KR20000002389A - Manufacturing method for rice soup without rice grains by using a gelatinized rice powder - Google Patents
Manufacturing method for rice soup without rice grains by using a gelatinized rice powder Download PDFInfo
- Publication number
- KR20000002389A KR20000002389A KR1019980023107A KR19980023107A KR20000002389A KR 20000002389 A KR20000002389 A KR 20000002389A KR 1019980023107 A KR1019980023107 A KR 1019980023107A KR 19980023107 A KR19980023107 A KR 19980023107A KR 20000002389 A KR20000002389 A KR 20000002389A
- Authority
- KR
- South Korea
- Prior art keywords
- rice
- malt
- added
- sikhye
- manufacturing
- Prior art date
Links
- 241000209094 Oryza Species 0.000 title claims abstract description 71
- 235000007164 Oryza sativa Nutrition 0.000 title claims abstract description 71
- 235000009566 rice Nutrition 0.000 title claims abstract description 71
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 25
- 239000000843 powder Substances 0.000 title claims abstract description 9
- 235000013339 cereals Nutrition 0.000 title abstract description 20
- 235000014347 soups Nutrition 0.000 title abstract 2
- 235000000346 sugar Nutrition 0.000 claims abstract description 26
- GXCLVBGFBYZDAG-UHFFFAOYSA-N N-[2-(1H-indol-3-yl)ethyl]-N-methylprop-2-en-1-amine Chemical compound CN(CCC1=CNC2=C1C=CC=C2)CC=C GXCLVBGFBYZDAG-UHFFFAOYSA-N 0.000 claims abstract description 23
- 229920002472 Starch Polymers 0.000 claims abstract description 23
- 239000008107 starch Substances 0.000 claims abstract description 23
- 235000019698 starch Nutrition 0.000 claims abstract description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 102000004190 Enzymes Human genes 0.000 claims abstract description 20
- 108090000790 Enzymes Proteins 0.000 claims abstract description 20
- 235000006886 Zingiber officinale Nutrition 0.000 claims abstract description 9
- 235000008397 ginger Nutrition 0.000 claims abstract description 9
- 238000010025 steaming Methods 0.000 claims abstract 3
- 244000273928 Zingiber officinale Species 0.000 claims abstract 2
- 238000002156 mixing Methods 0.000 claims abstract 2
- 238000000034 method Methods 0.000 claims description 20
- 235000013312 flour Nutrition 0.000 claims description 18
- 239000008213 purified water Substances 0.000 claims description 18
- 239000000203 mixture Substances 0.000 claims description 16
- 230000000593 degrading effect Effects 0.000 claims description 12
- 241000234314 Zingiber Species 0.000 claims description 7
- 239000000706 filtrate Substances 0.000 claims description 2
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims 1
- 238000001816 cooling Methods 0.000 abstract description 2
- 238000001914 filtration Methods 0.000 abstract description 2
- 238000010438 heat treatment Methods 0.000 abstract description 2
- 239000000463 material Substances 0.000 abstract description 2
- 239000007788 liquid Substances 0.000 abstract 2
- 235000009508 confectionery Nutrition 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 229940088598 enzyme Drugs 0.000 description 17
- 238000003756 stirring Methods 0.000 description 8
- 239000000796 flavoring agent Substances 0.000 description 7
- 235000019634 flavors Nutrition 0.000 description 7
- 239000012467 final product Substances 0.000 description 6
- 229930006000 Sucrose Natural products 0.000 description 5
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 102000004139 alpha-Amylases Human genes 0.000 description 4
- 108090000637 alpha-Amylases Proteins 0.000 description 4
- 229940024171 alpha-amylase Drugs 0.000 description 4
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 description 3
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 description 3
- 238000011049 filling Methods 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 239000004382 Amylase Substances 0.000 description 2
- 102000013142 Amylases Human genes 0.000 description 2
- 108010065511 Amylases Proteins 0.000 description 2
- 235000019418 amylase Nutrition 0.000 description 2
- 235000013361 beverage Nutrition 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 238000004806 packaging method and process Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 229940100486 rice starch Drugs 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 150000008163 sugars Chemical class 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- PJVXUVWGSCCGHT-ZPYZYFCMSA-N (2r,3s,4r,5r)-2,3,4,5,6-pentahydroxyhexanal;(3s,4r,5r)-1,3,4,5,6-pentahydroxyhexan-2-one Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O.OC[C@@H](O)[C@@H](O)[C@H](O)C(=O)CO PJVXUVWGSCCGHT-ZPYZYFCMSA-N 0.000 description 1
- 229930091371 Fructose Natural products 0.000 description 1
- 239000005715 Fructose Substances 0.000 description 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
- 235000005135 Micromeria juliana Nutrition 0.000 description 1
- 240000002114 Satureja hortensis Species 0.000 description 1
- 235000007315 Satureja hortensis Nutrition 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 238000007429 general method Methods 0.000 description 1
- 230000013595 glycosylation Effects 0.000 description 1
- 238000006206 glycosylation reaction Methods 0.000 description 1
- 235000019534 high fructose corn syrup Nutrition 0.000 description 1
- 230000000887 hydrating effect Effects 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 235000019629 palatability Nutrition 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000036186 satiety Effects 0.000 description 1
- 235000019627 satiety Nutrition 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
- A23L2/84—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter using microorganisms or biological material, e.g. enzymes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L7/00—Cereal-derived products; Malt products; Preparation or treatment thereof
- A23L7/20—Malt products
- A23L7/25—Fermentation of cereal malt or of cereal by malting
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/20—Natural extracts
- A23V2250/21—Plant extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/10—Drying, dehydrating
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/14—Extraction
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/24—Heat, thermal treatment
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/31—Mechanical treatment
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Polymers & Plastics (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Nutrition Science (AREA)
- Microbiology (AREA)
- Molecular Biology (AREA)
- Zoology (AREA)
- Biotechnology (AREA)
- Non-Alcoholic Beverages (AREA)
- Cereal-Derived Products (AREA)
Abstract
Description
본 발명은 식혜의 제조방법에 관한 것으로, 특히 호화된 쌀가루를 이용한 밥알 없는 식혜의 제조방법에 관한 것이다.The present invention relates to a method for producing Sikhye, and more particularly, to a method for producing Sikhye without grains using luxury rice flour.
