KR20030053119A - A method for manufacturng spring steel without ferrite decarburization - Google Patents

A method for manufacturng spring steel without ferrite decarburization Download PDF

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KR20030053119A
KR20030053119A KR1020010083159A KR20010083159A KR20030053119A KR 20030053119 A KR20030053119 A KR 20030053119A KR 1020010083159 A KR1020010083159 A KR 1020010083159A KR 20010083159 A KR20010083159 A KR 20010083159A KR 20030053119 A KR20030053119 A KR 20030053119A
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temperature
rolling
billet
ferrite
spring steel
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KR1020010083159A
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Korean (ko)
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KR100516503B1 (en
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김경원
김진근
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주식회사 포스코
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B3/00Rolling materials of special alloys so far as the composition of the alloy requires or permits special rolling methods or sequences ; Rolling of aluminium, copper, zinc or other non-ferrous metals
    • B21B3/02Rolling special iron alloys, e.g. stainless steel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B37/00Control devices or methods specially adapted for metal-rolling mills or the work produced thereby
    • B21B37/16Control of thickness, width, diameter or other transverse dimensions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B37/00Control devices or methods specially adapted for metal-rolling mills or the work produced thereby
    • B21B37/74Temperature control, e.g. by cooling or heating the rolls or the product
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/02Ferrous alloys, e.g. steel alloys containing silicon
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/04Ferrous alloys, e.g. steel alloys containing manganese
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B15/00Arrangements for performing additional metal-working operations specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills
    • B21B2015/0057Coiling the rolled product
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B2261/00Product parameters
    • B21B2261/20Temperature
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B2265/00Forming parameters
    • B21B2265/14Reduction rate

Abstract

PURPOSE: A method for manufacturing suspension spring steel without peeling operation of ferrite decarburized layer is provided which is capable of skipping peeling process during processing of suspension spring steel wire rod by properly controlling hot rolling conditions, thereby suppressing formation of ferrite decarburized layer. CONSTITUTION: The method comprises the steps of preparing a billet comprising 0.4 to 0.6 wt.% of C, 1.3 to 1.6 wt.% of Si, 0.5 to 0.7 wt.% of Mn, 0.4 to 0.7 wt.% of Cr and a balance of Fe and other inevitable impurities; rough rolling the reheated billet after reheating the billet to a temperature of 1,000 to 1,100 deg.C; intermediate finish rolling the rough rolled billet at a temperature of 750 to 850 deg.C, and subsequently finish rolling the intermediate finish rolled billet to a final surface reduction ratio of 30% or more in the same temperature range; and cooling the coiled wire rod to a temperature of 600 to 650 deg.C at a cooling rate of 1 deg.C/sec or less after coiling the rolled wire rod in the temperature range of 750 to 800 deg.C, and subsequently air-cooling the resultant wire rod to an ordinary temperature in the air.

Description

페라이트 탈탄이 없는 스프링강의 제조방법{A method for manufacturng spring steel without ferrite decarburization}A method for manufacturng spring steel without ferrite decarburization}

본 발명은 자동차 현가용 스프링강의 제조방법에 관한 것으로, 보다 상세하게는 피로강도 및 변형저항성이 기존 스프링강과 유사하면서, 페라이트 탈탄이 없는 스프링강의 제조방법에 관한 것이다.The present invention relates to a method for manufacturing spring steel for automobile suspension, and more particularly, to a method for manufacturing spring steel without ferrite decarburization while having similar fatigue strength and deformation resistance to existing spring steel.

스프링강 제조공정중 재가열 및 열간압연공정에서는, 소재에 표면탈탄, 즉, 페라이트 탈탄층이 생성되는데, 이것은 소재의 피로수명을 저하시키므로, 통상적으로 표면가공, 즉 표면을 깍아내기 위해 실시되는 공정인 필링(Peeling)공정을 수행하고 있다. 그러나, 상기한 필링공정에는 많은 비용이 소요되기 때문에, 이를 생략하면 생산량을 14% 이상 증가시킬 수 있다.In the reheating and hot rolling processes of the spring steel manufacturing process, surface decarburization, or ferrite decarburization layer, is formed on the material, which reduces the fatigue life of the material, and is therefore usually a surface processing, i.e., a process for shaving the surface. Peeling process is performed. However, since the peeling process is very expensive, if omitted, the yield can be increased by 14% or more.

