의 함토가 필요하고 이 함토를 만들기 위한 인력은 대략 21명이 소요된다.The key to making a clay in tidal-flats is the overcoming of natural conditions and how to replace manpower. Hamtos have to be produced on Nep tide twice a month (about 10 to 12 days) on high quality tidal flats, and it is difficult to produce stable water because it depends on season and weather. In addition, since tidal flats are infiltrated by seawater twice a day except for 6-7 days (twice a month), it is impossible to wash the soil using large machines. Eventually, manpower or the smallest cultivator must be used. To produce 1 ton of salt with a salinity of 7-8%, 200 tons of clay are required, and the manpower for making this is about 21 people.

가열솥의 가열온도를 어떻게 조절하느냐에 따라 자염의 맛과 생산량이 좌우된다. 함수의 염도 비중 26∼30%에서 자염을 석출하고 남은 간수에는 소금으로 결정될 수 있는 많은 양의 염(NaCl)이 남는다. 이 염(NaCl)에는 쓴맛과 떫은맛을 내는 다량의 KCl MgCl2MgSO4등이 포함돼있는데 이 물질들을 간수에서 분리, 제거하므로써 자염의 질과 생산량을 높일 수 있다.How to adjust the heating temperature of the cooking pot depends on the taste and yield of suicide. The salinity of hydrate is precipitated at 26 to 30% of specific gravity, and the remaining amount of salt remains in the salt water (NaCl) which can be determined as salt. This salt (NaCl) contains a large amount of KCl MgCl 2 MgSO 4 , which has a bitter and astringent taste, and can be removed and removed from the brine to improve the quality and yield of suicide.

본 발명은 위와 같이 문제점을 해결하는 방법으로 함토를 함수에 침적하여 함수의 염도를 높이며 함토에 함유된 각종 미네랄을 용출시키는데 있다. 또한 함토 침적시 생기는 침전물은 단계별로 배출시키며 불순물은 가열솥의 가열온도 조절로 제거시켜 저염도의 미네랄이 풍부한 양질의 자염을 간단한 방법으로 만드는데 있다.The present invention is to increase the salinity of the water and to elute the various minerals contained in the soil by immersing the soil in the water in a way to solve the problem as described above. In addition, sediment produced during the deposition of the soil is discharged in stages, and impurities are removed by adjusting the heating temperature of the heating cooker to make a high-quality salt rich in low salinity in a simple way.

도 1은 자염 생산 전체 공정도.1 is a complete process diagram of suicide production.

도 2는 갯벌에서 함토를 말리는 공정도.Figure 2 is a process chart for drying the soil in the mudflat.

도 3은 갯벌에 만든 증발지에서 함수를 만드는 공정도.Figure 3 is a process for making a function in the evaporation paper made on the tidal flat.

도 4은 함토를 함수에 1차 침적하는 공정도.4 is a process diagram of first depositing clay into a function;

도 5는 함토를 함수에 2차 침적하는 공정과 가열솥의 배치 및 가열방법 공정도5 is a process of secondary depositing the soil in the water and the arrangement and heating method process diagram of the heating cooker

[도면 주요 부분에 대한 부호의 설명][Description of Symbols for Major Parts of Drawing]

1: 경운작업 공정 2: 파쇄작업 공정1: tillage process 2: crushing process

3: 반복작업 공정 4: 함토3: repetitive process 4: clay

5: 여과포에 함토 투입 공정 6: 함수저장고에 함토 운반 공정5: Filling the soil into the filter cloth 6: Transporting the soil into the water storage

7: 1차 증발지 8: 2차 증발지7: first evaporator 8: second evaporator

9: 3차 증발지 10: 증발지 함수저장고9: tertiary evaporator 10: evaporator reservoir

11: 해수 이송 펌프 12: 증발지 함수저장고 이송펌프11: seawater transfer pump 12: evaporation pond water reservoir transfer pump

13: 함토 침적 공정 14: 함수저장고에 함수 이송 공정13: Soil deposition process 14: Water transfer process to water storage

15: 함수 16: 함수 저장고15: Function 16: Function Storage

17: 여과포 18: 함수저장고 함수 이송 밸브17: filter cloth 18: water reservoir water transfer valve

19: 1차 침전물 배출 밸브 20: 2단계 가열솥19: Primary sediment discharge valve 20: Second stage heating cooker

21: 2차 침전물 배출 밸브 22: 1단계 가열솥 함수 이송 밸브21: Secondary sediment discharge valve 22: First stage heater cooker transfer valve

