KR20010047197A - The dyeing method of fabric using natural pigment - Google Patents
The dyeing method of fabric using natural pigment Download PDFInfo
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- KR20010047197A KR20010047197A KR1019990051302A KR19990051302A KR20010047197A KR 20010047197 A KR20010047197 A KR 20010047197A KR 1019990051302 A KR1019990051302 A KR 1019990051302A KR 19990051302 A KR19990051302 A KR 19990051302A KR 20010047197 A KR20010047197 A KR 20010047197A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
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Abstract
Description
본 발명은 천연안료를 이용한 직물의 염색방법에 관한 것으로, 보다 상세하게는 면직물 및 면섬유 등의 각종 제품에 천연안료의 분말이 단단하게 염착될 수 있도록 한 천연안료를 이용한 직물의 염색방법에 관한 것이다.The present invention relates to a method of dyeing fabrics using natural pigments, and more particularly, to a method of dyeing fabrics using natural pigments so that the powder of natural pigments can be firmly dyed to various products such as cotton fabrics and cotton fibers. .
일반적으로 안료에는 천연안료와 합성안료로 구분되며, 천연안료에는 옥, 머드, 송연, 숯 및 황토 등 그 종류가 다양하며, 상기한 천연안료는 각종 냄새제거, 습기제거, 살균효과 등의 다양한 효과가 알려지면서 천연안료를 이용한 각종 제품들이 개발되고 연구되어 오고 있다.In general, pigments are classified into natural pigments and synthetic pigments, and natural pigments include various kinds of jade, mud, smoke, charcoal, and ocher, and the above-mentioned natural pigments have various effects such as various odor removal, moisture removal, and sterilization effect. As is known, various products using natural pigments have been developed and researched.
특히 근래에는 상기한 바와 같이 다양한 효과를 나타내는 천연안료를 직물에 염착시켜 의류나 각종제품을 제조함으로써 인체에 유익하도록 한 많은 방법들이 시도되고 있다.In particular, in recent years, a number of methods have been attempted to produce a garment or various products by dyeing a natural pigment having various effects on the fabric as described above.
천연안료를 직물에 염착하는 방법 중에서 천연안료를 물에 현탁시켜 염욕을 제조한 다음, 상기 제조된 염욕을 100내지 130℃에서 1내지 3분동안 가열하면서 염색하고자 하는 섬유를 침적시켜 천연안료의 고착을 증진시킬 수 있도록 한 방법이 제시되었다.In the method of dyeing the natural pigment on the fabric to prepare a dye bath by suspending the natural pigment in water, and then by depositing the fiber to be dyed while heating the prepared salt bath at 100 to 130 ℃ for 1 to 3 minutes of the natural pigment One way has been proposed to promote fixation.
그러나 상기한 방법에 의해 제조된 제품의 경우, 염착이 불량하여 세탁견뢰도가 떨어지고, 따라서 염착된 직물을 세탁하는 경우 탈색이 쉽게 되어 제품의 수명이 짧아진다는 문제점이 발생하였다.However, in the case of the product produced by the above-described method, poor dyeing resulted in poor washing fastness, and thus, when washing the dyed fabric, it is easy to decolorize and shorten the life of the product.
그에 따라 상기한 문제점을 해결하기 위해 천연안료를 아크릴 수지 등의 각종 수지에 첨가하여 혼합한 다음, 그 혼합액을 이용하여 직물에 코팅하여 부착시키는 방법이 제시되었다.Accordingly, in order to solve the above problems, a method of adding natural pigments to various resins such as acrylic resins, mixing them, and then coating and attaching the fabrics to the fabrics using the mixed solution has been proposed.
그러나 상기한 코팅방법에 의해 제조된 제품의 경우, 코팅된 고분자 수지가 천연안료의 표면에 코팅되어 천연안료가 가지는 고유한 효과를 충분히 발휘하지 못한다는 문제점이 발생하였다.However, in the case of the product produced by the coating method, the coating polymer resin is coated on the surface of the natural pigment has a problem that does not fully exhibit the inherent effects of the natural pigment.