한편 변형저항성을 크게 약화시키지 않는 성분범위에서 표면탈탄을 조장하는 실리콘(Si)을 감소시키고 탈탄방지에 효과적인 원소인 크롬(Cr)을 첨가한 SAE9254가 개발되었다. 그러나 이 경우, 페라이트 탈탄층을 완벽하게 제어하지 못하여, 스프링선재의 표면을 깍아 가공하는 공정이 통상 실시되어야 했다.On the other hand, SAE9254 has been developed in which silicon (Si), which promotes surface decarburization, is added and chromium (Cr), an element effective in preventing decarburization, has been developed in a component range that does not significantly reduce deformation resistance. In this case, however, the ferrite decarburized layer could not be completely controlled, and a step of shaving the surface of the spring wire rod had to be carried out normally.

또한, 스프링제조시 발생하는 탈탄층을 억제하기 위한 종래기술로는, 일본특개(평)2-301541호, (평)1-31960호, (소)63-216591, (소)63-153240호,(소)58-67847호 및 (소)58-27956호 등을 들 수 있는데, 상기한 기술들의 경우에는, 크롬함량을 증가 시키거나 탄소함량을 낮추면서, 구리, 몰리브덴, 주석 등을 첨가하는 방법이 제시하고 있다. 그러나, 이 경우, 탈탄층의 감소에는 효과가 있었으나 완벽히 제어하지 못하였다. 또한, 고가의 합금원소첨가로 비경제적인 단점이 있었다Further, conventional techniques for suppressing the decarburized layer generated during spring production include Japanese Patent Laid-Open Nos. 2-301541, No. 1-31960, No. 63-216591, No. 63-153240 And (S) 58-67847 and (S) 58-27956. In the above-described techniques, copper, molybdenum, tin, etc. may be added while increasing the chromium content or lowering the carbon content. The method is presented. However, in this case, it was effective in reducing the decarburized layer but was not completely controlled. In addition, there was an uneconomical disadvantage due to the addition of expensive alloying elements.

이에, 본 발명의 발명자들은 상기와 같은 문제점을 해결하기 위하여 연구와 실험을 거듭하였으며, 그 결과에 근거하여 본 발명을 제안하는 것으로, 본 발명은 강성분 및 사상압연에서의 소재감면율등 열연조건을 적절히 제어하여 페라이트탈탄층의 생성을 억제함으로써, 스프링강 선재의 가공시 필링공정을 생략할 수 있는 스프링강의 제조방법을 제공함에 그 목적이 있다.Accordingly, the inventors of the present invention have repeatedly conducted research and experiments to solve the above problems, and based on the results, the present invention proposes a hot rolling condition such as steel reduction and material reduction rate in finishing rolling. It is an object of the present invention to provide a method for producing a spring steel which can omit the filling process during the processing of the spring steel wire by appropriately controlling the formation of the ferrite decarburized layer.

도 1은 본 발명에서 이용한 선재압연설비의 개략 구성도1 is a schematic configuration diagram of a wire rod rolling equipment used in the present invention

도 2은 본 발명의 발명재(1,2,3)의 페라이트탈탄조직을 나타내는 사진(배율: X100)Figure 2 is a photograph (magnification: X100) showing the ferrite decarburization structure of the inventive material (1, 2, 3) of the present invention

도 3은 본 비교재(종래재)(1,2,3)의 페라이트탈탄조직을 나타내는 사진(배율: X100)Figure 3 is a photograph (magnification: X100) showing the ferrite decarburization structure of the present comparative material (primary material) (1, 2, 3)

*도면의 주요부분에 대한 부호설명** Description of Signs of Main Parts of Drawings *

1. 가열로 2. 조압연기1. Heating Furnace 2. Roughing Mill

3. 제1 중간수냉대 4. 중간사상압연기3. First intermediate water chiller 4. Intermediate sand mill

