KR102663928B1 - Cosmetic creams for wash-off tone-up and manufacturing method thereof - Google Patents

Cosmetic creams for wash-off tone-up and manufacturing method thereof Download PDF

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KR102663928B1
KR102663928B1 KR1020210133378A KR20210133378A KR102663928B1 KR 102663928 B1 KR102663928 B1 KR 102663928B1 KR 1020210133378 A KR1020210133378 A KR 1020210133378A KR 20210133378 A KR20210133378 A KR 20210133378A KR 102663928 B1 KR102663928 B1 KR 102663928B1
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parts
weight
tone
purified water
filtrate
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송영석
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라온커머스 주식회사
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4993Derivatives containing from 2 to 10 oxyalkylene groups
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/58Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
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    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8158Homopolymers or copolymers of amides or imides, e.g. (meth) acrylamide; Compositions of derivatives of such polymers
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    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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    • AHUMAN NECESSITIES
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    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract

본 발명은 워시오프 톤업 화장용 크림에 관한 것으로, 정제수 100 중량부, 부틸렌글라이콜 2 ~ 9 중량부, 나이아신아마이드 1 ~ 4 중량부, 세테아릴올리베이트 0.5 ~ 1.1 중량부, 다이소듐 EDTA 0.01 ~ 0.03 중량부, 글리세린 4.5 ~ 6.3 중량부, 티타늄디옥사이드 0.5 ~ 3.5 중량부, 사이클로펜타실록세인 1.7 ~ 4.3 중량부, 다이메티콘 2.1 ~ 2.5 중량부, 시어버터 1.3 ~ 2.0 중량부, PEG-100 스테아레이트 0.1 ~ 1.1 중량부, 올리브오일 0.4 ~ 0.8 중량부, 폴리솔베이트80 0.1 ~ 0.5 중량부, 알루미늄하이드록사이드 1.0 ~ 2.3 중량부, 폴리아크릴아마이드 1.4 ~ 3.0 중량부 및 다이메티콘올 0.3 ~ 1.2 중량부를 함유함으로써, 톤업 효과가 양호한 워시오프 톤업 화장용 크림을 대량 제조할 수 있는 효과가 있다.The present invention relates to a wash-off tone-up cosmetic cream, comprising 100 parts by weight of purified water, 2 to 9 parts by weight of butylene glycol, 1 to 4 parts by weight of niacinamide, 0.5 to 1.1 parts by weight of cetearyl olivate, and disodium EDTA. 0.01 to 0.03 parts by weight, glycerin 4.5 to 6.3 parts by weight, titanium dioxide 0.5 to 3.5 parts by weight, cyclopentasiloxane 1.7 to 4.3 parts by weight, dimethicone 2.1 to 2.5 parts by weight, shea butter 1.3 to 2.0 parts by weight, PEG- 100 0.1 to 1.1 parts by weight of stearate, 0.4 to 0.8 parts by weight of olive oil, 0.1 to 0.5 parts by weight of polysorbate 80, 1.0 to 2.3 parts by weight of aluminum hydroxide, 1.4 to 3.0 parts by weight of polyacrylamide, and dimethiconol. By containing 0.3 to 1.2 parts by weight, it is possible to mass-produce a wash-off tone-up cosmetic cream with a good tone-up effect.

Description

워시오프 톤업 화장용 크림 및 이의 제조방법 {Cosmetic creams for wash-off tone-up and manufacturing method thereof}Wash-off tone-up cosmetic cream and manufacturing method thereof {Cosmetic creams for wash-off tone-up and manufacturing method thereof}

본 발명은 워시오프 톤업 화장용 크림 및 이의 제조방법에 관한 것이다.The present invention relates to a wash-off tone-up cosmetic cream and a method for manufacturing the same.

대한민국 등록특허 제1802144호(등록일자: 2017.11.22., 발명의 명칭: 클레이 버블 워스 오프 클렌징 팩 화장료 조성물)는 트레할로스, 글리세린 및 메칠프로판디올로 구성되는 피부보습제와 정제수를 75℃에서 균질하게 교반하는 제1공정; 포타슘코코일글리시네이트, 코카미도프로필베타인 및 소듐코코일애플아미노산으로 이루어진 세정 성분을 상기 제1공정의 혼합물에 투입하고, 75℃에서 호모믹서로 균질하게 교반하는 제2공정; 카올린과 벤토나이트로 이루어진 클레이 성분을 상기 제2공정의 혼합물에 투입하고 75℃에서 호모믹서로 균질하게 교반하는 제3공정; 상기 제3공정까지 교반 혼합된 혼합물을 실온까지 냉각 후, 디실록산인 기포발생기제를 첨가한 후 실온에서 호모믹서로 균질혼합하는 제4공정을 포함하여 클레이 버블 워시 오프 클렌징 팩 화장료 조성물을 제조하며, 상기 클레이 버블 워시 오프 클렌징 팩 화장료 조성물은 상기 클레이 성분이 10~25중량% 첨가되어 피부 피지조절기능이 있는 것을 특징으로 하는 클레이 버블 워시 오프 클렌징 팩 화장료 조성물의 제조방법이 개시되어 있다. 이러한 종래 기술은, 간단한 사용에 의해 피부 피지조절 기능을 가지며, 자연적으로 발생하는 기포에 의해, 사용상의 재미와 세정 시간을 단축시킬 수 있는 효과가 있다고 주장하는 반면, 조성이 복잡하여 대량생산이 용이치 못한 단점이 있었다.Republic of Korea Patent No. 1802144 (registration date: 2017.11.22., title of invention: Clay Bubble Wash Off Cleansing Pack Cosmetic Composition) is a skin moisturizer composed of trehalose, glycerin, and methylpropanediol and purified water are homogeneously stirred at 75°C. The first process of doing; A second step of adding a cleaning ingredient consisting of potassium cocoyl glycinate, cocamidopropyl betaine, and sodium cocoyl apple amino acid to the mixture of the first step and stirring it homogeneously at 75°C with a homomixer; A third step of adding the clay component consisting of kaolin and bentonite to the mixture of the second step and stirring it homogeneously at 75°C with a homomixer; A clay bubble wash off cleansing pack cosmetic composition is manufactured, including the fourth step of cooling the mixture stirred and mixed up to the third step to room temperature, adding a foam generator, which is disiloxane, and homogeneously mixing it at room temperature with a homomixer. A method of manufacturing a clay bubble wash off cleansing pack cosmetic composition is disclosed, wherein the clay bubble wash off cleansing pack cosmetic composition has a skin sebum control function by adding 10 to 25% by weight of the clay component. While this prior art claims to have the function of controlling skin sebum through simple use and to have the effect of making it fun to use and shortening the cleaning time due to naturally occurring bubbles, the composition is complex, making mass production difficult. There was an unreasonable drawback.

상기와 같은 문제점을 해결하고자 창출된 본 발명의 목적은, 저자극 조성으로 피부트러블을 최소화할 수 있음은 물론, 톤업 효과가 양호한 워시오프 톤업 화장용 크림 및 이의 제조방법을 제공하는 데 있다.The purpose of the present invention, which was created to solve the above problems, is to provide a wash-off tone-up cosmetic cream that can minimize skin troubles with a hypoallergenic composition and has a good tone-up effect, and a method of manufacturing the same.

