KR20030008746A - Manufacturing method of water treatment agent using mineral - Google Patents

Manufacturing method of water treatment agent using mineral Download PDF

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Publication number
KR20030008746A
KR20030008746A KR1020010043626A KR20010043626A KR20030008746A KR 20030008746 A KR20030008746 A KR 20030008746A KR 1020010043626 A KR1020010043626 A KR 1020010043626A KR 20010043626 A KR20010043626 A KR 20010043626A KR 20030008746 A KR20030008746 A KR 20030008746A
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South Korea
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treatment agent
water
water treatment
sulfuric acid
solution
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KR1020010043626A
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Korean (ko)
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최연수
장중기
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최연수
장중기
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Priority to KR1020010043626A priority Critical patent/KR20030008746A/en
Publication of KR20030008746A publication Critical patent/KR20030008746A/en

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    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/68—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water

Abstract

PURPOSE: A method for preparing water treatment agent using minerals is provided to mix the water treatment agent with water injected into a water purifier so that mineral materials are contained in drinking water, and supply a mixture of the water treatment agent and water to plants so that growth of the plants is promoted. CONSTITUTION: The method for preparing water treatment agent using minerals comprises first process of crushing minerals such as sericite, veinstone or phyllite in the ore state to a particle size corresponding to a sieve size of 60 to 150 mesh, and removing impurities by refining the crushed mineral; second process of heating and agitating the mixture after adding some of sulfuric acid solution and water to the mineral in the state that the refined mineral is put into a container having a high corrosion resistance so as to extract distilled water from the mixture; third process of preparing 20 to 40% aqueous sulfuric acid solution by mixing the distilled water extracted from the second process with an undiluted sulfuric acid solution; fourth process of heating the mixture in a sealed container to a temperature of 80 deg.C or higher for 10 hours after mixing the 20 to 40% aqueous sulfuric acid solution with the minerals agitated in the second process in a mixing ratio of 1:1; fifth process of extracting water treatment agent from which crushed ore is filtered by pressing the solution using a filter press, thereby penetrating the solution into a filter paper having a pore size of 2 microns; sixth process of thickening concentration of the water treatment agent by heating the extracted water treatment agent; and seventh process of extracting a sediment removed solution from a mixed solution in which sediments are settled down by leaving the mixture still for 24 hours after mixing the thickened water treatment agent with germanium contained underground water in a mixing ratio of 1:4.

Description

광물을 이용한 수처리제의 제조방법{omitted}Manufacturing method of water treatment agent using minerals {omitted}

본 발명은 광물을 이용한 수처리제의 제조방법에 관한 것으로, 견운모 광석, 맥반석, 천매암 등의 광물을 파쇄하고 정제한 원료를 황산용액과 섞으면서 증류수를 추출한 후 황산원액을 혼합하여 황산수용액을 제조하고, 이 황산수용액과 광물을 1:1로 혼합하면서 가열하여 광물이 걸러진 수처리제를 진하게 한 후 지하수와 혼합하여 수처리제를 제조하도록 함으로써 정수장치에 삽입되는 물에 혼합하여 미네랄물질이 포함될 수 있도록 하거나 식물의 성장을 촉진시킬 수 있도록 한 광물을 이용한 수처리제의 제조방법에 관한 것이다.The present invention relates to a method for producing a water treatment agent using minerals, and to prepare a sulfuric acid solution by extracting distilled water while crushing minerals such as biotite ore, ganban stone, cheonmaeum and the like with a sulfuric acid solution, and distilled water, The sulfuric acid aqueous solution and minerals are mixed in a 1: 1 ratio to heat the filtered water treatment agent, and then mixed with the groundwater to prepare the water treatment agent. It relates to a method for producing a water treatment agent using a mineral that can promote the.

