KR20030080286A - Manufacturing method of silver coating ceramic tile by high vacuum deposition - Google Patents
Manufacturing method of silver coating ceramic tile by high vacuum deposition Download PDFInfo
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- KR20030080286A KR20030080286A KR1020020018702A KR20020018702A KR20030080286A KR 20030080286 A KR20030080286 A KR 20030080286A KR 1020020018702 A KR1020020018702 A KR 1020020018702A KR 20020018702 A KR20020018702 A KR 20020018702A KR 20030080286 A KR20030080286 A KR 20030080286A
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- magnetic tile
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/88—Metals
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/4505—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements characterised by the method of application
- C04B41/4515—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements characterised by the method of application application under vacuum or reduced pressure
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- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04C—STRUCTURAL ELEMENTS; BUILDING MATERIALS
- E04C2/00—Building elements of relatively thin form for the construction of parts of buildings, e.g. sheet materials, slabs, or panels
- E04C2/02—Building elements of relatively thin form for the construction of parts of buildings, e.g. sheet materials, slabs, or panels characterised by specified materials
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2103/00—Function or property of ingredients for mortars, concrete or artificial stone
- C04B2103/60—Agents for protection against chemical, physical or biological attack
- C04B2103/67—Biocides
- C04B2103/69—Fungicides
Abstract
Description
본 발명은 고진공 증착법에 의한 은코팅 자기 타일 제조방법에 관한 것이다. 더욱 상세하게는, 진공 증착(vacuum deposition)방법을 이용하여 건축 마감재로 사용되는 자기 타일(ceramic tile)의 표면에 은코팅막을 형성하는 것으로서, 진공 탱크 안에 은 박판과 자기 타일을 넣은 후 은의 용융 온도까지 가열함으로써 은 입자가 자기 타일의 표면에 흡착되어 얻어지는 고진공 증착법에 의한 은코팅 자기 타일 제조방법에 관한 것이다.The present invention relates to a method of manufacturing silver coated magnetic tiles by high vacuum deposition. More specifically, a silver coating film is formed on the surface of a ceramic tile used as a building finishing material by using a vacuum deposition method, and the silver melting temperature of the silver plate and the magnetic tile in the vacuum tank are placed. The present invention relates to a method for producing a silver coated magnetic tile by a high vacuum deposition method in which silver particles are adsorbed onto the surface of a magnetic tile by heating to.
일반적으로, 진공 증착은 금속 또는 비금속의 작은 조각을 진공 탱크 속에서 가열하여 그 증기를 물체면에 부착시키는 일을 말한다. 특히, 진공 상태에 있는 탱크 속에 피복될 물체와 그 표면에 부착시키려는 금속 등의 입자를 넣어 둔 다음 히터에 전류를 흘려서 가열함으로써 그 금속입자를 증발시켜 차가운 물체 표면에 응축해서 부착하는 것을 이용하여 표피를 붙이는 방식이다. 이러한 진공 증착은 모든 물품에 적용될 수 있다는 것이 특색이며, 천에 알루미늄을 붙이거나 플라스틱에 은을 붙일 수도 있어 물체에 박막을 입히는 코팅 과정에서 널리 사용된다.In general, vacuum deposition refers to heating small pieces of metal or nonmetal in a vacuum tank to attach the vapor to an object surface. In particular, the surface of the skin is deposited by placing an object to be coated in the vacuum tank and particles such as a metal to be attached to the surface thereof, and then heating the current by flowing a heater to condense and attach the metal particles to the surface of a cold object. This is how you attach. This vacuum deposition is characterized by being applicable to all articles and is widely used in the coating process in which aluminum may be attached to the cloth or silver may be attached to the plastic to coat the object with a thin film.
또한, 금속 은(Ag)은 항균 특성을 가지고 있으며, 그 은의 효능은 다음과 같다. 은(Ag)으로부터 방출되는 은이온(Ag+)은 그 전기적 부하에 의해 970여 가지의 세균을 인체에 전혀 독성을 주는 일이 없이 6분 이내에 박멸시켜 병을 치료하는 것으로 이미 알려져 있다. 상기와 같은 은의 고유한 특성은 여러 산업 분야에서 이용되며, 특히 살균, 소독기능으로 특징되는 항균성을 이용하여 의약품, 화학품 및 생활용품 분야에서 널리 활용되고 있다.In addition, the metal silver (Ag) has antibacterial properties, the efficacy of the silver is as follows. Silver ions (Ag +) released from silver (Ag) is already known to cure the disease by eliminating about 970 bacteria in less than six minutes without any toxicity to the human body by the electrical load. Such unique properties of silver are used in various industrial fields, and are widely used in medicine, chemical products, and household goods, in particular, using antibacterial properties characterized by sterilization and disinfection functions.