이러한 본 발명의 목적은, 정제수 100 중량부에 대하여, 부틸렌글라이콜 2 ~ 9 중량부, 나이아신아마이드 1 ~ 4 중량부, 세테아릴올리베이트 0.5 ~ 1.1 중량부, 다이소듐 EDTA 0.01 ~ 0.03 중량부, 글리세린 4.5 ~ 6.3 중량부, 티타늄디옥사이드 0.5 ~ 3.5 중량부, 사이클로펜타실록세인 1.7 ~ 4.3 중량부, 다이메티콘 2.1 ~ 2.5 중량부, 시어버터 1.3 ~ 2.0 중량부, PEG-100 스테아레이트 0.1 ~ 1.1 중량부, 올리브오일 0.4 ~ 0.8 중량부, 폴리솔베이트80 0.1 ~ 0.5 중량부, 알루미늄하이드록사이드 1.0 ~ 2.3 중량부, 폴리아크릴아마이드 1.4 ~ 3.0 중량부 및 다이메티콘올 0.3 ~ 1.2 중량부를 포함하는 워시오프 톤업 화장용 크림에 의해 달성될 수 있다.The purpose of the present invention is to use 2 to 9 parts by weight of butylene glycol, 1 to 4 parts by weight of niacinamide, 0.5 to 1.1 parts by weight of cetearyl olivate, and 0.01 to 0.03 parts by weight of disodium EDTA, based on 100 parts by weight of purified water. parts, 4.5 to 6.3 parts by weight of glycerin, 0.5 to 3.5 parts by weight of titanium dioxide, 1.7 to 4.3 parts by weight of cyclopentasiloxane, 2.1 to 2.5 parts by weight of dimethicone, 1.3 to 2.0 parts by weight of shea butter, 0.1 parts by weight of PEG-100 stearate. ~ 1.1 parts by weight, olive oil 0.4 ~ 0.8 parts by weight, polysorbate 80 0.1 ~ 0.5 parts by weight, aluminum hydroxide 1.0 ~ 2.3 parts by weight, polyacrylamide 1.4 ~ 3.0 parts by weight, and dimethiconol 0.3 ~ 1.2 parts by weight. This can be achieved by a wash-off tone-up cosmetic cream containing booze.

바람직하게는, 본 발명은 상기 정제수 100 중량부에 대하여, 솔비탄올리베이트 0.3 ~ 0.5 중량부, 사이클로헥사실록세인 1.2 ~ 2.3 중량부, 코코넛야자오일 및 코코-카프릴레이트/카프레이트 0.2 ~ 0.8 중량부, 트라이에톡시카프릴실레인 0.2 ~ 2.3 중량부, C13-14아이소파라핀 0.2 ~ 2.2 중량부 및 라우레스-7 0.2 ~ 0.4 중량부를 더 포함하는 것을 특징으로 한다.Preferably, the present invention contains 0.3 to 0.5 parts by weight of sorbitan olivate, 1.2 to 2.3 parts by weight of cyclohexasiloxane, and 0.2 to 0.8 parts by weight of coconut palm oil and coco-caprylate/caprate, based on 100 parts by weight of purified water. parts, 0.2 to 2.3 parts by weight of triethoxycaprylsilane, 0.2 to 2.2 parts by weight of C13-14 isoparaffin, and 0.2 to 0.4 parts by weight of laureth-7.

바람직하게는, 본 발명은 상기 정제수 100 중량부에 대하여, 톤업 보강제 2 ~ 7 중량부를 더 포함하되, 상기 톤업 보강제는 ① 도라지 100 중량부에 대하여, 가시오가피 30 ~ 70 중량부, 레몬밤 분말 3 ~ 5 중량부 및 설탕 100 ~ 130 중량부를 밀폐충전한 후 34 ~ 37℃에서 30 ~ 35일간 발효하여 제 1 발효물을 제조하는 단계와; ② 상기 제 1 발효물 100 중량부에 대하여, 물 300 ~ 350 중량부 및 천일염 50 ~ 55 중량부를 혼합한 후 10 ~ 15시간 교반한 다음 여과하여 제 1 여과물을 제조하는 단계와; ③ 상기 제 1 여과물 100 중량부에 대하여, 풋사과 12 ~ 15 중량부, 청매실 5 ~ 8 중량부 및 설탕 30 ~ 50 중량부를 밀폐충전후 30 ~ 32℃에서 6 ~ 7개월간 발효하여 제 2 발효물을 제조하는 단계와; ④ 상기 제 2 발효물 100 중량부에 대하여, 에탄올 150 ~ 450 중량부를 혼합한 후 40 ~ 45℃에서 24 ~ 30시간 정치한 다음, 여과하여 제 2 여과물을 제조하는 단계와; ⑤ 상기 제 2 여과물 100 중량부에 대하여, 구연산 0.5 ~ 1.2 중량부 및 비타민 C 3 ~ 4 중량부를 혼합하여 제조되는 것을 특징으로 한다.Preferably, the present invention further includes 2 to 7 parts by weight of a tone-up enhancer based on 100 parts by weight of the purified water, wherein the tone-up enhancer is ① 30 to 70 parts by weight of Acanthopanax per 100 parts by weight of bellflower root, and 3 to 3 parts by weight of lemon balm powder. Preparing a first fermented product by tightly filling 5 parts by weight and 100 to 130 parts by weight of sugar and then fermenting at 34 to 37°C for 30 to 35 days; ② mixing 300 to 350 parts by weight of water and 50 to 55 parts by weight of sea salt with 100 parts by weight of the first fermented product, stirring for 10 to 15 hours, and then filtering to prepare a first filtrate; ③ For 100 parts by weight of the first filtrate, 12 to 15 parts by weight of green apples, 5 to 8 parts by weight of green plums, and 30 to 50 parts by weight of sugar are sealed and fermented at 30 to 32°C for 6 to 7 months to produce a second fermented product. manufacturing steps; ④ mixing 150 to 450 parts by weight of ethanol with 100 parts by weight of the second fermentation product, leaving it to stand at 40 to 45°C for 24 to 30 hours, and then filtering to prepare a second filtrate; ⑤ It is characterized in that it is prepared by mixing 0.5 to 1.2 parts by weight of citric acid and 3 to 4 parts by weight of vitamin C with respect to 100 parts by weight of the second filtrate.

바람직하게는, 본 발명은 상기 정제수 100 중량부에 대하여, 보습 강화제 2 ~ 5 중량부 및 비타민 C 0.5 ~ 1.5 중량부를 더 포함하되, 상기 보습 강화제는 코코넛 과육 100 중량부에 대하여, 아보카도오일 5 ~ 7 중량부 및 꽃착즙액 10 ~ 15 중량부를 함유하되, 상기 꽃착즙액은 백장미 100 중량부에 대하여, 수선화 50 ~ 75 중량부 및 흰색국화 10 ~ 25 중량부를 혼합 압착하여 제조되는 것을 특징으로 한다.Preferably, the present invention further includes 2 to 5 parts by weight of a moisture enhancer and 0.5 to 1.5 parts by weight of vitamin C based on 100 parts by weight of the purified water, wherein the moisture enhancer is 5 to 5 parts by weight of avocado oil based on 100 parts by weight of coconut meat. It contains 7 parts by weight and 10 to 15 parts by weight of flower juice, wherein the flower juice is manufactured by mixing and pressing 50 to 75 parts by weight of daffodils and 10 to 25 parts by weight of white chrysanthemum for 100 parts by weight of white roses. .