5. 제2 중간수냉대 6. 사상압연기5. Second intermediate water cooler 6. Filament mill

7. 수냉대 8. 권취기7. Water chiller 8. Winder

9. 공냉대 10. 집적기9. Air Cooler 10. Integrator

상기한 목적을 달성하기 위한 본 발명은,The present invention for achieving the above object,

중량%로, 탄소(C):0.4~0.6%, 실리콘(Si):1.3~1.6%, 망간(Mn):0.5~0.7%, 크롬(Cr):0.4~0.7%, 잔부 Fe 및 기타 불가피한 불순물로 조성되는 빌렛(Billet)을 마련하는 단계; 상기 빌렛을 1000~1100℃의 온도로 재가열한 다음 조압연하는 단계; 상기 조압연된 빌렛을 750~850℃에서 중간사상압연하고, 이어 동일한 온도범위에서 소재의 최종 감면율이 30%이상이 사상압연하는 단계; 상기 압연된 선재를 750~800℃에서 권취한 후 600~650℃의 온도까지 1℃/s이하의 속도로 냉각하고, 이어 상온까지 공냉하는 단계;를 포함하는 페라이트 탈탄이 없는 스프링강의 제조방법에 관한 것이다.By weight%, carbon (C): 0.4-0.6%, silicon (Si): 1.3-1.6%, manganese (Mn): 0.5-0.7%, chromium (Cr): 0.4-0.7%, balance Fe and other unavoidable impurities Providing a billet (Billet) is composed of; Reheating the billet to a temperature of 1000 ~ 1100 ℃ and then rough rolling; Intermediate rough rolling of the roughly rolled billet at 750 ° C. to 850 ° C., followed by finishing rolling at a final reduction rate of 30% or more in the same temperature range; After winding the rolled wire at 750 ~ 800 ℃ to the temperature of 600 ~ 650 ℃ 1 ℃ / s or less cooling rate, and then air-cooled to room temperature; comprising a method for producing ferrite decarburization-free spring steel It is about.

이하, 본 발명의 강 성분 및 그 제한사유를 설명한다.Hereinafter, the steel component of the present invention and the reason for limitation thereof will be described.

본 발명의 강 성분중 C의 함량은 0.4~0.6중량%(이하, 단지%라 한다)로 제한하는데, 그 이유는 탄소의 함량이 0.4%미만이면 소입,소려에 의한 고응력 스프링용강으로서 충분한 강도를 확보하기 어렵고, 0.80%를 초과하면 인성의 확보가 불충분하고 고실리콘의 함량으로 파생되는 소재탈탄을 억제하기 어렵기 때문이다.The content of C in the steel component of the present invention is limited to 0.4 to 0.6% by weight (hereinafter referred to as only%), because the carbon content is less than 0.4%, sufficient strength as a high stress spring steel by hardening and consideration This is because it is difficult to secure, and when it exceeds 0.80%, securing of toughness is insufficient and it is difficult to suppress material decarburization derived from the content of high silicon.

Si의 함량은 1.3~1.6%로 제한하는데, 그 이유는 Si의 함량이 1.3%미만이면 실리콘이 페라이트내에 고용되어 모재의 강도를 강화시키고 변형저항성을 개선하는 효과가 충분하지 못한 반면에, 1.6%를 초과하면 변형저항성의 개선효과가 포화되고 열처리시 탈탄의 가능성이 높기 때문이다.The content of Si is limited to 1.3 to 1.6%, because if the content of Si is less than 1.3%, silicon is dissolved in the ferrite, and the effect of strengthening the strength of the base material and improving the deformation resistance is insufficient, whereas 1.6% If it exceeds, the effect of improving the deformation resistance is saturated and there is a high possibility of decarburization during heat treatment.

Mn의 함량은 0.5~0.7%로 제한하는데, 그 이유는 망간의 함량이 0.5%미만이면 스프링용강으로서 강도 및 소입성이 부족하고, 0.7%를 초과하면 인성이 저하하기 때문이다.The content of Mn is limited to 0.5 to 0.7%, because if the content of manganese is less than 0.5%, the strength and quenchability as spring steel is insufficient, and if the content exceeds 0.7%, the toughness decreases.

