KR20090038645A - Manufacturing method of pine needles essence and the essence which it uses - Google Patents

Abstract

A method for preparing pine needles concentrate is provided to obtain 100% of pine needles concentrate by distilling, evaporating and fermenting the pine needles under the condition of predetermined temperature and time. A method for preparing pine needles concentrate comprises the following steps of: selecting pine needles(100); washing the selected pine needles(200); drying the washed pine needles(300); cutting and pulverizing the dried pine needles(400); mixing the pulverized pine needles and water and distilling the mixture to prepare a condensed liquid(500); preparing crude extract from the condensed liquid and removing foreign materials(600); dehydrating the crude extract and filtering the dehydrated crude extract(700); and aging the filtered crude extract(800). The pine needles and water are mixed at 95°C or greater and distilled for 2-6 hours.

Description

Method of manufacturing pine needle distillate and pine needle distillate using the same {MANUFACTURING METHOD OF PINE NEEDLES ESSENCE AND THE ESSENCE WHICH IT USES}

The present invention relates to a method for preparing pine needle distillate and a pine needle distillate using the same, and more particularly, to collect pine needles of North Korean red pine and to prepare a pine needle distillate concentrate of 100% concentration using the same and the method It relates to a pine needle distillate concentrate prepared.

Pine trees should have brilliance grown in deep mountains, and leaves, berries, and rosin are used for the prevention and treatment of adult diseases. Among pines, red pine, a native species of medicinal plant, is the best medicinal and uses raw or dried leaves in the shade. It is effective for gastrointestinal diseases, high blood pressure, stroke, neuralgia and asthma.

Pine needles are rich in essential amino acids, which are important protein sources that form the human body, which cannot be synthesized in the body, so they have to be ingested from the outside. There are 22 different types of amino acids, eight of which are needed for adults and ten for growing children. Pine needles surprisingly contain all eight essential amino acids needed by adults.

In Dongbogam, if you reproduce pine needles for a long time, they will not grow old, become vigorous, darken your head, and may not know the cold and hunger. Hyangyakbangbang introduces the same effect that if you chop pine needles into small pieces like millet and eat it, your body will be warmed, your strength will rise and you won't get cold. One of the key components of pine needles is terpene, a volatile component that flies into the air. Currently, more than 40 species of terpenes in pine needles have been identified. The most constituents are alpha-pinene, beta-pinene, beta-phellandrene, beta-cayfilene, myrcene, campain, alpha-terpinolene and the like. Hardwoods also have unique terpenes, but they have terpenes that are much richer.

When pine toxins are absorbed by the human body, they stimulate the walls of blood vessels to help blood flow, activate various functions of the body, and drive off parasites and germs. After all, we use the poison produced by pine trees to prevent and cure our diseases.

On the one hand, pine needles are bitter, but the nature is warm and non-toxic, mainly acts on the heart and parenteral. Recent pharmacological experiments in China and North Korea have revealed that the redox process of biological tissues promotes the elimination of astringent inflammation and stops blood. Another advantage of pine needles is that they are not related to people's constitution, unlike herbs that increase or decrease body heat.

In Dongbobogam and Herbal Cortex, pine needles are said to be good longevity medicine for stroke and high blood pressure. There is a good reason why pine needles receive this praise. The stimulation and physical activity of the terpene and blood circulation and blood vessel wall strengthening may be one reason, but the unique fatty acids in pine needles also make a big contribution. The fatty acids in pine needles are different from animal fats and the same vegetable fats. Pine needles contain about 20% of linolenic acid, followed by palmitic acid for 10%. In addition, there are many polyunsaturated fatty acids, including 5-olefinic acid, which is not easily oxidized. Because it does not oxidize, it does not produce harmful substances such as lipid peroxide and prevents aging.

Aging is caused by free radicals in the human body. The more active free radicals, the faster the body ages and the less resistance to disease. Looking at what harmful oxygen does to the human body is as follows. In the process of energy metabolism in which oxygen is reduced to water in the body, active oxygen is produced when oxygen does not get as much hydrogen as it needs. Isolated and alienated free radicals rush around in search of other substances, leaving their binding rings open.

These oxygens in particular damage the inner walls of fragile cell membranes or arteries, and in some cases may produce mutant cells that cause cancer. This harmful oxygen is made more by overeating, and it can also occur through pollutants, which can damage genes. These oxygens also combine with fats absorbed by meat intake, forming harmful lipid peroxides. That's why they eat a lot of unsaturated fatty acids. When the lipid peroxide corrodes blood vessels, the blood vessels become blocked and cholesterol, etc., adheres to the blood vessel walls, causing arteriosclerosis. In severe cases, myocardial infarction or stroke may also occur. The human body then releases an antioxidant enzyme called "SOD (Superoxide Dismutase)" to inhibit the action of oxidative activity, which varies with man and with age. After all, in order to suppress aging, we need to consume substances that promote or produce antioxidant enzymes from the outside.

