KR102581367B1 - zzoyo zzoyo Cosmetic lifting ampoule composition and its manufacturing method - Google Patents

Abstract

The present invention relates to a lifting ampoule composition for improving skin elasticity and wrinkles, including a first ampoule composition; a second ampoule composition; and a third ampoule composition; and a method for manufacturing the same. will be.
In addition, it relates to a lifting ampoule composition for improving skin elasticity and wrinkles, which further contains conchiolin powder to maximize the skin improvement effect, and a method for manufacturing the same.

Description

Lifting ampoule composition for improving skin elasticity and wrinkles and its manufacturing method {zzoyo zzoyo Cosmetic lifting ampoule composition and its manufacturing method}

The present invention relates to a lifting ampoule composition for improving skin elasticity and wrinkles, including a first ampoule composition; a second ampoule composition; and a third ampoule composition; and a method for manufacturing the same. will be.

In addition, it relates to a lifting ampoule composition for improving skin elasticity and wrinkles, which further contains conchiolin powder to maximize the skin improvement effect, and a method for manufacturing the same.

Generally, in order to improve skin elasticity and wrinkles, the procedure is performed to lift up sagging skin and induce collagen regeneration to give elasticity to the skin. A lifting effect that pulls the skin upward occurs immediately after the procedure, and it lasts for several months or years depending on the type of thread. Helps maintain skin elasticity. However, these procedures have the problem of being expensive and difficult to manage on an ongoing basis.

Therefore, in order to solve this problem, lifting ampoules were released and it is known that good results can be expected quickly in a short period of time, but it was difficult to feel actual skin changes. Therefore, the present inventor seeks to provide a lifting ampoule that can achieve immediate changes within 30 days with 20 minutes of daily care.

Republic of Korea Public Patent No. 10-2022-0056454 (Publication Date: May 6, 2022)

To achieve the above purpose,

The present invention includes a first ampoule composition; a second ampoule composition; and a third ampoule composition; to improve skin elasticity and wrinkles,

In addition, the purpose of the invention is to provide a lifting ampoule composition for improving skin elasticity and wrinkles, which further contains conchiolin powder to maximize the skin improvement effect, and a method for manufacturing the same.

To solve the above problem,

The present invention contains 10 to 70 wt% of purified water, 10 to 70 wt% of sodium polystyrene sulfonate, 0.05 to 0.15 wt% of polysorbate 20, 1 to 5 wt% of ammonium acryloyldimethyl taurate/VPicopolymer, and xanthan gum. 0.5 ~ 1 wt%, polyvinyl alcohol 0.2 ~ 0.3 wt%, butylene glycol 5 ~ 10 wt%, ethylhexylglycerin 1 ~ 5 wt%, disodium EDTA 0.01 ~ 0.05 wt%, propanediol 2 ~ 5 wt%, 1-2 hexanediol 0.01 ~ 0.02 wt%, camellia flower extract 0.2 ~ 1 wt%, black mulberry fruit extract 0.2 ~ 1 wt%, propolis extract 0.2 ~ 1 wt%, rosehip fruit extract 0.2 ~ 1 wt%, vitamin tree fruit extract 0.2 ~ 1 wt%, serolta cherry tree flower extract 0.2 ~ 1 wt%, prickly peach tree flower extract 0.2 ~ 1 wt%, royal jelly extract 0.2 ~ 1 wt%, port marigold flower extract 0.2 ~ 1 wt%, fragrance 0.01 ~ 0.02 wt%, sodium acetate 0.1 ~ 0.5 wt%, linalool 0.01 ~ 0.02 wt%, hexylcinnamal 0.01 ~ 0.02 wt%, alpha-isomethylionone 0.01 ~ 0.02 wt% and adenosine Provided is a lifting composition for improving skin elasticity and wrinkles, comprising 0.01 to 1 wt%.

In order to solve the above problem, the present invention uses 10 to 70 wt% of purified water, 10 to 70 wt% of sodium polystyrene sulfonate, 0.05 to 0.15 wt% of polysorbate 20, and ammonium acryloyl dimethyl taurate/VPicopolymer 1. ~ 5 wt%, xanthan gum 0.5 ~ 1 wt%, polyvinyl alcohol 0.2 ~ 0.3 wt%, butylene glycol 5 ~ 10 wt%, ethylhexylglycerin 1 ~ 5 wt%, disodium EDTA 0.01 ~ 0.05 wt %, propanediol 2 ~ 5 wt%, 1-2 hexanediol 0.01 ~ 0.02 wt%, camellia flower extract 0.2 ~ 1 wt%, black mulberry fruit extract 0.2 ~ 1 wt%, propolis extract 0.2 ~ 1 wt %, rosehip fruit extract 0.2 ~ 1 wt%, vitamin tree fruit extract 0.2 ~ 1 wt%, serolta cherry tree flower extract 0.2 ~ 1 wt%, prickly pear flower extract 0.2 ~ 1 wt%, royal jelly extract 0.2 ~ 1 wt% , pot marigold flower extract 0.2 ~ 1 wt%, fragrance 0.01 ~ 0.02 wt%, sodium acetate 0.1 ~ 0.5 wt%, linalool 0.01 ~ 0.02 wt%, hexyl cinnamal 0.01 ~ 0.02 wt%, alpha-isomethyl ionone A first ampoule composition prepared by adding a first mixture of 0.01 to 0.02 wt% and 0.01 to 1 wt% of adenosine into a stirrer (HOMO MIXER) and stirring it at 5,000 to 6,000 rpm for 3 to 8 minutes;