우리 나라의 전통음료인 식혜는 통상 밥알 10 중량%, 엿기름 10중량%, 물 80중량%에 설탕을 가하여 만드는데, 이러한 전통적인 식혜의 제조방법에서는 미지근한 물에 엿기름을 3 내지 4 시간 동안 추출하여 엿기름액을 얻고 여기에 고두밥을 가하여 엿기름 속에 들어있는 맥아효소에 의해 쌀 전분을 분해시킴으로써 맥아당(maltose) 및 기타 당류를 생성시킨다. 또한, 전통적인 식혜의 제법은 각 지방마다 특색있는 원료를 사용한 다양한 형태의 제조방법들이 있다.Sikhye, the traditional beverage of our country, is usually made by adding sugar to 10% by weight of rice grains, 10% by weight of malt, and 80% by weight of water. In the traditional method of manufacturing Sikhye, malt oil is extracted from lukewarm water for 3 to 4 hours. The maltose and other sugars are produced by adding rice flour to the rice starch and degrading the rice starch by malt enzyme in the malt. In addition, the traditional Sikhye recipe has a variety of manufacturing methods using raw materials that are characteristic of each province.
근래에 전통음료인 식혜가 많은 사람들이 쉽게 마실 수 있도록 상업적으로 생산·판매되고 있다. 이러한 상업적으로 판매되는 식혜에는 통상 전통적인 식혜와 마찬가지로 밥알이 포함되어 있는데, 식혜에 포함된 밥알은 포만감을 느끼게 하고 식혜 고유의 풍미를 느낄 수 있게 하므로 좋아하는 사람들이 있는 반면, 싫어하는 사람들도 있다. 특히, 캔포장과 같은 즉석 음료의 형태로 판매되는 상업적 식혜의 경우 밥알이 포함되어 있으면 음용이 불편해질 뿐만 아니라 밥알이 용기 바닥에 남게 되므로 용기의 재활용에도 장애가 되고 있다.Recently, Sikhye, a traditional drink, has been produced and sold commercially so that many people can easily drink it. These commercially sold Sikhye usually contains rice grains, like traditional Sikhye, and the rice grains included in Sikhye allow people to feel fuller and feel the inherent flavor of Sikhye, while others do not like them. In particular, in the case of commercial sikhye sold in the form of instant drinks such as can packaging, if the rice grains are not only inconvenient to drink, but also because the rice grains remain on the bottom of the container is also a barrier to recycling the container.
따라서, 본 발명은 밥알이 포함되어 있지 않지만 밥알이 포함되어 있는 식혜와 마찬가지로 포만감을 주며 식혜 고유의 풍미가 느껴지는 밥알 없는 식혜의 제조방법을 제공하는 것을 목적으로 한다.Therefore, an object of the present invention is to provide a manufacturing method of rice grain-free Sikhye gives a feeling of satiety and feel the unique flavor of Sikhye like Sikhye that does not contain rice grains.
이를 위해 본 발명에서는 호화된 쌀가루를 이용하여 밥알 없는 식혜를 제조하는데, 구체적으로는 쌀을 스팀으로 찐 후 건조시키고 160℃이상에서 로스팅(roasting)한 후 분쇄한 호화된 쌀가루를 엿기름 추출액에 혼합하여 전분 분해 효소로 당화시키는 제조방법과 엿기름 추출액만을 전분분해 효소로 당화시킨 후 호화된 쌀가루를 첨가하는 제조방법을 제공한다.To this end, in the present invention, using a luxury rice flour to prepare a grain-free Sikhye, specifically steamed rice steamed and dried, then roasted (roasting) at 160 ℃ or more mixed with the milled rice flour malt extract The present invention provides a preparation method of saccharifying with starch degrading enzyme and a method of adding dehydrated rice flour after saccharifying only malt extract with starch degrading enzyme.