이에 본 발명은 상기한 종래의 문제점을 해결하기 위한 것으로, 면직물 및 면섬유 등의 각종 제품의 내부에 천연안료가 단단하게 고착될 수 있도록 함으로써, 탈색을 방지하여 우수한 세탁견뢰도를 가질 뿐만 아니라 천연안료가 지니는 기능을 충분히 발휘할 수 있도록 한 천연안료를 이용한 직물의 염색방법을 제공하는 데 그 목적이 있다.Accordingly, the present invention is to solve the above-mentioned problems, by allowing the natural pigments to be firmly fixed to the inside of various products such as cotton fabrics and cotton fibers, to prevent discoloration to have excellent washing fastness as well as natural pigments It is an object of the present invention to provide a method of dyeing fabrics using natural pigments to fully exhibit the function.
상기한 목적을 달성하기 위한 본 발명은 제조된 알칼리 용액에 염색하고자 하는 직물을 넣고 가열 교반하면 직물을 정련시키는 전처리공정, 천연안료염액에 전처리된 직물을 침적시켜 염착하는 염색공정 및 염착된 직물을 건조하고 충분히 수세하는 마무리공정으로 이루어지는 천연안료를 이용한 직물의 염색방법에 있어서,The present invention for achieving the above object is a pre-treatment step of refining the fabric by putting the fabric to be dyed in the alkali solution prepared by heating and agitation, the dyeing process and dyeing the fabric by depositing the dye pretreated in a natural pigment salt solution In the dyeing method of the fabric using a natural pigment consisting of a finishing process of drying and washing with water sufficiently,
상기 염색공정은 물 100중량부에 대하여 전처리된 직물 5중량부 및 양이온 계면활성제 5내지 8중량부를 첨가하여 70내지 85℃에서 10내지 20분간 1차 침적시키고, 물 100중량부에 대하여 325메쉬 이상의 천연안료분말 10내지 15중량부 및 음이온 계면활성제 10내지 15중량부를 포함하는 염액에 상기 1차 침적시킨 직물을 넣고 90내지 95℃에서 1내지 2시간동안 2차 침적시킨 다음, 상기 2차 침적된 직물을 물 100중량부에 대하여 아크릴산(Acrylic acid) 고착제를 5내지 10중량부 첨가하여 제조된 용액에 넣고 30내지 40℃에서 20내지 30분동안 침적시키는 것을 특징으로 하는 천연안료를 이용한 직물의 염색방법을 제공함으로써 달성할 수 있다.The dyeing process is 5 parts by weight of pre-treated fabric and 5 to 8 parts by weight of cationic surfactant is added to 100 parts by weight of water, and firstly deposited at 70 to 85 ° C. for 10 to 20 minutes, and at least 325 mesh based on 100 parts by weight of water. 10 to 15 parts by weight of the natural pigment powder and 10 to 15 parts by weight of the anionic surfactant was added to the first immersed fabric and the second immersed for 1 to 2 hours at 90 to 95 ℃, the second immersed Dyeing the fabric using a natural pigment, characterized in that the fabric is added to a solution prepared by adding 5 to 10 parts by weight of acrylic acid fixing agent with respect to 100 parts by weight of water and deposited for 20 to 30 minutes at 30 to 40 ℃ By providing a method.
본 발명에서는 통상적으로 사용하는 전처리공정 후 염색공정을 실시하게 되는데 일반적인 염색방법에서 사용되는 전처리 공정은 알칼리인 탄산나트륨 정련제를 이용하여 pH 12내지 14인 용액을 제조하고, 상기 용액에 염색하고자 하는 직물을 넣은 다음 90℃에서 약 10분 동안 교반하면서 침적시켜 정련하고, 정련이 완료된 후 물을 빼고 새로운 물로 50내지 60℃에서 깨끗이 씻어주는 공정이다.In the present invention, a dyeing process is performed after a pretreatment process that is commonly used. The pretreatment process used in a general dyeing method prepares a solution having a pH of 12 to 14 using an alkali sodium carbonate refining agent, and fabrics to be dyed in the solution. After the addition, it is immersed by stirring for about 10 minutes at 90 ° C., and then refining. After the refining is completed, the water is removed and washed with fresh water at 50 to 60 ° C.