Lotus leaf 1 ~ 30 wt%, hydrangea leaf 1 ~ 30 wt%, pine needle 1 ~ 30 wt%, banana leaf 1 ~ 30 wt%, moringa leaf 1 ~ 30 wt%, dill leaf 1 ~ 30 wt%, amaranth leaf 1 ~ 30 wt% of the second mixture of 30 wt%, 1 ~ 30 wt% of ramie leaves, 1 ~ 30 wt% of okra leaves, and 1 ~ 30 wt% of arrowroot leaves was mixed with 60 ~ 70 wt% of distilled water. Then, a second extract was prepared by shaking extraction for 10 to 15 hours at 30 to 70°C and 140 to 200 rpm, and the second extract was centrifuged in a centrifuge at 7,000 to 9,000 rpm for 10 to 30 minutes. A second ampoule composition prepared by filtering the supernatant and concentrating the filtrate under reduced pressure with a vacuum rotation evaporator for 5 to 7 hours under conditions of 0.1 to 0.3 mPA;

Cheongung 1 ~ 30 wt%, Baekbokryeong 1 ~ 30 wt%, Angelica 1 ~ 30 wt%, Elm bark 1 ~ 30 wt%, Black garlic 1 ~ 30 wt%, Lotus root 1 ~ 30 wt%, and Wasong 1 ~ 30 wt% After adding 30 to 40 wt% of the third mixture mixed with 60 to 70 wt% of distilled water, the third extract was prepared by shaking extraction for 10 to 15 hours under conditions of 30 to 70 ℃ and 140 to 200 rpm. After centrifuging the third extract for 10 to 30 minutes at 7,000 to 9,000 rpm in a centrifuge, the supernatant was filtered and the filtrate was evaporated under vacuum rotation evaporator for 5 to 7 hours under conditions of 0.1 to 0.3 mPA. ) The third ampoule composition prepared by concentration under reduced pressure;

90 to 95 wt% of the first ampoule composition; 1 to 5 wt% of the second ampoule composition; and 1 to 5 wt% of the third ampoule composition to prepare the final ampoule composition,

After stirring the final ampoule composition at 2,000 to 3,000 rpm for 2 to 3 minutes, the stirred liquid was subjected to a high pressure emulsification process 2 to 3 times under conditions of 700 to 1,100 bar using a high pressure emulsifier,

A lifting composition for improving skin elasticity and wrinkles is provided, which is manufactured by cooling the final ampoule composition that has undergone the high-pressure emulsification process and then aging it at room temperature for 30 to 40 hours.

In order to solve the above problem, the present invention uses 10 to 70 wt% of purified water, 10 to 70 wt% of sodium polystyrene sulfonate, 0.05 to 0.15 wt% of polysorbate 20, and ammonium acryloyl dimethyl taurate/VPicopolymer 1. ~ 5 wt%, xanthan gum 0.5 ~ 1 wt%, polyvinyl alcohol 0.2 ~ 0.3 wt%, butylene glycol 5 ~ 10 wt%, ethylhexylglycerin 1 ~ 5 wt%, disodium EDTA 0.01 ~ 0.05 wt %, propanediol 2 ~ 5 wt%, 1-2 hexanediol 0.01 ~ 0.02 wt%, camellia flower extract 0.2 ~ 1 wt%, black mulberry fruit extract 0.2 ~ 1 wt%, propolis extract 0.2 ~ 1 wt %, rosehip fruit extract 0.2 ~ 1 wt%, vitamin tree fruit extract 0.2 ~ 1 wt%, serolta cherry tree flower extract 0.2 ~ 1 wt%, prickly pear flower extract 0.2 ~ 1 wt%, royal jelly extract 0.2 ~ 1 wt% , pot marigold flower extract 0.2 ~ 1 wt%, fragrance 0.01 ~ 0.02 wt%, sodium acetate 0.1 ~ 0.5 wt%, linalool 0.01 ~ 0.02 wt%, hexyl cinnamal 0.01 ~ 0.02 wt%, alpha-isomethyl ionone A first mixture of 0.01 to 0.02 wt% and 0.01 to 1 wt% of adenosine was added to a stirrer (HOMO MIXER) and then stirred at 5,000 to 6,000 rpm for 3 to 8 minutes to prepare a first ampoule composition (S1) )and,

Lotus leaf 1 ~ 30 wt%, hydrangea leaf 1 ~ 30 wt%, pine needle 1 ~ 30 wt%, banana leaf 1 ~ 30 wt%, moringa leaf 1 ~ 30 wt%, dill leaf 1 ~ 30 wt%, amaranth leaf 1 ~ 30 wt% of the second mixture of 30 wt%, 1 ~ 30 wt% of ramie leaves, 1 ~ 30 wt% of okra leaves, and 1 ~ 30 wt% of arrowroot leaves was mixed with 60 ~ 70 wt% of distilled water. Then, a second extract was prepared by shaking extraction for 10 to 15 hours at 30 to 70°C and 140 to 200 rpm, and the second extract was centrifuged in a centrifuge at 7,000 to 9,000 rpm for 10 to 30 minutes. After filtering the supernatant, the filtrate is concentrated under reduced pressure with a vacuum rotation evaporator for 5 to 7 hours under conditions of 0.1 to 0.3 mPA to prepare a second ampoule composition (S2);