또한, 본 발명의 다른 목적은, (a) 정제수 100 중량부, 부틸렌글라이콜 2 ~ 9 중량부, 나이아신아마이드 1 ~ 4 중량부, 세테아릴올리베이트 및 솔비탄올리베이트 0.5 ~ 2.7 중량부, 다이소듐 EDTA 0.01 ~ 0.03 중량부를 혼합하여 70 ~ 83℃로 가온한 후 10 ~ 20분간 교반하여 완전 용해한 다음 메인 믹서로 여과하여 이송하는 단계와; (b) 정제수 100 중량부에 대하여, 글리세린 4.5 ~ 6.3 중량부 및 티타늄디옥사이드 0.5 ~ 1.0 중량부를 별도의 용기에서 70 ~ 83℃ 온도로 15 ~ 30분간 교반하여 완전분산시킨 다음 메인 믹서에 투입하는 단계와; (c) 정제수 100 중량부에 대하여, 사이클로펜타실록세인 및 사이클로헥사실록세인 1.7 ~ 4.3 중량부, 다이메티콘 2.1 ~ 2.5 중량부, 시어버터 1.3 ~ 2.0 중량부, PEG-100 스테아레이트 및 글리세릴스테아레이트 0.1 ~ 1.1 중량부, 올리브오일 0.4 ~ 0.8 중량부, 코코넛야자오일 및 코코-카프릴레이트/카프레이트 0.2 ~ 0.8 중량부와, 폴리솔베이트80 0.1 ~ 0.5 중량부를 별도의 용기에서 70 ~ 83℃ 온도로 3 ~ 10분간 교반하여 완전 용해한 상기 메인 믹서로 여과 이송하여 유화한 후 58 ~ 62℃까지 냉각하는 단계와; (d) 정제수 100 중량부에 대하여, 티타늄디옥사이드 1.5 ~ 2.5 중량부, 트라이에톡시카프릴실레인 0.2 ~ 2.3 중량부, 알루미늄하이드록사이드 1.0 ~ 2.3 중량부, 폴리아크릴아마이드 1.4 ~ 3.0 중량부, C13-14아이소파라핀 0.2 ~ 2.2 중량부, 라우레스-7 0.2 ~ 0.4 중량부, 사이클로펜타실록세인 0.2 ~ 0.5 중량부 및 다이메티콘올 0.3 ~ 1.2 중량부를 별도의 용기에서 55 ~ 63℃ 온도로 20 ~ 25분간 교반하여 완전 분산시킨 다음 상기 메인 믹서로 투입한 후 교반 균일화하여 43 ~ 46℃까지 냉각하여 톤업 화장용 크림을 제조하는 단계와; (e) 상기 톤업 화장용 크림 100 중량부에 대하여, 방부재, 향료, 색소 0.1 ~ 2.3 중량부 및 톤업 보강제 2 ~ 7 중량부, 보습 강화제 2 ~ 5 중량부 및 비타민 C 0.5 ~ 1.5 중량부를 더 포함첨가한 후 40 ~ 47℃에서 10 ~ 15분간 교반한 후 30℃까지 냉각한 진공 탈포하는 단계로 이루어지되, 상기 톤업 보강제는 ① 도라지 100 중량부에 대하여, 가시오가피 30 ~ 70 중량부, 레몬밤 분말 3 ~ 5 중량부 및 설탕 100 ~ 130 중량부를 밀폐충전한 후 34 ~ 37℃에서 30 ~ 35일간 발효하여 제 1 발효물을 제조하는 단계와; ② 상기 제 1 발효물 100 중량부에 대하여, 물 300 ~ 350 중량부 및 천일염 50 ~ 55 중량부를 혼합한 후 10 ~ 15시간 교반한 다음 여과하여 제 1 여과물을 제조하는 단계와; ③ 상기 제 1 여과물 100 중량부에 대하여, 풋사과 12 ~ 15 중량부, 청매실 5 ~ 8 중량부 및 설탕 30 ~ 50 중량부를 밀폐충전후 30 ~ 32℃에서 6 ~ 7개월간 발효하여 제 2 발효물을 제조하는 단계와; ④ 상기 제 2 발효물 100 중량부에 대하여, 에탄올 150 ~ 450 중량부를 혼합한 후 40 ~ 45℃에서 24 ~ 30시간 정치한 다음, 여과하여 제 2 여과물을 제조하는 단계와; ⑤ 상기 제 2 여과물 100 중량부에 대하여, 구연산 0.5 ~ 1.2 중량부 및 비타민 C 3 ~ 4 중량부를 혼합하여 제조되고, 상기 보습 강화제는 코코넛 과육 100 중량부에 대하여, 아보카도오일 5 ~ 7 중량부 및 꽃착즙액 10 ~ 15 중량부를 함유하되, 상기 꽃착즙액은 백장미 100 중량부에 대하여, 수선화 50 ~ 75 중량부 및 흰색국화 10 ~ 25 중량부를 혼합 압착하여 제조되는 것을 특징으로 하는 워시오프 톤업 화장용 크림의 제조방법에 의해 달성될 수 있다.In addition, another object of the present invention is (a) 100 parts by weight of purified water, 2 to 9 parts by weight of butylene glycol, 1 to 4 parts by weight of niacinamide, 0.5 to 2.7 parts by weight of cetearyl olivate and sorbitan olivate, Mixing 0.01 to 0.03 parts by weight of disodium EDTA, heating to 70 to 83°C, stirring for 10 to 20 minutes to completely dissolve, and then filtering and transferring to the main mixer; (b) For 100 parts by weight of purified water, 4.5 to 6.3 parts by weight of glycerin and 0.5 to 1.0 parts by weight of titanium dioxide are stirred in a separate container at a temperature of 70 to 83°C for 15 to 30 minutes to completely disperse and then added to the main mixer. and; (c) Based on 100 parts by weight of purified water, 1.7 to 4.3 parts by weight of cyclopentasiloxane and cyclohexasiloxane, 2.1 to 2.5 parts by weight of dimethicone, 1.3 to 2.0 parts by weight of shea butter, PEG-100 stearate and glyceryl. 0.1 to 1.1 parts by weight of stearate, 0.4 to 0.8 parts by weight of olive oil, 0.2 to 0.8 parts by weight of coconut palm oil and coco-caprylate/caprate, and 0.1 to 0.5 parts by weight of polysorbate 80 in a separate container at 70 ~ 0.8 parts by weight. Stirring at a temperature of 83°C for 3 to 10 minutes to completely dissolve, filter and transfer to the main mixer for emulsification and then cooling to 58 to 62°C; (d) Based on 100 parts by weight of purified water, 1.5 to 2.5 parts by weight of titanium dioxide, 0.2 to 2.3 parts by weight of triethoxycaprylsilane, 1.0 to 2.3 parts by weight of aluminum hydroxide, 1.4 to 3.0 parts by weight of polyacrylamide, 0.2 to 2.2 parts by weight of C13-14 isoparaffin, 0.2 to 0.4 parts by weight of laureth-7, 0.2 to 0.5 parts by weight of cyclopentasiloxane, and 0.3 to 1.2 parts by weight of dimethiconol are placed in a separate container at a temperature of 55 to 63°C. completely dispersing by stirring for 20 to 25 minutes, then adding it to the main mixer, stirring to homogenize, and cooling to 43 to 46°C to prepare a tone-up cosmetic cream; (e) Based on 100 parts by weight of the tone-up cosmetic cream, it further contains 0.1 to 2.3 parts by weight of preservatives, fragrances, and pigments, 2 to 7 parts by weight of tone-up enhancers, 2 to 5 parts by weight of moisturizing enhancers, and 0.5 to 1.5 parts by weight of vitamin C. After addition, it is stirred at 40 to 47℃ for 10 to 15 minutes and then cooled to 30℃ and vacuum defoamed. The tone-up enhancer is ① per 100 parts by weight of bellflower root, 30 to 70 parts by weight of Acanthopanax, and lemon balm powder. Preparing a first fermented product by tightly filling 3 to 5 parts by weight and 100 to 130 parts by weight of sugar and then fermenting at 34 to 37°C for 30 to 35 days; ② Mixing 300 to 350 parts by weight of water and 50 to 55 parts by weight of sea salt with 100 parts by weight of the first fermented product, stirring for 10 to 15 hours, and then filtering to prepare a first filtrate; ③ For 100 parts by weight of the first filtrate, 12 to 15 parts by weight of green apples, 5 to 8 parts by weight of green plums, and 30 to 50 parts by weight of sugar are sealed and fermented at 30 to 32°C for 6 to 7 months to produce a second fermented product. manufacturing steps; ④ mixing 150 to 450 parts by weight of ethanol with 100 parts by weight of the second fermentation product, leaving it to stand at 40 to 45°C for 24 to 30 hours, and then filtering to prepare a second filtrate; ⑤ It is prepared by mixing 0.5 to 1.2 parts by weight of citric acid and 3 to 4 parts by weight of vitamin C with respect to 100 parts by weight of the second filtrate, and the moisturizing enhancer is 5 to 7 parts by weight of avocado oil with respect to 100 parts by weight of coconut meat. and 10 to 15 parts by weight of flower juice, wherein the flower juice is manufactured by mixing and pressing 50 to 75 parts by weight of daffodils and 10 to 25 parts by weight of white chrysanthemum with respect to 100 parts by weight of white roses. This can be achieved by a method for manufacturing cosmetic cream.

이상과 같은 본 발명은 톤업 효과가 양호한 워시오프 톤업 화장용 크림을 대량 제조할 수 있는 효과가 있다.The present invention as described above is effective in mass producing a wash-off tone-up cosmetic cream with a good tone-up effect.

이하, 본 발명의 실시예를 참조하여 설명하기로 한다.Hereinafter, the present invention will be described with reference to embodiments.