상기와 같은 전처리공정을 수행하면 염색하고자 하는 직물에 부착되어 있는 염색에 장애를 주는 유지 왁스류 등의 불순물이 제거되어 염색이 잘 이루어지게 되는 것이다.When the pretreatment process is performed as described above, impurities such as oils and waxes that interfere with dyeing attached to the fabric to be dyed are removed, and dyeing is performed well.
상기 전처리 공정 후 본 발명은 물 100중량부에 대하여 전처리된 직물 5중량부 및 양이온 계면활성제 5내지 8중량부를 첨가하여 70내지 85℃에서 10내지 20분간 1차 침적시키게 된다.After the pretreatment process, the present invention is added to 5 parts by weight of the pretreated fabric and 5 to 8 parts by weight of cationic surfactant based on 100 parts by weight of water to be first deposited for 10 to 20 minutes at 70 to 85 ℃.
이때 양이온 계면활성제는 천연안료의 염착성을 증진시키기 위해 첨가하는 것으로 본 발명에서는 양이온 계면활성제로 카치온화제를 사용하였으며, 그 첨가량이 8중량부를 초과할 경우 그 이상은 염착성이 없으므로 8중량부를 초과할 필요는 없으며, 5중량부 미만일 경우 안료의 염착이 잘 이루어지지 않는다는 문제점이 발생하므로 5내지 8중량부 첨가하는 것이 바람직하다.In this case, the cationic surfactant is added to enhance the dyeing property of the natural pigment. In the present invention, a cationic agent is used as the cationic surfactant. If the amount is more than 8 parts by weight, the cationic surfactant is more than 8 parts by weight because it has no dyeing property. If it is less than 5 parts by weight, it is preferable to add 5 to 8 parts by weight because a problem occurs that the dye is not well formed.
또한 양이온 계면활성제를 첨가한 다음 70내지 85℃에서 10내지 20분 동안 침적시키게 되는데, 상기한 조건에서 직물을 침적시킬 경우 직물을 이루는 섬유가 열에 의해 팽창 되고, 그에 따라 섬유사이에 틈이 생겨 천연안료의 입자가 그 틈사이로 침투하게 되어 직물에 천연안료가 골고루 염착이 되게 되는 것이다.In addition, the cationic surfactant is added and then deposited at 70 to 85 ° C. for 10 to 20 minutes. When the fabric is deposited under the above conditions, the fibers constituting the fabric are expanded by heat, and there is a gap between the fibers, thereby creating natural Particles of pigment penetrate through the gaps, and natural pigments are evenly dyed on the fabric.
따라서 70℃ 미만에서 10분 미만으로 침적시킬 경우 천연안료의 염착이 잘 이루어지지 않는다는 문제점이 발생하며, 85℃를 초과한 온도에서 20분을 초과하여 침적시킬경우 천연안료의 염착은 증진되지만 오히려 직물을 손상시킬 염려가 있으므로 70내지 85℃에서 10내지 20분 동안 침적 시키는 것이 바람직하다.Therefore, when it is deposited in less than 10 minutes at less than 70 ℃ occurs a problem that the dyeing of the natural pigment is not made well, if the deposition for more than 20 minutes at a temperature exceeding 85 ℃ is enhanced the dyeing of the natural pigment but rather fabric It is preferable to deposit for 10 to 20 minutes at 70 to 85 ℃ because it may damage the.
상기 1차 침적이 완료된 후, 물 100중량부에 대하여 325메쉬 이상의 천연안료분말 10내지 15중량부 및 음이온 계면활성제 10내지 15중량부를 포함하는 염액에 1차 침적된 직물을 넣고 90내지 95℃에서 1내지 2시간 동안 2차 침적시키게 된다.After the first deposition was completed, the fabric was first placed in a salt solution containing 10 to 15 parts by weight of natural pigment powder and 10 to 15 parts by weight of anionic pigment and relative to 100 parts by weight of water at 90 to 95 ℃ Secondary deposition is performed for one to two hours.