23: 부유(淨遊)불순물 24: 1단계 가열솥23: suspended impurity 24: first stage heating cooker

25: 3차 침전물 배출 밸브 26: 탈수 공정25: 3rd sediment discharge valve 26: dewatering process

27: 건조 공정 28: 포장 공정27: drying process 28: packaging process

29: 제품 출하29: shipping

먼저 도 1은, 자염을 만드는 과정의 전체 공정도이다. 자염을 만들기 위해서는 갯벌에서 함토(4)를 만들어 여과포에 담는 공정과, 증발지를 이용하여 해수의 염도를 높여 함수(15)를 만드는 공정, 함토(4)를 함수에 침적(13)하는 공정, 함수(15)를 끓여 자염을 석출하는 공정으로 나뉜다.First, FIG. 1 is an overall process diagram of the process of making suicide. To make suicide, the process of making clay (4) from the tidal flat and putting it in the filter cloth, making the seawater (15) by increasing the salinity of seawater using evaporation paper, and depositing the clay (4) in the water, It is divided into the process of boiling (15) to precipitate suicide.

도 2는, 함토(4)를 만드는 공정이다. 자염 생산을 위한 갯벌의 조건은 조금(小潮 Neap tide) 때인 13물,조금,1물,2물,3물,4물,5물까지 약 6∼7일 동안 바닷물이 유입되지 않는, 모래가 20% 정도 섞인 갯벌이어야 한다.2 is a step of making the clay 4. The condition of the tidal flat for the production of suicide is that the sand does not flow for about 6-7 days from 13 water, a little, 1 water, 2 water, 3 water, 4 water, 5 water, which is a little Neap tide. It should be mudflat mixed about%.

갯벌의 구조는 사리(大溯 Spring tide)가 끝난 13물(대객기), 조금, 동안에도 갯벌의 표면이 마르지 않기 때문에 소(牛)나 인력, 혹은 최소형 경운기로 경운(1)하여 건조시킨다. 갯벌의 물기가 걷히기 시작하면 흙덩이를 파쇄(2)하고 다시 경운(1)작업을 한다. 갯벌의 수분이 완전히 증발할 때까지 경운(1), 파쇄(2)작업을 반복(3)하여 만든 함토(4)를 여과포에 투입(5), 함수 저장고로 운반(6)한다.The structure of the tidal flats is tilled (1) with 13 small waters (large air planes), and the surface of the tidal flats does not dry out for a while. When the water on the tidal flat begins to break up, the soil block is crushed (2) and tilled (1). The soil (4) made by repeating the tillage (1) and crushing (2) operations (3) is introduced into the filter cloth (5) and transported to the brine reservoir (6) until the water in the tidal flat evaporates completely.

도 3은, 함수(15)를 만드는 공정이다. 조금(Neap tide)때 갯벌에 만든 증발지(7.8.9)의 함수저장고(16)에 사리(Spring tide)때 유입된 해수를 이송펌프(11)를 통해 1차 증발지(7)에 이송한다. 1차 증발지(7)의 해수는 조금 동안 단계별로 2차 증발지(8), 3차 증발지(9)로 이동시키며 수분을 증발시켜 염도 비중이 10∼12%가 됐을 때 증발지 함수저장고(10)로 모은 다음, 함수이송펌프(12)를 이용하여 함수저장고(16)로 이송한다.3 is a step of making the function 15. Neat tide is transferred to the primary evaporator (7) through the transfer pump (11) through the transfer pump (11) to the water reservoir (16) of the evaporator (7.8.9) made on the tidal flat. . The seawater of the primary evaporation basin (7) is moved to the secondary evaporation basin (8) and the tertiary evaporation basin (9) step by step for a while, and when the salinity ratio reaches 10 to 12% by evaporating moisture, the evaporation basin reservoir Gathered to (10), and then transferred to the water reservoir (16) using the water transfer pump (12).

도 4는,함토(4)를 함수(15)에 침적하는 공정이다. 도 1과 같은 공정을 거쳐 여과포(17)에 담은 함토를 함수저장고(16)로 이송한 함수(15)에 침적하는데, 이는 함수(15)의 염도를 2∼3% 높여 자염의 생산량을 증가시키며 함토(4)가 함유한 미네랄을 용출시켜 양질의 자염을 만들기 위해서다. 침적 방법은 함수(15)의 양 = 함토(4) × 2 의 비율로 96시간 이상 침적한다. 침적이 끝난 함토(4)는 갯벌에 환원하고 함수(15)는 이송밸브(18)를 통해 2단계 가열솥(20)으로 보낸다. 함수저장고(16) 밑바닥의 침전물은 배출밸브(19)를 통해 배출시킨다.4 is a step of depositing the clay 4 in the function 15. 1, the soil contained in the filter cloth (17) is deposited in the water function (15) transferred to the water storage (16), which increases the salinity of the water function (15) by 2-3%, increasing the yield of suicide. This is to make high-quality suicide by eluting minerals contained in the clay (4). The deposition method deposits more than 96 hours at the ratio of the amount of function 15 = clay (4) x 2. The immersed soil 4 is reduced to the tidal flat and the water 15 is sent to the second stage heating cooker 20 through the transfer valve (18). Sediment at the bottom of the water reservoir 16 is discharged through the discharge valve (19).