1. 워시오프 톤업 화장용 크림1. Wash-off tone-up cosmetic cream

본 발명에 의한 워시오프 톤업 화장용 크림은 정제수 100 중량부에 대하여, 부틸렌글라이콜(Butylene Glycol) 2 ~ 9 중량부, 나이아신아마이드(Niacinamide) 1 ~ 4 중량부, 세테아릴올리베이트(Cetearyl Olivate) 0.5 ~ 1.1 중량부, 다이소듐 EDTA(Disodium Ethylenediaminetetraaceticacid) 0.01 ~ 0.03 중량부, 글리세린(Glycerin) 4.5 ~ 6.3 중량부, 티타늄디옥사이드(Titanium Dioxide) 0.5 ~ 3.5 중량부, 사이클로펜타실록세인(Cyclopentasiloxane) 1.7 ~ 4.3 중량부, 다이메티콘(Dimethicone) 2.1 ~ 2.5 중량부, 시어버터(Shea Butter) 1.3 ~ 2.0 중량부, PEG-100 스테아레이트(Polyethylene Glycol-100 Stearate) 0.1 ~ 1.1 중량부, 올리브오일(Olive Oil) 0.4 ~ 0.8 중량부, 폴리솔베이트80(Polysorbate80) 0.1 ~ 0.5 중량부, 알루미늄하이드록사이드(Aluminum Hydroxide) 1.0 ~ 2.3 중량부, 폴리아크릴아마이드(Polyacrylamide) 1.4 ~ 3.0 중량부, 다이메티콘올(Dimethiconol) 0.3 ~ 1.2 중량부를 포함하여 조성되어 있다. 여기서, 부틸렌글라이콜, 나이아신아마이드, 세테아릴올리베이트, 솔비탄올리베이트 및 다이소듐 EDTA는 수상(水狀)이다. 사이클로펜타실록세인, 사이클로헥사실록세인, 다이메티콘, 시어버터, PEG-100 스테아레이트, 글리세릴스테아레이트, 올리브오일, 코코넛야자오일, 코코-카프릴레이트/카프레이트 및 폴리솔베이트80은 유상(油狀)이다.The wash-off tone-up cosmetic cream according to the present invention contains 2 to 9 parts by weight of Butylene Glycol, 1 to 4 parts by weight of Niacinamide, and Cetearyl olivate, based on 100 parts by weight of purified water. Olivate) 0.5 to 1.1 parts by weight, Disodium EDTA (Disodium Ethylenediaminetetraaceticacid) 0.01 to 0.03 parts by weight, Glycerin 4.5 to 6.3 parts by weight, Titanium Dioxide 0.5 to 3.5 parts by weight, Cyclopentasiloxane 1.7 to 4.3 parts by weight, Dimethicone 2.1 to 2.5 parts by weight, Shea Butter 1.3 to 2.0 parts by weight, PEG-100 Stearate (Polyethylene Glycol-100 Stearate) 0.1 to 1.1 parts by weight, olive oil (Olive Oil) 0.4 to 0.8 parts by weight, Polysorbate80 0.1 to 0.5 parts by weight, Aluminum Hydroxide 1.0 to 2.3 parts by weight, Polyacrylamide 1.4 to 3.0 parts by weight, die It is composed of 0.3 to 1.2 parts by weight of methiconol (Dimethiconol). Here, butylene glycol, niacinamide, cetearyl olivate, sorbitan olivate, and disodium EDTA are aqueous phase. Cyclopentasiloxane, cyclohexasiloxane, dimethicone, shea butter, PEG-100 stearate, glyceryl stearate, olive oil, coconut palm oil, coco-caprylate/caprate and polysorbate 80 are oily. It is (oil).

또한, 본 실시예에 의한 워시오프 톤업 화장용 크림은 정제수 100 중량부에 대하여, 솔비탄올리베이트(Sorbitan Olivate) 0.3 ~ 0.5 중량부, 사이클로헥사실록세인(Cyclohexasiloxane) 1.2 ~ 2.3 중량부, 코코넛야자오일(Cocos Nucifera Coconut Oil) 및 코코-카프릴레이트/카프레이트 0.2 ~ 0.8 중량부, 트라이에톡시카프릴실레인(Coco-Caprylate/Caprate) 0.2 ~ 2.3 중량부, C13-14아이소파라핀(C13-14 Isoparaffin) 0.2 ~ 2.2 중량부 및 라우레스-7(Laureth-7) 0.2 ~ 0.4 중량부를 더 포함한다. 여기서, 솔비탄올리베이트는 수상이고, 사이클로헥사실록세인, 코코넛야자오일, 코코-카프릴레이트/카프레이트는 유상이다.In addition, the wash-off tone-up cosmetic cream according to this example contains 0.3 to 0.5 parts by weight of Sorbitan Olivate, 1.2 to 2.3 parts by weight of Cyclohexasiloxane, and coconut palm oil, based on 100 parts by weight of purified water. (Cocos Nucifera Coconut Oil) and Coco-Caprylate/Caprate 0.2 to 0.8 parts by weight, Triethoxycaprylsilane (Coco-Caprylate/Caprate) 0.2 to 2.3 parts by weight, C13-14 isoparaffin (C13-14) It further includes 0.2 to 2.2 parts by weight of Isoparaffin and 0.2 to 0.4 parts by weight of Laureth-7. Here, sorbitan olivate is the water phase, and cyclohexasiloxane, coconut palm oil, and coco-caprylate/caprate are the oil phase.

본 발명에 의한 워시오프 톤업 화장용 크림은 정제수 100 중량부에 대하여, 톤업 보강제 2 ~ 7 중량부, 보습 강화제 2 ~ 5 중량부 및 비타민 C 0.5 ~ 1.5 중량부를 더 포함한다.The wash-off tone-up cosmetic cream according to the present invention further includes 2 to 7 parts by weight of a tone-up enhancer, 2 to 5 parts by weight of a moisturizing enhancer, and 0.5 to 1.5 parts by weight of vitamin C, based on 100 parts by weight of purified water.

톤업 보강제는 하기와 같은 공정을 거쳐 제조된다.The tone-up enhancer is manufactured through the following process.

① 도라지 100 중량부에 대하여, 가시오가피 30 ~ 70 중량부, 레몬밤 분말 3 ~ 5 중량부 및 설탕 100 ~ 130 중량부를 밀폐충전한 후 34 ~ 37℃에서 30 ~ 35일간 발효하여 제 1 발효물을 제조한다. 여기서, 도라지는 박피된 것을 사용하고, 가시오가피는 100 ~ 220mm로 절단하여 사용한다.① For 100 parts by weight of bellflower root, 30 to 70 parts by weight of Acanthopanax, 3 to 5 parts by weight of lemon balm powder, and 100 to 130 parts by weight of sugar are tightly packed and fermented at 34 to 37°C for 30 to 35 days to produce the first fermented product. manufacture. Here, the peeled bellflower is used, and the acanthophyllum is cut into pieces of 100 to 220 mm.

또한, 도라지는 톤업 보강제의 가장 주요한 재료로서, 콜라겐의 생성 촉진 및 멜라닌의 침착 방지제로 사용되며 주요한 유효 원료이다. 가시오가피는 혈행개선제이고, 레몬밤은 항염제이다.In addition, bellflower root is the most important ingredient in tone-up enhancers, and is used as an agent to promote collagen production and prevent melanin deposition, and is a major effective raw material. Acanthopanax is a blood circulation improver, and lemon balm is an anti-inflammatory.

② 제 1 발효물 100 중량부에 대하여, 물 300 ~ 350 중량부 및 천일염 50 ~ 55 중량부를 혼합한 후 10 ~ 15시간 교반한 다음 여과하여 제 1 여과물을 제조한다. 여기서, 천일염은 천연 방부제이다.② For 100 parts by weight of the first fermentation product, 300 to 350 parts by weight of water and 50 to 55 parts by weight of sea salt are mixed, stirred for 10 to 15 hours, and then filtered to prepare the first filtrate. Here, sea salt is a natural preservative.

