KR19980019769A - Manufacturing method of ceramic composition for freshness - Google Patents

Manufacturing method of ceramic composition for freshness Download PDF

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KR19980019769A
KR19980019769A KR1019960038006A KR19960038006A KR19980019769A KR 19980019769 A KR19980019769 A KR 19980019769A KR 1019960038006 A KR1019960038006 A KR 1019960038006A KR 19960038006 A KR19960038006 A KR 19960038006A KR 19980019769 A KR19980019769 A KR 19980019769A
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weight
effect
freshness
manufacturing
parts
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KR1019960038006A
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KR0163360B1 (en
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변상율
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변상율
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    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00—Clay-wares
    • C04B33/02—Preparing or treating the raw materials individually or as batches
    • C04B33/04—Clay; Kaolin
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00—Clay-wares
    • C04B33/02—Preparing or treating the raw materials individually or as batches
    • C04B33/13—Compounding ingredients
    • C04B33/131—Inorganic additives
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00—Clay-wares
    • C04B33/32—Burning methods
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/0045—Irradiation; Radiation, e.g. with UV or IR
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427—Silicates other than clay, e.g. water glass
    • C04B2235/3463—Alumino-silicates other than clay, e.g. mullite

Abstract

본 발명은 식품의 선도를 장기간 유지시켜 주고, 탈취효과 및 정수효과가 우수한 세라믹 조성물 및 그 제조방법에 관한 것으로, 맥반석 20-30중량%, 견운모 25-35중량%, 황토 40-50중량%로 구성된 조성물 100중량부에 경명주사를 0.0005-0.05중량부를 가하고 이를 물에 넣고 잘 혼련한 후 150-200℃의 온도에서 48-72시간 동안 숙성시킨 다음, 700-1200℃의 온도에서 3-8시간 동안 소성시키고, 얻어진 소성체에 1000-1250가우스의 자력을 조사하는 것을 특징으로 한다.The present invention relates to a ceramic composition for maintaining the freshness of food for a long time, excellent in deodorizing effect and water purification effect, and a method of manufacturing the same, with 20-30% by weight of barbanite, 25-35% by weight of mica, and 40-50% by weight of ocher. 0.0005-0.05 parts by weight of light injection was added to 100 parts of the composition, which was then kneaded well and aged for 48-72 hours at a temperature of 150-200 ° C., followed by 3-8 hours at a temperature of 700-1200 ° C. It is characterized in that the magnetic body of 1000-1250 gauss is irradiated to the resulting fired body.

Description

선도유지용 세라믹조성물의 제조방법Manufacturing method of ceramic composition for freshness

본 발명은 선도유지용 세라믹조성물의 제조방법에 관한 것으로, 보다 상세하게는 식품의 선도를 장기간 유지시켜 주고, 탈취효과 및 정수효과가 우수한 세라믹 조성물 및 그 제조방법에 관한 것이다.The present invention relates to a method for producing a fresh ceramic holding composition, and more particularly, to a ceramic composition which maintains freshness of a food for a long time, and has an excellent deodorizing effect and a water purification effect, and a method of manufacturing the same.

최근, 원적외선을 이용한 가열, 건조 및 치료에 대한 연구개발이 활발히 진행되고 있으며, 그 사용분야도 난방, 의료, 조리, 식품가공, 측정, 건강산업 등에 파급되고 있다. 예를들면, 타원상 구체 등으로 소결된 세라믹스는 음식물의 조리시 직접 첨가하여 가열함으로써 열효율을 증가시켜 에너지를 절감할 수 있고 음식의 맛이 좋아지며, 알콜음료에 넣을 경우는 숙성을 촉징시키며, 김치에 넣을 경우는 초산발효를 억제시켜 장기간 보존할 수 있고, 어항에 넣어 둘 경우에는 어류의 생육이 좋아지고 질병이 감소되며, 또한 벤드상으로 소결된 세라믹스는 인체에 부착되어 원적외선 방사에 의한 찜질효과를 나타내는 것으로 알려져 있다.In recent years, research and development on heating, drying, and treatment using far infrared rays have been actively conducted, and its use field is also spreading to heating, medical, cooking, food processing, measuring, and health industries. For example, ceramics sintered into elliptical spheres, etc., can be added directly when cooking to heat the food to increase thermal efficiency, thereby saving energy, improving the taste of the food, and encouraging aging in the case of alcoholic beverages. If you put it in kimchi, it can be preserved for a long time by suppressing the fermentation of acetic acid.If you put it in a fish tank, the growth of fish is improved and the disease is reduced.In addition, ceramics sintered in the bend form are attached to the human body It is known to have an effect.