호화된 전분과 엿기름 추출액의 혼합물을 전분분해 효소로 당화시키는 방법Method of saccharifying a mixture of gelatinized starch and malt extract with starch enzyme
(a) 제 1공정(a) First step
정제수에 엿기름을 가하여 추출한 후 착즙하여 엿기름 추출액을 만든다. 본 발명에 따른 제조방법에서 식혜는 농축타입과 일반타입으로 제조될 수 있는데, 농축타입의 경우 바람직하게는 50∼70℃ 정도의 온도에서 정제수 100 중량부에 대해 엿기름 6∼8 중량부를 가하여 혼합한 후 1∼2시간 동안 교반하면서 추출하고 압착기를 이용하여 착즙함으로써 엿기름 추출액을 얻는다. 또한, 일반타입의 경우 정제수 100 중량부에 대해 엿기름 2∼4 중량부를 가하여 혼합한 후 1∼2시간 동안 교반하면서 추출하고 압착기를 이용하여 착즙함으로써 엿기름 추출액을 얻는다.Extract malt oil by adding malt to purified water, and then extract it to make malt extract. Sikhye in the manufacturing method according to the present invention can be prepared in a concentrated type and a general type, in the case of the concentrated type is preferably added by adding 6 to 8 parts by weight of malt oil to 100 parts by weight of purified water at a temperature of about 50 ~ 70 ℃ After extraction for 1 to 2 hours with stirring and juiced using a compress to obtain malt extract. In addition, in the case of the general type, 2 to 4 parts by weight of malt oil is added to 100 parts by weight of purified water, mixed, extracted with stirring for 1 to 2 hours, and juiced using a press to obtain malt extract.
(b) 제 2공정(b) second process
별도로, 쌀을 스팀으로 증자한 후 건조시키고 고온, 고압에서 로스팅(roasting)하여 쌀의 전분구조를 변화시킨 후 분쇄하여 호화된 쌀가루를 얻는다. 로스팅은 160∼200℃, 1∼2 기압에서 행하는 것이 바람직하며, 100메쉬의 체를 통과할 수 있을 정도로 분쇄시키는 것이 바람직하다. 본 공정을 거쳐 분쇄된 호화된 쌀가루는 물과의 수화력이 우수하므로 다음 공정에서 엿기름 추출액과 용이하게 혼합될 수 있다.Separately, the rice is steamed and then dried, roasted at high temperature and high pressure to change the starch structure of the rice, and then pulverized to obtain a luxurious rice powder. It is preferable to perform roasting at 160-200 degreeC and 1-2 atmospheres, and to grind | pulverize so that it can pass a 100 mesh sieve. The refined rice flour pulverized by the present process is excellent in the hydrating power with water and can be easily mixed with the malt extract in the next step.
(c) 제 3공정(c) third process
제 1공정에서 얻은 엿기름 추출액에 제 2공정에서 얻은 호화된 쌀가루를 첨가·혼합시키고, 혼합물의 온도를 60℃ 정도로 상승시킨 후, 전분분해 효소를 투입하여 당화시킨다. 호화된 쌀가루는 100메쉬의 체를 통과한 것을 사용하는 것이 바람직하며, 엿기름 추출액에 대해 0.3∼3 중량%로 혼합되는 것이 바람직하다.The malted rice powder obtained in the second step is added and mixed with the malt extract obtained in the first step, the temperature of the mixture is raised to about 60 ° C., and then starch degrading enzyme is added to saccharify it. It is preferable to use the rice powder which passed through the sieve of 100 mesh, and to mix it with 0.3 to 3 weight% with respect to malt extract.
전분분해 효소로는 주로 아밀라제, 특히 α-아밀라제 등이 사용될 수 있으며, 당화는 60℃ 정도로 온도를 일정하게 유지시키면서 1시간 내지 3시간 정도 행하는 것이 바람직하다.Amylase, in particular α-amylase, may be used as the starch degrading enzyme, and saccharification is preferably performed for about 1 hour to 3 hours while keeping the temperature constant at about 60 ° C.
(d) 제 4공정(d) fourth process
제 3공정에서 얻은 당화물에 생강을 가미하고 가열, 냉각, 여과, 가당하는 일련의 공정을 거치면 기존의 식혜보다 고소한 풍미와 깔끔한 맛을 주는 밥알 없는 식혜가 제조된다. 농축타입의 제조방법에서는 당도를 35∼45%로 한 다음 정제수를 가하여 최종제품의 당도를 조정하며, 일반타입의 제조방법에서는 바로 최종제품의 당도로 조정한다. 최종제품의 당도는 10∼12% 정도가 바람직하다. 일정량 충진하여 레토르트 챔버에 넣고 121℃에서 10∼15분간 살균하면 본 발명에 따른 밥알 없는 식혜가 제조된다.Ginger is added to the sugars obtained in the third process, followed by a series of heating, cooling, filtration, and sweetening processes. In the manufacturing method of the concentrated type, the sugar content of the final product is adjusted to 35-45% and then purified water is added. In the general method, the sugar content of the final product is adjusted immediately. The sweetness of the final product is preferably about 10 to 12%. After filling a certain amount into the retort chamber and sterilized at 121 ℃ for 10 to 15 minutes to prepare a grain-free Sikhye according to the present invention.
엿기름 추출액만을 전분분해 효소로 당화시키는 방법Method of saccharifying only malt extract with starch enzyme
엿기름 추출액만을 전분분해 효소로 당화시킨 후 호화된 쌀가루를 가하여 밥알 없는 식혜를 제조할 수도 있다. 구체적인 제조공정은 다음과 같다.Only malt extract can be saccharified with starch degrading enzyme, and then, added with luxurious rice flour, can be prepared without rice grains. The specific manufacturing process is as follows.