③ 제 1 여과물 100 중량부에 대하여, 풋사과 12 ~ 15 중량부, 청매실 5 ~ 8 중량부 및 설탕 30 ~ 50 중량부를 밀폐충전후 30 ~ 32℃에서 6 ~ 7개월간 발효하여 제 2 발효물을 제조한다. 여기서, 풋사과는 항산화제이고, 청매실은 항염제이다.③ For 100 parts by weight of the first filtrate, 12 to 15 parts by weight of green apples, 5 to 8 parts by weight of green plums, and 30 to 50 parts by weight of sugar are sealed and fermented at 30 to 32°C for 6 to 7 months to produce the second fermented product. manufacture. Here, green apple is an antioxidant and green plum is an anti-inflammatory.

④ 제 2 발효물 100 중량부에 대하여, 에탄올 150 ~ 450 중량부를 혼합한 후 40 ~ 45℃에서 24 ~ 30시간 정치한 다음, 여과하여 제 2 여과물을 제조한다.④ Mix 150 to 450 parts by weight of ethanol with 100 parts by weight of the second fermentation product, allow to stand at 40 to 45°C for 24 to 30 hours, and then filter to prepare the second filtrate.

⑤ 제 2 여과물 100 중량부에 대하여, 구연산 0.5 ~ 1.2 중량부 및 비타민 C 3 ~ 4 중량부를 혼합하여 톤업 보강제를 제조한다.⑤ For 100 parts by weight of the second filtrate, prepare a tone-up enhancer by mixing 0.5 to 1.2 parts by weight of citric acid and 3 to 4 parts by weight of vitamin C.

보습 강화제는 코코넛 과육 100 중량부에 대하여, 아보카도오일 5 ~ 7 중량부 및 꽃착즙액 10 ~ 15 중량부를 교반하여 제조된다. 여기서, 코코넛 과육 및 아보카도오일은 강력한 천연 보습제이다.The moisturizing enhancer is prepared by stirring 5 to 7 parts by weight of avocado oil and 10 to 15 parts by weight of flower juice with respect to 100 parts by weight of coconut meat. Here, coconut meat and avocado oil are powerful natural moisturizers.

꽃착즙액은 백장미 100 중량부에 대하여, 수선화 50 ~ 75 중량부 및 흰색국화 10 ~ 25 중량부를 혼합한 후 압착하여 꽃착즙액을 제조하여 준비한다. 여기서 백장미, 수선화 및 흰색국화는 꽃잎만 선별된 것으로, 암술머리(주두), 암술대(화주), 수술대(꽃실), 꽃밥 등은 제거된 것이다. 또한, 본 실시예에서 사용되는 꽃들은 모두 흰색이며, 꽃착즙액은 어혈을 풀어주고 혈액순환을 잘되게 하는 활혈기능을 통해 피부톤을 맑고 투명하게 하는 효과가 있다.The flower juice is prepared by mixing 50 to 75 parts by weight of daffodils and 10 to 25 parts by weight of white chrysanthemum with respect to 100 parts by weight of white roses, and then pressing the mixture. Here, only the petals of white roses, daffodils, and white chrysanthemums were selected, and the stigma (cap), style (flower stem), stamens (threads), and anthers were removed. In addition, the flowers used in this example are all white, and the flower juice has the effect of making the skin tone clear and transparent through the blood-boosting function of relieving stagnant blood and improving blood circulation.

2. 워시오프 톤업 화장용 크림의 제조방법2. Manufacturing method of wash-off tone-up cosmetic cream

(가) 정제수 100 중량부에 대하여, 부틸렌글라이콜 2 ~ 9 중량부, 나이아신아마이드 1 ~ 4 중량부, 세테아릴올리베이트 및 솔비탄올리베이트 0.5 ~ 2.7 중량부, 다이소듐 EDTA 0.01 ~ 0.03 중량부를 혼합하여 70 ~ 83℃로 가온한 후 10 ~ 20분간 교반하여 완전 용해한 다음 메인 믹서로 여과하여 이송한다.(A) Based on 100 parts by weight of purified water, 2 to 9 parts by weight of butylene glycol, 1 to 4 parts by weight of niacinamide, 0.5 to 2.7 parts by weight of cetearyl olivate and sorbitan olivate, and 0.01 to 0.03 parts by weight of disodium EDTA. The parts are mixed and heated to 70-83℃, stirred for 10-20 minutes to completely dissolve, and then filtered and transferred to the main mixer.

(나) 상기 정제수 100 중량부에 대하여, 글리세린 4.5 ~ 6.3 중량부 및 티타늄디옥사이드 0.5 ~ 1.0 중량부를 별도의 용기에서 70 ~ 83℃ 온도로 15 ~ 30분간 교반하여 완전분산시킨 다음 메인 믹서에 투입한다.(B) For 100 parts by weight of purified water, 4.5 to 6.3 parts by weight of glycerin and 0.5 to 1.0 parts by weight of titanium dioxide are stirred in a separate container at a temperature of 70 to 83°C for 15 to 30 minutes to completely disperse, and then added to the main mixer. .

(다) 상기 정제수 100 중량부에 대하여, 사이클로펜타실록세인 및 사이클로헥사실록세인 1.7 ~ 4.3 중량부, 다이메티콘 2.1 ~ 2.5 중량부, 시어버터 1.3 ~ 2.0 중량부, PEG-100 스테아레이트 및 글리세릴스테아레이트 0.1 ~ 1.1 중량부, 올리브오일 0.4 ~ 0.8 중량부, 코코넛야자오일 및 코코-카프릴레이트/카프레이트 0.2 ~ 0.8 중량부와, 폴리솔베이트80 0.1 ~ 0.5 중량부를 별도의 용기에서 70 ~ 83℃ 온도로 3 ~ 10분간 교반하여 완전 용해한 상기 메인 믹서로 여과 이송하여 유화한 후 58 ~ 62℃까지 냉각한다.(c) Based on 100 parts by weight of purified water, 1.7 to 4.3 parts by weight of cyclopentasiloxane and cyclohexasiloxane, 2.1 to 2.5 parts by weight of dimethicone, 1.3 to 2.0 parts by weight of shea butter, PEG-100 stearate and glycerol. 0.1 to 1.1 parts by weight of lyl stearate, 0.4 to 0.8 parts by weight of olive oil, 0.2 to 0.8 parts by weight of coconut palm oil and coco-caprylate/caprate, and 0.1 to 0.5 parts by weight of polysorbate 80 in a separate container. Completely dissolved by stirring for 3 to 10 minutes at a temperature of ~83℃, filtered and transferred to the main mixer for emulsification and then cooled to 58~62℃.

(라) 상기 정제수 100 중량부에 대하여, 티타늄디옥사이드 1.5 ~ 2.5 중량부, 트라이에톡시카프릴실레인 0.2 ~ 2.3 중량부, 알루미늄하이드록사이드 1.0 ~ 2.3 중량부, 폴리아크릴아마이드 1.4 ~ 3.0 중량부, C13-14아이소파라핀 0.2 ~ 2.2 중량부, 라우레스-7 0.2 ~ 0.4 중량부, 사이클로펜타실록세인 0.2 ~ 0.5 중량부 및 다이메티콘올 0.3 ~ 1.2 중량부를 별도의 용기에서 55 ~ 63℃ 온도로 20 ~ 25분간 교반하여 완전 분산시킨 다음 상기 메인 믹서로 투입한 후 교반 균일화하여 43 ~ 46℃까지 냉각하여 워시오프 톤업 화장용 크림을 제조한다.(D) Based on 100 parts by weight of purified water, 1.5 to 2.5 parts by weight of titanium dioxide, 0.2 to 2.3 parts by weight of triethoxycaprylsilane, 1.0 to 2.3 parts by weight of aluminum hydroxide, and 1.4 to 3.0 parts by weight of polyacrylamide. , 0.2 to 2.2 parts by weight of C13-14 isoparaffin, 0.2 to 0.4 parts by weight of laureth-7, 0.2 to 0.5 parts by weight of cyclopentasiloxane, and 0.3 to 1.2 parts by weight of dimethiconol in a separate container at a temperature of 55 to 63°C. Completely disperse by stirring for 20 to 25 minutes, then add to the main mixer, stir and homogenize, and cool to 43 to 46°C to prepare wash-off tone-up cosmetic cream.