상기 2차 침적시키는 과정에서 천연안료 분말의 입도가 325메쉬 미만일 경우 섬유사이로 천연안료 분말의 침투가 용이하지 못하다는 문제점이 발생하므로 325메쉬 이상의 분말을 사용하는 것이 바람직하며, 그 첨가량은 10중량부 미만일 경우 천연안료의 염착되는 양이 적어 천연안료의 고유한 기능을 충분히 발휘할 수 없으며, 15중량부를 초과할 경우 세탁시 견뢰도가 나빠지는 문제점이 발생하므로 10내지 15중량부 첨가하는 것이 바람직하다.If the particle size of the natural pigment powder is less than 325 mesh in the second deposition process, it is not easy to penetrate the natural pigment powder between fibers, so it is preferable to use a powder of 325 mesh or more, and the amount of the additive is 10 parts by weight. If less than the amount of dyeing the natural pigment is not enough to fully exhibit the inherent function of the natural pigment, if it exceeds 15 parts by weight it is preferable to add 10 to 15 parts by weight because the problem of the fastness of washing occurs.
이때 천연안료 분말로는 맥반석, 머드, 옥, 숯, 황토 및 게르마늄 등의 광물성물질을 325메쉬 이상으로 분쇄한 것을 사용할 수 있다.At this time, as a natural pigment powder, it can be used to grind mineral materials such as ganban stone, mud, jade, charcoal, ocher and germanium 325 mesh or more.
또한 양이온 계면활성제와 함께 천연안료의 염착성을 증진시키기 위하여 음이온 계면활성제를 첨가하게 되는데, 본 발명에서는 음이온 계면활성제로 술폰산염인 알킬 벤젠 설포네이트(Alkyl benzene sulfonate)를 사용하였으며, 그 첨가량은 15중량부를 초과할 경우 그 이상은 염착성이 없으므로 15중량부를 초과할 필요는 없으며, 10중량부 미만일 경우 천연안료의 염착이 잘 이루어지지 않는다는 문제점이 발생하므로 10내지 15중량부 첨가하는 것이 바람직하다.In addition, anionic surfactants are added to enhance the dyeing property of the natural pigment together with the cationic surfactant. In the present invention, an alkyl benzene sulfonate, which is a sulfonate, is used as the anionic surfactant. If the amount is more than 15 parts by weight is not necessary because there is no dyeing, if it is less than 10 parts by weight it is preferable to add 10 to 15 parts by weight because the problem occurs that the dyeing of the natural pigment is not good.
천연안료분말 및 음이온 계면활성제를 첨가한 다음 90내지 95℃에서 1내지 2시간동안 침적시키게 되는데, 상기와 같은 조건에서 침적시킬 경우 1차 침적시키는 과정에서 열에 의해 팽창되어 생긴 섬유의 틈이 그대로 유지되면서 틈사이로 천연안료 입자가 침투하게 되어 섬유에 골고루 염착 되게 되는 것이다.After adding natural pigment powder and anionic surfactant, it is deposited for 1 to 2 hours at 90 to 95 ℃. If it is deposited under the above conditions, the gap of fiber expanded by heat during the first deposition process is maintained as it is. As the natural pigment particles penetrate through the gaps, they are evenly dyed to the fibers.
상기 천연안료분말 및 계면활성제를 첨가하여 제조한 염액에 살균력을 증진시키기 위해 목초액을 첨가 할 수도 있는데, 그 첨가량이 10중량부 미만일 경우 살균 효과가 적다는 문제점이 발생하며, 20중량부를 초과할 경우 목초액이 고가이므로 오히려 경제성이 떨어지는 문제점이 발생하므로 10내지 20중량부 첨가하는 것이 바람직하다.Wood vinegar may be added to the salt solution prepared by adding the natural pigment and the surfactant to increase sterilization power, but when the amount is less than 10 parts by weight, there is a problem that the sterilization effect is small, and when it exceeds 20 parts by weight. Wood grass liquor is expensive, so economical rather poor problem occurs, it is preferable to add 10 to 20 parts by weight.
상기 2차 침적된 직물은 물 100중량부에 대하여 아크릴산 고착제를 5내지 10중량부 첨가하여 제조된 용액에 넣고 30내지 40℃에서 20내지 30분동안 침적시키게 된다.The secondary immersed fabric is placed in a solution prepared by adding 5 to 10 parts by weight of an acrylic acid fixing agent with respect to 100 parts by weight of water, and is then deposited for 20 to 30 minutes at 30 to 40 ° C.
