KR20030026380A - Propolis Extract Grain Whiskey - Google Patents

Abstract

PURPOSE: Provided is a method for manufacturing grain whisky containing propolis extract. Therefore, the manufactured grain whisky has hangover removal effect, anti-oxidation effect, anti-bacterial effect, anti-inflammation effect, immunity activation effect and blood purification effect to prevent various diseases, displays amber color, and has flavonoid aroma. CONSTITUTION: The method for manufacturing grain whisky containing propolis extract characteristically comprises the steps of: mixing 60% of water extracted propolis with 40% of barley; heating at 65-70 deg. C for 2-3 hours and drying at 45-50 deg.C for 3-4 hours the mixture; mixing the dried ingredient with 30% of corn then followed by saccharifying, smoking, homogenizing, fermenting with 70% of ethanol extracted propolis and 30% of yeast; and centrifuging the fermentate then followed by distilling, cooling, filtering and aging it.

Description

Propolis Extract Grain Whiskey Containing Propolis Extract

The present invention relates to a method for producing a grain whiskey containing a propolis extract, more specifically, alcoholic extract as a food and drinking alcohol purified by using water or alcohol as a solvent to optimize the propolis biochemical and microbiological (EEP, Ethanol Extracted Propolis) or Water Extracted Propolis (WEP) is a raw material of grain whiskey which is mixed with barley and heated, mixed and saccharified with a smoker, fermented with yeast, and then distilled to health. A method for producing grain whiskey containing beneficial propolis extracts.

In general, whiskey refers to a distilled liquor obtained by fermenting cereals, especially barley, maize, and oats, and distilling again.Grain Whiskey is a whiskey made by saccharifying non-germinated malt. Unlike whiskey, the flavor is weak and light.

Propolis Alcoholic refers to beverages containing 0.01% or more of Propolis and 1% or more of alcohol or alcohol, which is a dense fat component called "good cholesterol" in the blood cholesterol. Increasing High Density Lard) and inhibiting the action of Low Density Lard (LDL), a "bad cholesterol" that causes arteriosclerosis.

The above-mentioned propolis liquor is divided into propolis brewing liquor and distilled liquor according to the preparation method, and the propolis distillation liquor is divided into propolis fermented liquor with propolis ethanol extract (EEP) or propolis water soluble extract (WEP). As a distillation method, the alcohol content is much higher than that of the original brew, and the alcohol content is relatively high and does not change well.Propolis grain whiskey belongs to the distillation of propolis.

About 20% of the propolis liquor ingested in our body is absorbed by the stomach, the other 80% is absorbed by the small intestine, and only 2-10% of the absorbed propolis liquor is urinated or exhaled through the kidneys or lungs. It is excreted from the body and more than 90% of the ingested propolis liquor is metabolized in the liver at a high rate, and the propolis liquor is broken down into acetaldehyde by alcohol dehydrogenase (ADH) in the liver. Decomposed acetaldehyde is converted to acetic acid by the action of Aldehyde dehydrogenase (ALDH) and disappears in the liver. During the metabolic process, alcohol is oxidized to produce acetaldehyde and acetic acid. ) Into water and carbon dioxide, which is discharged from the lungs and out of the body by the kidneys. Acetaldehyde, which is an intermediate product of alcohol decomposition in the body, is the cause of hangover. Acetaldehyde is not excreted in the body, causing redness of the face, heart palpitations, and headache and stomach pain. Quercechin-QUERCETIN relieves hangover pain by rapidly breaking down acetaldehyde and protecting liver tissue cells.

In addition, the flavonoids (quercechin-QUERCETIN), the center of the chemical composition of propolis, act as an antioxidant to prevent the formation of harmful free radicals in the blood. Activation, oral odor removal effect, vascular strengthening effect to expand and strengthen capillaries, and lower GPT level and protect liver damage. have.