특히, 건축 현장에서 마감재나 장식재로서 사용되는 각종의 자재들은 각각의 개별적인 특징과 기능에 따라 사용자의 선택에 의해 건물이나 집을 짓는 데 사용된다. 이러한 건축 자재들의 경우, 방음, 방습, 항열, 단열 등의 기능을 위해 화학적 처리가 되며, 그 화학적 성분은 유독물질로서 새로 지은 건물이나 집에서는 건축자재에 잔류하는 유독 화학성분으로 인해 인체에 해를 미치는 문제점이 있었다.In particular, various materials used as finishing materials or decorative materials in building sites are used to build buildings or houses at the user's choice according to their individual characteristics and functions. These building materials are chemically treated for the functions of sound insulation, moisture proof, heat insulation, heat insulation, etc. The chemical components are toxic substances, and in new buildings or houses, the toxic chemicals remaining in the building materials are harmful to the human body. There was a problem.
상기와 같은 문제점을 해결하기 위해 은의 효능과 진공 증착 방법을 이용한 본 발명에 따른 고진공 증착법에 의한 은코팅 자기 타일 제조방법은, 건축용 마감재로 사용되는 자기 타일에 있어서, 그 표면을 은코팅막으로 처리하여 항균 기능을 부여함으로써 인체의 건강에 유익하며 자연 친화적인 고진공 증착법에 의한 은코팅 자기 타일 제조방법을 제공하는 것을 목적으로 한다.In order to solve the above problems, the silver coated magnetic tile manufacturing method according to the high vacuum deposition method according to the present invention using the effect of silver and vacuum deposition method, in the magnetic tile used as a building finishing material, by treating the surface with a silver coating film An object of the present invention is to provide a method of manufacturing silver-coated magnetic tiles by high vacuum deposition, which is beneficial to human health by providing antibacterial function.
도 1은 본 발명의 일 실시예에 따른 고진공 증착법에 의한 은코팅 자기 타일의 사시도.1 is a perspective view of a silver coated magnetic tile by a high vacuum deposition method according to an embodiment of the present invention.
도 2는 본 발명의 일 실시예에 따른 고진공 증착법에 의한 은코팅 자기 타일의 제조방법의 순서도.2 is a flow chart of a method of manufacturing a silver-coated magnetic tile by a high vacuum deposition method according to an embodiment of the present invention.
도 3은 본 발명의 일 실시예에 따른 은코팅 자기 타일의 은 박편의 생성단계의 순서도.Figure 3 is a flow chart of the step of producing the silver flakes of the silver-coated magnetic tile according to an embodiment of the present invention.
* 도면의 주요 부분에 대한 부호의 설명 *Explanation of symbols on the main parts of the drawings
1 : 은코팅 자기 타일 11 : 자기 타일1: silver coated magnetic tile 11: magnetic tile
12 : 은코팅층12: silver coating layer
상기한 바와 같은 목적을 달성하기 위한 본 발명에 따른 고진공 증착법에 의한 은코팅 자기 타일 제조방법은, 건축용 마감재로 사용되는 자기 타일에 있어서, 은 박편을 제조하는 은 박편 제조단계와; 상기 은 박편 제조단계에서 얻어진 은 박편과 상기 자기 타일을 고진공 탱크 속에서 가열하는 가열단계와; 상기 고진공 탱크의 내부 온도를 은의 용융점 이상으로 유지하여 상기 은 박편을 증발시켜 상기 자기 타일의 표면에 부착시키는 표면 증착단계와; 상기 표면 증착단계에서 얻어진 은코팅 자기 타일의 표면에 60 ~ 970℃에서 열처리하는 열처리 마감단계;를 포함하여 이루어진 것을 특징으로 한다.Silver coated magnetic tile manufacturing method according to the high vacuum deposition method according to the present invention for achieving the above object, in the magnetic tile used as a building finishing material, silver flake manufacturing step of producing a silver flake; A heating step of heating the silver flakes and the magnetic tile obtained in the silver flake manufacturing step in a high vacuum tank; A surface deposition step of maintaining the internal temperature of the high vacuum tank above the melting point of silver and evaporating the silver flakes to attach to the surface of the magnetic tile; It characterized in that it comprises a; heat treatment finish step of heat treatment at 60 ~ 970 ℃ to the surface of the silver-coated magnetic tile obtained in the surface deposition step.