상기에서 아크릴산은 섬유사이에 고착된 천연안료 분말의 고착을 증대시키기 위해 고착제로 첨가하게 되는데, 그 첨가량이 5중량부 미만일 경우 천연안료의 고착력이 떨어지는 문제점이 발생하며, 10중량부를 초과하여 첨가될 경우 제조된 제품이 고착제로 인해 딱딱하게 굳어지는 문제점이 발생하므로 5내지 10중량부 첨가하는 것이 바람직하다.In the above acrylic acid is added as a fixing agent to increase the adhesion of the natural pigment powder fixed between the fibers, when the addition amount is less than 5 parts by weight, the problem occurs that the adhesion strength of the natural pigment is lowered, more than 10 parts by weight If it is a problem that the produced product is hardened due to the fixing agent occurs, it is preferable to add 5 to 10 parts by weight.
또한 30내지 40℃의 물을 이용하여 침적시키는 이유는 고온에 의해 팽창된 섬유를 다시 수축시키기 위한 것으로, 수축이 이루어지게 되면 섬유사이의 틈새로 침투된 천연안료 분말이 그 상태로 고착이 되어 단단히 고정되게 되는 것이다.In addition, the reason for depositing using water of 30 to 40 ℃ is to shrink the fibers expanded by the high temperature again, when the shrinkage is made, the natural pigment powder penetrated into the gap between the fibers are fixed as it is It will be fixed.
따라서 30℃미만일 경우 고착제가 온도저하로 인해 골고루 섞이지 않는다는 문제점이 발생하며, 40℃를 초과할 경우 수축이 제대로 이루어지지 않아 섬유에 고착된 숯 분말이 쉽게 이탈되어 세탁견뢰도가 저하 된다는 문제점이 발생하므로 30내지 40℃로 냉각시키는 것이 바람직하다.Therefore, if it is less than 30 ℃ problem occurs that the fixing agent is not evenly mixed due to the temperature decrease, and if it exceeds 40 ℃ shrinkage is not properly made, the charcoal powder adhered to the fiber is easily released and the laundry fastness decreases because It is preferable to cool to 30 to 40 ° C.
상기 염색공정 후에는 통상적으로 행하는 마무리 공정을 행하게 되는 데 일반적으로 사용되는 마무리 공정은 염색공정을 통해 염착된 직물을 건조하고 직물의 표면에 남아 있는 미고착 염료를 충분히 씻어준 다음, 다시 가성소다(NaOH)를 첨가한 다음 약 90℃에서 10분동안 가열한 후 탈수하고, 탈수된 섬유를 열풍건조하는 것이다.After the dyeing process, the finishing process is generally used to perform a finishing process that is usually performed by drying the dye-dyed fabric through the dyeing process, and sufficiently wash the unfixed dye remaining on the surface of the fabric, and then caustic soda ( NaOH) is added, followed by heating at about 90 ° C. for 10 minutes, followed by dehydration, followed by hot air drying of the dehydrated fibers.
이하 본 발명을 하기한 실시예 및 비교예를 통하여 상세하게 설명하기로 하나 본 발명은 하기한 설명에 한정되는 것은 아니다.Hereinafter, the present invention will be described in detail with reference to the following Examples and Comparative Examples, but the present invention is not limited to the following description.
<실시예 1><Example 1>
물 100중량부에 대하여 전처리된 면직물 5중량부 및 양이온 계면활성제 8중량부를 첨가하여 80℃에서 15분간 침적시킨 다음, 상기 침적된 직물을 물 100중량부에 대하여 325메쉬 이상의 숯 분말 15중량부 및 음이온 계면활성제 15중량부를 첨가하여 제조된 염액에 넣고 95℃에서 1시간동안 침적시킨 다음, 상기 침적된 직물을 물 100중량부에 대하여 아크릴산 고착제 8중량부 첨가하여 제조된 용액에 넣고 35℃에서 20분동안 침적시켜 면직물에 숯분말을 염착시킨 다음, 상기 염착된 면직물을 건져내어 건조한 후 3회 세탁하여 면직물 표면에 붙어 있는 미고착 숯분말을 제거한 다음, KS K 0430에 규정된 방법으로 세탁견뢰도중 변퇴색을 측정하여 표 1에 나타내었다.5 parts by weight of pretreated cotton fabric and 8 parts by weight of cationic surfactant were added to 100 parts by weight of water, and the resultant fabric was immersed for 15 minutes at 80 ° C. 15 parts by weight of the anionic surfactant was added to the prepared salt solution and deposited at 95 ° C. for 1 hour. The deposited fabric was then added to a solution prepared by adding 8 parts by weight of an acrylic acid fixing agent to 100 parts by weight of water. After dipping for a minute to dye the charcoal powder on the cotton fabric, the dried cotton fabric is dried, washed and washed three times to remove the unfixed charcoal powder on the surface of the cotton fabric, and then wash fastness by the method prescribed in KS K 0430 The fading color was measured and shown in Table 1.