한편, 이러한 세라믹조성물에 인체에 유익한 효과를 주는 맥반석을 첨가하여 그 효과를 더욱 향상시킨 기술들이 최근에 개발되기 시작하였으며, 그 예로는 일본국 공개특허 평1-299691호를 들 수 있다.On the other hand, the addition of the ganban stone that has a beneficial effect on the human body to such a ceramic composition has been recently developed to further improve the effect, for example, Japanese Patent Laid-Open No. 1-299691.

이 기술은 무수한 규소, 산화알루미늄, 산화철, 산화티탄, 산화칼슘, 산화마그네슘, 산화칼륨, 무수산망간 등으로 이루어진 맥반석 분말 80-90중량%에 실리카, 알루미나 성분을 포함한 것을 분말화하여 이를 20중량% 혼합한 것에 물유리를 첨가하여 형성된 구형의 성형물을 소성로에 넣어 1400-1600℃의 온도로 소성한 것으로 주로 오염된 물을 재생시키는 정수기의 여과재로 사용되고 있다. 그러나 이 기술은 첨가된 물유리에 의하여 성형은 용이하게 되나 함유된 미네랄 성분들의 활성이 저하되어 실용화에 문제점이 있었다.This technique powders 80-90% by weight of gannetite powder composed of innumerable silicon, aluminum oxide, iron oxide, titanium oxide, calcium oxide, magnesium oxide, potassium oxide, manganese anhydride, and the like containing silica and alumina components, and then 20% by weight. The spherical molded product formed by adding water glass to the% mixture was put into a kiln and fired at a temperature of 1400-1600 ° C. It is mainly used as a filter material for water purifiers to regenerate contaminated water. However, this technique is easy to mold by the added water glass, but there is a problem in practical use because the activity of the mineral components contained is reduced.

이 외에 비교적 장피장의 원적외선을 방사하는 특징을 갖는 세라믹스에 관한 기술로는 일본국 특허공고 소 53-44928호, 소 50-2421호 및 소 54-21844호 등이 있으며, 이러한 기술들은 그 소성제품의 강도가 낮고 고온에서 사용시 크랙이 발생하는 등의 결점을 가지고 있을 뿐만 아니라, 특히 항상 고온에서 원적외선이 효과적으로 방사되기 때문에 실용적인 면에서 문제가 있었다.In addition, techniques related to ceramics having a characteristic of emitting far infrared rays in relatively long coats include Japanese Patent Publication Nos. 53-44928, 50-2421, and 54-21844. In addition to the disadvantages such as low strength and cracking when used at high temperatures, there is a problem in terms of practical use, because the far infrared radiation is always radiated effectively at high temperatures.

본 발명은 상기한 바와 같은 문제점을 해결하기 위한 것으로, 상온에서 높은 효율로 원적외선을 방사함으로써 식품의 선도유지 효과가 뛰어남과 동시에, 얻어진 제품의 강도가 우수하고, 특히 얻어진 제품의 살균력이 향상됨으로써 탈취효과 및 정수효과가 향상된 세라믹조성물을 제공하는 것을 목적으로 한다.The present invention is to solve the problems described above, by deodorizing far infrared rays at high temperature at room temperature, excellent in freshness maintaining effect of the food, the strength of the obtained product is excellent, in particular, the sterilization power of the obtained product is deodorized An object of the present invention is to provide a ceramic composition having improved effects and water purification effects.

제 1도는 실온에서 11일 경과 후의 토마토 사진Figure 1 shows tomatoes after 11 days at room temperature

본 발명은 맥반석 20-30중량%, 견운모 25-35중량%, 황토 40-50중량%로 구성된 조성물 100중량부에 경명주사를 0.0005-0.05중량부를 가하고 이를 물에 넣고 잘 혼련한 후 150-200℃의 온도에서 48-72시간 동안 숙성시킨 다음, 700-1200℃ 온도에서 3-8시간 동안 소성시키고 여기에 1000-1250가우스의 자력을 조사하는 것을 특징으로 한다.The present invention is added to 0.0005-0.05 parts by weight of light injection in 100 parts by weight of the composition consisting of 20-30% by weight of gandolite, 25-35% by weight, ocher 40-50% by weight and kneaded well in water and then 150-200 After aging for 48-72 hours at a temperature of ℃, it is calcined for 3-8 hours at a temperature of 700-1200 ℃ characterized in that the magnetic force of 1000-1250 gauss is investigated.