Cr은 페라이트탈탄층을 저감시키는 원소로서, 본 발명에서는 그 함량범위를 0.4~0.7%로 제한한다. 만일 상기 Cr의 함량이 0.4% 미만이면 충분한 소입성 및 탈탄억제의 효과를 얻기 어렵고, 0.7%를 초과하면 탈탄억제효과가 포화되어 개선효과가 없기 때문이다.Cr is an element for reducing the ferrite decarburized layer, and the content of the present invention is limited to 0.4 to 0.7%. If the content of Cr is less than 0.4%, it is difficult to obtain an effect of sufficient hardenability and decarburization, and if it exceeds 0.7%, the decarburization inhibitory effect is saturated and there is no improvement effect.

본 발명에서는 상기와 같이 조성되는 빌렛을 제조한 후, 이를 재가열, 열간압연 및 권취 등의 공정을 거친 다음, 이후 스프링 용으로 사용되는데, 이하에서는 제조공정에 대하여 상세히 설명한다.In the present invention, after the billet is prepared as described above, and then subjected to a process such as reheating, hot rolling and winding, and then used for the spring, the manufacturing process will be described in detail below.

먼저, 상기 재가열온도는 1000~1100℃로 설정하는 것이 바람직한데, 그 이유는 상기 재가열온도가 1100℃를 초과하면 탄소의 활동성이 매우 증가되어 표면에서 외부로 탄소가 빠져나가서 탈탄이 매우 조장되며, 1000℃미만이면 스프링강의 특성을 위해 첨가된 합금원소의 영향으로 조압연에서 압연부하로 인해 압연이 불가능하기 때문이다.First, the reheating temperature is preferably set to 1000 ~ 1100 ℃, the reason is that when the reheating temperature exceeds 1100 ℃ the carbon activity is very increased, carbon is escaped from the surface to the outside to facilitate decarburization, If it is less than 1000 ℃ due to the effect of the alloying elements added for the characteristics of the spring steel is not possible due to the rolling load in the rough rolling.

다음, 열간압연을 실시하는데, 이하, 도 1을 참조하여 본 발명의 열간압연조건을 상세히 설명한다.Next, hot rolling is performed. Hereinafter, the hot rolling conditions of the present invention will be described in detail with reference to FIG. 1.

도 1에 나타난 바와 같이, 일반적으로 열간압연은 크게 조압연(2)-수냉(3)-중간사상압연 (4)-수냉(5)-사상압연(6)-수냉으로 이루어지는데, 본 발명은 이러한 열간압연공정중 중간사상압연 및 사상압연의 온도조건을 제어하고, 압연시 소재의 감면율을 제어함에 그 특징이 있다.As shown in Figure 1, hot rolling generally consists of rough rolling (2) -water cooling (3) -medium sand rolling (4) -water cooling (5) -ideal rolling (6) -water cooling. It is characterized by controlling the temperature conditions of intermediate sand rolling and finishing rolling during the hot rolling process, and controlling the reduction rate of the raw material during rolling.

즉, 본 발명에서는 통상의 온도범위인 950~1050℃에서 조압연된 강 빌렛을 750~850℃에서 중간사상압연하여, 가열로에서 생성되어 성장한 페라이트 탈탄층의 페라이트층을 원주형태(Columnar)에서 폴리고날(Polygonal)형태로 미세화한다.That is, in the present invention, the steel billet roughly rolled at a temperature range of 950 to 1050 ° C. is intermediately rolled at 750 to 850 ° C., and the ferrite layer of the ferrite decarburized layer, which is generated and grown in a heating furnace, is formed in a columnar shape. It is refined to polygonal form.

그리고 복열된 소재를 수냉하여 다시 750~850℃의 온도범위로 제어한 다음, 소재의 감면율을 30%이상이 되도록 사상압연을 실시함으로써 미세화된 탈탄층이 압연중 성장이 억제되어 더욱 미세화되고, 일부 결정립 성장에 의해 조대화된 표면의 페라이트 탈탄부위를 다시 미세화시켜 페라이트가 성장하지 못하게 하며, 아울러, 소재에 일정이상의 감면율을 주어서 활성화에너지를 향상시켜 초석페라이트가 생성되는 구간을 빨리 지나가게 된다.Then, the reheated material is cooled to a temperature range of 750 ° C. to 850 ° C., and then subjected to filament rolling so that the reduction rate of the material is 30% or more. The ferrite decarburized part of the surface coarsened by grain growth is further refined to prevent ferrite from growing, and the material is given a certain reduction rate to improve the activation energy, thereby quickly passing the section where the formation of ferrite is made.