(마) 최종적으로, 소비자의 기호에 적합하도록 상기 톤업 화장용 크림 100 중량부에 대하여, 방부재, 향료, 색소를 미소량(0.1 ~ 2.3 중량부) 첨가한 후 40 ~ 47℃에서 10 ~ 15분간 교반한 후 30℃까지 냉각한 진공 탈포한다. 여기서, 워시오프 톤업 화장용 크림은 상기 정제수 100 중량부에 대하여, 톤업 보강제 2 ~ 7 중량부, 보습 강화제 2 ~ 5 중량부 및 비타민 C 0.5 ~ 1.5 중량부를 더 포함한다. 톤업 보강제와 보습 강화제는 전술된 내용과 동일하다.(e) Finally, add a small amount (0.1 to 2.3 parts by weight) of preservatives, fragrances, and pigments to 100 parts by weight of the tone-up cosmetic cream to suit the consumer's preference, and then leave for 10 to 15 minutes at 40 to 47°C. After stirring, the mixture is cooled to 30°C and vacuum degassed. Here, the wash-off tone-up cosmetic cream further includes 2 to 7 parts by weight of a tone-up enhancer, 2 to 5 parts by weight of a moisturizing enhancer, and 0.5 to 1.5 parts by weight of vitamin C, based on 100 parts by weight of the purified water. The tone-up enhancer and moisturizing enhancer are the same as described above.

3. 워시오프 톤업 효과테스트3. Wash-off tone-up effect test

20대에서 40대까지 피부질환 및 만성질환이 없는 여성 5명을 대상자로 선정하여, 액상의 비교예와 크림 제형의 실시예를 각각 얼굴에 균일하게 도포한 후 워시오프 톤업 효과를 테스트하였다. 여기서, 비교예는 비타민 C 3 ~ 5wt%가 함유된 액상(잔량 정제수)이고, 실시예들의 조성은 하기와 같다.Five women in their 20s to 40s without skin diseases or chronic diseases were selected as subjects, and the liquid comparative example and the cream formulation example were uniformly applied to the face and the wash-off tone-up effect was tested. Here, the comparative example is a liquid containing 3 to 5 wt% of vitamin C (remaining amount purified water), and the composition of the examples is as follows.

실시예 1은 정제수 100 중량부에 대하여, 부틸렌글라이콜 7 중량부, 나이아신아마이드 3 중량부, 세테아릴올리베이트 0.7 중량부, 다이소듐 EDTA 0.02 중량부, 글리세린 4.8 중량부, 티타늄디옥사이드 2.5 중량부, 사이클로펜타실록세인 3.3 중량부, 다이메티콘 2.2 중량부, 시어버터 1.5 중량부, PEG-100 스테아레이트 0.7 중량부, 올리브오일 0.6 중량부, 폴리솔베이트80 0.3 중량부, 알루미늄하이드록사이드 1.9 중량부, 폴리아크릴아마이드 2.0 중량부, 다이메티콘올 0.8 중량부, 솔비탄올리베이트 0.4 중량부, 사이클로헥사실록세인 1.9 중량부, 코코넛야자오일 및 코코-카프릴레이트/카프레이트 0.6 중량부, 트라이에톡시카프릴실레인 1.7 중량부, C13-14아이소파라핀 1.2 중량부 및 라우레스-7 0.3 중량부로 조성되어 있다.Example 1 contains 7 parts by weight of butylene glycol, 3 parts by weight of niacinamide, 0.7 parts by weight of cetearyl olivate, 0.02 parts by weight of disodium EDTA, 4.8 parts by weight of glycerin, and 2.5 parts by weight of titanium dioxide, based on 100 parts by weight of purified water. parts, 3.3 parts by weight of cyclopentasiloxane, 2.2 parts by weight of dimethicone, 1.5 parts by weight of shea butter, 0.7 parts by weight of PEG-100 stearate, 0.6 parts by weight of olive oil, 0.3 parts by weight of polysorbate 80, aluminum hydroxide 1.9 parts by weight, polyacrylamide 2.0 parts by weight, dimethiconol 0.8 parts by weight, sorbitan olivate 0.4 parts by weight, cyclohexasiloxane 1.9 parts by weight, coconut palm oil and coco-caprylate/caprate 0.6 parts by weight, It is composed of 1.7 parts by weight of triethoxycaprylsilane, 1.2 parts by weight of C13-14 isoparaffin, and 0.3 parts by weight of laureth-7.

실시예 2: 실시예 1에 톤업 보강제 2 ~ 4 중량부 첨가Example 2: Addition of 2 to 4 parts by weight of tone-up enhancer to Example 1

실시예 3: 실시예 1에 톤업 보강제 5 ~ 7 중량부 첨가Example 3: Addition of 5 to 7 parts by weight of tone-up enhancer to Example 1

실시예 4: 실시예 1에 톤업 보강제 2 ~ 4 중량부 및 보습 강화제 2 ~ 3 중량부 첨가Example 4: Addition of 2 to 4 parts by weight of tone-up enhancer and 2 to 3 parts by weight of moisturizing enhancer to Example 1.

실시예 5: 실시예 1에 톤업 보강제 2 ~ 4 중량부 및 보습 강화제 4 ~ 5 중량부Example 5: 2 to 4 parts by weight of tone-up enhancer and 4 to 5 parts by weight of moisturizing enhancer in Example 1

실시예 6: 실시예 1에 톤업 보강제 5 ~ 7 중량부 및 보습 강화제 2 ~ 3 중량부 첨가Example 6: Addition of 5 to 7 parts by weight of tone-up enhancer and 2 to 3 parts by weight of moisturizing enhancer to Example 1.

실시예 7: 실시예 1에 톤업 보강제 5 ~ 7 중량부 및 보습 강화제 4 ~ 5 중량부Example 7: 5 to 7 parts by weight of tone-up enhancer and 4 to 5 parts by weight of moisturizing enhancer in Example 1

상기 실시예 2 내지 실시예 7에 각기 첨가된 톤업 보강제 또는 보습 강화제는 정제수 100 중량부에 대한 중량부이다.The tone-up enhancer or moisturizing enhancer added in Examples 2 to 7 is an amount by weight based on 100 parts by weight of purified water.

그리고 피부 톤의 피부밝기(Lightness Value, △L)는 일본 미놀타사의 색차계 CR-10PLUS를 사용하여 측정하였으며, 이의 워시오프 톤업 효과테스트 결과는 하기 표 1과 같다. 여기서, 피부 톤의 피부밝기는 색소가 침착되지 않는 동일한 부위를 측정한 것이며, 비교예 또는 실시예들을 각기 얼굴에 도포하여 세안한 다음 30분 경과후 평균 측정치를 나타낸다.The skin brightness (Lightness Value, △L) of the skin tone was measured using a colorimeter CR-10PLUS manufactured by Minolta, Japan, and the results of the wash-off tone-up effect test are shown in Table 1 below. Here, the skin brightness of the skin tone is measured on the same area where pigment is not deposited, and represents the average measurement value 30 minutes after applying each of the comparative examples or examples to the face and washing the face.

표 1을 참조하면, 비교예는 세안에 의해 극히 미비한 톤업효과가 있는 반면, 실시예 1은 △L=5.5으로 비교예 대비 크게 피부밝기가 개선됨을 확인되었으며, 톤업 보강제 및 보습 강화제의 함량이 높을수록 피부 톤업효과가 개선됨을 확인할 수 있었다.Referring to Table 1, the comparative example had a very slight tone-up effect by washing the face, while the skin brightness of Example 1 was confirmed to be significantly improved compared to the comparative example with △L = 5.5, and the content of the tone-up enhancer and moisturizing enhancer was high. It was confirmed that the skin tone-up effect improved as time went on.

이상과 같은 본 발명은 일 실시예에 한정되어 설명되었으나, 이에 한정되지 않고 본 발명의 기술적 사상을 토대로 변형되는 실시예들은 모두 본 발명의 권리범위에 속함이 분명하다.Although the present invention has been described as limited to one embodiment, it is clear that it is not limited thereto and that all embodiments modified based on the technical idea of the present invention fall within the scope of the present invention.