(a) 제 1공정(a) First step
정제수에 엿기름을 가하여 추출한 후 착즙하여 엿기름 추출액을 만든다. 본 발명에 따른 제조방법에서 식혜는 농축타입과 일반타입으로 제조될 수 있는데, 농축타입의 경우 바람직하게는 50∼70℃ 정도의 온도에서 정제수 100 중량부에 대해 엿기름 6.5∼8.5 중량부를 가하여 혼합한 후 1∼2시간 동안 교반하면서 추출하고 압착기를 이용하여 착즙함으로써 엿기름 추출액을 얻는다. 또한, 일반타입의 경우 정제수 100 중량부에 대해 엿기름 2∼4 중량부를 가하여 혼합한 후 1∼2시간 동안 교반하면서 추출하고 압착기를 이용하여 착즙함으로써 엿기름 추출액을 얻는다.Extract malt oil by adding malt to purified water, and then extract it to make malt extract. Sikhye in the manufacturing method according to the present invention can be prepared in a concentrated type and a general type, in the case of the concentrated type is preferably added by adding 6.5 to 8.5 parts by weight of malt oil to 100 parts by weight of purified water at a temperature of about 50 ~ 70 ℃ After extraction for 1 to 2 hours with stirring and juiced using a compress to obtain malt extract. In addition, in the case of the general type, 2 to 4 parts by weight of malt oil is added to 100 parts by weight of purified water, mixed, extracted with stirring for 1 to 2 hours, and juiced using a press to obtain malt extract.
(b) 제 2공정(b) second process
별도로, 쌀을 스팀으로 증자한 후 건조시키고 고온, 고압에서 로스팅(roasting)하여 쌀의 전분구조를 변화시킨 후 분쇄한다. 로스팅은 160∼200℃, 1∼2 기압에서 행하는 것이 바람직하며, 로스팅된 것은 100메쉬의 체를 통과할 수 있을 정도로 분쇄시킨다.Separately, the rice is steamed and then dried and roasted at high temperature and high pressure to change the starch structure of the rice and then crushed. Roasting is preferably performed at 160 to 200 ° C. and 1 to 2 atmospheres, and the roasted material is pulverized to a degree that can pass through a 100 mesh sieve.
(c) 제 3공정(c) third process
제 1공정에서 얻은 엿기름 추출액의 온도를 60℃ 정도로 상승시킨 후 전분분해 효소를 투입하여 당화시킨다. 전분분해 효소로는 주로 아밀라제, 특히 α-아밀라제 등이 사용될 수 있으며, 당화는 60℃ 정도로 온도를 일정하게 유지시키면서 1시간 내지 2시간 정도 행하는 것이 바람직하다.After raising the temperature of the malt extract obtained in the first step to about 60 ℃, the starch degrading enzyme is added to saccharify. Amylase, in particular α-amylase, may be used as the starch degrading enzyme, and glycosylation is preferably performed for about 1 hour to 2 hours while keeping the temperature constant at about 60 ° C.
(d) 제 4공정(d) fourth process
제 3공정에서 얻은 당화물에 생강을 가하고 가열, 냉각, 여과한 후, 제 2공정에서 얻은 호화된 쌀가루를 가하고 가당하면 고소한 풍미와 깔끔한 맛을 주는 밥알 없는 식혜가 제조된다. 농축타입의 제조방법에서는 호화된 쌀가루를 1∼6 중량%로 가하고 가당하여 당도를 20∼30%로 조정한 다음 정제수를 가하여 최종제품의 당도를 조절한다. 일반타입의 제조방법에서는 호화된 쌀가루를 0.3∼3 중량%로 가하고 가당하여 최종제품의 당도로 조정한다. 최종제품의 당도는 10∼12% 정도가 바람직하다. 일정량 충진하여 레토르트 챔버에 넣고 121℃에서 10∼15분간 살균하면 본 발명에 따른 밥알 없는 식혜가 제조된다.Ginger is added to the sugar obtained in the third step, heated, cooled, and filtered, and then added to the luxurious rice powder obtained in the second step and sweetened to produce a grain-free Sikhye that gives a savory flavor and a refreshing taste. In the production method of concentrated type, 1 to 6% by weight of luxurious rice flour is added, the sugar content is adjusted to 20 to 30%, and purified water is added to adjust the sugar content of the final product. In the manufacturing method of the general type, the added rice flour 0.3 to 3% by weight, and added to adjust the sugar content of the final product. The sweetness of the final product is preferably about 10 to 12%. After filling a certain amount into the retort chamber and sterilized at 121 ℃ for 10 to 15 minutes to prepare a grain-free Sikhye according to the present invention.
이하, 실시예를 통해 본 발명을 보다 상세히 설명한다.Hereinafter, the present invention will be described in more detail with reference to Examples.
실시예 1 (제조예)Example 1 (Manufacturing Example)
호화된 전분과 엿기름 추출액의 혼합물을 전분분해 효소로 당화시켜 밥알 없는 식혜를 제조하는 방법 (농축타입 제조법)Method for preparing Sikhye without rice grains by saccharifying a mixture of gelatinized starch and malt extract with starch enzyme (concentrated production method)
(ⅰ) 60℃의 온도에서 정제수 1900g에 엿기름 135g을 가한 후 잘 교반하면서 1시간 30분 동안 추출하고 압착기를 이용하여 착즙하여 엿기름 추출액을 얻었다.(Iii) 135 g of malt oil was added to 1900 g of purified water at a temperature of 60 ° C., and the mixture was extracted for 1 hour and 30 minutes while stirring well, and juiced using a press machine to obtain malt extract.