이에 따라, 페라이트가 성장하여 소재표면에 원주형태(Columnar)의 밴드를 이루는 페라이트 탈탄층은 제거되고, 압연중 또는 냉각중에 미세화된 조직을 통해 표면에서 빠져나가는 탄소의 양보다 소재내부에서 계면을 통해 확산되는 탄소량을 많게되고, 초석 페라이트의 생성량도 줄일 수가 있어, 표면에 탄소량과 내부조직의 탄소량을 동일하게 유지함으로써, 페라이트 탈탄층을 효과적으로 제거할 수 있는 것이다.As a result, the ferrite decarburized layer, in which ferrite grows to form columnar bands on the surface of the material, is removed, and through the interface inside the material rather than the amount of carbon that escapes from the surface through the microstructured structure during rolling or cooling. It is possible to increase the amount of carbon to be diffused and to reduce the amount of the formation of the cornerstone ferrite, and to maintain the same amount of carbon on the surface and the amount of carbon in the internal structure, thereby effectively removing the ferrite decarburized layer.

한편, 본 발명에서 중간사상압연 온도와 사상압연온도를 750~850℃로 한정하는 이유는 다음과 같다.Meanwhile, in the present invention, the reason for limiting the intermediate sand rolling temperature and the finishing rolling temperature to 750 to 850 ° C is as follows.

본 발명에서는 통상의 압연방법과는 달리 조압연된 소재를 미재결정영역 (750~850℃)까지 냉각한 후 중간사상압연을 실시하며, 이때 발생된 가공발열을 다시 수냉에 의해 제거하여 그 온도를 소재의 미재결정영역(750~850℃)까지 냉각한 다음 사상압연을 실시함을 특징으로 하며, 이에 따라 소재 내부에는 전위밀도가 급격히 증가하고, 결정립 또한 매우 미세하게 된다.In the present invention, unlike the conventional rolling method, the roughly rolled material is cooled to the unrecrystallized region (750 ~ 850 ℃) and then subjected to intermediate sand rolling, and the process heat generated at this time is removed again by water cooling to remove the temperature. After cooling to the unrecrystallized region (750 ~ 850 ℃) of the material is characterized in that the finishing rolling, the dislocation density is rapidly increased inside the material, the grain is also very fine.

만일 중간사상 압연온도와 사상압연온도가 850℃보다 높으면, 통상압연방법 대비 조직미세화의 효과는 있으나 압연중 조직미세화가 미흡하여 냉각중에 국부적으로 페라이트 그레인(Grain)이 성장하여, 소재단면에 일부 원주형 (Columnar) 페라이트층이 생성되고, 이에 따라, 페라이트 탈탄층이 발생되어 소재 전체에 대한 페라이트 탈탄을 제어할 수 없게 된다. 그리고 750℃ 미만이면, 중간사상압연기와 사상압연기의 압연능력 부족으로 압연이 불가능하게 된다.If intermediate sand rolling temperature and finishing rolling temperature are higher than 850 ℃, there is an effect of microstructure in comparison with the conventional rolling method, but there is insufficient microstructure in rolling, so that ferrite grain grows locally during cooling, so that some circumference in the material section A columnar ferrite layer is generated, and thus, a ferrite decarburization layer is generated, which makes it impossible to control the ferrite decarburization over the entire material. And if it is less than 750 degreeC, rolling will become impossible due to the lack of rolling capability of an intermediate sand mill and a finishing mill.