일반적으로 사람들은 살아가는 것에 물이 반드시 필요하다. 따라서 사람이 물을 마시게 되어 신체에 필요한 수분을 보충하면서 살아가는 것이다. 그러나 요즈음에는 공해 등에 의하여 하천의 물을 정제하지 않은 상태에서 마시는 것이 곤란하게 되었기 때문에 정수장치가 반드시 필요하였다. 따라서, 정부에서는 통합적으로 정제된 수돗물을 일반 가정에 보내기는 하지만 염소 등이 섞여 나오기 때문에 가정에서도 정수장치를 부착하여 실시하는 실정이다.In general, people need water to live. Therefore, people drink water to live while replenishing the body's needed moisture. However, these days, water purification equipment is necessary because it is difficult to drink the water of the river without purification due to pollution and the like. Therefore, although the government sends integrated tap water to general households, chlorine and the like are mixed in the home, so the household is equipped with a water purifier.

따라서, 종래에는 가정에서도 활성탄과 필터를 이용한 정수장치를 사용하여 염소나 수도관에서 발생된 녹 등을 제거하여 정수된 물을 사용자가 음용하고 있는 것이다.Therefore, conventionally, the user is drinking water purified by removing chlorine or rust generated from a water pipe using a water purifier using activated carbon and a filter at home.

그러나 상기와 같은 종래에는 정수장치가 단순히 물 속에 포함된 불순물만을 제거하는 것이기 때문에 사람에게 해로운 유기물을 걸러내지 못하였으며, 사람에게 유용한 미세한 성분은 정수장치에 의하여 걸러지기 때문에 무기물 중에서 미네랄성분까지 정수되므로 유용한 성분을 마시지 못하게 되는 단점이 있었다.However, in the related art, the water purifier simply removes impurities contained in the water, and thus, it is not possible to filter out organic substances harmful to humans. There was a disadvantage of not drinking the useful ingredients.

따라서 본 발명은 이와 같은 사정을 고려하여 착안한 것으로 견운모 광석, 맥반석, 천매암 등의 광물을 파쇄하고 정제한 원료를 황산용액과 섞으면서 증류수를 추출한 후 황산원액을 혼합하여 황산수용액을 제조하고, 이 황산수용액과 광물을 1:1로 혼합하면서 가열하여 광물이 걸러진 수처리제를 진하게 한 후 지하수와 혼합하여 수처리제를 제조하도록 함으로써 정수장치에 삽입되는 물에 혼합하여 미네랄물질이 포함될 수 있도록 하거나 식물의 성장을 촉진시킬 수 있도록 한 광물을 이용한 수처리제의 제조방법을 제공하는 것을 그 목적으로 한다.Therefore, the present invention has been conceived in view of such circumstances, and the distilled water is extracted while crushing minerals, such as sorghum feldspar, elvan, and feldspar, with purified sulfuric acid, and then distilled water is mixed to prepare an aqueous sulfuric acid solution. Sulfate aqueous solution and minerals are mixed 1: 1, heated to thicken the filtered water treatment agent, and then mixed with groundwater to prepare the water treatment agent. It is an object of the present invention to provide a method for producing a water treatment agent using minerals which can be promoted.

상기와 같은 목적을 달성하기 위하여 본 발명은 견운모 광석, 맥반석, 천매암 등의 광물을 파쇄하여 정제하는 공정과,In order to achieve the above object, the present invention is a process for crushing and refining minerals, such as biotite ore, elvan

그 정제된 원료를 황산용액과 섞어 용기 내에서 가열, 교반하여 증류수를 추출하는 공정과,Mixing the purified raw material with a sulfuric acid solution and heating and stirring in a container to extract distilled water;

상기의 증류수와 황산원액을 혼합하여 20∼40%의 황산수용액을 제조하는 공정과,Mixing distilled water and sulfuric acid stock solution to produce a 20-40% sulfuric acid solution,

상기의 황산수용액과 교반을 끝낸 광물을 1:1로 혼합한 후 밀폐용기에서 80℃ 이상의 온도에서 10시간 이상 가열하는 공정과,Mixing the aqueous sulfuric acid solution and the stirred minerals in a 1: 1 ratio and then heating the resultant container at a temperature of 80 ° C. or higher for at least 10 hours,

상기의 용액을 프레스로 누른 후에 거름종이를 통과시켜서 광물이 걸러진 수처리제를 추출하는 공정과,Pressing the solution with a press and then passing the filter paper to extract the filtered water treatment agent with minerals;