(ⅱ) 별도로, 쌀을 스팀으로 증자한 후 건조시키고 고온, 고압에서 로스팅한 후 분쇄하여 100메쉬(mesh)의 체를 통과시켰다.(Ii) Separately, the rice was steamed, steamed, dried, roasted at high temperature and high pressure, and ground to pass through a 100-mesh sieve.
(ⅲ) (ⅱ)에서 얻은 100메쉬의 체를 통과한 호화된 쌀가루 35g을 18℃의 정제수 300g에 분산시킨 후 (ⅰ)에서 얻은 엿기름 추출액과 혼합시키고, 이 혼합물의 온도를 60℃로 상승시킨 후 α-아밀라제 1g을 가하고 일정하게 온도를 유지시키면서 1시간 30분 동안 당화시켰다.(Iii) 35 g of the luxurious rice flour passed through 100 mesh sieve obtained in (ii) was dispersed in 300 g of purified water at 18 ° C., and then mixed with the malt extract obtained in (iii), and the temperature of the mixture was raised to 60 ° C. 1 g of α-amylase was then added and saccharified for 1 hour and 30 minutes while maintaining a constant temperature.
(ⅳ) (ⅲ)에서 얻은 당화액에 생강 4g을 가하고 100℃에서 3분간 자비한 후 80℃이하로 냉각시켜 200메쉬의 체로 여과했다. 여과된 액에 정백당을 가하여 당도 40%가 되도록 한 후, 정제수로 희석하여 다시 당도를 11%로 조정한 다음 일정량 충진하여 레토르트 챔버에 넣고 121℃에서 12분간 살균함으로써 밥알 없는 식혜를 제조했다.(Iii) 4 g of ginger was added to the saccharified solution obtained in (iii), and after boiling at 100 ° C. for 3 minutes, the mixture was cooled to 80 ° C. or lower, and filtered through a 200 mesh sieve. White sugar was added to the filtered solution so that the sugar content was 40%, and then diluted with purified water to adjust the sugar content to 11% again, and then filled in a predetermined amount into a retort chamber to sterilize for 12 minutes at 121 ℃ to prepare a rice grain free.
실시예 2 (제조예)Example 2 (Manufacturing Example)
호화된 전분과 엿기름 추출액의 혼합물을 전분분해 효소로 당화시켜 밥알 없는 식혜를 제조하는 방법 (일반타입 제조법)Method to prepare Sikhye without rice by saccharifying a mixture of gelatinized starch and malt extract with starch degrading enzyme (general type manufacturing method)
(ⅰ) 60℃의 온도에서 정제수 4,750g에 엿기름 135g을 가한 후 잘 교반하면서 1시간 30분 동안 추출하고 압착기를 이용하여 착즙하여 엿기름 추출액을 얻었다.(Iii) After adding malt 135g to 4,750g of purified water at a temperature of 60 ° C, the mixture was extracted for 1 hour and 30 minutes while stirring well, and juiced using a compress to obtain malt extract.
(ⅱ) 별도로, 쌀을 스팀으로 증자한 후 건조시키고 고온, 고압에서 로스팅한 후 분쇄하여 100메쉬(mesh)의 체를 통과시켰다.(Ii) Separately, the rice was steamed, steamed, dried, roasted at high temperature and high pressure, and ground to pass through a 100-mesh sieve.
(ⅲ) (ⅱ)에서 얻은 100메쉬의 체를 통과한 호화된 쌀가루 35g을 18℃의 정제수 300g에 분산시킨 후 (ⅰ)에서 얻은 엿기름 추출액과 혼합시키고, 이 혼합물의 온도를 60℃로 상승시킨 후 α-아밀라제 1g을 가하고 온도를 일정하게 유지시키면서 1시간 30분 동안 당화시켰다.(Iii) 35 g of the luxurious rice flour passed through 100 mesh sieve obtained in (ii) was dispersed in 300 g of purified water at 18 ° C., and then mixed with the malt extract obtained in (iii), and the temperature of the mixture was raised to 60 ° C. 1 g of α-amylase was then added and saccharified for 1 hour and 30 minutes while keeping the temperature constant.
(ⅳ) (ⅲ)에서 얻은 당화액에 생강 4g을 가하고 100℃에서 3분간 자비한 후 80℃이하로 냉각시켜 200메쉬의 체로 여과했다. 여과액에 정백당을 가하여 당도를 11%로 조정한 후 일정량 충진하여 레토르트 챔버에 넣고 121℃에서 12분간 살균함으로써 밥알 없는 식혜를 제조했다.(Iii) 4 g of ginger was added to the saccharified solution obtained in (iii), and after boiling at 100 ° C. for 3 minutes, the mixture was cooled to 80 ° C. or lower, and filtered through a 200 mesh sieve. White sugar was added to the filtrate to adjust the sugar content to 11%, and then filled in a predetermined amount into the retort chamber to sterilize for 12 minutes at 121 ℃ to prepare a rice grain without rice.