Cheongung 1 ~ 30 wt%, Baekbokryeong 1 ~ 30 wt%, Angelica 1 ~ 30 wt%, Elm Bark 1 ~ 30, Black Garlic 1 ~ 30 wt%, Lotus root 1 ~ 30 wt%, and Japanese Pine 1 ~ 30 wt%. 30 to 40 wt% of the mixed third mixture was added to 60 to 70 wt% of distilled water, and then extracted by shaking for 10 to 15 hours at 30 to 70°C and 140 to 200 rpm to prepare the third extract, After centrifuging the third extract for 10 to 30 minutes at 7,000 to 9,000 rpm in a centrifuge, the supernatant was filtered and the filtrate was evaporated in a vacuum rotation evaporator for 5 to 7 hours under conditions of 0.1 to 0.3 mPA. A step (S3) of producing a third ampoule composition prepared by concentrating under reduced pressure,

90 to 95 wt% of the first ampoule composition; 1 to 5 wt% of the second ampoule composition; and 1 to 5 wt% of the third ampoule composition to prepare the final ampoule composition (S4),

After stirring the final ampoule composition at 2,000 to 3,000 rpm for 2 to 3 minutes, the stirred liquid is subjected to a high pressure emulsification process 2 to 3 times at 700 to 1,100 bar using a high pressure emulsifier (S5);

A method of manufacturing a lifting composition for improving skin elasticity and wrinkles is provided, comprising the step of cooling the final ampoule composition that has undergone the high-pressure emulsification process and then maturing it at room temperature for 30 to 40 hours (S6).

The present invention adds skin elasticity within 20 minutes after application to the face, allowing the user to feel an immediate effect, and has the effect of positively improving the user's overall skin, including skin texture, wrinkles, freckles, and skin tone. .

Figure 1 is a diagram showing positive improvement in the skin after using the lifting ampoule for 30 days in Example 3 of a lifting ampoule composition that improves skin elasticity and wrinkles and a method for manufacturing the same.

Below, we will look at the specific details.

Purified water 10 ~ 70 wt%, sodium polystyrene sulfonate 10 ~ 70 wt%, polysorbate 20 0.05 ~ 0.15 wt%, ammonium acryloyl dimethyl taurate/V picopolymer 1 ~ 5 wt%, xanthan gum 0.5 ~ 1 wt%, polyvinyl alcohol 0.2 ~ 0.3 wt%, butylene glycol 5 ~ 10 wt%, ethylhexylglycerin 1 ~ 5 wt%, disodium EDTA 0.01 ~ 0.05 wt%, propanediol 2 ~ 5 wt% , 1-2 hexanediol 0.01 ~ 0.02 wt%, camellia flower extract 0.2 ~ 1 wt%, black mulberry fruit extract 0.2 ~ 1 wt%, propolis extract 0.2 ~ 1 wt%, rosehip fruit extract 0.2 ~ 1 wt% , Vitamin tree fruit extract 0.2 ~ 1 wt%, Cerolta cherry tree flower extract 0.2 ~ 1 wt%, Aspen tree flower extract 0.2 ~ 1 wt%, Royal jelly extract 0.2 ~ 1 wt%, Port marigold flower extract 0.2 ~ 1 wt %, fragrance 0.01 ~ 0.02 wt%, sodium acetate 0.1 ~ 0.5 wt%, linalool 0.01 ~ 0.02 wt%, hexylcinnamal 0.01 ~ 0.02 wt%, alpha-isomethyl ionone 0.01 ~ 0.02 wt%, and adenosine 0.01 ~ 1 A step (S1) of preparing a first ampoule composition by adding the first mixture containing wt% to a stirrer (HOMO MIXER) and stirring it at 5,000 to 6,000 rpm for 3 to 8 minutes,

Lotus leaf 1 ~ 30 wt%, hydrangea leaf 1 ~ 30 wt%, pine needle 1 ~ 30 wt%, banana leaf 1 ~ 30 wt%, moringa leaf 1 ~ 30 wt%, dill leaf 1 ~ 30 wt%, amaranth leaf 1 ~ 30 wt% of the second mixture of 30 wt%, 1 ~ 30 wt% of ramie leaves, 1 ~ 30 wt% of okra leaves, and 1 ~ 30 wt% of arrowroot leaves was mixed with 60 ~ 70 wt% of distilled water. Then, a second extract was prepared by shaking extraction for 10 to 15 hours at 30 to 70°C and 140 to 200 rpm, and the second extract was centrifuged in a centrifuge at 7,000 to 9,000 rpm for 10 to 30 minutes. After filtering the supernatant, the filtrate is concentrated under reduced pressure with a vacuum rotation evaporator for 5 to 7 hours under conditions of 0.1 to 0.3 mPA to prepare a second ampoule composition (S2);

Cheongung 1 ~ 30 wt%, Baekbokryeong 1 ~ 30 wt%, Angelica 1 ~ 30 wt%, Elm bark 1 ~ 30 wt%, Black garlic 1 ~ 30 wt%, Lotus root 1 ~ 30 wt%, and Wasson 1 ~ 30 wt%. After adding 30 to 40 wt% of the third mixture mixed with 60 to 70 wt% of distilled water, the third extract was prepared by shaking extraction for 10 to 15 hours under conditions of 30 to 70 ℃ and 140 to 200 rpm. After centrifuging the third extract for 10 to 30 minutes at 7,000 to 9,000 rpm in a centrifuge, the supernatant was filtered and the filtrate was evaporated under vacuum rotation evaporator for 5 to 7 hours under conditions of 0.1 to 0.3 mPA. ), a step (S3) of producing a third ampoule composition prepared by concentrating under reduced pressure,

90 to 95 wt% of the first ampoule composition, 1 to 5 wt% of the second ampoule composition; and 1 to 5 wt% of the third ampoule composition; preparing a final ampoule composition (S4);

After stirring the final ampoule composition at 2,000 to 3,000 rpm for 2 to 3 minutes, the stirred liquid is subjected to a high pressure emulsification process 2 to 3 times at 700 to 1,100 bar using a high pressure emulsifier (S5);

After cooling the final ampoule composition that has undergone the high-pressure emulsification process, it includes a step (S6) of maturing at room temperature for 30 to 40 hours.