상기의 수처리제를 가열하여 용액을 진하게 하는 공정과,Heating the water treatment agent to thicken the solution,

상기의 용액을 게르마늄 등이 포함된 지하수와 1:4의 비율로 혼합한 후에 24시간 방치하여 침전물이 제거된 용액을 추출하는 공정에 의하여 수처리제를 제조함으로써, 정수장치에 삽입되는 물에 본 발명에 의하여 제조된 수처리제를 혼합하여 사람에게 유용하지만 부족하기 쉬운 미네랄물질이 식수에 포함될 수 있도록 하며, 본 발명의 수처리제를 물과 혼합하여 식물에 공급하여 식물의 성장을 촉진시키도록 할 수 있는 것이다.The above solution is mixed with groundwater containing germanium at a ratio of 1: 4, and left for 24 hours to prepare a water treatment agent by extracting a solution from which precipitates are removed. It is possible to mix the water treatment agent prepared by the present invention so that mineral materials useful to humans, but not easily deficient, may be included in the drinking water, and the water treatment agent of the present invention may be mixed with water and supplied to plants to promote plant growth.

도 1은 본 발명의 제조방법을 도시한 공정도.1 is a process chart showing the manufacturing method of the present invention.

도 1은 본 발명의 제조공정을 도시한 공정도로써, 광석 상태의 견운모, 맥반석 또는 천매암의 광물을 분쇄기에 의하여 60∼150Mesh로 파쇄하고, 그 파쇄된 광물을 정제하여 불순물을 제거하는 제 1 공정과,1 is a process chart showing the manufacturing process of the present invention, the first step of crushing the minerals of the minerals of the ore state, elvan or feldspar to 60 ~ 150Mesh by the pulverizer, purifying the crushed minerals to remove impurities ,

정제된 광물을 내식성이 강한 용기에 넣은 상태에서 약간의 황산용액과 물을 섞어 가열하면서 교반함으로써, 혼합물에서 증류수를 추출하는 제 2 공정과,A second step of extracting distilled water from the mixture by stirring while heating a purified sulfuric acid solution and a mixture of some sulfuric acid solution in a state of strong corrosion resistance;

상기의 제 2 공정에서 추출된 증류수와 황산원액(H2SO4, 20℃, 비중 1.834인 98.29%용액)을 혼합하여 20∼40%의 황산수용액을 제조하는 제 3 공정과,A third step of preparing 20-40% aqueous sulfuric acid solution by mixing distilled water extracted from the second process with a sulfuric acid stock solution (H 2 SO 4 , 20 ° C., 98.29% solution having a specific gravity of 1.834),

상기 20∼40%의 황산수용액과 제 2공정에서 교반을 끝낸 광물을 1:1로 혼합한 후 밀폐용기에서 80℃ 이상의 온도로 10시간 가열하는 제 4공정과,A fourth step of mixing the aqueous solution of 20-40% sulfuric acid with the mineral which has been stirred in the second step in a 1: 1 manner, and then heating the resultant container at a temperature of 80 ° C. or higher for 10 hours;

상기의 제 4 공정을 거친 상기의 용액을 필터프레스로 누르면서 2미크론의 거름종이를 통과시켜서 분쇄된 광석이 걸러진 수처리제를 추출하는 제 5 공정과,A fifth step of extracting the water treatment agent filtered out of the crushed ore by passing the solution having passed through the fourth step through a filter press of 2 microns while pressing the filter press;

상기의 제 5 공정에서 추출된 수처리제를 가열하여 원액의 농도를 진하게 하는 제 6 공정과,A sixth step of heating the water treatment agent extracted in the fifth step to increase the concentration of the stock solution;

제 6 공정에 의하여 진하게 된 수처리제를 게르마늄이 포함된 지하수와 1:4의 비율로 혼합한 후에 24시간 방치하여 침전물이 생긴 혼합액에서 침전물이 제거된 용액을 추출하는 제 7 공정에 의해 광물을 이용한 수처리제를 제조하는 것이다.Water treatment agent using minerals by mixing the water treatment agent thickened by the sixth process with groundwater containing germanium at a ratio of 1: 4 and left for 24 hours to extract the solution from which the precipitate is removed from the mixed solution in which the precipitate is formed. To prepare.