실시예 3 (제조예)Example 3 (Manufacturing Example)
엿기름 추출액만을 전분분해 효소로 당화시켜 밥알 없는 식혜를 제조하는 방법 (농축타입 제조법)Method to prepare Sikhye without rice by saccharifying only malt extract with starch enzyme (concentrated production method)
(ⅰ) 60℃의 온도에서 정제수 1,900g에 엿기름 145g을 가한 후 잘 교반하면서 1시간 30분 동안 추출하고 압착기를 이용하여 착즙함으로써 엿기름 추출액을 얻었다.(Ix) 145 g of malt oil was added to 1,900 g of purified water at a temperature of 60 ° C., and the mixture was extracted for 1 hour and 30 minutes while stirring well, and juiced using a press machine to obtain malt extract.
(ⅱ) 별도로, 쌀을 스팀으로 증자한 후 건조시키고 고온, 고압에서 로스팅한 후 분쇄하여 100메쉬(mesh)의 체를 통과시켰다.(Ii) Separately, the rice was steamed, steamed, dried, roasted at high temperature and high pressure, and ground to pass through a 100-mesh sieve.
(ⅲ) (ⅰ)에서 얻은 엿기름 추출액에 전분분해 효소 0.5g을 가하고 온도를 일정하게 유지시키면서 1시간 동안 당화시켰다.(Iii) 0.5 g of starch degrading enzyme was added to the malt extract obtained in (iii), and saccharified for 1 hour while keeping the temperature constant.
(ⅳ) (ⅲ)에서 얻은 당화액에 생강 4g을 가하고 100℃에서 3분간 자비한 후 80℃이하로 냉각시켜 200메쉬의 체로 여과한 다음, 이 여과액에 (ⅱ)에서 얻은 100메쉬의 체를 통과한 호화된 쌀가루 2 중량%와 정백당을 가하여 30%의 당도가 되도록 했다. 이것을 정제수로 희석하여 당도 11%가 되도록 조정한 후 일정량 충진하여 레토르트 챔버에 넣고 121℃에서 12분간 살균함으로써 밥알 없는 식혜를 제조했다.(Iii) 4 g of ginger was added to the saccharified solution obtained in (iii), and then boiled at 100 DEG C for 3 minutes, cooled to 80 DEG C or lower, filtered through a 200 mesh sieve, and then filtered into a 100 mesh sieve obtained in (ii). 2% by weight of deluxe rice flour and white sugar were added to make the sugar content 30%. After diluting this with purified water so that the sugar content was adjusted to 11%, it was filled in a predetermined amount and placed in a retort chamber for sterilization at 121 ° C. for 12 minutes to prepare rice grains without rice.
실시예 4 (제조예)Example 4 (Manufacturing Example)
엿기름 추출액만을 전분분해 효소로 당화시켜 밥알 없는 식혜를 제조하는 방법 (일반타입 제조법)Method to prepare Sikhye without rice by saccharifying only malt extract with starch enzyme (general type manufacturing method)
(ⅰ) 60℃의 온도에서 정제수 4,750g에 엿기름 145g을 가한 후 잘 교반하면서 1시간 30분 동안 추출하고 압착기를 이용하여 착즙함으로써 엿기름 추출액을 얻었다.(Iii) 145 g of malt oil was added to 4,750 g of purified water at a temperature of 60 ° C., and the mixture was extracted for 1 hour and 30 minutes while stirring well, and juiced using a press machine to obtain malt extract.
(ⅱ) 별도로, 쌀을 스팀으로 증자한 후 건조시키고 고온, 고압에서 로스팅한 후 분쇄하여 100메쉬(mesh)의 체를 통과시켰다.(Ii) Separately, the rice was steamed, steamed, dried, roasted at high temperature and high pressure, and ground to pass through a 100-mesh sieve.
(ⅲ) (ⅰ)에서 얻은 엿기름 추출액에 전분분해 효소 0.5g을 가하고 온도를 일정하게 유지시키면서 1시간 동안 당화시켰다.(Iii) 0.5 g of starch degrading enzyme was added to the malt extract obtained in (iii), and saccharified for 1 hour while keeping the temperature constant.
(ⅳ) (ⅲ)에서 얻은 당화액에 생강 4g을 가하고 100℃에서 3분간 자비한 후 80℃이하로 냉각시켜 200메쉬의 체로 여과한 다음, 이 여과액에 (ⅳ)에서 얻은 100메쉬의 체를 통과한 호화된 쌀가루 1중량%를 첨가·혼합하고, 정백당을 가하여 당도 11%가 되도록 했다. 혼합액을 일정량 충진한 후 레토르트 챔버에 넣고 121℃에서 12분간 살균함으로써 밥알 없는 식혜를 제조했다.(Iii) 4 g of ginger was added to the saccharified solution obtained in (iii), and then boiled for 3 minutes at 100 ° C., cooled to 80 ° C. or less, filtered through a 200 mesh sieve, and then 100 mesh sieve obtained in (iii). 1% by weight of the refined rice flour passed through was added and mixed, and white sugar was added so that the sugar content was 11%. After filling a predetermined amount of the mixed solution into the retort chamber was sterilized for 12 minutes at 121 ℃ to prepare a rice grain without rice.