Many functional beverages or compositions have been developed and marketed to promote hangover, by promoting alcohol decomposition, adding aspartic acid, or fermenting rice bran and soybeans. Even if the composition has not been proved and the diarrhea effect has been verified, it is cumbersome and a wasteful factor to drink it before and after drinking. In addition, a method of preparing a liquor containing propolis, which is a natural substance that functions to relieve hangover of the above-mentioned functional beverage or composition, has conventionally been used as an antioxidant, anti-salt function, Korean Patent Office (KR) Registered Patent Publication (B1) of the present applicant, which is a method of preparing a liquor containing a propolis extract prepared by using an antibacterial function, an antibiotic function and a cholesterol lowering function in the body, Manufacturing method "(notice date 2000.3.15, registration No. 10-0247125), which are pulverized propolis lumps collected from beehives at low temperature, soaked in cool water to settle, remove impurities, and then add dry solid powder as solvent. Homogenize the mixture and centrifuge the extracted propolis suspension into a supernatant and solids. After separation, the separated supernatant was filtered at low temperature to remove wax and dried, and then the propolis semi-solid stock solution was added to various liquors to prepare liquor containing propolis extract. There is a problem in producing high-quality distilled spirits of fermentation or maturing conditions that can be optimally combined with the propolis extract by adding with various liquors prepared.

The present invention has been made to solve the above-mentioned problems, the ethanol extract (EEP, Ethanol Extracted Propolis) of the most suitable biochemical and microbiological conditions extracted using 70% ethanol as a solvent of propolis Water extracted propolis (WEP) is used as a raw material by mixing together the grains of barley as a raw material, heating, mixing and saccharifying them with a smoker, fermenting with yeast, distilling and ripening to produce propolis grain whiskey. It is a method, which can be easily shared with grains such as barley compared to the solids of propolis itself, and the propolis (flavonoid) components of EEP and WEP can be used biologically and biochemically by using poplar trees as materials of ripening tanks or storage tanks. The fermentation tanks were prepared with the raw materials under the most appropriate conditions. The use of ceramic provides sufficient air, temperature, and humidity for fermentation or ripening of grains, and it is beneficial to human body by the action of flavonoids (Quercechin-QUERCETIN) as a way to keep propolis ingredients fresh and unchanged for a long time. It is aimed to provide high quality propolis grain whiskey.

1 is a flow chart showing the manufacturing process of the grains whiskey containing the propolis extract of the present invention

Figure 2 is a process chart showing the manufacturing process of the propolis extract containing grain whiskey of the present invention

The configuration of the present invention will be described in detail as follows.

The present invention is mixed with aged ethanol extract (EEP, Ethanol Extracted Propolis) or water-soluble extract (WEP, Water Extracted Propolis) barley (Barley), dried and mixed together and then saccharified together fermentation, centrifugation, distillation, It is cooled and aged to provide a method for producing grain whiskey containing a propolis extract, which is aged in a poplar barrel as a high alcohol content.

The ethanol extract (EEP) or water soluble extract (WEP) of propolis used in the present invention is the same as the present invention, as described in Korean Patent No. 10-0247125, "Preparation method of liquor containing propolis extract". Get in the way.

Reference Example 1: Preparation of Ethanol Extract (EEP)

Propolis lumps collected from beehives are ground at low temperature below -4 ℃, immersed in cooling water and precipitated for 30-60 minutes to remove impurities, and mixed with dry solid powder in 70: 1 ethanol as a solvent at a ratio of 1: 2 Homogenize at 3000rpm for 30 minutes to extract propolis suspension, centrifuge the extracted suspension for 30 minutes at 5000rpm, separate the supernatant and solids, and separate the supernatant from low temperature with filter paper. Filtered to remove wax, dried with a dryer so as not to change the content of the propolis, and filtered at -20 ℃--10 ℃ according to the type of liquor and left for 24 hours to maximize physiological function of pure brown brown propolis ethanol extract ( EEP, Ethanol Extracted Propolis).