상기와 같은 본 발명의 구성을 보다 상세히 설명하면 다음과 같다.Referring to the configuration of the present invention as described above in more detail.

광산에서 광석 상태의 광물을 캐낸 후에 그 광석을 분쇄기에 투입하여 작은 입자의 형태로 광물을 60∼150Mesh의 크기로 파쇄하고, 그 파쇄된 광물을 정제하여 광물 이외의 다른 물질인 불순물을 제거한다.After mining ore minerals in the mine, the ore is put into a grinder to crush the mineral in the form of small particles in the size of 60 ~ 150Mesh, the crushed mineral is purified to remove impurities other than minerals.

상기의 불순물이 제거된 광물을 내식성이 강한 용기(예를 들면 스테인레스 36종 용기 등)에 넣은 상태에서 약간의 황산용액과 물을 섞어 가열, 교반하여 혼합물에서 증류수를 추출하게 된다.In the state in which the above-mentioned impurities are removed, the sulfuric acid solution and water are mixed and heated and stirred in a highly corrosion-resistant container (for example, 36 kinds of stainless steel containers) to extract distilled water from the mixture.

상기에서 추출한 증류수는 다음의 공정에서 황산용액과 섞는 증류수가 일반적인 물과 혼합하여 사용하는 것에 비하여 후술하는 식물의 성장촉진이나 음용수 등에 그 효과에서 대단한 차이가 발생되므로 증류수를 광물에서 추출하여 황산용액과 혼합하도록 하게 된다.The distilled water extracted in the above process produces a great difference in the effects of growth promotion or drinking water of plants described later, compared to distilled water mixed with sulfuric acid solution in the following process, so that distilled water is extracted from minerals and sulfuric acid solution and Have to mix.

상기와 같이 추출된 증류수는 황산원액(H2SO4, 20℃, 비중 1.834인 98.29%용액)과 혼합하여 20∼40%의 황산수용액을 제조하게 된다. 이때, 황산수용액은 광물에서 추출한 증류수와 혼합하게 되어 증류수와 함께 얻게 되는 미세한 물질을 함께 포함하게 된다.The distilled water extracted as described above is mixed with a sulfuric acid stock solution (H 2 SO 4 , 20 ℃, 98.29% solution having a specific gravity of 1.834) to prepare a 20-40% sulfuric acid solution. At this time, the aqueous sulfuric acid solution is mixed with distilled water extracted from the mineral to include a fine substance obtained with the distilled water.

상기와 같이 제조된 20∼40%의 황산수용액과 교반을 끝내고, 증류수를 추출하고 난 광물을 1:1로 혼합한 후 밀폐용기에서 80℃ 이상의 온도로 10시간 가열하게 된다. 이때, 밀폐용기를 사용하는 이유는 80℃ 이상으로 가열하게 될 때, 증류수와 함께 추출한 미세한 물질이 용기의 외부로 이탈되는 것이 방지되도록 하는 것이다. 또한, 황산수용액과 광물을 혼합하여 가열하는 것은 광물이 황산수용액과 반응하여 황산염 등을 생성하도록 하는 과정이 보다 빠르게 진행되도록 황산수용액과 광물을 가열하게 된다.After the 20-40% sulfuric acid solution prepared as described above and the stirring was finished, the minerals extracted with distilled water were mixed 1: 1, and then heated in a closed container at a temperature of 80 ° C. or higher for 10 hours. In this case, the reason for using the sealed container is to prevent the fine substance extracted with distilled water from being separated to the outside of the container when heated to 80 ℃ or more. In addition, heating by mixing the aqueous sulfuric acid solution and the mineral will heat the aqueous sulfuric acid solution and the mineral so that the process of the mineral reacts with the aqueous sulfuric acid solution to produce a sulfate.

