KR20020097084A - Manufacturing Process of Red Pigment - Google Patents
Manufacturing Process of Red Pigment Download PDFInfo
- Publication number
- KR20020097084A KR20020097084A KR1020020065641A KR20020065641A KR20020097084A KR 20020097084 A KR20020097084 A KR 20020097084A KR 1020020065641 A KR1020020065641 A KR 1020020065641A KR 20020065641 A KR20020065641 A KR 20020065641A KR 20020097084 A KR20020097084 A KR 20020097084A
- Authority
- KR
- South Korea
- Prior art keywords
- red
- iron oxide
- pigment
- red pigment
- tio
- Prior art date
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/22—Compounds of iron
- C09C1/24—Oxides of iron
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/36—Compounds of titanium
- C09C1/3607—Titanium dioxide
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
Abstract
Description
본 발명은 적색 안료의 제조 방법에 관한 것으로 이를 보다 상세하게 설명하면 페인트나, 플라스틱 등의 색상용으로 사용되는 적색 안료(색소)가 인체에 무해하고 환경 친화적인 것으로 된 적색 안료의 제조 방법에 관한 것이다.The present invention relates to a method for producing a red pigment, which will be described in more detail. will be.
종래에는 페인트나 잉크 또는 플라스틱의 색상을 적색으로 할 경우에 사용하는 안료는 인체에 유해한 납(Pb)과 크롬(Cr)을 주 성분으로 조성 되어 있어 이의 납과 크롬은 인체에 치명적인 손상을 줄 뿐만 아니라 자연 환경을 파괴하고 있기 때문에 이와 같은 성분은 현재 세계적으로 사용을 규제하는 추세인 것이다.Conventionally, the pigments used to make the color of paint, ink or plastic red are composed mainly of lead (Pb) and chromium (Cr), which are harmful to the human body. Rather, because they are destroying the natural environment, these ingredients are now being regulated worldwide.
본 발명은 상기의 문제점을 해결하고자 발명한 것으로 이의 발명요지는 페인트나 플라스틱 등의 색사용으로 사용 할 때 인체에 무해하고 환경 친화적인 적색안료이고 제조 방법에 있어 중량 비로는 황색 산화철(Fe2O3) 30wt%, 적색 산화철(Fe2O3) 30wt%, 이산화탄소(TiO2)20wt% 및 퍼머넌트 레드(Permanent Red)(C26H22N4O4) 20wt%비로 조성하고 이의 제조 공정은 소재(원재료)의 투입 → 분쇄 → 혼합 → 조색(검사) → 포장의 5단계로 실시된다.The present invention has been invented to solve the above problems, the present invention is a red pigment which is harmless to the human body and is environmentally friendly when used in the use of color such as paint or plastic and yellow iron oxide (Fe 2 O by weight ratio in the manufacturing method) 3 ) 30wt%, red iron oxide (Fe 2 O 3 ) 30wt%, carbon dioxide (TiO 2 ) 20wt% and Permanent Red (C 26 H 22 N 4 O 4 ) 20wt% ratio and the manufacturing process of the material It is carried out in five stages: (raw material) → grinding → mixing → coloration (inspection) → packaging.
도 1은 본 발명의 공정도1 is a process diagram of the present invention
도 2는 본 발명의 실시예도2 is an embodiment of the present invention
*도면의 중요 부분에 대한 부호의 설명* Explanation of symbols for important parts of drawing
(A) - 소재의 투입 공정(A)-input process of material
(B) - 분쇄 공정(B)-grinding process
(C) - 혼합공정(C)-mixing process
(D) - 조색(검사)공정(D)-Toning (Inspection) Process
(E) - 포장공정(E)-Packing process
1- 혼합 분쇄기 조작 패널 2-호퍼 3-분쇄기 4-이송라인1- Mixing Mill Operation Panel 2-Hopper 3-Crusher 4-Feed Line
5-집진 설비 6-혼합기 7-스크류 8-포대5-dust collector 6-mixer 7-screw 8-bag
9-디지털 밸런스 10-포장기 조작 패널9-digital balance 10-packer control panel
이를 도면에 의거하여 상세하게 설명하면 다음과 같다.This will be described in detail with reference to the drawings as follows.