<실시예 2><Example 2>
천연안료로 325메쉬 이상의 황토분말 15중량부를 사용한 것을 제외하고는 실시예 1과 동일한 방법으로 실시하여 면직물에 황토분말을 염착시킨 후 세탁견뢰도중 변퇴색을 측정하여 표 1에 나타내었다.Except for using 15 parts by weight of ocher powder of 325 mesh or more as a natural pigment was carried out in the same manner as in Example 1 after dyeing the ocher powder on the cotton fabric was measured in the color fastness to wash fastness is shown in Table 1.
<실시예 3><Example 3>
천연안료로 325메쉬 이상의 옥분말 15중량부를 사용한 것을 제외하고는 실시예 1과 동일한 방법으로 실시하여 면직물에 황토분말을 염착시킨 후 세탁견뢰도중 변퇴색을 측정하여 표 1에 나타내었다.Except for using 15 parts by weight of 325 mesh or more jade powder as a natural pigment was carried out in the same manner as in Example 1 after dyeing the ocher powder on the cotton fabric was measured in the color fastness to wash fastness is shown in Table 1.
<비교예 1>Comparative Example 1
물 100중량부에 대하여 숯 10중량부를 첨가하여 현탁시켜 염욕을 제조한 다음, 상기 염욕을 100℃에서 5분동안 가열하면서 염색하고자 하는 면직물을 침적시켜 염착한 다음, 상기 염착된 면직물을 건져내어 건조한 후 3회 세탁하여 면직물 표면에 붙어 있는 미고착 숯분말을 제거한 다음, 실시예 1과 동일한 방법으로 세탁견뢰도중 변퇴색을 측정하여 표 1에 나타내었다.Suspended by adding 10 parts by weight of charcoal to 100 parts by weight of water to prepare a salt bath, and then dipped and dyed the cotton fabric to be dyed while heating the salt bath at 100 ° C. for 5 minutes, and then the dried cotton fabric was taken out and dried. After washing three times to remove the unfixed charcoal powder adhering to the surface of the cotton fabric, it was shown in Table 1 by measuring the discoloration of color fastness to wash fastness in the same manner as in Example 1.
세탁견뢰도에서 1급은 아주 심하게 퇴색된다는 것을 나타내며, 그 수치가 클수록, 즉 4-5급으로 갈수록 퇴색이 되지 않는다는 것을 나타내며 세탁시 퇴색이 없을 경우 가장 우수한 4-5급으로 나타낸다.In the fastness of washing, the first grade indicates that the color fades very severely, and the higher the value, that is, the less the color fades toward the 4-5 level, and the best 4-5 grade in the absence of color fading during washing.
상기 표 1에서 보는 바와 같이 본 발명에 의해 숯분말을 염착시킨 실시예 1과 황토분말을 염착시킨 실시예 2 및 옥분말을 염착시킨 실시예 3의 경우 세탁견뢰도중 변퇴색이 3-4급으로 종래의 일반적인 제조방법에 의해 숯분말을 직물에 염착시킨 비교예 1의 1급보다 퇴색이 거의 되지 않는 것을 보여준다.As shown in Table 1, in the case of Example 1 salted charcoal powder and Example 2 salted ocher powder and Example 3 salted jade powder according to the present invention, the color fading during washing fastness to 3-4 grade It shows that there is little fading than the first grade of Comparative Example 1 in which the charcoal powder is dyed to a fabric by a conventional general manufacturing method.
따라서 본 발명에 의한 경우 종래의 염색방법보다 숯분말이나 황토분말 및 옥분말이 직물에 단단하게 고착되어 염착정도가 우수다는 것을 나타낸다.Therefore, according to the present invention, the charcoal powder, the ocher powder and the jade powder are firmly fixed to the fabric than the conventional dyeing method, indicating that the dyeing degree is superior.