Claims (5)

정제수 100 중량부에 대하여, 부틸렌글라이콜 2 ~ 9 중량부, 나이아신아마이드 1 ~ 4 중량부, 세테아릴올리베이트 0.5 ~ 1.1 중량부, 다이소듐 EDTA 0.01 ~ 0.03 중량부, 글리세린 4.5 ~ 6.3 중량부, 티타늄디옥사이드 0.5 ~ 3.5 중량부, 사이클로펜타실록세인 1.7 ~ 4.3 중량부, 다이메티콘 2.1 ~ 2.5 중량부, 시어버터 1.3 ~ 2.0 중량부, PEG-100 스테아레이트 0.1 ~ 1.1 중량부, 올리브오일 0.4 ~ 0.8 중량부, 폴리솔베이트80 0.1 ~ 0.5 중량부, 알루미늄하이드록사이드 1.0 ~ 2.3 중량부, 폴리아크릴아마이드 1.4 ~ 3.0 중량부 및 다이메티콘올 0.3 ~ 1.2 중량부를 포함하되,
상기 정제수 100 중량부에 대하여, 솔비탄올리베이트 0.3 ~ 0.5 중량부, 사이클로헥사실록세인 1.2 ~ 2.3 중량부, 코코넛야자오일 및 코코-카프릴레이트/카프레이트 0.2 ~ 0.8 중량부, 트라이에톡시카프릴실레인 0.2 ~ 2.3 중량부, C13-14아이소파라핀 0.2 ~ 2.2 중량부 및 라우레스-7 0.2 ~ 0.4 중량부를 더 포함하는 것을 특징으로 하는 워시오프 톤업 화장용 크림.
Based on 100 parts by weight of purified water, 2 to 9 parts by weight of butylene glycol, 1 to 4 parts by weight of niacinamide, 0.5 to 1.1 parts by weight of cetearyl olivate, 0.01 to 0.03 parts by weight of disodium EDTA, 4.5 to 6.3 parts by weight of glycerin. parts, titanium dioxide 0.5 to 3.5 parts by weight, cyclopentasiloxane 1.7 to 4.3 parts by weight, dimethicone 2.1 to 2.5 parts by weight, shea butter 1.3 to 2.0 parts by weight, PEG-100 stearate 0.1 to 1.1 parts by weight, olive oil 0.4 to 0.8 parts by weight, 0.1 to 0.5 parts by weight of polysorbate 80, 1.0 to 2.3 parts by weight of aluminum hydroxide, 1.4 to 3.0 parts by weight of polyacrylamide, and 0.3 to 1.2 parts by weight of dimethiconol,
Based on 100 parts by weight of purified water, 0.3 to 0.5 parts by weight of sorbitan olivate, 1.2 to 2.3 parts by weight of cyclohexasiloxane, 0.2 to 0.8 parts by weight of coconut palm oil and coco-caprylate/caprate, and triethoxycapryl. A wash-off tone-up cosmetic cream further comprising 0.2 to 2.3 parts by weight of silane, 0.2 to 2.2 parts by weight of C13-14 isoparaffin, and 0.2 to 0.4 parts by weight of laureth-7.
삭제delete 제 1 항에 있어서,
상기 정제수 100 중량부에 대하여, 톤업 보강제 2 ~ 7 중량부를 더 포함하되,
상기 톤업 보강제는 ① 도라지 100 중량부에 대하여, 가시오가피 30 ~ 70 중량부, 레몬밤 분말 3 ~ 5 중량부 및 설탕 100 ~ 130 중량부를 밀폐충전한 후 34 ~ 37℃에서 30 ~ 35일간 발효하여 제 1 발효물을 제조하는 단계와; ② 상기 제 1 발효물 100 중량부에 대하여, 물 300 ~ 350 중량부 및 천일염 50 ~ 55 중량부를 혼합한 후 10 ~ 15시간 교반한 다음 여과하여 제 1 여과물을 제조하는 단계와; ③ 상기 제 1 여과물 100 중량부에 대하여, 풋사과 12 ~ 15 중량부, 청매실 5 ~ 8 중량부 및 설탕 30 ~ 50 중량부를 밀폐충전후 30 ~ 32℃에서 6 ~ 7개월간 발효하여 제 2 발효물을 제조하는 단계와; ④ 상기 제 2 발효물 100 중량부에 대하여, 에탄올 150 ~ 450 중량부를 혼합한 후 40 ~ 45℃에서 24 ~ 30시간 정치한 다음, 여과하여 제 2 여과물을 제조하는 단계와; ⑤ 상기 제 2 여과물 100 중량부에 대하여, 구연산 0.5 ~ 1.2 중량부 및 비타민 C 3 ~ 4 중량부를 혼합하여 제조되는 것을 특징으로 하는 워시오프 톤업 화장용 크림.
According to claim 1,
Based on 100 parts by weight of the purified water, 2 to 7 parts by weight of a tone-up enhancer is further included,
The tone-up enhancer is prepared by sealing 30 to 70 parts by weight of Acanthopanax, 3 to 5 parts by weight of lemon balm powder, and 100 to 130 parts by weight of sugar for 100 parts by weight of bellflower root and then fermenting at 34 to 37°C for 30 to 35 days. 1 preparing a fermented product; ② Mixing 300 to 350 parts by weight of water and 50 to 55 parts by weight of sea salt with 100 parts by weight of the first fermented product, stirring for 10 to 15 hours, and then filtering to prepare a first filtrate; ③ For 100 parts by weight of the first filtrate, 12 to 15 parts by weight of green apples, 5 to 8 parts by weight of green plums, and 30 to 50 parts by weight of sugar are sealed and fermented at 30 to 32°C for 6 to 7 months to produce a second fermented product. manufacturing steps; ④ mixing 150 to 450 parts by weight of ethanol with 100 parts by weight of the second fermentation product, leaving it to stand at 40 to 45°C for 24 to 30 hours, and then filtering to prepare a second filtrate; ⑤ Wash-off tone-up cosmetic cream, characterized in that it is manufactured by mixing 0.5 to 1.2 parts by weight of citric acid and 3 to 4 parts by weight of vitamin C with 100 parts by weight of the second filtrate.
제 1 항에 있어서,
상기 정제수 100 중량부에 대하여, 보습 강화제 2 ~ 5 중량부 및 비타민 C 0.5 ~ 1.5 중량부를 더 포함하되,
상기 보습 강화제는 코코넛 과육 100 중량부에 대하여, 아보카도오일 5 ~ 7 중량부 및 꽃착즙액 10 ~ 15 중량부를 함유하되, 상기 꽃착즙액은 백장미 100 중량부에 대하여, 수선화 50 ~ 75 중량부 및 흰색국화 10 ~ 25 중량부를 혼합 압착하여 제조되는 것을 특징으로 하는 워시오프 톤업 화장용 크림.
According to claim 1,
Based on 100 parts by weight of purified water, 2 to 5 parts by weight of a moisturizing enhancer and 0.5 to 1.5 parts by weight of vitamin C are further included,
The moisturizing enhancer contains 5 to 7 parts by weight of avocado oil and 10 to 15 parts by weight of flower juice based on 100 parts by weight of coconut flesh, and the flower juice contains 50 to 75 parts by weight of daffodil and 100 parts by weight of white rose. A wash-off tone-up cosmetic cream produced by mixing and pressing 10 to 25 parts by weight of white chrysanthemum.
(a) 정제수 100 중량부, 부틸렌글라이콜 2 ~ 9 중량부, 나이아신아마이드 1 ~ 4 중량부, 세테아릴올리베이트 및 솔비탄올리베이트 0.5 ~ 2.7 중량부, 다이소듐 EDTA 0.01 ~ 0.03 중량부를 혼합하여 70 ~ 83℃로 가온한 후 10 ~ 20분간 교반하여 완전 용해한 다음 메인 믹서로 여과하여 이송하는 단계와;
(b) 정제수 100 중량부에 대하여, 글리세린 4.5 ~ 6.3 중량부 및 티타늄디옥사이드 0.5 ~ 1.0 중량부를 별도의 용기에서 70 ~ 83℃ 온도로 15 ~ 30분간 교반하여 완전분산시킨 다음 메인 믹서에 투입하는 단계와;
(c) 정제수 100 중량부에 대하여, 사이클로펜타실록세인 및 사이클로헥사실록세인 1.7 ~ 4.3 중량부, 다이메티콘 2.1 ~ 2.5 중량부, 시어버터 1.3 ~ 2.0 중량부, PEG-100 스테아레이트 및 글리세릴스테아레이트 0.1 ~ 1.1 중량부, 올리브오일 0.4 ~ 0.8 중량부, 코코넛야자오일 및 코코-카프릴레이트/카프레이트 0.2 ~ 0.8 중량부와, 폴리솔베이트80 0.1 ~ 0.5 중량부를 별도의 용기에서 70 ~ 83℃ 온도로 3 ~ 10분간 교반하여 완전 용해한 상기 메인 믹서로 여과 이송하여 유화한 후 58 ~ 62℃까지 냉각하는 단계와;