이하, 본 발명을 상세히 설명한다.Hereinafter, the present invention will be described in detail.

본 발명에서 사용되는 맥반석과 견운모는 무수규산과 산화알루미늄을 주구성으로 하고 있으며, 우리나라에 흔히 존재하는 광물질로서 생체에 유익한 효과를 발휘하는 것은 잘 알려져 있다. 황토 역시 우리나라에 풍부하게 존재하는 것으로 생체에 유익한 효과를 나타내며, 이러한 황토의 성질을 이용하여 황토타일 내장형 고기구이기(출원번호 94-32712호), 방바닥 온돌용 황토흙 판재(출원번호 94-8928호) 등과 같은 황토를 이용한 특허출원이 이어지고 있다.The elvan and biotite used in the present invention are composed mainly of silicic anhydride and aluminum oxide, and it is well known to exert a beneficial effect on the living body as a mineral commonly present in Korea. Ocher is also present in Korea abundantly and has a beneficial effect on the living body, using the properties of the ocher tile ocher tile built-in meat grinder (Application No. 94-32712), loess soil plate for flooring (Application No. 94-8928) Patent application using loess such as) is continued.

맥반석과 견운모, 황토의 적절한 사용비율은 20-30중량%; 25-35중량%; 40-50중량%로서 이 범위의 것이 상호간의 조성성분이 잘 조화되어 식품의 선도유지효과 및 탈취효과 및 정수효과가 우수할 뿐만 아니라, 소성체의 강도 및 내구성이 향상된다.Suitable use ratio of elvan, biotite and loess is 20-30% by weight; 25-35% by weight; 40-50% by weight of this range is well harmonized with the composition of each other, not only excellent freshness, deodorizing effect and water purification effect of food, but also improves the strength and durability of the fired body.

상기 맥반석, 견운모, 황토로 구성된 조성물 100중량부에 경명주사를 0.0005-0.05중량부를 첨가하는 것이 필요하며, 경명주사는 부적을 만들 때 사용되는 붉은 흙으로서 첨가된 경명주사에 의하여 살균력이 현저하게 향상된다. 살균력이 향상됨에 따라 탈취효과는 더욱 향상된다. 적절한 사용량은 맥반석, 견운모, 황토로 구성된 조성물 100중량부에 대하여 0.0005-0.05중량부이며, 이 범위 미만인 경우에는 살균효과가 부족하게 되며, 이 범위를 초과하게 되면 더 이상 살균효과가 증가하지 아니한다.It is necessary to add 0.0005-0.05 parts by weight of light injection to 100 parts by weight of the composition consisting of elvan, biotite and loess, and the light injection is remarkably improved by the light injection added as red soil used when making an amulet. do. As sterilizing power is improved, the deodorizing effect is further improved. Appropriate amount is 0.0005-0.05 parts by weight based on 100 parts by weight of the composition consisting of elvan, biotite, ocher, if less than this range, the bactericidal effect is insufficient, and if this range is exceeded, the bactericidal effect no longer increases.

훈련한 후 성형된 성형체를 숙성시키는 이유는 맥반석 및 견운모 특유의 결정을 충분히 형성시키기 위함이다. 결정이 충분히 형성된 소성체는 선도유지효과 및 탈취효과가 향상된다.The reason for aging the molded body after training is to sufficiently form crystals peculiar to elvan and biotite. The calcined body in which crystals are sufficiently formed improves freshness retaining effect and deodorizing effect.

숙성 후 이어지는 소성공정에 의하여 성형체는 충분한 강도 및 내구성을 얻을 수 있으며, 숙성과정에 의하여 형성된 결정이 그대로 유지된다. 적절한 소성온도는 700-1200℃이며, 더욱 바람직하게로는 750-1050℃이다.After the aging process, the molded body can obtain sufficient strength and durability, and the crystal formed by the aging process is maintained as it is. Suitable firing temperatures are 700-1200 ° C., more preferably 750-1050 ° C.

소성 후에 자력을 조사하는 이유는 소성과정에서 상실된 구성원소에 자기력을 부여하기 위함이며, 자기력이 부여된 소성체는 선도유지효과가, 탈취효과 및 정수효과가 더욱 향상될 뿐만 아니라, 인체에 유해한 중금속을 포집하는 데에 있어서 탁월한 효과를 발휘한다.The reason for investigating the magnetic force after firing is to give the magnetic force to the element lost in the firing process, and the plastic body with the magnetic force not only has the leading maintenance effect, the deodorizing effect and the water purification effect, but also the heavy metal which is harmful to the human body. It has an excellent effect on collecting.