소재의 선택 및 조성에 있어, 소재로는 황색 산화철(Fe2O3)과 적색 산화철(Fe2O3), 이산화탄소(TiO2) 및 퍼머넌트 레드(C26H22N4O4)를 선택하고 이의 조성비는 황색 산화철 30wt%, 적색 산화철 30wt%, 이산화 티타늄 20wt% 및 퍼머넌트 레드 20wt%의 중량비로 하되, 색상의 명도(밝기)에 따라 가감 할 수 있는 것이다.In the selection and composition of materials, yellow iron oxide (Fe 2 O 3 ) and red iron oxide (Fe 2 O 3 ), carbon dioxide (TiO 2 ) and permanent red (C 26 H 22 N 4 O 4 ) are selected as the material. Its composition ratio is a weight ratio of 30 wt% of yellow iron oxide, 30 wt% of red iron oxide, 20 wt% of titanium dioxide, and 20 wt% of permanent red, but may be added or decreased depending on the brightness (brightness) of the color.
제 1 공정 이는 소재 투입공정(A)으로서, 상기한 황색 산화철(Fe2O3)과 적색 산화철(Fe2O3), 이산화탄소(TiO2) 및 퍼머넌트 레드(C26H22N4O4)을 일정한 중량비로 측정하여 호퍼(2)에 투입한다.The first step, which as a material In the process (A), the above yellow iron oxide (Fe 2 O 3) and red iron oxide (Fe 2 O 3), carbon dioxide (TiO 2) and permanent red (C 26 H 22 N 4 O 4) Is measured in a constant weight ratio and injected into the hopper (2).
제 2공정 이는 분쇄공정(B)으로서, 호퍼(2)에 투입된 소재는 그 하방에 설치된 분쇄기(3)에 투입하여 분쇄한다.2nd process This is a grinding | pulverization process (B) in which the raw material thrown in the hopper 2 is thrown into the grinding | pulverization machine 3 installed below, and grind | pulverized.
이 분쇄 공정(B)은 재료의 혼합을 용이하게 하기 위한 것으로 상기 호퍼(2)에 소재가 없어질때까지 계속 미세(500메쉬이상)하게 분해한다.This crushing step (B) is for facilitating mixing of the materials and continues to disintegrate finely (more than 500 mesh) until the hopper 2 has no material.
제 3공정 이는 혼합공정(C)으로서, 제 2공정의 분쇄기(3)에서 미분된 분쇄물은 에어 콤프레셔를 사용하여 이송라인(4)을 통해 혼합기(6)에 이송한다.Third process This is a mixing process (C), and the finely ground pulverized product in the pulverizer 3 of the second process is transferred to the mixer 6 through the transfer line 4 using an air compressor.
집진설비(5)를 갖춘 혼합기(6)에서는 내부의 기계장치를 통하여 1시간 정도 혼합한다.In the mixer 6 equipped with the dust collector 5, the mixture is mixed for about 1 hour through an internal mechanism.
제 4공정 이는 조색(검사) 공정(D)으로서, 상기 혼합공정(C)을 거친 혼합물 중에서 샘플을 채취하여 검사를 실시한다.4th process This is a coloring (inspection) process (D), and a sample is taken from the mixture which passed the said mixing process (C), and an inspection is performed.
제 5공정 이는 포장공정(E)으로서, 상기 조색 공정(D)에서 합격한 제품은스크류(7)를 거쳐 포대에 투입하여 밀봉한다. 이때 포장은 디지털 밸런스(9)를 사용하여 순량 25㎏으로 포대(8)에 담아서 포장하여 출하한다.5th process This is a packaging process (E), and the product which passed the said coloration process (D) is put into a bag through the screw 7, and sealed. At this time, the packaging is packaged and shipped in the bag 8 with a net quantity of 25 kg using the digital balance 9.
다음으로 본 발명의 실시예는 다음과 같다.Next, an embodiment of the present invention is as follows.
적색 안료 1M/T의 생산시는 황색 산화철(Fe2O3) 300㎏, 적색 산화철(Fe2O3) 300㎏, 이산화탄소(TiO2) 200㎏ 및 퍼머넌트 레드(C26H22N4O4) 200㎏을 정확하게 측정하여 제 1공정(A)인 호퍼(2)에 투입한 다음 제 2공정인 분쇄공정(B)에서 분쇄기(3)를 가동시켜 호퍼(2)에 담겨 있는 재료가 없어질때까지 계속 분쇄하여 잘 혼합되게 미분쇄(500 매쉬 이상)한다.300 kg yellow iron oxide (Fe 2 O 3 ), 300 kg red iron oxide (Fe 2 O 3 ), 200 kg carbon dioxide (TiO 2 ) and permanent red (C 26 H 22 N 4 O 4) When 200 kg is accurately measured and put into the hopper 2 which is the first process (A), and then the grinder 3 is operated in the crushing process (B) which is the second process, the material contained in the hopper 2 disappears. Continue grinding until finely ground (over 500 mesh).