본 발명에서는 또한 그 소재감면율을 30%이상이 되도록 사상압연하는 것이 바람직하다. 왜냐하면 비록 중간사상압연과 사상압연을 750~850℃온도범위에서 행하더라도, 그 소재의 감면율이 30%미만이면 결정립미세화의 효과가 미흡하여, 가열로에서 생성되어 성장한 페라이트 탈탄층의 페라이트층을 원주형태(Columnar)에서 폴리고날 (Polygonal)형태로 미세화할 수 없으며, 아울러, 일부 미세화된 결정립도, 사상압연중 2차 조직미세화의 효과를 얻을수 없어 그 결정립이 성장하여, 페라이트층을 형성하여 페라이트 탈탄층을 형성하기 때문이다.In the present invention, it is also preferable that the rolling is performed so that the material reduction ratio is 30% or more. Because intermediate sanding and finishing rolling are carried out at the temperature range of 750 ~ 850 ℃, if the reduction rate of the material is less than 30%, the effect of grain refinement is insufficient, and the ferrite layer of ferrite decarburization layer produced and grown in the furnace is circumferential. It cannot be refined from columnar to polygonal form, and also, it is impossible to obtain some micronized grains, the effect of secondary tissue micronization during finishing rolling, and the grains grow to form a ferrite layer to form a ferrite decarburized layer. Because it forms.

상기한 바와 열간압연된 강선재는 이후 권취되는데, 이때 그 온도를 750~800℃로 제한함이 바람직하다. 만일 권취온도가 750℃미만이면, 수냉장치에서 순간적으로 소재의 온도를 목표온도까지 도달하기 위해, 고압의 물로 소재를 냉각해야 하므로, 수냉 장치내에서 소재와 수냉장치와의 마찰 및 소재의 온도하락으로 인한 강성이 높아져서 발생하는 권취기와의 마찰로 인하여 표면흠을 유발하게 된다.As described above, the hot rolled steel wire is then wound, and at this time, the temperature is preferably limited to 750 to 800 ° C. If the coiling temperature is less than 750 ° C, in order to reach the target temperature instantaneously in the water cooling system, the material must be cooled with high pressure water, so the friction between the material and the water cooling system and the temperature drop of the material in the water cooling system are reduced. Due to the increased rigidity caused by the friction with the winder causes surface scratches.

또한, 권취온도가 800℃를 초과하면 열간압연후에도 많은 변형에너지를 내포하게 되어 변태가 촉진되어 CCT 곡선상에 변태시간이 빨라지고, 이에 따라, 취성조직인 베이나트, 마르텐사이트등의 저온조직이 발생하게 되는 문제가 있다.In addition, when the coiling temperature exceeds 800 ℃, the deformation energy is contained even after hot rolling, and the transformation is accelerated, and the transformation time is accelerated on the CCT curve, thereby causing the low temperature structure of brittle tissue such as bainart and martensite. There is a problem.

이와 같이 권취된 선재는 통상의 방법으로 600~650℃온도범위까지 1℃/s 이하의 속도로 서냉하고, 이후 상온까지는 공냉함으로써 페라이트탈탄이 없는 스프링강으로 제조할 수 있는 것이다.The wire wound in this way can be manufactured in a spring steel without ferrite decarburization by slow cooling at a rate of 1 ° C./s or less to a temperature range of 600 to 650 ° C. in a conventional manner and then air cooling to room temperature.

이하, 실시예를 통하여 본 발명을 상세히 설명한다.Hereinafter, the present invention will be described in detail through examples.

(실시예)(Example)

중량%로, C: 0.53%, Si:1.41%, Cr:0.58%, Mn:0.61%, P:0.001%, S:0.008%, 잔부 Fe 및 기타 불가피한 불순물로 조성된 빌렛을 다수 마련하였다. 그리고 이와 같이 마련된 빌렛을 표 1과 같이 그 재가열온도를 달리하여 재가열한 후 980~1020 ℃에서 조압연하고, 이후, 표 1과 같이 그 중간사상압연과 사상압연, 감면율 및 열연권취온도를 달리하면서 열간압연하였다.By weight%, billets composed of C: 0.53%, Si: 1.41%, Cr: 0.58%, Mn: 0.61%, P: 0.001%, S: 0.008%, balance Fe and other unavoidable impurities were prepared. The billet thus prepared is reheated by varying its reheating temperature as shown in Table 1, and then roughly rolled at 980 to 1020 ° C. Then, as shown in Table 1, while varying the intermediate sand rolling, filamentous rolling, reduction rate and hot rolling temperature, Hot rolled.