상기의 공정을 끝낸 황산수용액과 광물의 혼합액을 필터프레스(좌우로 움직이는 프레스, 도자기공장 등에서 주로 사용됨)로 필터링하고, 다시 거름종이를 통과시켜서 미세한 광물이 걸러진 수처리제를 추출하게 된다.The sulfuric acid aqueous solution and mineral mixture solution of the above process is filtered with a filter press (mainly used in a left and right press, a pottery factory, etc.), and passed through a filter paper to extract a fine mineral filtered water treatment agent.

상기의 광물은 분쇄되었다고는 하나 광석으로 인체에 들어가 쌓이게 되면 건강에 좋지 않게 되므로 상기의 광물은 수처리제에 포함되지 않도록 하기 위하여 2미크론 정도의 고운 거름종이로 광물을 거르게 된다.The minerals are crushed, but the minerals are not good for health if they are accumulated in the human body as ore, so the minerals are filtered with a fine filter paper of about 2 microns in order not to be included in the water treatment agent.

상기와 같이 광물을 걸러낸 수처리제를 저온으로 가열하여 낮은 온도에서 수분만을 증발시키게 되면 수처리제가 약 50%의 부피를 만들게 된다. 이때, 증류수와 함께 증발되는 미세한 성분은 황산수용액과 반응하게 되어 그 성분이 증발되지 않게 되며, 황산수용액과 반응하지 않은 성분이라 하더라도 저온으로 가열하게 되므로 최대한 증발을 억제시킬 수 있게 된다. 이때의 수처리제의 Ph농도는 약 1.5정도가 된다.As described above, when the water treatment agent that has filtered the mineral is heated to a low temperature to evaporate only water at a low temperature, the water treatment agent has a volume of about 50%. At this time, the fine components to be evaporated with the distilled water will react with the sulfuric acid solution so that the components do not evaporate, even if the component does not react with the sulfuric acid solution is heated to a low temperature it is possible to suppress the evaporation as possible. At this time, the pH concentration of the water treatment agent is about 1.5.

상기의 공정에서 생성된 수처리제를 게르마늄(Ge)이 함유된 지하수와 1:4의 비율로 혼합하여 24시간 방치하게 된다. 이때, 24시간 동안 방치된 수처리제는 침전물이 가라않게 되어 혼합액의 하측에 위치하게 되고, 그 상부에 위치한 용액만을 분리하여 본 발명의 수처리제를 제조하게 된다.The water treatment agent produced in the above process is mixed with groundwater containing germanium (Ge) in a ratio of 1: 4 and left to stand for 24 hours. At this time, the water treatment agent is left for 24 hours, the sediment does not go away is located on the lower side of the mixed solution, to separate only the solution located on the top to prepare the water treatment agent of the present invention.

이때의 수처리제의 Ph농도는 지하수와 혼합하게 되어 강한 산성에서 중성으로 변하게 된다.At this time, the pH concentration of the water treatment agent is mixed with the groundwater and is changed from strong acid to neutral.

상기와 같이 제조된 광물을 이용한 수처리제의 사용상태를 상세히 설명하면 다음과 같이 된다.Referring to the state of use of the water treatment agent using the mineral prepared as described above is as follows.

먼저, 수처리제를 정수장치에 사용하게 되면 다음과 같다.First, when the water treatment agent is used in the water purification device is as follows.