본 발명의 실시예는 다음과 같다.Embodiments of the present invention are as follows.

이하의 실시예에서 사용된 맥반석의 조성은 아래와 같다.The composition of elvan rock used in the following examples is as follows.

견운모의 조성은 아래와 같다.The composition of the biotite is as follows.

[제조실시예]Production Example

맥반석과 견운모, 황토의 사용비율을 25중량% : 30중량% : 45중량%로 구성된 조성물 100중량부에 대하여 0.005중량부의 경명주사를 넣고 잘 분쇄한 다음, 300-500매쉬의 망체에 통과시켜 분말을 얻었다. 얻어진 분말을 물과 함께 교반기에 넣고 충분히 교반한 다음 0.3 × 10 × 10(㎝)의 형틀에 넣고 가압하여 성형체를 얻고 이 성형체를 200℃에서 72시간 동안 건조, 숙성시킨 후 850℃의 온도에서 4시간 동안 소성시켜 소성체를 얻었다.The use rate of elvan, biotite and loess is 25% by weight: 30% by weight: 45% by weight of 100% by weight of the composition, which is added 0.005 parts by weight of light injection, pulverized well, and passed through a mesh of 300-500 mesh. Got. The obtained powder was put into a stirrer with water, stirred sufficiently, put into a mold of 0.3 × 10 × 10 (cm), and pressed to obtain a molded product. The molded product was dried and aged at 200 ° C. for 72 hours, and then aged at 4 ° C. at 850 ° C. It baked for time and obtained the fired body.

얻어진 소성체에 1200 가우스의 자장을 걸어서 디스크 형의 최종 소성물을 얻었다.A 1200 Gauss magnetic field was applied to the resulting fired body to obtain a disc-shaped final fired product.

[실시예 1 ]Example 1

*선도유지테스트 1* Lead maintenance test 1

비닐봉지 2개에 각각 상추를 넣고 1개에는 제조실시예에서 얻어진 디스크형의 소성물을 얻은 후 5일동안 실온(15-22℃)에 방치한 후 관찰한 결과, 소성물을 넣지 아니한 봉지에서는 심한 악취가 남과 동시에 상추가 시커먼 물로 변하였으나, 소성물을 넣은 봉투에서는 약간의 냄새가 났으나 상추는 그대로 유지되었다.Lettuce was put in two plastic bags, and one was obtained in a disc-shaped burned product obtained in the manufacturing example, and left at room temperature (15-22 ° C.) for 5 days. At the same time, the odor turned to black and white water, but the plastic bag had a slight smell, but the lettuce remained intact.

[실시예 2]Example 2

*선도유지테스트 2* Lead Maintenance Test 2

약간의 흡집을 낸 같은 크기의 토마토 2개를 45 × 41 × 37(㎝)의 종이박스에 각각 넣고 한쪽에는 제조실시예에 의하여 얻어진 소성물을 넣은 다음, 실온(15-22℃)에서 11일간 방치한 결과는 제 1도와 같았다.Put two equally sized tomatoes, each of which was slightly collected, in a paper box of 45 × 41 × 37 (cm), and put the burned material obtained by the manufacturing example on one side, and then at room temperature (15-22 ° C.) for 11 days. The neglect result was the same as that of FIG.

제 1도의 좌측의 것은 소성물을 넣지 아니한 것이고, 우측의 것은 소성물을 넣은 것이다. 좌측의 것은 우측의 것에 비하여 크기가 상당히 줄었으며, 악취도 심하였으나, 우측의 것은 처음 넣었을 때의 크기가 거의 그대로 유지될 뿐만 아니라 악취도 나지 아니하였다.The left side of FIG. 1 does not contain a fired substance, and the right side contains a fired substance. The one on the left was significantly smaller in size than the one on the right, and the odor was severe. On the right, the size of the first one was almost kept intact and no odor.

[실시예 3]Example 3

*탈취효과테스트* Deodorization test

시판되고 있는 냉장고에 제조실시예에 의하여 얻어진 소성체를 각각 2개씩 넣고 2개월간에 걸쳐 냄새발생 유무를 관찰한 결과는 아래의 표 1과 같다.Two fired bodies obtained according to the production examples were put into commercially available refrigerators, and the results of odor generation were observed over two months, as shown in Table 1 below.