Reference Example 2: Preparation of Water Soluble Extract (WEP)

Propolis lumps collected from beehives are ground at low temperature below -4 ℃, soaked in cooling water and settled for 30-60 minutes to remove impurities, and mixed with dry solid powder in pure water (distilled water) at a ratio of 1: 2 as a solvent. Homogenize with a homogenizer for 30 minutes at 3000 rpm to extract the propolis suspension, centrifuge the extracted suspension for 30 minutes at 5000 rpm with a centrifuge, separate the supernatant and solids, and then separate the separated supernatant with filter paper at low temperature. Purified to remove wax, dried with a dryer to prevent changes in the content of the propolis, filtered at -20 ℃--10 ℃ according to the type of liquor and left to stand for 24 hours to maximize the physiological function of pure propolis alcohol A water-soluble extract (WEP, Water Extracted Propolis) is obtained, which is cloudyly mixed with water.

In the above Reference Example 1 of the present invention, the propolis solid powder was mixed with 70% ethanol as a solvent at a ratio of 1: 2 and homogenized at 3000 rpm for 30 minutes using a homogenizer to extract a propolis suspension. Flavonoids are extracted by flavonoids, which are Resin, which accounts for 45% to 55% of the polys. The flavonoids are measured by UV-Spectrometer (366nm) and are flavonoids within the band range of up to 288nm to 325nm. Obtain (Quercetin).

Barley is mixed, aged, dried and mixed with high-quality propolis ethanol extract (EEP) or water extracted propolis (WEP) obtained by the above-mentioned method, and then saccharified together, followed by fermentation and centrifugation. Propolis grain whiskey is prepared by distillation, cooling and aging.

According to the present invention, a poplar tree is used as a material for a storage container, and as a result, a poplar tree contains antibiotics, and most bees are known to obtain propolis from a poplar tree. Since the collected propolis has a high flavonoid content, especially the high content of quercechin, which makes it an excellent value for propolis, the propolis (flavonoid) component of EEP or WEP can be used as a biological material (microbiology). ), To be shared with other raw materials under the most suitable biochemical conditions.

In addition, the reason why the fermentation tank is made of bio-ceramic is that it is corrosion-resistant and porous, so it is effectively used for separating and filtering various mixtures, and fermentation of cereals requiring sufficient air and humidity. In fermentation, bio-ceramic not only provides the most suitable microbiological conditions for yeast fermentation, but also provides the most suitable microbiological conditions such as temperature, humidity and air. To preserve.

In addition, vacuuming using a vacuum machine is intended to extract pure components quickly without destroying the original components.

A detailed manufacturing method according to the fractional distillation method (DDM) of the propolis grain whiskey of the present invention will be described in detail with reference to the accompanying drawings.

The present invention adds 40% of the bark to 60% water extracted Propolis (WEP) and aged in the poplar wood maturing tank for 2 to 3 days at 55 ℃-60 ℃ (S10, raw material) Mixed aging process), burning poplar charcoal at 65 ° C.-70 ° C. in a heating tank made of stainless steel for 2 to 3 hours (S11, heating tank heating step) and 3-4 at a temperature of 45 ° C. to 50 ° C. in a dryer. Drying time (S12, dryer drying step). 30% of the ungerminated corn and dried raw materials are mixed in a mixing bath (S13, raw material mixing step). Mixed aged raw materials were sugared in a sugar bath at a temperature of 55 ℃ -60 ℃ with 60% WEP, 40% rye and wheat for 4-5 hours (S14, Saccharification tank saccharification process). Smoke and burn fragrance (S15, smoker smoker process), fermentation tank made of bio-ceramic fermentation tank made of bio ceramics at 60 ℃ -65 ℃ for 3-4 hours with 70% EEP and 30% yeast After treatment (S16, bio-ceramic fermentation tank fermentation process), centrifuged at 7000 rpm for 15 minutes using a centrifuge (S17, centrifugation process), and the crude liquor, which had undergone saccharification, fermentation, and centrifugation, was subjected to 60 ° C in a primary fractionator. Fractional distillation with% WEP was used to extract the distillate, second distillation was performed with 70% EEP, and the first concentrated distillate was collected (S18, 3). Step fractional distillation process), followed by three successive cooling filtration processes (S 19, three-stage cooling filtration process), put into a poplar cask and aged at a temperature of 4 ℃-9 ℃ for 3-4 years cool and high humidity (S20, Poplar barrel ripening process)