상기에서 설명한 바와 같이 본 발명은 양이온 계면활성제와 음이온 계면활성제 및 고착제를 이용하여 섬유내부에 숯이 단단히 염착될 수 있도록 함으로써 탈색을 방지하여 우수한 세탁견뢰도를 나타내는 천연안료를 이용한 섬유의 염색방법을 제공하는 유용한 발명인 것이다.As described above, the present invention provides a method of dyeing fibers using natural pigments, which exhibits excellent washing fastness by preventing discoloration by allowing the char to be firmly dyed into the fiber using cationic surfactants, anionic surfactants, and fixing agents. It is a useful invention to.
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Cited By (10)
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| KR20000072332A (en) * | 2000-08-29 | 2000-12-05 | 김삼경 | Fine fiber containing finely divided jade and its manufacturing method |
| KR20010081732A (en) * | 2000-02-18 | 2001-08-29 | 정혜향 | A Knit dyed with natural dye and The Process for dyeing Thereof |
| KR20030064144A (en) * | 2002-01-26 | 2003-07-31 | 주식회사 오픈하우스 | Blind textile using active carbon and manufacturing method therefor |
| KR20030076809A (en) * | 2002-03-21 | 2003-09-29 | 김영자 | A natural dye in the form of fineness and method for menufacturing such dye |
| KR20030076807A (en) * | 2002-03-21 | 2003-09-29 | 김영자 | A natural dye in the form of fineness and method for menufacturing such dye |
| KR20030083027A (en) * | 2002-04-18 | 2003-10-30 | 정길선 | charcoal natural Dyeing & assisatant. |
| KR100662514B1 (en) * | 2005-04-28 | 2006-12-28 | 주식회사 파코라인 | Method of forming Penetration Layer in Polymer Substrate |
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| KR880003064A (en) * | 1986-08-07 | 1988-05-13 | 배윤근 | Dyeing method using pigments of plants |
| JPH04281079A (en) * | 1991-03-06 | 1992-10-06 | Takao Kimura | Method for dyeing yarn and woven fabric |
| KR100262351B1 (en) * | 1998-01-16 | 2000-08-01 | 주병진 | Method of dyeing fiber using loess |
| KR100292986B1 (en) * | 1998-10-13 | 2001-11-22 | 박준하 | Dyeing method of natural dyes |
| KR100335594B1 (en) * | 1999-09-14 | 2002-05-08 | 박윤만 | Cotton garment dyed with natural coloring material radiating far-infrared ray and method for dyeing thereof |
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| KR20010081732A (en) * | 2000-02-18 | 2001-08-29 | 정혜향 | A Knit dyed with natural dye and The Process for dyeing Thereof |
| KR20000072332A (en) * | 2000-08-29 | 2000-12-05 | 김삼경 | Fine fiber containing finely divided jade and its manufacturing method |
| KR20030064144A (en) * | 2002-01-26 | 2003-07-31 | 주식회사 오픈하우스 | Blind textile using active carbon and manufacturing method therefor |
| KR20030076809A (en) * | 2002-03-21 | 2003-09-29 | 김영자 | A natural dye in the form of fineness and method for menufacturing such dye |
| KR20030076807A (en) * | 2002-03-21 | 2003-09-29 | 김영자 | A natural dye in the form of fineness and method for menufacturing such dye |
| KR20030083027A (en) * | 2002-04-18 | 2003-10-30 | 정길선 | charcoal natural Dyeing & assisatant. |
| KR100662514B1 (en) * | 2005-04-28 | 2006-12-28 | 주식회사 파코라인 | Method of forming Penetration Layer in Polymer Substrate |
| KR100704164B1 (en) * | 2006-04-04 | 2007-04-09 | 최광영 | Textile printing composition |
| CN104894890A (en) * | 2015-05-20 | 2015-09-09 | 东华大学 | One-bath dyeing method of wool fabric or silk fabric based on natural xanthophyll |
| KR20210067382A (en) * | 2019-11-29 | 2021-06-08 | 한국생산기술연구원 | Natural ink for DTP composition comprising Calendula arvensis extract |
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