This function is the pine needle. Well known antioxidants or anti-aging agents include vitamins A and E and beta carotene. Pine needles contain all of these ingredients except vitamin E. The terpene, which is rich in pine needles, also combines with oxygen to form oxides, which can reduce significant amounts of free radicals. According to an experiment conducted by a research institute in Japan, pine needle solution showed 50% oxidation inhibition rate.

None of the ancestors and saints who tell the record that they were born by fire did not eat pine-related things, such as pine needles, pine nuts, pine nuts (Sol-se or pine nuts) and Bokryong. It may be an exaggeration to say that they lived hundreds of years, but it is clear that pine needles are longevity foods.

The present invention is made to produce a pine needle distillate concentrate from pine needles having the above-mentioned efficacy, the main object of the present invention is a manufacturing method for extracting pine needle distillate concentrate of 100% concentration from pine needles of North Korean red pine and manufactured using the same The purpose of the present invention is to provide distillate concentrate.

In order to achieve the above object, a pine needle distillation concentrate production method of the present invention and pine needle distillation concentrate using the same, the first step of collecting and selecting pine needles; A second step of washing the selected pine needles; A third step of drying the washed pine needles; A fourth step of cutting and pulverizing the dried pine needles; A fifth step of mixing and distilling the ground pine needles and water to make condensed water; A sixth step of fractionating foreign matters from the production of crude oil from the condensate; A seventh step of removing water through the evaporator and adjusting the fractionated oil separated by the foreign matter and filtering the result by a micro filter; An eighth step of aging a product obtained through the seventh step; The ninth step of measuring the quality standards of the matured product; is achieved by including, and is also achieved by producing a pine needle distillate concentrate using this.

Here, the second step is characterized in that to remove foreign substances by washing three steps with clean water.

In addition, the third step, and put the washed pine needles in a dryer, characterized in that the drying to less than 5% moisture content.

On the other hand, the fourth step, after cutting the dried pine needles to 10mm, it is characterized by pulverizing to less than 3mm using a grinder.

In addition, the fifth step, 150 kg of pine needles and 230 kg of water, characterized in that the distillation by heating for 2-6 hours at 95 ℃ or more.

In addition, the seventh step is characterized in that the evaporator removes water at least 95 hours at 95 ℃ or more and then filtered.

In addition, the eighth step, it is characterized in that aged for 10 to 40 days in a cool dark place.

According to the present invention as described above, by using the method of producing pine needle extract of 100% concentration from pine needles of the North Korean red pine and pine needle extract prepared by this method helps to maintain healthy blood sugar, anti-aging, diabetes, There is an effect that can be used to prepare health foods and supplements that are effective in hypertension, strengthening stamina, improving liver function, bad breath, cerebral hemorrhage and skin care.

Hereinafter, exemplary embodiments of the present invention will be described in detail with reference to the accompanying drawings.

1 is a view showing a manufacturing method according to an example of a pine needle distillation concentrate and pine needle distillation extract using the same according to the present invention.

First, as shown in FIG. 1, a first step 100 of collecting and selecting pine needles; A second step (200) of washing the selected pine needles; A third step (300) of drying the washed pine needles; A fourth step 400 of cutting and grinding the dried pine needles; A fifth step (500) of mixing and distilling the pulverized pine needle and water to make condensed water; A sixth step (600) of separating the foreign matter and production of the adjustment oil from the condensate; A seventh step (700) of removing the moisture through the evaporator to separate the foreign matter and the fractionating oil and filtering the resultant with a micro filter; An eighth step 800 of aging a product obtained through the seventh step 700; A ninth step (900) of measuring the quality standards of the matured product; is made, including, to prepare a pine needle distillation concentrate prepared using this.

Here, in the first step (100), the red pine tree (Oak tree) of Pyonganbukdo is collected in May to June, and then only the fresh pine needles are selected, and the fresh pine needles are collected and diseased or worms are picked and removed. .

 In addition, the second step 200, three steps of washing with clean water to remove foreign substances, the selected pine needles are put into the washing tank and washed three times in running water. The washing step is a first step of removing foreign matter from pine needles, which helps to lower the impurity content of the pine needle distillate concentrate.

On the other hand, the third step 300, and put the washed pine needles in a dryer to dry less than 5% moisture content, the fourth step 400, cut the dried pine needles to 10mm After that, it is characterized by pulverizing 3mm or less using a grinder. The ground pine needles are transferred to a distillation tank.

In addition, the fifth step 500, 150kg and 230kg of water mixed with pine needles, characterized in that the distillation by heating for 2-6 hours at 95 ℃ or more, although not shown dried in a 300L steam distillation tank 150 kg of pine needles and 230 kg of purified water are added, the lid of the distillation tank is closed and the air control valve of the air compressor is opened and supplied to the lid to maintain complete airtightness. In addition, although not shown, the steam of about 9 bar generated by the steam boiler passes through a pressure reducing valve installed at the boiler outlet, and is decompressed to about 6 bar and sent to the steam distributor, and the 6 bar of steam supplied from the steam distributor is external to the distillation tank. It is supplied to the casing high pressure steam line to quickly increase the temperature of the pine needle grinding material of the distillation tank to more than 95 ℃, the high pressure steam line (6bar) through the pressure reducing valve 1bar low pressure steam through the bottom of the distillation tank into the distillation tank Other components, including the essential oil component contained in the pine needle pulverized, are volatilized by steam supplied from the bottom, and the steam containing the essential oil flowing out after heating at 95 ° C or higher for 2 to 6 hours or more. Moves to the cooler.