이와 같이 제조된 각각의 선재에 대하여 페라이트 탈탄깊이와 점유율을 측정하고, 그 결과를 표 2에 나타내었다. 한편, 여기서 페라이트 탈탄깊이란 선재압연후 선재표면에 생성된 최대 깊이를 의미하며, 페라이트 탈탄 점유율은 선재압연후 선재표면의 원주를 점유한 퍼센트를 의미한다. 또한 전탈탄 깊이는 표면 탈탄층에서 기지조직의 탄소농도와 같은조직을 갖는 거리를 의미한다.The ferrite decarburization depth and the occupancy rate of each wire rod thus manufactured were measured, and the results are shown in Table 2. Meanwhile, the ferrite decarburization depth means the maximum depth generated on the wire rod surface after the wire rod rolling, and the share of ferrite decarburization means the percentage of the circumference of the wire rod surface after the wire rod rolling. In addition, the total decarburization depth means the distance having the same structure as the carbon concentration of the matrix in the surface decarburization layer.

구 분division 재가열온도(℃)Reheating Temperature (℃) 열간압연온도(℃)Hot Rolling Temperature (℃) 사상압연소재의감면율Reduction rate of filament rolling material 권취온도(℃)Winding temperature (℃) 중간사상압연Middle ideological rolling 사상압연Sasang Rolling 발명재1Invention 1 10001000 805805 830830 40%40% 780780 발명재2Invention 2 11001100 780780 810810 35%35% 772772 발명재3Invention 3 10201020 820820 830830 30%30% 790790 비교재1Comparative Material 1 10101010 820820 810810 20%20% 800800 비교재2Comparative Material 2 10201020 798798 820820 10%10% 792792 비교재3Comparative Material 3 10151015 10201020 996996 35%35% 780780

구분division 페라이트탈탄깊이(mm)Ferrite Decarburization Depth (mm) 페라이트탈탄점유율(%)Ferrite decarburization share (%) 전탈탄깊이(mm)Decarburization depth (mm) 발명재1Invention 1 00 00 0.130.13 발명재2Invention 2 00 00 0.110.11 발명재3Invention 3 0.0040.004 22 0.130.13 비교재1Comparative Material 1 0.020.02 4040 0.120.12 비교재2Comparative Material 2 0.040.04 6060 0.100.10 비교재3Comparative Material 3 0.060.06 100100 0.170.17

표 2에 나타난 바와 같이, 그 재가열온도 및 압연조건이 적정하게 제어된 발명재(1~3)의 경우, 페라이트 탈탄깊이가 0.004mm이하였던 반면에, 비교재(1~3)은 탈탄깊이가 0.02mm이상으로 되고 원주 점유율 또한 40%이상이 되는 것을 알 수 있다.As shown in Table 2, the ferrite decarburization depth was less than 0.004 mm for the invention materials 1 to 3 whose reheating temperature and rolling conditions were properly controlled, whereas the comparative materials 1 to 3 had a decarburization depth. It can be seen that more than 0.02mm and the share of the circumference is also more than 40%.

한편 도 2과 도 3은 상술한 본 발명재와 비교재의 페라이트탈탄 조직사진으로서, 본 발명의 발명재(1~3)이 비교재(1~3) 대비, 페라이트 탈탄의 깊이가 감소한 것을 잘 확인할 수 있다.Meanwhile, FIGS. 2 and 3 are ferrite decarburized tissue photographs of the present invention and the comparative material described above, and confirms that the inventive materials 1 to 3 have a reduced depth of ferrite decarburization compared to the comparative materials 1 to 3. Can be.

상술한 바와 같이, 본 발명은, 강성분 및 열간압연조건등을 최적으로 제어함으로써 페라이트 탈탄층의 생성을 억제함으로써, 종래의 필링공정을 행하지 않고서도 효과적으로 스프링강을 제조할 수 있으며, 이에따라 생산량을 14% 이상 향상시킴과 동시에 강재의 피로수명을 향상시킬 수 있는 효과가 있는 것이다.As described above, the present invention can effectively produce the spring steel without performing the conventional peeling process by suppressing the production of the ferrite decarburized layer by optimally controlling the steel component and the hot rolling conditions, etc. In addition to improving by more than 14%, there is an effect that can improve the fatigue life of steel.