본 발명의 바람적인 특징에 따르면, 상기 은 박편 제조단계는, 순도 100%의 은을 연금과정, 압연과정, 절편판 생성과정, 중간 은 박판 생성과정 및 은 박편 생성과정을 거침으로써 최종 완제품인 은 박편을 생성하는 것을 특징으로 한다.According to a wind feature of the present invention, the silver flake manufacturing step, the silver flakes of the final product by going through the alchemy process, rolling process, section plate production process, intermediate silver plate production process and silver flake generation process of 100% pure silver It characterized in that to generate.
또한, 상기 표면 증착단계는, 순도 100%의 은을 상기 진공 탱크 내에서 진공도 10-3mmHg(Torr) ~ 10-9mmHg(Torr) 유지되는 상태에서 은을 증발시킴으로써 상기 자기 타일의 표면에 부착시키는 건식법인 것을 특징으로 한다.In addition, the surface deposition step, the dry method of attaching to the surface of the magnetic tile by evaporating the silver in the state of maintaining a purity of 100% of the purity of 100% in the vacuum tank 10-3mmHg (Torr) ~ 10-9mmHg (Torr) in the vacuum tank It is characterized by that.
이상과 같이 구성된 본 발명에 따른 고진공 증착법에 의한 은코팅 자기 타일 제조방법은, 고진공 상태의 진공 탱크 내에 은 박편과 자기 타일을 넣은 후 은의 용융점 이상의 고온을 유지하여 증발된 은 입자를 자기 타일의 표면에 부착시킴으로써 얻어진다. 이러한 은코팅 자기 타일은 건축현장의 장식재나 마감재로서 사용되어 인체에 무해하며 또한 항균기능을 발휘하게 된다.In the method of manufacturing a silver-coated magnetic tile by the high vacuum deposition method according to the present invention configured as described above, after the silver flakes and the magnetic tile are placed in a vacuum tank in a high vacuum state, the silver particles evaporated by maintaining the high temperature above the melting point of silver are coated on the surface of the magnetic tile. It is obtained by adhering to. Such silver coated magnetic tiles are used as decorative materials or finishing materials in construction sites, which are harmless to the human body and exhibit antibacterial function.
이하, 이상과 같은 구성요소 들을 포함하여 이루어진 본 발명의 바람직한 일 실시예를 첨부 도면을 통하여 보다 구체적으로 살펴본다.Hereinafter, a preferred embodiment of the present invention including the above components will be described in more detail with reference to the accompanying drawings.
도 1은 본 발명의 일 실시예에 따른 고진공 증착법에 의한 은코팅 자기 타일의 사시도이고, 도 2는 그 은코팅 자기 타일의 제조방법의 순서도이고, 도 3은 그 은코팅 자기 타일의 은 박편의 생성단계의 순서도이다.1 is a perspective view of a silver-coated magnetic tile by a high vacuum deposition method according to an embodiment of the present invention, Figure 2 is a flow chart of a manufacturing method of the silver-coated magnetic tile, Figure 3 is a silver flake of the silver-coated magnetic tile This is a flowchart of the generation step.
도 1은 본 발명의 일 실시예에 따른 고진공 증착법을 이용하여 자기 타일(11)의 표면에 은코팅층(12)을 형성한 은코팅 자기 타일(1)을 도시한다. 본 발명에서는 건축의 내외장재로서 사용하고 있는 자기 타일(11)의 표면에 고진공 증착법으로 순도 100%의 은을 진공탱크 속에 두고 열을 가해 증발시킴으로써 그 은을 마주보고 있는 자기 타일(11)의 일 표면에 은코팅 박막을 형성한다.1 shows a silver coated magnetic tile 1 in which a silver coating layer 12 is formed on a surface of a magnetic tile 11 using a high vacuum deposition method according to an embodiment of the present invention. According to the present invention, one surface of the magnetic tile 11 facing the silver is applied to a surface of the magnetic tile 11 which is used as interior and exterior materials of a building by heating and evaporating by applying heat of 100% purity in a vacuum tank. To form a silver coated thin film.
이하 도 2및 도 3을 참조하여 본 발명의 일 실시예에 따른 고진공 증착법을 이용한 은코팅 자기 타일(1)의 생성 과정을 설명한다. 도 2에 도시한 바와 같이, 은 박편 제조단계(S1)에서 은 박막을 형성하기 위해 순도 100%의 은으로부터 은 박편을 생성한다.Hereinafter, a process of generating the silver-coated magnetic tile 1 using the high vacuum deposition method according to an embodiment of the present invention will be described with reference to FIGS. 2 and 3. As shown in FIG. 2, silver flakes are produced from silver having a purity of 100% to form a silver thin film in the silver flake manufacturing step S1.