Hereinafter, we will look at the specific details of each step of Example 1.

[Step (S1) of manufacturing the first ampoule composition]

Purified water 10 ~ 70 wt%, sodium polystyrene sulfonate 10 ~ 70 wt%, polysorbate 20 0.05 ~ 0.15 wt%, ammonium acryloyl dimethyl taurate/V picopolymer 1 ~ 5 wt%, xanthan gum 0.5 ~ 1 wt%, polyvinyl alcohol 0.2 ~ 0.3 wt%, butylene glycol 5 ~ 10 wt%, ethylhexylglycerin 1 ~ 5 wt%, disodium EDTA 0.01 ~ 0.05 wt%, propanediol 2 ~ 5 wt% , 1-2 hexanediol 0.01 ~ 0.02 wt%, camellia flower extract 0.2 ~ 1 wt%, black mulberry fruit extract 0.2 ~ 1 wt%, propolis extract 0.2 ~ 1 wt%, rosehip fruit extract 0.2 ~ 1 wt% , Vitamin tree fruit extract 0.2 ~ 1 wt%, Cerolta cherry tree flower extract 0.2 ~ 1 wt%, Aspen tree flower extract 0.2 ~ 1 wt%, Royal jelly extract 0.2 ~ 1 wt%, Port marigold flower extract 0.2 ~ 1 wt %, fragrance 0.01 ~ 0.02 wt%, sodium acetate 0.1 ~ 0.5 wt%, linalool 0.01 ~ 0.02 wt%, hexylcinnamal 0.01 ~ 0.02 wt%, alpha-isomethyl ionone 0.01 ~ 0.02 wt%, and adenosine 0.01 ~ 1 The first ampoule composition mixed by wt% is put into a stirrer (HOMO MIXER) and stirred at 5,000 to 6,000 rpm for 3 to 8 minutes to prepare a first ampoule composition.

Here, the sodium polystyrene sulfonate can strengthen skin wrinkles and elasticity, and improve long-term storage stability.

If sodium polystyrene sulfonate is less than 10 wt% compared to the total weight of the first ampoule composition, the effect of pulling the skin and improving elasticity and wrinkles may be minimal, and if it exceeds 70 wt%, the viscosity may increase excessively and the feeling of use may not be good, so the range is limited. It is desirable to use it in.

Here, Polysorbate 20 is a polysorbate-type nonionic surfactant formed by ethoxylation of sorbitan monolaurate, and is stable and relatively non-toxic.

Polysorbate 20 can adsorb to the interface of the composition containing the first ampoule composition and play an active role in uniformly dispersing the composition that is difficult to mix.

If the amount of Polysorbate 20 relative to the total weight of the first ampoule composition is less than 0.05 wt%, it may be difficult to perform its active role, and if it exceeds 0.15 wt%, skin rash may occur in people with sensitive skin. As hives may occur throughout the body, it is advisable to use it within a limited range.

Here, the Ammonium Acryloyldimethyltaurate/VP Copolymer is a polymer of acryloyldimethyltaurate and vinylpyrrolidone monomer, and is stable to UV and functions in a wide pH range. It is a polymer gelling agent that is soluble in water and has excellent dispersing ability. This can provide a soft skin texture.

If the amount of Ammonium Acryloyldimethyltaurate/VP Copolymer is less than 1 wt% compared to the total weight of the first ampoule composition, it may not be able to provide a soft skin texture, and if it exceeds 5 wt%, it may be excessive. Viscosity may increase, so it is desirable to use it within a limited range.

Here, the xanthan gum is a polysaccharide extracted from fermentation of carbohydrates, and the xanthan gum is extracted from glucose or corn syrup. It can increase viscosity and enhance spreadability.

If xanthan gum is less than 0.5 wt% compared to the total weight of the first ampoule composition, it may be difficult to enhance spreadability, and if it exceeds 1 wt%, the increase in viscosity may become excessive and may have a negative effect on spreadability, so it is preferable to use it within a limited range. do.

Here, the polyvinyl alcohol is a polymer made by chemical bonding in an aqueous solution. The polyvinyl alcohol is also used to control the feeling of use so that an instant lifting feeling can be perceived.

If the amount of polyvinyl alcohol relative to the total weight of the first ampoule composition is less than 0.2 wt%, it may be meaningless as an adjustment for perceiving a lifting feeling, and if it exceeds 0.3 wt%, the viscosity may become excessive, so it can be used within a limited range. It is desirable to do so.

Here, butylene glycol has two alcohol functional groups, and the molecule is classified as diol, and is a colorless, bitter-tasting water-soluble liquid. Although it is light, it is not sticky and plays a role in preventing the ampoule of the present invention from rotting, and in addition, it can make the skin soft and moist due to its moisture-attracting properties.