실시예 5Example 5
당화시간에 따른 당함량(%)의 측정Measurement of sugar content (%) according to the saccharification time
실시예 1에 따른 제조방법에 있어서, 전분분해 효소를 첨가한 후 당화 시간에 따른 당함량을 측정하고 그 결과를 다음의 표 1에 나타내었다.In the preparation method according to Example 1, the sugar content according to the saccharification time after the starch enzyme was added and the results are shown in Table 1 below.
표 1. 당화시간에 따른 당함량(%)Table 1. Sugar content (%) by saccharification time
전통적인 식혜 제조방법에 의한 당화 4∼6시간 후의 당함량과 같은 수준의 당함량을 본 발명에서는 당화 2시간 후에 나타냈다.The sugar content equivalent to the sugar content after 4 to 6 hours of saccharification by the traditional Sikhye production method is shown after 2 hours of saccharification in the present invention.
실시예 6Example 6
본 발명에 따른 밥알 없는 식혜의 당 조성비 측정Measurement of sugar composition ratio of Sikhye without rice grains according to the present invention
실시예 1 및 실시예 3에서 제조된 밥알 없는 식혜의 당 조성비를 각각 측정한 후 그 결과를 다음의 표 2에 나타내었다.After measuring the sugar composition ratio of Sikhye without rice prepared in Examples 1 and 3, respectively, the results are shown in Table 2 below.
표 2. 당 조성비(%)Table 2. Sugar composition ratio (%)
실시예 7Example 7
본 발명에 따른 밥알 없는 식혜의 기호도 평가Evaluation of palatability of Sikhye without rice according to the present invention
실시예 1 및 실시예 3에 따라 제조된 밥알 없는 식혜와 전통적인 방법으로 제조된 식혜의 풍미, 전체적인 맛, 기호도를 비교 측정하였다. 측정은 관능테스트 (7점법)로 하였으며 결과를 다음의 표 3에 나타내었다.The flavor, overall taste, and preference of Sikhye without rice grains prepared according to Examples 1 and 3 and Sikhye prepared by the traditional method were measured. The measurement was performed by the sensory test (7-point method) and the results are shown in Table 3 below.
표 3. 기호도 평가Table 3. Preference Evaluation
(7: 아주 좋다, 6: 좋다, 5: 약간 좋다, 4: 보통이다, 3: 약간 싫다, 2: 싫다, 1: 아주 싫다)(7: Very good, 6: Good, 5: Slightly good, 4: Normal, 3: Slightly disliked, 2: Disliked, 1: Disliked)
관능테스트 결과 본 발명에 따른 밥알 없는 식혜는 전통식혜와 비교할 때 풍미, 전체적인 맛, 기호도 면에서 보다 우수한 것으로 나타났다.As a result of the sensory test, Sikhye without rice grains according to the present invention was found to be superior in terms of flavor, overall taste, and preference compared with traditional Sikhye.
상기 실시예로부터 알 수 있는 바와 같이, 본 발명에 따른 밥알 없는 식혜는 밥알이 포함되어 있지 않지만 밥알이 포함되어 있는 식혜와 마찬가지로 또는 그 이상으로 풍미, 전체적인 맛, 기호도면에서 매우 만족스러우며, 캔포장과 같은 즉석음료의 형태에 있어서 음용이 보다 용이해지고 용기의 재활용 또한 쉬워진다는 효과가 있다.As can be seen from the above examples, Sikhye without rice grains according to the present invention is not satisfactory in the flavor, overall taste, taste drawing like can or more than Sikhye containing rice grains, can packaging In the form of instant beverages, such as drinking is easier and the container is recycled.
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1019980023107A KR100277349B1 (en) | 1998-06-19 | 1998-06-19 | Manufacturing method of Sikhye without rice using luxury rice flour |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1019980023107A KR100277349B1 (en) | 1998-06-19 | 1998-06-19 | Manufacturing method of Sikhye without rice using luxury rice flour |
Publications (2)
Publication Number | Publication Date |
---|---|
KR20000002389A true KR20000002389A (en) | 2000-01-15 |
KR100277349B1 KR100277349B1 (en) | 2001-01-15 |
Family
ID=19540063
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019980023107A KR100277349B1 (en) | 1998-06-19 | 1998-06-19 | Manufacturing method of Sikhye without rice using luxury rice flour |
Country Status (1)
Country | Link |
---|---|
KR (1) | KR100277349B1 (en) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR101352655B1 (en) * | 2012-12-20 | 2014-01-17 | 경기도 | Rice beverage containing high proportion of amino acid and manufacturing method thereof |
KR101379116B1 (en) * | 2011-12-16 | 2014-04-01 | 한국식품연구원 | Preparation method of rice starch syrup comprising lycopene |
KR20170036986A (en) | 2015-09-25 | 2017-04-04 | 주식회사 이롬 | A method for grain drinks using rice |
KR20190056169A (en) | 2017-11-16 | 2019-05-24 | 씨제이제일제당 (주) | Method for preparing rice paste and rice paste prepared thereby |
KR102398102B1 (en) * | 2022-03-10 | 2022-05-13 | 이계수 | Potato sweet drink containing herbal concentrate |
KR102400869B1 (en) * | 2021-12-10 | 2022-05-23 | 농업회사법인 마음이가주식회사 | Sikhye manufacturing method by natural saccharification method |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100769628B1 (en) | 2001-11-02 | 2007-10-23 | 제해수 | An instant Sikhae powder and its manufacturing method |
KR100642869B1 (en) * | 2005-07-01 | 2006-11-10 | 서정옥 | Sikhye without grains of boiled rice produced by nano-filtering and a method for producing the same |
KR101014636B1 (en) * | 2010-02-09 | 2011-02-16 | 조상균 | Method for manufacturing sikhye, and sikhye manufactured by the same |