도 5는, 2차 함토(4)침적과 가열솥(20.24)의 가열 공정이다. 1차 침적(13)을 한 함수(15)는 2단계 가열솥(20)으로 이송하여 2차 침적과정을 거친다. 이 때의 침적비율은 함수(15)의 양 = 함토(4) × 5로 하고 침적 시간은 함수(15)의 온도가 50℃가 될 때까지 침적한다. 이는 함수(15) 온도 50℃에서 불순물이 부유하기 때문이다. 침적이 끝난 함수(15)는 이송밸브(22)를 통해 1단계 가열솥(24)으로 보내고 2단계 가열솥(20)의 침전물은 배출밸브(21)를 통해 배출시킨 후, 함수저장고(16)에서 1차 침적을 거친 함수(15)를 이송한다.5 is a process of depositing the secondary clay soil 4 and the heating pot 20.24. The function 15 having the primary deposition 13 is transferred to the second stage cooking pot 20 and undergoes the secondary deposition process. The deposition ratio at this time is the amount of the function 15 = clay (4) x 5, and the deposition time is deposited until the temperature of the function 15 reaches 50 ° C. This is because impurities are suspended at the water 15 temperature of 50 ° C. After the deposition function 15 is transferred to the first stage cooking pot 24 through the transfer valve 22, the precipitate of the second stage cooking pot 20 is discharged through the discharge valve 21, and the water storage reservoir 16 Transfers the function (15) after primary deposition.

1단계 가열솥(24)의 함수(15)를 가열하면 비중 염도 18%부터 불순물 CaSO4(23)이 부유하는데 함수(15)의 온도를 높여가며 불순물(23)은 여과포를 이용하여 제거하고, 2단계 가열솥(20)의 함수(15)를 추가로 이송한다. 위와 같은 공정을 2∼3차례 반복하여 연료 소모를 줄이면서 자염의 생산량을 증가시킨다.When heating the function 15 of the first stage cooker 24, the impurity CaSO 4 (23) is suspended from the specific gravity salinity of 18% and the temperature of the function 15 is increased, and the impurities 23 are removed using a filter cloth. Further transfer the function 15 of the two-stage heating cooker (20). This process is repeated two or three times to reduce the fuel consumption while increasing the yield of salt.

불순물(23) 제거 작업이 끝난 1단계 가열솥(24)의 함수(15)는 비중 염도가 26%부터 자염이 결정되기 시작하는데, 이 때 버너의 가열온도를 급속도로 낮추면 소금의 쓴맛과 떫은 맛을 내는 MgCl2MgSO4는 간수와 함께 침전되고 양질의 저염도 자염이 석출된다. 석출한 자염은 즉시 탈수(26), 건조(27), 포장(28) 공정을 거쳐 출하(29)한다.The function (15) of the first stage heating cooker (24) after the removal of the impurities (23) begins to determine the specific salt salinity from 26%. When the burner's heating temperature is lowered rapidly, the bitter and astringent taste of the salt is reduced. MgCl 2 MgSO 4 precipitates with the brine and precipitates a good low salinity salt. The precipitated magnetic salt is immediately shipped (29) through the dehydration (26), drying (27), and packaging (28) processes.

위에 기술한 바와 같이 본 발명은 경운으로 수분을 증발시켜 만든 함토(갯벌흙)를 함수에 침적하므로써 계절과 날씨에 구애받지 않고 천연 미네랄이 함유된 높은 염도의 함수를 안정적으로 확보할 수 있다. 이는 전통 자염 생산방식보다 노동력을 절감시키는 잇점이 있다. 또한 함토를 침적시키는 과정에서 생긴 침전물은 2단계에 걸쳐 완전 배출시키고, 가열솥의 가열 온도 조절로 끓는 함수 위로 떠오른 불순물을 제거하며 함수를 추가 투입하여 연료 소모를 줄이면서도 생산량을 높여 종전에 소량 생산되던 전통 자염을 대량 생산화 할 수 있다.As described above, the present invention can stably secure a high salinity function containing natural minerals regardless of seasons and weather by depositing a clay (mudflat soil) made by evaporating moisture with tillage to the function. This has the advantage of reducing labor than traditional suicide production. In addition, the sediment produced during the process of depositing the soil is completely discharged in two stages, and by controlling the heating temperature of the heating pot to remove impurities that rise above the boiling function, and additionally, the additional amount of water is used to reduce the fuel consumption and increase the production, thus producing a small amount previously. It is possible to mass-produce the traditional suicide.