If the amount of butylene glycol is less than 5 wt% relative to the total weight of the first ampoule composition, the effect of preventing rot and keeping the skin soft and moist due to its moisture-attracting properties may be minimal, and if the amount of butylene glycol is less than 5 wt%, the effect of soft and moisturizing the skin may be minimal. If it exceeds it, there is no significant change, so it is an economic loss.

Here, the ethylhexylglycerin or octoxyglycerin is a glyceryl ether commonly used as part of a preservative system in cosmetic preparations. This moisturizes the skin by retaining moisture, inhibits bacterial growth and also provides conditioning.

If the amount of ethylhexylglycerin relative to the total weight of the first ampoule composition is less than 1 wt%, the effect of retaining moisture and moisturizing the skin, inhibiting bacterial growth, and providing conditioning is minimal, and if it exceeds 5 wt%, there is a significant change accordingly. There is no economic loss.

Here, Disodium EDTA is a water-soluble component combined with two sodium ions in the existing EDTA component, and helps prevent quality deterioration by preventing rancidity caused by metal ions or air that may be mixed in during the manufacturing process. performs the role of giving.

If the disodium EDTA is less than 0.01 wt% compared to the total weight of the first ampoule composition, the effect of preventing quality degradation may be minimal, and if it exceeds 0.05 wt%, it may cause calcium deficiency by combining with metals beneficial to the body such as calcium and zinc due to the nature of EDTA. Alternatively, cells and enzymes may not be able to perform their duties properly, and the adsorption capacity of other ingredients may increase, which may increase the possibility of harmful substances penetrating the skin, so it is advisable to use it within a limited range.

Here, the propanediol is fermented and extracted from non-GMO (non-genetically modified) corn and is a non-irritating and non-toxic ingredient. It provides conditioning to the skin and has the ability to retain moisture, thereby improving skin moisturization and helping to maintain moist skin. It also helps stabilize the emulsification of other ingredients that do not mix with each other, and has a slight preservative effect, so it also serves as a quality protection maintainer. do.

If the propanediol is less than 2 wt% compared to the total weight of the first ampoule composition, it may not be used for the above-mentioned effects and for the above-mentioned purposes, and if it exceeds 5 wt%, there will be no special effect, so it is recommended to use it within a limited range. desirable.

Here, 1,2-hexanediol is a C6 polyol material with an -OH group attached to the 1,2 position, and serves as a moisturizer.

If the 1-2 hexanediol is less than 0.01 wt% based on the total weight of the first ampoule composition, the moisturizing effect may be reduced, and if it exceeds 0.02 wt%, there is no special effect, resulting in an economic loss.

Here, the camellia flower extract is extracted from the flowers of the camellia tree Camellia Japonica and can protect the skin from internal and external stimulation, preventing the skin from forming wrinkles and turning dull.

If the amount of camellia flower extract relative to the total weight of the first ampoule composition is less than 0.2 wt%, the effect of preventing wrinkles from becoming dull may be minimal, and if it exceeds 1 wt%, it may irritate the skin, so it is recommended to use it within a limited range. desirable.

Here, the black mulberry fruit extract is extracted from the fruit of the black mulberry tree Morus nigra. The black mulberry fruit extract reduces the melanin content produced by alpha-MSH in a concentration-dependent manner and has positive effects related to skin whitening, such as skin pigmentation and skin tone improvement. It can have an effect.

If the amount of black mulberry fruit extract is less than 0.2 wt% based on the total weight of the first ampoule composition, the skin improvement effect may be minimal, and 1 wt% may cause skin problems, so it is preferable to use it within a limited range.

Here, the propolis extract is a mixture of resinous substances that bees collect from plants such as tree buds or sap. This can be achieved through a micelle extraction method using a synthetic emulsifier, an eco-friendly extraction method using natural substances as a solvent, or It can be extracted using an alcohol extraction method, and can soothe the skin and make it shiny.

If the amount of the propolis extract relative to the total weight of the first ampoule composition is less than 0.2 wt%, the skin soothing and gloss enhancing effect may be minimal, and if it exceeds 1 wt%, it may cause trouble, so it is preferable to use it within a limited range.

Here, the rosehip fruit extract is extracted from the fruit of the wild rose, has a fragrant scent, and contains vitamins B, C, E and unsaturated fatty acids that revitalize the skin.

If the rosehip fruit extract is less than 0.2 wt% relative to the total weight of the first ampoule composition, the effect of vitamins B, C, E and unsaturated fatty acids in revitalizing the skin is minimal, and if it exceeds 1 wt%, the content of other ingredients will vary accordingly. This decreases, so it is desirable to use it within a limited range.

Here, the vitamin tree fruit extract is extracted from the fruit of the vitamin tree Hippophae rhamnoides and has the effect of improving skin eye wrinkles, facial cheek lifting, skin elasticity, skin density, skin tone, freckles, and pigmentation relief.

If the amount is less than 0.2 wt% based on the total weight of the first ampoule composition, the effects presented above may be minimal, and if it exceeds 1 wt%, the content of other ingredients is reduced accordingly, so it is preferable to use it within a limited range.

Here, the Serolta cherry tree flower extract is a skin conditioning agent extracted from the flowers of Prunus serrulata and plays a role in improving skin elasticity.

If the Serolta cherry blossom extract is less than 0.2 wt% compared to the total weight of the first ampoule composition, it may be difficult to perform the role of improving skin elasticity, and if it exceeds 1 wt%, the content of other ingredients is reduced accordingly, making it suitable for use in a limited range. It is desirable.