By smoking the poplar tree in the above-described smoking process, the incense comes from the smoke in which the peculiar McCoy Flavor permeates.

In the above fractional distillation process, the remaining emulsion from the second fractional distillation is sent to the first fractionation distillate and the remaining fraction from the third fractional distillation is sent to the second fractionation distillation unit.

In the centrifugation process, the rpm of the centrifuge is 7000 rpm and the time is 15 minutes, because the higher concentration of liquor, the easier it is to mix at high speed and the flavonoids are well extracted.

In addition, distillation of the fermented stock solution in three stages is carried out by using ethanol extract (EEP, Ethanol Extracted Propolis) or water extract (WEP, Water Extracted Propolis) and alcohol in primary vacuum using the difference between the concentrations of alcohol and water. When the heat for fractional distillation is applied, crystals and oils are removed secondarily due to the temperature difference, and as a result, only pure compounds are passed through the three stage cooler, As the boiling point of alcohol (78.325 ℃) is lower than the boiling point of water (99.975 ℃), the alcohol evaporates before water, and these evaporating gases are collected and cooled to become liquid and obtain alcohol containing high concentration of alcohol. have.

An embodiment of the present invention is described as follows.

Example 1.Propolis Grain Whiskey Preparation

1.Propolis Ethanol Extract (EEP) Extraction Process

1-1. Propolis Suspension Extraction Process

Propolis lumps collected from beehives are pulverized at -4 ℃ at low temperature, soaked in cooling water and precipitated for 60 minutes to remove impurities, and the dried solid powder is mixed with 70% ethanol as a solvent in a 1: 2 ratio to a homogenizer. Homogenize at 3000 rpm for 30 minutes to extract the propolis suspension.

1-2. Propolis Wax Removal Process

The suspension extracted in step 1-1 was centrifuged at 5000 rpm for 30 minutes by centrifugal separation, separated into a supernatant and a solid, and the separated supernatant was filtered through a filter paper at low temperature to remove wax.

1-3. Propolis Ethanol (EEP) Extraction Process

Dried with a dryer so as not to change the component content of the propolis obtained in step 1-2, filtered at -10 ℃ and left for 24 hours to obtain a pure brown ethanol extract (EEP, Ethanol Extracted Propolis) maximized physiological function Get

2. Propolis Grain Whiskey Manufacturing Process

2-1. Raw material mixing aging process

40% of barley is added to 60% of Water Extracted Propolis (WEP) and aged for 2-3 days in a poplar tree maturing bath at a temperature of 55 ° C. to 60 ° C.

2-2. Heating tank heating process

Burn poplar charcoal at 65 ℃ -70 ℃ in a heating tank made of stainless steel and heat it for 2-3 hours.

2-3. Dryer drying and mixing process

After drying for 3-4 hours at a temperature of 45 ℃-50 ℃ in a dryer and mixed with 30% of the ungerminated corn and dry raw material mixing bath.

2-4. Party Septic Tank Process

Mixed aged raw materials are glycosylated in a saccharification bath at temperatures between 55 ° C. and 60 ° C. with 60% WEP, 40% rye and wheat for 4-5 hours.

2-5. Smoking machine smoking process

Burn the poplar tree in the smoker to smoke and smell it.

2-6. Bio Ceramic Fermentation Tank Fermentation Process

The raw materials treated in the previous process are fermented as 70% EEP and 30% yeast at 60 ° C-65 ° C for 3-4 hours in a fermentation tank made of bio ceramics.