[비교예][Comparative Example]

제조실시예에서 경명주사를 넣지 아니한 것을 제외하고는 제조실시예와 동일하게 소성체를 제조하였으며, 이 소성체를 넣고 실시예 1과 동일하게 시행한 결과는 비닐봉지 내의 상추가 시커먼 물로 변하지 아니하였으나 악취가 비교적 많이 났다.Except that the light injection in the manufacturing example was prepared except that the fired body was prepared in the same manner as in the manufacturing example, and the result of the same procedure as in Example 1 with the fired body did not change the lettuce in the plastic bag water. I smelled a lot.

[실시예 4]Example 4

*정수효과 테스트* Integer test

수도물을 원수로 하고 이 원수 21에 제조실시에에서 얻어진 소성체를 담그고 24시간 방치한 후 이 물과 원수를 분석한 결과은 아래의 표 2 및 표 3과 같다.Using tap water as raw water and soaking the calcined body obtained in the manufacturing process in raw water 21 and leaving it for 24 hours, the result of analyzing the water and raw water is shown in Tables 2 and 3 below.

[표 2] 원수의 수지러분석표[Table 2] Resin Table of Raw Water

[표 3] 정수된 물의 수질분석표[Table 3] Water quality analysis table of purified water

이상의 실시예에 의하여 확인되는 바와 같이 본 발명에 의한 세라믹체는 탈취효과 및 선도유지효과가 우수할 뿐만 아니라, 특히 정수효과가 매우 우수하며 그 효과가 장기간 지속되는 장점이 있다.As confirmed by the above embodiment, the ceramic body according to the present invention not only has an excellent deodorizing effect and freshness maintaining effect, but also has a very good water purification effect and its effect lasts for a long time.

Claims (1)

맥반석 20-30중량%, 견운모 25-35중량%, 황토 40-50중량%로 구성된 조성물 100중량부에 경명주사를 0.0005-0.05중량부를 가하고 이를 물에 넣고 잘 혼련한 후 150-200℃의 온도에서 48-72시간 동안 숙성시킨 다음, 700-1200℃의 온도에서 3-8시간 동안 소성시키고, 얻어진 소성체에 1000-1250가우스의 자력을 조사하는 것을 특징으로 하는 선도유지용 세ㅐ라믹조성물의 제조방법.0.0005-0.05 parts by weight of light injection is added to 100 parts by weight of a composition consisting of 20-30% by weight of elvanite, 25-35% by weight of mica, and 40-50% by weight of ocher. Aged for 48-72 hours at, then calcined for 3-8 hours at a temperature of 700-1200 ℃, the resulting fired body is characterized in that the ceramic composition for freshness maintenance characterized in that the magnetic force of 1000-1250 gauss Manufacturing method.
KR1019960038006A 1996-09-03 1996-09-03 Process for the preparation of ceramic KR0163360B1 (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
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KR20020042043A (en) * 2000-11-29 2002-06-05 조봉희 Producing for Preparing Material Radiating Far Infrared
KR20020076058A (en) * 2001-03-27 2002-10-09 정재일 manufacture method of artificial mineral which contains emission matter
KR100455068B1 (en) * 2002-10-30 2004-11-06 주식회사 썬파이 Magnetized and sintered ceramics useful for treating or preventing diseases caused by the consumption of high-cholesterol foods

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KR100345208B1 (en) * 2000-03-08 2002-07-25 박영신 Matting Having Anti-fungal Activity, Anti-pest Activity and Slip-prevention Activity and the Method of Producing Thereof
KR100455067B1 (en) * 2002-10-30 2004-11-06 주식회사 썬파이 A dipping water composition of magnetized and sintered ceramics useful for protecting organs from damages caused by radiation
KR102197033B1 (en) * 2020-02-21 2020-12-30 성창윤 Fried Food of Sea Creature and Manufacturing Method of thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20020042043A (en) * 2000-11-29 2002-06-05 조봉희 Producing for Preparing Material Radiating Far Infrared
KR20020076058A (en) * 2001-03-27 2002-10-09 정재일 manufacture method of artificial mineral which contains emission matter
KR100455068B1 (en) * 2002-10-30 2004-11-06 주식회사 썬파이 Magnetized and sintered ceramics useful for treating or preventing diseases caused by the consumption of high-cholesterol foods

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