Here, the peach tree flower extract is extracted from the flowers of the peach tree (Peach) Prunus persica, and has an excellent ability to supply nutrients to the skin, playing a conditioning role and suppressing melanin production to create a bright skin tone.

If the amount of the peach tree flower extract relative to the total weight of the first ampoule composition is less than 0.2 wt%, the effect of brightening the skin tone may be minimal, and if it exceeds 1 wt%, there is no special effect and it is unnecessary, so it is preferable to use it within a limited range. .

Here, the royal jelly extract is an oily substance secreted by the other glands developing into sac glands only during the period when worker bees raise larvae, and is an extract extracted from royal jelly. It forms a film on the skin and gently envelops it, and has the function of supplying and fixing moisture to the skin, improving moisturized skin.

If the amount of the royal jelly extract relative to the total weight of the first ampoule composition is less than 0.2 wt%, the effect of improving moisturized skin due to its function of supplying and fixing moisture to the skin is minimal, and if it exceeds 1 wt%, it may cause trouble. It is desirable to use it within the range.

Here, the port marigold flower extract is extracted from the flowers of the port marigold Calendula Officinalis, and promotes the circulation of the skin cycle, plays a role in gently soothing sensitive and sensitive skin, and reduces the activity of harmful substances in the skin. It plays a role in conditioning the skin, improving and managing healthy skin, and providing skin regeneration and wound healing.

If the pot marigold flower extract is less than 0.2 wt% compared to the total weight of the first ampoule composition, the effects presented above may be minimal, and if it exceeds 1 wt%, there is no special effect, so it is preferable to use it within a limited range.

Here, the fragrance may be any one selected from animal, vegetable, natural or synthetic fragrances, and is not particularly limited, but lavender fragrance extracted from lavender flowers, which is a vegetable fragrance, is preferably used. In addition, it is used in the range of 0.01 to 0.02 wt% based on the total weight of the first ampoule composition.

Here, the sodium acetate is the sodium salt of acetic acid and serves as a preservative. It is used in the range of 0.1 to 0.5 wt% based on the total weight of the first ampoule composition.

Here, Linalool refers to two optical isomers of naturally occurring terpene alcohols found in numerous flowers and spice plants. Linalool can boost the overall scent, making the scent last longer.

If the amount is less than 0.01 wt% compared to the total weight of the first ampoule composition, it may be difficult to make the lingering scent last for a long time, and if it exceeds 0.02 wt%, the user may experience side effects such as memory loss, so it is preferable to use it within a limited range.

Here, the hexyl cinnamal (Hexyl Cinnamal), which is also called jasmonal, hexyl cinnamaldehyde, and cinnamic aldehyde, exists in a light yellow transparent liquid state and is used as a flavoring agent in the present invention.

If the hexylnamal is less than 0.01 wt%, it may be difficult to function as a flavoring agent, and if it exceeds 0.02 wt%, side effects may occur, so it is preferable to use it within a limited range.

Here, Alpha-Isomethyl Ionone is a flavoring agent and is used in the range of 0.01 to 0.02 wt% based on the total weight of the first ampoule composition.

Here, adenosine is a chemical substance that combines adenine and ribose, and plays a significant role in improving wrinkles and promoting collagen synthesis in the dermal layer, alleviating wrinkles and restoring elasticity.

If the adenosine is less than 0.01 wt%, the skin elasticity effect may be reduced, and if it exceeds 1 wt%, it may cause trouble, so it is preferable to use it within a limited range.

Additionally, specifically, 31.95 wt% of purified water, 40 wt% of sodium polystyrene sulfonate, 0.05 wt% of polysorbate 20, 1 wt% of ammonium acryloyl dimethyl taurate/V picopolymer, 0.5 wt% of xanthan gum, polyvinyl. Alcohol 0.3 wt%, butylene glycol 10 wt%, ethylhexylglycerin 5 wt%, disodium EDTA 0.01 wt%, propanediol 2 wt%, 1-2 hexanediol 0.01 wt%, camellia flower extract 1 wt%, black mulberry fruit extract 1 wt%, propolis extract 1 wt%, rosehip fruit extract 1 wt%, vitamin tree fruit extract 1 wt%, serolta cherry tree flower extract 1 wt%, peach tree flower extract 1 wt% , royal jelly extract 1 wt%, port marigold flower extract 1 wt%, fragrance 0.01 wt%, sodium acetate 0.1 wt%, linalool 0.01 wt%, hexyl cinnamal 0.01 wt%, alpha-isomethyl ionone 0.01 wt% A first ampoule composition containing 0.04 wt% of adenosine was added to a stirrer (HOMO MIXER) and stirred at 5,000 rpm for 8 minutes to prepare a first ampoule composition.

[Step of manufacturing the second ampoule composition (S2)]

Lotus leaf 1 ~ 30 wt%, hydrangea leaf 1 ~ 30 wt%, pine needle 1 ~ 30 wt%, banana leaf 1 ~ 30 wt%, moringa leaf 1 ~ 30 wt%, dill leaf 1 ~ 30 wt%, amaranth leaf 1 ~ A second mixture is prepared by mixing 30 wt%, 1 to 30 wt% of ramie leaves, 1 to 30 wt% of okra leaves, and 1 to 30 wt% of arrowroot leaves.