KR101183963B1 (en) | 2012-02-23 | 2012-09-18 | 주식회사 자연과사람들 | Manufacturing method of grain-free traditional rice punch |
KR102583072B1 (en) | 2021-01-08 | 2023-09-27 | (주)새암푸드먼트 | Manufacturing Method for Sikhye having Rice Shape |
KR20230086033A (en) | 2021-12-08 | 2023-06-15 | 롯데칠성음료주식회사 | A manufacture method of rice grain-free sikhye that can be made without rice steaming and cooking process |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100192059B1 (en) * | 1996-06-13 | 1999-08-02 | 김부곤 | Beverage of fermented rice punch |
-
1998
- 1998-06-19 KR KR1019980023107A patent/KR100277349B1/en not_active IP Right Cessation
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR101379116B1 (en) * | 2011-12-16 | 2014-04-01 | 한국식품연구원 | Preparation method of rice starch syrup comprising lycopene |
KR101352655B1 (en) * | 2012-12-20 | 2014-01-17 | 경기도 | Rice beverage containing high proportion of amino acid and manufacturing method thereof |
KR20170036986A (en) | 2015-09-25 | 2017-04-04 | 주식회사 이롬 | A method for grain drinks using rice |
KR20190056169A (en) | 2017-11-16 | 2019-05-24 | 씨제이제일제당 (주) | Method for preparing rice paste and rice paste prepared thereby |
KR102400869B1 (en) * | 2021-12-10 | 2022-05-23 | 농업회사법인 마음이가주식회사 | Sikhye manufacturing method by natural saccharification method |
KR102398102B1 (en) * | 2022-03-10 | 2022-05-13 | 이계수 | Potato sweet drink containing herbal concentrate |
Also Published As
Publication number | Publication date |
---|---|
KR100277349B1 (en) | 2001-01-15 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US20090081328A1 (en) | Fermented Beverage Using Fractionated Corn | |
KR101336776B1 (en) | Manufacturing method of brown rice sweet drink and brown rice grain syrup, brown rice taffy and brown rice sugar using the brown rice sweet drink | |
KR101159173B1 (en) | Method for preparing beer with ginseng and rice | |
JP5695323B2 (en) | Beer-taste beverage using colored malt and brown rice and method for producing the same | |
CN103468464B (en) | The beer flavor beverage of high voitol and high furanone content | |
KR100277349B1 (en) | Manufacturing method of Sikhye without rice using luxury rice flour | |
CN103126030A (en) | Non-alcoholic beer-flavored beverage with tangy taste | |
CN100460495C (en) | Double yeast white spirit with different fragrance and its prepn process | |
WO2018061370A1 (en) | Beer-flavored beverage, method for producing beer-flavored beverage, and method for imparting excellent richness and quality of aftertaste to beer-flavored beverage | |
JPH10229868A (en) | Production of alcoholic drink | |
US20040180112A1 (en) | Process for the production of alcoholic coffee drinks | |
JP5607379B2 (en) | Beer-taste beverage using brown rice and method for producing the same | |
JP2019205385A (en) | Malt-fermented beverage and method for producing the same | |
JP7470512B2 (en) | Beer-flavored beverages | |
KR102204551B1 (en) | Method for producing regional alcoholic beverage using 6JUL barley grains | |
JP6534254B2 (en) | Method for producing beer-like effervescent beverage | |
CN110643444B (en) | Preparation method of Chinese yam health beer | |
KR102094197B1 (en) | Method for Preparing Buckwheat Beer | |
KR101999746B1 (en) | Preparation method of fermented alcoholic beverage with beer flavour using herb | |
KR20220073305A (en) | Beer manufacturing method using potato and red bean paste | |
JP7215820B2 (en) | Beer-taste beverage, method for producing same, and method for improving flavor of beer-taste beverage | |
CN103907989A (en) | Alcohol-free beer flavor beverage with astringency endowed taste | |
KR102621087B1 (en) | Manufacturing method of fermented liquor or soup containing the hazelnut fruit extract or powder and the fermented liquor or soup containing the hazelnut fruit extract or powder prepared thereby | |
KR102600744B1 (en) | Zanthoxylum piperitum Beer and Manufacturing Method thereof | |
KR102591999B1 (en) | Rice fermentated beverage for dessert and Manaufacturing method of the same |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
A201 | Request for examination | ||
E902 | Notification of reason for refusal | ||
E701 | Decision to grant or registration of patent right | ||
GRNT | Written decision to grant | ||
FPAY | Annual fee payment |
Payment date: 20121008 Year of fee payment: 13 |
|
FPAY | Annual fee payment |
Payment date: 20131008 Year of fee payment: 14 |
|
FPAY | Annual fee payment |
Payment date: 20141010 Year of fee payment: 15 |
|
FPAY | Annual fee payment |
Payment date: 20151007 Year of fee payment: 16 |
|
FPAY | Annual fee payment |
Payment date: 20161011 Year of fee payment: 17 |
|
EXPY | Expiration of term |