상기 분쇄기(3)에서 분쇄가 끝나면 제 3공정인 혼합공정(C)을 실시 하기 위하여 분쇄된 재료를 에어콤프레셔를 이용하여 이송라인(4)을 통해 혼합기(6)로 이송한다. 혼합기(6)에 이송된 상기 재료는 이 혼합기(6)에서 1시간 정도 혼합한 다음, 제 4공정인 조색(검사) 공정(D)을 실시하기 위하여 혼합된 제품 중에서 약간(10g)의 샘플을 채취하여 통상의 검사기를 사용하여 검사를 실시한다.After the pulverization is completed in the pulverizer 3, the pulverized material is transferred to the mixer 6 through the transfer line 4 using an air compressor in order to perform the third mixing process (C). The material transferred to the mixer 6 is mixed for about 1 hour in the mixer 6, and then a small amount (10 g) of the sample is mixed among the mixed products to perform the fourth process, the coloration (inspection) process (D). Collect it and inspect it using a normal inspection machine.
조색 공정(D)이 끝나면 제 5공정인 포장공정(E)을 실시한다.After the toning step (D) is completed, the fifth step, the packing step (E) is performed.
이 포장공정(E)에서는 디지털 밸런스(9)를 사용하여 순량 25㎏씩으로 포대(8)에 담아 포장한 다음 출하 한다.In this packaging step (E), the digital balance 9 is used to pack the bag in the bag 8 in a net quantity of 25 kg and then ship.
상기와 같이 본 발명은 인체에 무해한 황색 산화철(Fe2O3)과 적색 산화철(Fe2O3), 이산화탄소(TiO2) 및 퍼머넌트 레드(C26H22N4O4)를 혼합하되, 이의 조성비는 황색산화철 30wt% : 적색 산화철 30wt% : 이산화 티타늄 20wt% : 퍼머넌트 레드 20wt%의 중량비로 조성 하였기 때문에 종래의 납(Pb)과 크롬(Cr)을 사용한 안료에 비하여 내산성, 내 알칼리성, 내열성, 은폐력 및 내후성이 월등하게 우수하고 인체에 무해할 뿐만 아니라 자연 환경에 친화적이며 생산 비용이 저렴하므로 산업적으로 매우 유용한 발명이다.As described above, the present invention mixes yellow iron oxide (Fe 2 O 3 ) and red iron oxide (Fe 2 O 3 ), carbon dioxide (TiO 2 ) and permanent red (C 26 H 22 N 4 O 4 ), which are harmless to humans. The composition ratio is 30wt% of yellow iron oxide: 30wt% of red iron oxide: 20wt% of titanium dioxide: 20wt% of permanent red. It is an industrially useful invention because it has excellent hiding power and weather resistance, is harmless to the human body, is friendly to the natural environment, and the production cost is low.
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KR1020020065641A KR20020097084A (en) | 2002-10-26 | 2002-10-26 | Manufacturing Process of Red Pigment |
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Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR19990037192A (en) * | 1997-10-20 | 1999-05-25 | 볼프강 에렌스타인, 크누트 샤우에르테 | Iron oxide red pigment, method for producing iron oxide red pigment and use thereof |
JP2000239559A (en) * | 1999-02-15 | 2000-09-05 | Merck Patent Gmbh | Strong interference pigment |
KR20010071143A (en) * | 1999-12-03 | 2001-07-28 | 가부시끼가이샤 다까라 | Colored magnetic particles for magnetophoretic display and method for manufacturing same |
KR20020097083A (en) * | 2002-10-26 | 2002-12-31 | 주식회사동진정밀화학공업 | Manufacturing process of Green Pigment |
-
2002
- 2002-10-26 KR KR1020020065641A patent/KR20020097084A/en not_active Application Discontinuation
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR19990037192A (en) * | 1997-10-20 | 1999-05-25 | 볼프강 에렌스타인, 크누트 샤우에르테 | Iron oxide red pigment, method for producing iron oxide red pigment and use thereof |
JP2000239559A (en) * | 1999-02-15 | 2000-09-05 | Merck Patent Gmbh | Strong interference pigment |
KR20010071143A (en) * | 1999-12-03 | 2001-07-28 | 가부시끼가이샤 다까라 | Colored magnetic particles for magnetophoretic display and method for manufacturing same |
KR20020097083A (en) * | 2002-10-26 | 2002-12-31 | 주식회사동진정밀화학공업 | Manufacturing process of Green Pigment |
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