After mixing 30 to 40 wt% of the second mixture with 60 to 70 wt% of distilled water, the second extract is prepared by shaking extraction for 10 to 15 hours at 30 to 70°C and 140 to 200 rpm.

After centrifuging the second extract for 10 to 30 minutes at 7,000 to 9,000 rpm in a centrifuge, the supernatant was filtered and the filtrate was evaporated under reduced pressure evaporator (vacuum rotation evaporator) for 5 to 7 hours under conditions of 0.1 to 0.3 mPA. A second ampoule composition is prepared by concentrating under reduced pressure.

Here, lotus leaf is a perennial herb with an underground stem that crawls in the soil. At the end of fall, the tip grows larger to form lotus root. Lotus leaves are used for edible and medicinal purposes, and the stems (lotus roots) of the lotus are often used as food.

Lotus leaf tea contains a large amount of various antioxidant ingredients such as polyphenols and flavonoids, which can help prevent and prevent skin aging by eliminating free radicals, which are major factors that accelerate aging, and helping with cell regeneration.

If the amount of the lotus leaf relative to the total weight of the second mixture is less than 1 wt%, the anti-aging effect may be minimal, and if it exceeds 30 wt%, there is no special effect, resulting in an economic loss.

Here, the hydrangea is a reed-leafed bush native to East Asia. Hydrangea flowers are called bundanhwa or hydrangea flower, and are also called hydrangea or octopus flower in relation to Baekui. Here, hydrangea leaves are very excellent in moisturizing the skin.

If the amount of hydrangea leaves compared to the total weight of the second mixture is less than 1 wt%, the moisturizing effect may be minimal, and if it exceeds 30 wt%, it may have a negative effect, so it is preferable to use it within a limited range.

Here, the pine needle 'pine' in pine means 'best', meaning that pine is the best tree among trees. Because the tree trunk is red, it is called ‘red pine’, and because it grows mainly in inland areas, it is also called ‘yuk pine’.

Pine needles contain esters, phenols, glycoginine, turpentine, vitamins A, C, K, and chlorophyll, which eliminate oxygen radicals and prevent aging and acne by inhibiting the consumption and damage of antioxidants caused by oxidative stress within cells. It can be effective in improving.

If the pine needles are less than 1 wt% compared to the total weight of the second mixture, the effect in preventing aging and improving acne may be minimal by scavenging the above-mentioned free radicals and suppressing the consumption and damage of antioxidants due to oxidative stress within cells. , exceeding 30 wt% may actually cause skin diseases, so it is advisable to use it within a limited range.

Banana is a plant belonging to the Panaceae family of the ginger order and is mainly produced and cultivated in the Philippines, Malaysia, and Thailand.

Allantoin contained in the banana leaves used in the present invention can remove dead skin cells from the skin.

If the amount of the banana leaf relative to the total weight of the second mixture is less than 1 wt%, the effect of removing dead skin cells may be minimal, and if it exceeds 30 wt%, the phytochemical contained in the banana leaf is closely related to enhancing male sexual desire. This can cause skin side effects if used excessively, so it is advisable to use it within the limited range given above.

Here, the Moringa is a deciduous tree of the Moringa family. It is the most widely cultivated species among the Moringa genus, the only genus of the Moringa family.

Moringa leaves used in the present invention are rich in beta-carotene, protein, vitamin C, calcium, etc., and have a soothing effect in healing skin inflammation and skin troubles.

If the moringa leaf is less than 1 wt% compared to the total weight of the second mixture, the soothing effect in curing skin inflammation and skin troubles may be minimal, and if it exceeds 30 wt%, side effects may be caused. It is desirable to use it within a limited range.

Here, the dill is a type of herb, and is called a perennial herb or an annual herb depending on where it grows. It is the only species of the genus Anethum, and is also called syrah and small fennel.

If the amount of dill leaves compared to the total weight of the second mixture is less than 1 wt%, the effect on scent expression may be minimal, and if it exceeds 30 wt%, the scent may be too strong and may have a negative effect on the scent, so it is best to use it in a limited range. .

Amaranth is also called Amaranth grain, and Amaranth is a genus of the Amaranth family. It consists of annual, biennial, or short-lived perennial plants and is distributed worldwide. Flowers of the cyme inflorescence, similar to the inflorescence, bloom in summer or fall.

The amaranth leaves used in the present invention can greatly help prevent skin aging by removing free radicals, which can be said to be the main cause of disease, due to the strong antioxidant effect of squalene contained in large amounts.

If the amount of amaranth leaves is less than 1 wt% compared to the total weight of the second mixture, it may be difficult to achieve an antioxidant effect, and if it exceeds 30 wt%, it may cause trouble, so it is preferable to use it in a limited range.

Here, the above-mentioned plant is a perennial plant belonging to the Nettle family of the dicotyledonous plant Nettle family and native to Southeast Asia.

Ramie leaves used in the present invention are rich in moisture, protein, fat, manganese and amino acids, which are helpful for skin care because they help collagen production.

If the ramie leaf is less than 1 wt% compared to the total weight of the second mixture, the improvement in skin beauty may be minimal, and if it exceeds 30 wt%, it has no special meaning and is used in a limited range.

Okra is an angiosperm belonging to the Malvaceae family. The green-colored Jongsilhyeop is edible. The geographical origin of okra is known to be South Asia, Ethiopia, and West Africa. This plant is cultivated worldwide in tropical, subtropical, and warm climate regions.