Claims (1)

중량%로, 탄소(C):0.4~0.6%, 실리콘(Si):1.3~1.6%, 망간(Mn):0.5~0.7%, 크롬(Cr):0.4~0.7%, 잔부 Fe 및 기타 불가피한 불순물로 조성되는 빌렛(Billet)을 마련하는 단계;By weight%, carbon (C): 0.4-0.6%, silicon (Si): 1.3-1.6%, manganese (Mn): 0.5-0.7%, chromium (Cr): 0.4-0.7%, balance Fe and other unavoidable impurities Providing a billet (Billet) is composed of; 상기 빌렛을 1000~1100℃의 온도로 재가열한 다음 조압연하는 단계;Reheating the billet to a temperature of 1000 ~ 1100 ℃ and then rough rolling; 상기 조압연된 빌렛을 750~850℃에서 중간사상압연하고, 이어 동일한 온도범위에서 소재의 최종 감면율이 30%이상이 사상압연하는 단계;Intermediate rough rolling of the roughly rolled billet at 750 ° C. to 850 ° C., followed by finishing rolling at a final reduction rate of 30% or more in the same temperature range; 상기 압연된 선재를 750~800℃에서 권취한 후 600~650℃의 온도까지 1℃/s이하의 속도로 냉각하고, 이어 상온까지 공냉하는 단계;를 포함하는 페라이트 탈탄이 없는 스프링강의 제조방법Winding the rolled wire at 750 ~ 800 ℃ and then cooled to a temperature of less than 1 ℃ / s to a temperature of 600 ~ 650 ℃, and then air-cooled to room temperature; manufacturing method of the ferrite decarburization-free spring steel
KR10-2001-0083159A 2001-12-22 2001-12-22 A method for manufacturng spring steel without ferrite decarburization KR100516503B1 (en)

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KR20040027003A (en) * 2002-09-27 2004-04-01 주식회사 포스코 A manufacturing method of steel for spring without ferrite decarburization
CN102151693A (en) * 2010-12-02 2011-08-17 大冶特殊钢股份有限公司 Method for rolling low-hardness small-sized spring steel
KR101490600B1 (en) * 2013-07-01 2015-02-05 주식회사 포스코 Method for manufacturing wire rod
CN115055531A (en) * 2022-05-31 2022-09-16 鞍钢股份有限公司 Production method of automobile suspension spring with defect-free surface

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JPS5814857B2 (en) * 1979-01-25 1983-03-22 新日本製鐵株式会社 Method for preventing decarburization of steel materials for high Si springs
JPS5873718A (en) * 1981-10-26 1983-05-04 Kobe Steel Ltd Manufacture of steel material for high-silicon spring
JPH0672282B2 (en) * 1986-05-20 1994-09-14 大同特殊鋼株式会社 Low decarburized spring steel
KR100349148B1 (en) * 1997-12-11 2003-02-07 주식회사 포스코 A method for manufacturing wire roe for high silicon spring having high strength
KR100435483B1 (en) * 1999-12-28 2004-06-10 주식회사 포스코 A method for manufacturing wire rod for train rail creep with no surface defect and superior surface decarborization
KR100478088B1 (en) * 2000-12-21 2005-03-23 주식회사 포스코 A method for manufacturing spring steel without ferrite decaburization

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Publication number Priority date Publication date Assignee Title
KR20040027003A (en) * 2002-09-27 2004-04-01 주식회사 포스코 A manufacturing method of steel for spring without ferrite decarburization
CN102151693A (en) * 2010-12-02 2011-08-17 大冶特殊钢股份有限公司 Method for rolling low-hardness small-sized spring steel
KR101490600B1 (en) * 2013-07-01 2015-02-05 주식회사 포스코 Method for manufacturing wire rod
CN115055531A (en) * 2022-05-31 2022-09-16 鞍钢股份有限公司 Production method of automobile suspension spring with defect-free surface
CN115055531B (en) * 2022-05-31 2024-04-16 鞍钢股份有限公司 Production method of surface non-defective automobile suspension spring

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