2-7. Centrifugation process

Centrifuge for 15 minutes at 7000 rpm with a centrifuge.

2-8. Three stage fractional distillation process

The distillate was extracted by fractional distillation with 60% WEP in the first fractionation distillate and the second fractionation distillation with 70% EEP in the first fractionation process. The concentrated milk is collected and fractionated for the third time.

2-9. Three stage cold filtration process

The distillate is passed through a cold filter three times and filtered by cooling.

2-10. Poplar barrel aging process

It is placed in a poplar barrel and aged at 3-4 years at a temperature of 4 ° C.-9 ° C. to cool and high humidity to prepare a high concentration of propolis grain whiskey with an alcohol content of 35-40 °.

Propolis grain whiskey of the present invention prepared in this way increases the content of high density fat (HDL) of cholesterol in the blood and inhibits the action of low density fat (LDL) to prevent atherosclerosis and produced by drinking alcohol The flavonoids (quercechin) of propolis grain whiskey decompose acetaldehyde quickly to protect liver tissue cells and to prevent flavonoids from forming harmful oxygen (FreeRadical) in the blood. In particular, it contains four Di-Ocaffeoyl Quinic Acid-related substances in Propolis Grain Whiskey Extract, which provides excellent liver protection, lowers GPT levels and protects damaged livers. In addition, Chlorogenic Acid, Caffeic Acid and Dihydrocaffeic Acid were highly protective. It is of importance in designing effective pharmacological therapies that can fully cure or control diseases caused by bacteria with very strong antitoxin resistance. Propolis itself acts very strongly as a biological agent-its antimicrobial sexual importance was assessed by +++ (Grochowsk et al. 1985). In addition, propolis grain whiskey has a hangover, antioxidant, and antibacterial effect, and it is effective to prevent various diseases and improve health by inhibiting inflammation, activating immune system, blood purification and vascular strengthening, and it is mild in taste and inherent flavor of flavonoids. Easy to drink by smell

Claims (1)

A propolis liquor comprising a propolis extract purified by extracting a mass of propolis from a beehive, Mixed raw material ripening process (S10) by adding 40% of barley to 60% of water extracted propolis (WEP) for 2-3 days at a temperature of 55 ° C. to 60 ° C. in a poplar maturing bath, Heating tank heating process for burning Poplar wood charcoal at 65 ℃ -70 ℃ in heating tank made of stainless steel for 2 ~ 3 hours (S11), drying process drying for 3-4 hours at 45 ℃ -50 ℃ in dryer (S12). Raw material mixing process (S13) which mixes 30% of ungerminated corn and dried raw material in a mixing tank. Saccharification tank saccharification process (S14), where the mixed aged raw materials are liquefied for 4-5 hours with 60% WEP, 40% rye and wheat at a temperature of 55 ℃ -60 ℃ in a sugar tank, and a poplar tree is burned in a smoke machine. Smoker process to smoke and scent fragrance (S15), fermentation process of raw material processed in the whole process as 70% EEP and 30% yeast at 60 ℃ -65 ℃ in fermentation tank made of bio-ceramic for 3-4 hours Bio-ceramic fermentation tank fermentation process (S16), centrifugation process (S17) for 15 minutes centrifugation at 7000rpm with centrifuge, and the crude liquor, which has undergone saccharification, fermentation and centrifugation, with 60% WEP in the primary fractionator. Fractional distillation to extract the distillate, second fractional distillation with 70% EEP, second fractional distillation with the first concentrated distillate and third fractional distillation Distillation process (S18), chiller continuous Three-stage cooling filtration process (S19) to cool the filtration by passing through three times, and put into a poplar barrel into a poplar barrel aging process (S20) to ripen at a high temperature and cool the humidity 3-4 years at 4 ℃-9 ℃ (S20) Method for producing grain whiskey containing the propolis extract, characterized in that