수처리제를 물과 함께 정수장치에 투입하여 걸러진 물을 사용자가 음용하는 것이다. 이때, 본 발명의 수처리제와 물은 300∼400배로 희석하게 되어 Ph농도를 6.5 ∼ 7.5정도로 하여 정수장치에 투입하게 된다. 이때, 수처리제와 함께 투입된 물은 물 속에 혼합된 유기물과 상기의 수처리제가 반응하게 되어 침전물이 발생하게 되고, 상기의 침전물에 의하여 유기물은 침전되면서 물이 정수된다. 이때, 정수장치는 일반적인 활성탄과 필터를 정수장치에 본 발명에 의하여 제조된 수처리제를 물과 함께 사용하는 것이 좋은 실시예이다. 따라서, 수처리제에 의하여 유기물질이 침전된 후 물은 다시 2 미크론의 세라믹 필터와 활성탄에 의하여 걸러지게 되어 일반적으로 마시게 되는 정수된 물보다도 한층 더 정수된 물을 사용자가 마시게 된다. 그리고, 본 발명의 수처리제는 광물에서 추출된 미세한 성분(Ca, P, Mg, K, Na, Se, Si, Ge, Zn, Mn, Fe, Ni, Mo, Li, V, W, Ba, Ti, Rb, Al 등)을 포함하고 있어, 물과 함께 사용자가 음용하게 된다.The user is drinking the filtered water by adding the water treatment agent to the water purification device together with the water. At this time, the water treatment agent and water of the present invention are diluted 300 to 400 times, and the pH is adjusted to 6.5 to 7.5, and then introduced into the water purification device. At this time, the water added with the water treatment agent is the organic material mixed in the water and the water treatment agent is reacted to generate a precipitate, the organic matter is precipitated by the precipitate, the water is purified. At this time, the water purification device is a preferred embodiment using a water treatment agent prepared according to the present invention to the water purification device using a general activated carbon and a filter. Therefore, after the organic material is precipitated by the water treatment agent, the water is again filtered by the 2 micron ceramic filter and the activated carbon, so that the user drinks more purified water than the generally purified water. In addition, the water treatment agent of the present invention is a fine component extracted from the mineral (Ca, P, Mg, K, Na, Se, Si, Ge, Zn, Mn, Fe, Ni, Mo, Li, V, W, Ba, Ti, Rb, Al, etc.), and the user is drinking with water.

또한 본 발명에 의하여 제조된 광물을 이용한 수처리제는 식물의 성장을 촉진시키게 된다. 포도에 실험한 결과는 다음과 같다. 즉, 수처리제를 1000배 내지 1500배 희석하여 희석액을 만들고, 그 희석액을 1주일에 1회씩 포도에 공급한 결과 수확기에 수확한 포도의 당도가 보통의 포도는 평균 15.6%인 반면에 본 발명의 수처리제를 공급한 포도는 평균 19.9%의 당도를 유지하는 것으로 실험결과 밝혀졌다.In addition, the water treatment agent using the mineral produced by the present invention will promote the growth of plants. The results of the experiment on grapes are as follows. That is, the dilution is made by diluting the water treatment agent 1000 to 1500 times, and the diluent is supplied to the grapes once a week. As a result, the average sugar content of grapes harvested at the harvester is 15.6%, whereas the water treatment agent of the present invention The grapes fed were found to maintain an average sugar content of 19.9%.

아직은 식물 내에서 어떠한 작용으로 식물의 성장에 도움이 되는지는 확실히 밝혀내지는 못하였지만 본 실험에서와 같이 식물의 성장에 미치는 효과는 대단히 큰 것으로 밝혀졌다.It is not yet clear what kind of action in the plant is beneficial to the growth of the plant, but as shown in this experiment, the effect on the growth of the plant was found to be very large.

이와 같은 본 발명은 사람이 물을 정수장치에 투입할 때 본 발명에 의하여 제조된 수처리제를 물에 혼합하여 정수시킴으로써, 정수된 물에 사람에게 유용한 물질을 포함시켜서 사람들에게 유용한 물질을 함께 음용할 수 있게 된다.As described above, the present invention mixes the water treatment agent prepared in accordance with the present invention with water when water is added to the water purification device, and includes the material useful to humans in the purified water to drink the material useful to the people together. Will be.

또한 본 발명은 본 발명에 의하여 제조된 수처리제를 식물에 물과 함께 공급하여 식물의 성장을 촉진시키도록 하며, 수처리제를 오폐수에 투입하여 오폐수에 포함된 유기물이 침전되도록 하는 효과가 있다.In addition, the present invention is to supply the water treatment agent prepared according to the present invention with water to promote the growth of the plant, and to put the water treatment agent in the waste water has an effect that the organic matter contained in the waste water precipitates.