At this time, although not shown, the steam discharged from the steam tank is controlled in conjunction with the pressure sensor for checking the internal pressure of the distillation tank by the flow control valve, and controls the amount of steam passed to maintain the internal pressure of the distillation tank at 1 bar. Will be moved to the cooler. Since the coolant supplied from the cooling tower is circulated inside the cooler, water vapor containing the essential oil components passing through the cooler is condensed through heat exchange in the cooler, and the condensate is maintained at a temperature of about 30 ° C. and collected in the oil / water separator. do.

In the oil / water separator, a lighter component that is lighter than water floats on the upper layer, and is checked through a transparent window of the oil / water separator, and then, by opening a valve provided in an oil refinery discharge pipe located above the boundary, the oil is collected and sent to the crude oil storage tank, and separated into the lower layer. The collected effluent and foreign matter are drained and stored in the effluent storage tank through the discharge pipe.

In addition, although not shown, the crude oil obtained by the above method is subjected to water removal and filtration through an evaporator. The crude oil is placed in an evaporator and heated at 95 ° C. or more for 7 hours to evaporate moisture, and the micro filtration filter. Impurities are removed using.

After the above process, although not shown, the final pine leaf extract solution (essential oil) is moved to the refined oil aging tank is aged for 10-40 days in the dark place for the balance (stabilization) and flavor and flavor of the final chemical components.

Pine needle distillate concentrated after the aging process is measured by the following quality standards.

A) Properties and general characteristics

-Light yellow transparent oil, fresh pine smell

Specific gravity: d ₂₀ 0.865 ~ 0.8740

Refractive index: nD 1.4745 ~ 1.4780

-Luminous intensity: αd -23.47 ° ~ -24.22 °

B) Acid value: 0.50 or less

C) Peroxide value: below 10.0

D) Coliform group: should be negative.

E) 3-karen: more than 12.00%

F) limonene: more than 5.00%

Terpinolene: 17.50% or more

That is, the final pine needle distillate concentrate to meet the standard through the above quality standards.

In addition, genotoxicity test was performed on the pine needle distillate concentrate prepared by the above method. According to the results of the test conducted by the Korea Testing Institute from November 23, 2006 to December 27, 2006, the microbial return mutation test was negative. Negative reaction in the reaction, chromosomal aberration test, negative reaction in the micronucleus test (Test method: Korea Food and Drug Administration Notification No. 2005-60)

While the present invention has been illustrated and described with respect to preferred embodiments, the invention is not limited to the above-described embodiments, and is commonly used in the field of the invention without departing from the spirit of the invention as claimed in the claims. Anyone with a variety of variations will be possible.

1 is a view showing a manufacturing method according to an example of a pine needle distillation concentrate and pine needle distillation extract using the same according to the present invention.

<Description of Symbols for Major Parts of Drawings>

100: 1st stage 200: 2nd stage

300: step 3 400: step 4

500: 5 steps 600: 6 steps

700: 7 steps 800: 8 steps

900: 9 steps

Claims (8)

A first step (100) of collecting and selecting pine needles; A second step (200) of washing the selected pine needles; A third step (300) of drying the washed pine needles; A fourth step 400 of cutting and grinding the dried pine needles; A fifth step (500) of mixing and distilling the pulverized pine needle and water to make condensed water; A sixth step (600) of separating the foreign matter and production of the adjustment oil from the condensate; A seventh step (700) of removing the moisture through the evaporator to separate the foreign matter and the fractionating oil and filtering the resultant with a micro filter; An eighth step 800 of aging a product obtained through the seventh step; A ninth step 900 of measuring quality standards of the matured product; Method of producing a pine needle distillation concentrate, characterized in that comprises a. The method of claim 1, wherein the second step 200, Method of producing a pine needle distillate, characterized in that to remove foreign matter by three steps of washing with clean water. The method of claim 1, wherein the third step 300, Put the washed pine needles in a dryer to dry the pine needle distillate concentrate, characterized in that the dried to less than 5% moisture content. The method of claim 1, wherein the fourth step 400, After cutting the dried pine needles to 10mm, using a pulverizer pulverized to 3mm or less characterized in that the method for producing a distillate concentrate. The method of claim 1, wherein the fifth step 500, Method of producing a pine needle distillate concentrate, characterized in that the pine needles 150kg and water 230kg mixed to distill by heating for 2-6 hours at 95 ℃ or more. The method of claim 1, wherein the seventh step 700, Method of producing a pine needle distilled liquid, characterized in that the filter after removing water for 7 hours at 95 ℃ or more in the evaporator. The method of claim 1, wherein the eighth step 800, A method for producing pine needle distillate, characterized in that aged for 10 to 40 days in a cool dark place. Pine needle distillate concentrate prepared by the method of claim 1.

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