Claims (4)

말린 함토를 여과포에 담아 갯벌의 3단계 자연 증발지에서 염도를 높인 해수에 1차 침적하여 함수의 염도 비중을 높이고 각종 미네랄을 용출 시키는 방법.A method of increasing the salinity of salt and eluting various minerals by first depositing dried clay in filter cloth and immersing it in seawater with high salinity at the three stage natural evaporation site of the tidal flat. 함수를 2단계 가열솥에 넣고 저은으로 가열하며 함토를 2차 침적하는 과정에서 소금이 결정되기 직전의 온도(50℃)까지 침적하여 불순물을 제거하는 방법.A method of removing impurities by placing a hydride in a two-stage heating cooker and heating it with low mercury and immersing it to a temperature (50 ° C) just before salt is determined in the second deposition of the clay. 고온에서 자염을 석출하는 1단계 가열솥과 저온에서 함토 침적과 수분 증발, 불순물 제거, 침전물 배출을 용이하게 할수 있는 2단계 가열솥의 배치 방법.A method of arranging a one-stage heating cooker that precipitates magnetic salts at high temperature and a two-stage heating cooker that can facilitate the deposition of soil, evaporation of water, removal of impurities, and discharge of sediment at low temperatures. 1단계 가열솥의 함수를 끓이는 과정에서 함수의 비중 염도가 26∼30%일 때 추가 함수를 투입하고 가열 온도를 급속히 낮춰 자염(NaCl)과 침전물(MgCl2,MgSO4)을 분리하여 질 좋은 자염을 석출하는 방법.When boiling water in the first stage cooker, when the specific gravity salinity of the water is 26-30%, add additional water and rapidly lower the heating temperature to separate nasal salt (NaCl) and sediment (MgCl 2 , MgSO 4 ) How to precipitate it.
KR1020020046196A 2002-08-05 2002-08-05 Preparation and heating method of suicide using dried clay KR20040013334A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100799880B1 (en) * 2004-07-12 2008-02-04 서희동 Producing method of salt and bittern from the tidal flate
KR100883513B1 (en) * 2007-05-28 2009-02-11 윤영성 Method for manufacturing boil down salt and bath salt by the salty-soil plate
WO2014066111A1 (en) * 2012-10-28 2014-05-01 Jae Hyun Lim Floating salt farm
KR20160078702A (en) * 2014-12-24 2016-07-05 맑고밝고따뜻한협동조합 manufacturing method of boiled salt

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR19990052499A (en) * 1997-12-13 1999-07-15 조인래 How to prepare alkaline salt
KR20020046267A (en) * 2002-05-25 2002-06-20 서영진 Manufacturing method of boil down salt and salty water by using energy of waste wood boiler
KR20030012055A (en) * 2001-07-30 2003-02-12 이영남 salt manufacturing method, and apparatus for the same
KR20030093668A (en) * 2002-06-04 2003-12-11 김규종 Salt from deep sea water in the East Sea

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR19990052499A (en) * 1997-12-13 1999-07-15 조인래 How to prepare alkaline salt
KR20030012055A (en) * 2001-07-30 2003-02-12 이영남 salt manufacturing method, and apparatus for the same
KR20020046267A (en) * 2002-05-25 2002-06-20 서영진 Manufacturing method of boil down salt and salty water by using energy of waste wood boiler
KR20030093668A (en) * 2002-06-04 2003-12-11 김규종 Salt from deep sea water in the East Sea

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100799880B1 (en) * 2004-07-12 2008-02-04 서희동 Producing method of salt and bittern from the tidal flate
KR100883513B1 (en) * 2007-05-28 2009-02-11 윤영성 Method for manufacturing boil down salt and bath salt by the salty-soil plate
WO2014066111A1 (en) * 2012-10-28 2014-05-01 Jae Hyun Lim Floating salt farm
KR20160078702A (en) * 2014-12-24 2016-07-05 맑고밝고따뜻한협동조합 manufacturing method of boiled salt

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