(d) 정제수 100 중량부에 대하여, 티타늄디옥사이드 1.5 ~ 2.5 중량부, 트라이에톡시카프릴실레인 0.2 ~ 2.3 중량부, 알루미늄하이드록사이드 1.0 ~ 2.3 중량부, 폴리아크릴아마이드 1.4 ~ 3.0 중량부, C13-14아이소파라핀 0.2 ~ 2.2 중량부, 라우레스-7 0.2 ~ 0.4 중량부, 사이클로펜타실록세인 0.2 ~ 0.5 중량부 및 다이메티콘올 0.3 ~ 1.2 중량부를 별도의 용기에서 55 ~ 63℃ 온도로 20 ~ 25분간 교반하여 완전 분산시킨 다음 상기 메인 믹서로 투입한 후 교반 균일화하여 43 ~ 46℃까지 냉각하여 톤업 화장용 크림을 제조하는 단계와;
(e) 상기 톤업 화장용 크림 100 중량부에 대하여, 방부재, 향료, 색소 0.1 ~ 2.3 중량부 및 톤업 보강제 2 ~ 7 중량부, 보습 강화제 2 ~ 5 중량부 및 비타민 C 0.5 ~ 1.5 중량부를 더 포함첨가한 후 40 ~ 47℃에서 10 ~ 15분간 교반한 후 30℃까지 냉각한 진공 탈포하는 단계로 이루어지되,
상기 톤업 보강제는 ① 도라지 100 중량부에 대하여, 가시오가피 30 ~ 70 중량부, 레몬밤 분말 3 ~ 5 중량부 및 설탕 100 ~ 130 중량부를 밀폐충전한 후 34 ~ 37℃에서 30 ~ 35일간 발효하여 제 1 발효물을 제조하는 단계와; ② 상기 제 1 발효물 100 중량부에 대하여, 물 300 ~ 350 중량부 및 천일염 50 ~ 55 중량부를 혼합한 후 10 ~ 15시간 교반한 다음 여과하여 제 1 여과물을 제조하는 단계와; ③ 상기 제 1 여과물 100 중량부에 대하여, 풋사과 12 ~ 15 중량부, 청매실 5 ~ 8 중량부 및 설탕 30 ~ 50 중량부를 밀폐충전후 30 ~ 32℃에서 6 ~ 7개월간 발효하여 제 2 발효물을 제조하는 단계와; ④ 상기 제 2 발효물 100 중량부에 대하여, 에탄올 150 ~ 450 중량부를 혼합한 후 40 ~ 45℃에서 24 ~ 30시간 정치한 다음, 여과하여 제 2 여과물을 제조하는 단계와; ⑤ 상기 제 2 여과물 100 중량부에 대하여, 구연산 0.5 ~ 1.2 중량부 및 비타민 C 3 ~ 4 중량부를 혼합하여 제조되고,
상기 보습 강화제는 코코넛 과육 100 중량부에 대하여, 아보카도오일 5 ~ 7 중량부 및 꽃착즙액 10 ~ 15 중량부를 함유하되, 상기 꽃착즙액은 백장미 100 중량부에 대하여, 수선화 50 ~ 75 중량부 및 흰색국화 10 ~ 25 중량부를 혼합 압착하여 제조되는 것을 특징으로 하는 워시오프 톤업 화장용 크림의 제조방법.
(a) Mix 100 parts by weight of purified water, 2 to 9 parts by weight of butylene glycol, 1 to 4 parts by weight of niacinamide, 0.5 to 2.7 parts by weight of cetearyl olivate and sorbitan olivate, and 0.01 to 0.03 parts by weight of disodium EDTA. heating to 70 to 83°C, stirring for 10 to 20 minutes to completely dissolve, and then filtering and transferring to the main mixer;
(b) For 100 parts by weight of purified water, 4.5 to 6.3 parts by weight of glycerin and 0.5 to 1.0 parts by weight of titanium dioxide are stirred in a separate container at a temperature of 70 to 83°C for 15 to 30 minutes to completely disperse and then added to the main mixer. and;
(c) Based on 100 parts by weight of purified water, 1.7 to 4.3 parts by weight of cyclopentasiloxane and cyclohexasiloxane, 2.1 to 2.5 parts by weight of dimethicone, 1.3 to 2.0 parts by weight of shea butter, PEG-100 stearate and glyceryl. 0.1 to 1.1 parts by weight of stearate, 0.4 to 0.8 parts by weight of olive oil, 0.2 to 0.8 parts by weight of coconut palm oil and coco-caprylate/caprate, and 0.1 to 0.5 parts by weight of polysorbate 80 in a separate container at 70 ~ 0.8 parts by weight. Stirring at a temperature of 83°C for 3 to 10 minutes to completely dissolve, filter and transfer to the main mixer for emulsification and then cooling to 58 to 62°C;
(d) Based on 100 parts by weight of purified water, 1.5 to 2.5 parts by weight of titanium dioxide, 0.2 to 2.3 parts by weight of triethoxycaprylsilane, 1.0 to 2.3 parts by weight of aluminum hydroxide, 1.4 to 3.0 parts by weight of polyacrylamide, 0.2 to 2.2 parts by weight of C13-14 isoparaffin, 0.2 to 0.4 parts by weight of laureth-7, 0.2 to 0.5 parts by weight of cyclopentasiloxane, and 0.3 to 1.2 parts by weight of dimethiconol are placed in a separate container at a temperature of 55 to 63°C. completely dispersing by stirring for 20 to 25 minutes, then adding it to the main mixer, stirring to homogenize, and cooling to 43 to 46°C to prepare a tone-up cosmetic cream;
(e) Based on 100 parts by weight of the tone-up cosmetic cream, it further contains 0.1 to 2.3 parts by weight of preservatives, fragrances, and pigments, 2 to 7 parts by weight of tone-up enhancers, 2 to 5 parts by weight of moisturizing enhancers, and 0.5 to 1.5 parts by weight of vitamin C. After addition, it is stirred at 40 to 47°C for 10 to 15 minutes, then cooled to 30°C and vacuum degassed.
The tone-up enhancer is prepared by sealing 30 to 70 parts by weight of Acanthopanax, 3 to 5 parts by weight of lemon balm powder, and 100 to 130 parts by weight of sugar for 100 parts by weight of bellflower root and then fermenting at 34 to 37°C for 30 to 35 days. 1 preparing a fermented product; ② Mixing 300 to 350 parts by weight of water and 50 to 55 parts by weight of sea salt with 100 parts by weight of the first fermented product, stirring for 10 to 15 hours, and then filtering to prepare a first filtrate; ③ For 100 parts by weight of the first filtrate, 12 to 15 parts by weight of green apples, 5 to 8 parts by weight of green plums, and 30 to 50 parts by weight of sugar are sealed and fermented at 30 to 32°C for 6 to 7 months to produce a second fermented product. manufacturing steps; ④ mixing 150 to 450 parts by weight of ethanol with 100 parts by weight of the second fermentation product, leaving it to stand at 40 to 45°C for 24 to 30 hours, and then filtering to prepare a second filtrate; ⑤ It is prepared by mixing 0.5 to 1.2 parts by weight of citric acid and 3 to 4 parts by weight of vitamin C with respect to 100 parts by weight of the second filtrate,
The moisturizing enhancer contains 5 to 7 parts by weight of avocado oil and 10 to 15 parts by weight of flower juice based on 100 parts by weight of coconut flesh, and the flower juice contains 50 to 75 parts by weight of daffodils and 100 parts by weight of white rose. A method of manufacturing a wash-off tone-up cosmetic cream, characterized in that it is manufactured by mixing and pressing 10 to 25 parts by weight of white chrysanthemum.
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