Claims (1)

광석 상태의 견운모, 맥반석 또는 천매암의 광물을 분쇄기에 의하여 60∼150Mesh로 파쇄하고, 그 파쇄된 광물을 정제하여 불순물을 제거하는 제 1 공정과,A first step of crushing minerals in the ore state of mica, elvan or feldspar into 60 to 150 meshes by a mill, and purifying the crushed minerals to remove impurities; 정제된 광물을 내식성이 강한 용기에 넣은 상태에서 약간의 황산용액과 물을 섞어 가열하면서 교반함으로써, 혼합물에서 증류수를 추출하는 제 2 공정과,A second step of extracting distilled water from the mixture by stirring while heating a purified sulfuric acid solution and a mixture of some sulfuric acid solution in a state of strong corrosion resistance; 상기의 제 2 공정에서 추출된 증류수와 황산원액을 혼합하여 20∼40%의 황산수용액을 제조하는 제 3 공정과,A third step of preparing a 20-40% sulfuric acid solution by mixing distilled water and sulfuric acid stock solution extracted in the second step; 상기 20∼40%의 황산수용액과 제 2 공정에서 교반을 끝낸 광물을 1:1로 혼합한 후 밀폐용기에서 80℃ 이상의 온도로 10시간 가열하는 제 4 공정과,A fourth step of mixing the aqueous solution of 20-40% sulfuric acid with the mineral which has been stirred in the second step in a 1: 1 manner, and then heating the resultant container at a temperature of 80 ° C. or higher for 10 hours; 상기의 용액을 필터프레스로 누르면서 2미크론의 거름종이를 통과시켜서 분쇄된 광석이 걸러진 수처리제를 추출하는 제 5 공정과,A fifth step of extracting the water treatment agent in which the crushed ore is filtered by passing the above solution with a filter press of 2 microns; 상기의 추출된 수처리제를 가열하여 농도를 진하게 하는 제 6 공정과,A sixth step of heating the extracted water treatment agent to increase the concentration; 진하게 된 수처리제를 게르마늄이 포함된 지하수와 1:4의 비율로 혼합한 후에 24시간 방치하여 침전물이 생긴 혼합액에서 침전물이 제거된 용액을 추출하는 제 7 공정에 의해 제조됨을 특징으로 하는 광물을 이용한 수처리제의 제조방법.Water treatment agent using mineral, characterized in that prepared by mixing the thickened water treatment agent with germanium-containing ground water at a ratio of 1: 4 and left for 24 hours to extract the solution from which the precipitate is removed from the mixed solution formed precipitate Manufacturing method.
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Publication number Priority date Publication date Assignee Title
KR100938606B1 (en) * 2008-04-15 2010-01-22 남정우 Mineral extraction method and extracted mineral from composite clay mineral

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JPS61271084A (en) * 1985-05-28 1986-12-01 Jitsuo Inagaki Sterilizing water-purifying agent for drinking water
KR890002143A (en) * 1987-07-01 1989-04-08 디이터 라우딘, 루돌프 호프만 Use of 12-amino-pyridazino [4 ', 5': 3.4] pyrrolo- [2.1-a] -isoquinoline as cardioprotective and neuroprotective agent
JPH05192566A (en) * 1992-01-17 1993-08-03 Sou Giken:Kk Light rock, light gravel or light sand having deodorizing and water cleaning function
KR19990009259A (en) * 1997-07-08 1999-02-05 소치재 Method for preparing mineral stock using biotite
KR19990073583A (en) * 1999-07-27 1999-10-05 정효익 Purifying material for quality of water

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61271084A (en) * 1985-05-28 1986-12-01 Jitsuo Inagaki Sterilizing water-purifying agent for drinking water
KR890002143A (en) * 1987-07-01 1989-04-08 디이터 라우딘, 루돌프 호프만 Use of 12-amino-pyridazino [4 ', 5': 3.4] pyrrolo- [2.1-a] -isoquinoline as cardioprotective and neuroprotective agent
JPH05192566A (en) * 1992-01-17 1993-08-03 Sou Giken:Kk Light rock, light gravel or light sand having deodorizing and water cleaning function
KR19990009259A (en) * 1997-07-08 1999-02-05 소치재 Method for preparing mineral stock using biotite
KR19990073583A (en) * 1999-07-27 1999-10-05 정효익 Purifying material for quality of water

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100938606B1 (en) * 2008-04-15 2010-01-22 남정우 Mineral extraction method and extracted mineral from composite clay mineral

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