전술한 은 박편 제조단계(S1)는 도 3에 도시한 과정을 거친다. 먼저 순도 100%의 은을 연금과정(S11)을 거치게 한 후 압연과정(S12)을 거쳐서 절편판 생성과정(S13)에서 은 절편판을 생성한다. 다음에 중간 은 박판 생성과정(S14)에서 은 박판을 생성하고 최종 단계인 은 박편 생성과정(S15)에서 진공 탱크에 넣어질 은 박편을 생성한다.The silver flake manufacturing step (S1) described above is subjected to the process shown in FIG. First, the silver having a purity of 100% is subjected to the pension process (S11), and then a silver plate is generated in the section plate generation process (S13) through the rolling process (S12). Next, the silver plate is generated in the middle silver plate generation process (S14), and the silver foil to be put into the vacuum tank is produced in the final step, the silver plate formation process (S15).
다음에, 은 박편은 자기 타일(11)과 같이 진공 탱크에 넣어져 가열단계(S2)를 거친다. 진공 탱크 내에 넣어진 은 박편이 증발할 만큼의 고온이 형성되면 표면 증착단계(S3)에서 증발이 일어나기 시작한다. 은 박편이 증발하면 표면 증착단계(S3)에서 증발된 은 입자가 자기 타일(11)의 표면에 흡착함으로써 은코팅층(12)을 형성한다. 만약 은이 진공이 아닌 대기 중에서 증발할 경우 산화나 원하지 않는 반응이 일어나기 때문에 이를 억제하기 위하여 고진공이 필요하다. 또한 은이 증발할 때 공간에 있는 가스분자와 충돌하는 것은 자기 타일(11)의 표면에 흡착시키는 것이 방해되어 균일한 은코팅층(12)을 형성할 수 없기에 고진공이 필요한 것이다.Next, the silver flakes are put in a vacuum tank like the magnetic tiles 11 and undergo a heating step S2. When the high temperature enough to evaporate the silver flakes contained in the vacuum tank is formed, evaporation starts to occur in the surface deposition step (S3). When the silver flakes evaporate, the silver particles evaporated in the surface deposition step S3 are adsorbed on the surface of the magnetic tile 11 to form the silver coating layer 12. If silver evaporates in the atmosphere, not in a vacuum, oxidation or unwanted reactions occur, so high vacuum is required to suppress them. In addition, colliding with the gas molecules in the space when the silver evaporates is hindered by the adsorption on the surface of the magnetic tile 11, it is necessary to high vacuum because the uniform silver coating layer 12 can not be formed.
이와 같이 표면 증착단계(S3)에서는 마치 대기 중에서 그릇 속의 물이 증발하는 것처럼 진공 탱크 내에서 은 박편이 날아서 자기 타일 표면에 은이 흡착하는 것이다. 특히 진공도 10-3mmHg(Torr) ~ 10-9mmHg(Torr)의 고진공 상태에서 은을 증발 부착시키는 것을 건식법이라고 하며 이것은 공해 방지에도 기여할 수 있다. 일반적인 도금은 화공약품으로 은을 녹여서 사용하기 때문에 콜로이드 상태의 은 용액은 100% 순도가 아니며, 공기 중에서 작업을 하기 때문에 산화로 인해 변색의 우려가 있으며, 도금 후의 용액은 유독성 폐수가 되어 환경오염의 주원인이 된다.As described above, in the surface deposition step S3, silver flakes are blown in the vacuum tank as if the water in the vessel evaporates in the air, and the silver is adsorbed on the magnetic tile surface. In particular, evaporation of silver in a high vacuum state with a vacuum degree of 10-3 mmHg (Torr) to 10-9 mmHg (Torr) is called a dry method, which may contribute to pollution prevention. In general, plating is used as a chemical that dissolves silver, so the colloidal silver solution is not 100% pure, and because it works in the air, there is a risk of discoloration due to oxidation, and the solution after plating becomes a toxic wastewater. It is the main cause.
다음으로, 표면 증착단계(S3)로부터 얻어진 은코팅 자기 타일(1)의 표면에 60 ~ 970℃에서 열처리하는 열처리 마감단계(S4)를 거치면, 은코팅층(12)을 영구적으로 보호할 수 있어 코팅의 안정성과 더불어 지속적인 살균효과를 발휘할 수 있게 된다.Next, the surface of the silver-coated magnetic tile (1) obtained from the surface deposition step (S3) is subjected to a heat treatment finish step (S4) to heat treatment at 60 ~ 970 ℃, the silver coating layer 12 can be permanently protected coating In addition to the stability of the sterilization effect can be exhibited.
상술한 바와 같이, 본 발명에 따른 고진공 증착법에 의한 은코팅 자기 타일 제조방법의 실시예가 구성된다. 본 발명의 기술적인 범위는 반드시 상술한 실시예에 한정되는 것은 아니며, 본 발명의 기술적 범위를 해치지 않는 범위에서 다양한 변형이나 응용예가 가능하다.As described above, an embodiment of the silver-coated magnetic tile manufacturing method by the high vacuum deposition method according to the present invention is configured. The technical scope of the present invention is not necessarily limited to the above-described embodiment, and various modifications and applications can be made without departing from the technical scope of the present invention.
본 발명에 따른 고진공 증착법에 의한 은코팅 자기 타일 제조방법은, 진공 탱크 내에 은 박편과 자기 타일을 넣고, 은의 용융점 이상의 고온 상태에서 은을 증발시켜 마주하는 자기 타일의 표면에 증발된 은 입자를 코팅함으로써, 자기 타일에 항균기능을 부여하여 인체에 무독한 건축용 내외장재를 제공한다. 따라서 본 발명에 따른 고진공 증착법에 의한 은코팅 자기 타일은 우수한 살균효과를 가지며 건축용 마감재 및 장식재로 사용될 수 있어 목욕탕, 병원, 주택, 사우나, 수영장과 같은 건축 현장에서 실생활에 꼭 필요한 건축 마감재와 건강 활용품으로 사용할 수 있는 효과를 제공한다.In the method of manufacturing silver-coated magnetic tiles by the high vacuum deposition method according to the present invention, silver flakes and magnetic tiles are placed in a vacuum tank, and the evaporated silver particles are coated on the surface of the magnetic tiles facing by evaporating silver at a high temperature above the melting point of silver. By providing the antimicrobial function to the magnetic tiles, thereby providing a building interior and exterior materials harmless to the human body. Therefore, the silver-coated magnetic tile by the high vacuum deposition method according to the present invention has excellent sterilization effect and can be used as a building finishing material and decoration material, so that the building finishing materials and health necessary for real life in building sites such as bathrooms, hospitals, houses, saunas and swimming pools are utilized. It provides an effect that can be used as a product.
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Cited By (2)
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KR100817107B1 (en) * | 2005-11-17 | 2008-03-26 | 박옥순 | Method for manufacturing color tile using thin film deposition method |
KR20230091607A (en) | 2021-12-16 | 2023-06-23 | 서창환 | Manufacturing method of porcelain tile having antibacterial and deodorant function and porcelain tile using the same |
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JPH0967181A (en) * | 1995-06-22 | 1997-03-11 | Inax Corp | Antimincrobial ceramic material and its production |
US5681575A (en) * | 1992-05-19 | 1997-10-28 | Westaim Technologies Inc. | Anti-microbial coating for medical devices |
KR200221533Y1 (en) * | 2000-11-30 | 2001-04-16 | 코오롱글로텍주식회사 | A silver-vacuum evaporation's texture of cloth for lining |
KR20010068102A (en) * | 2001-04-23 | 2001-07-13 | 신홍대 | A silver tile and the manufacturing method of the same |
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Publication number | Priority date | Publication date | Assignee | Title |
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US5681575A (en) * | 1992-05-19 | 1997-10-28 | Westaim Technologies Inc. | Anti-microbial coating for medical devices |
JPH0967181A (en) * | 1995-06-22 | 1997-03-11 | Inax Corp | Antimincrobial ceramic material and its production |
KR200221533Y1 (en) * | 2000-11-30 | 2001-04-16 | 코오롱글로텍주식회사 | A silver-vacuum evaporation's texture of cloth for lining |
KR20010068102A (en) * | 2001-04-23 | 2001-07-13 | 신홍대 | A silver tile and the manufacturing method of the same |
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Publication number | Priority date | Publication date | Assignee | Title |
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KR100817107B1 (en) * | 2005-11-17 | 2008-03-26 | 박옥순 | Method for manufacturing color tile using thin film deposition method |
KR20230091607A (en) | 2021-12-16 | 2023-06-23 | 서창환 | Manufacturing method of porcelain tile having antibacterial and deodorant function and porcelain tile using the same |
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