If the okra leaves used in the present invention are less than 1 wt% compared to the total weight of the second mixture, the effect to help prevent skin aging may be minimal, and if it exceeds 30 wt%, the okra leaves may have a negative effect. It is desirable to use it within a limited range.

The arrow tree is a plant from the vine family. The scientific name is Euonymus alatus. The genus names are Homorrhoids, Quercus, Quercus, and Chambic. Arrow tree leaves have excellent anti-inflammatory properties and are effective against skin diseases such as acne. They also relieve itching and have a skin-soothing effect.

If the amount of arrowroot leaves relative to the total weight of the second mixture is less than 1 wt%, the effect may be minimal, and if it exceeds 30 wt%, the content of other ingredients is reduced accordingly, so it is preferable to use it within a limited range.

In addition, more specifically, 20 wt% lotus leaves, 20 wt% hydrangea leaves, 20 wt% pine needles, 10 wt% banana leaves, 1 wt% moringa leaves, 1 wt% dill leaves, 5 wt% amaranth leaves, 21 wt% ramie leaves. %, 1 wt% of okra leaves, and 1 wt% of arrowroot leaves are mixed to prepare a second mixture.

30 wt% of the second mixture is mixed with 70 wt% of distilled water, and then extracted by shaking for 15 hours at 70°C and 200 rpm to prepare the second extract.

After centrifuging the second extract in a centrifuge at 7,000 rpm for 30 minutes, the supernatant was filtered and the filtrate was concentrated under reduced pressure with a vacuum rotation evaporator for 7 hours under conditions of 0.1 to 0.3 mPA to produce a second ampoule. A composition is prepared.

[Step of manufacturing third ampoule composition (S3)]

Cheongung 1 ~ 30 wt%, Baekbokryeong 1 ~ 30 wt%, Angelica 1 ~ 30 wt%, Elm bark 1 ~ 30 wt%, Black garlic 1 ~ 30 wt%, Lotus root 1 ~ 30 wt%, and Wasong 1 ~ 30 wt% A third mixture is prepared by mixing %.

After mixing 30 to 40 wt% of the third mixture with 60 to 70 wt% of distilled water, the third extract is prepared by shaking extraction for 10 to 15 hours at 30 to 70 ° C. and 140 to 200 rpm.

After centrifuging the third extract for 10 to 30 minutes at 7,000 to 9,000 rpm in a centrifuge, the supernatant was filtered and the filtrate was evaporated in a vacuum rotation evaporator for 5 to 7 hours under conditions of 0.1 to 0.3 mPA. A third ampoule composition prepared by concentration under reduced pressure is prepared.

Here, the Cheongung is a medicinal herb from the Angelica family. The Cheongung contains ingredients such as vitamin E, essential oil, alkaloids, and phenolic components. It can also remove skin blemishes and relieve various skin problems.

If the amount of the above-mentioned skin is less than 1 wt% compared to the total weight of the third mixture, the effect of removing skin blemishes and alleviating various skin troubles may be minimal, and if it exceeds 30 wt%, it may have adverse effects, so it is used in a limited range.

Baekbokryeong is also called White Pine Pungpyeong. It grows and is cultivated in areas where pine trees have been cut down throughout Korea. It is parasitic on the roots of pine trees and grows like a lump. It can be collected by piercing the area around the pine stump with a skewer.

Baekbokryeong's rich organic acids and lecithin ingredients are effective in suppressing skin aging, improving skin elasticity, and eliminating blemishes such as freckles and freckles.

If the amount of Baekbokryeong relative to the total weight of the third mixture is less than 1 wt%, the effect of alleviating arthritis symptoms may be reduced, and if it exceeds 30 wt%, there are no significant side effects, but the content of other ingredients is reduced, so it is preferable to use it within a limited range.

Angelica is a perennial plant belonging to the Apiaceae family and is distributed in Korea, China, and Japan. For reference, it is also called new gamchae. The height is about 1 to 2 m, the entire stem is purple and has a lot of fragrance. The flowers are purple and bloom in clusters in compound umbels from August to September. They have the effect of improving skin wrinkles, pigmentation, and skin tone.

If angelica root is less than 1 wt% compared to the total weight of the third mixture, the skin tone improvement effect may be minimal, and if it exceeds 30 wt%, there is no better effect and it is meaningless, so it is preferable to use it within a limited range.

The elm tree is a plant in the elm family of the rose order. The scientific name is Ulmus davidiana var. japonica. The present invention uses the elm bark and is rich in antioxidants called phytosterols, which can help improve acne-prone skin.

If the elm bark is less than 1 wt% compared to the total weight of the third mixture, the efficacy in soothing skin troubles and acne, etc. may be reduced, and if it exceeds 30 wt%, it may have a negative effect, so it is recommended to use it within a limited range. desirable.

Black garlic is made from raw garlic through a fermentation and aging process rather than baking or boiling it. It contains sulfur, which has strong antioxidant properties, and has the effect of giving skin elasticity and moisturizing and improving shine.

If the amount of black garlic compared to the total weight of the third mixture is less than 1 wt%, the effect of giving elasticity to the skin and improving moisturizing and gloss may be minimal, and if it exceeds 30 wt%, it has no special effect and is therefore meaningless.

Lotus root is the same as the commonly called lotus root, and the vitamin C and pectin it contains remove blemishes, blemishes, and acne from the skin, and provide nutrients to the skin to maintain elastic skin.

If the amount of lotus root compared to the total weight of the third mixture is less than 1 wt%, the proposed effect may be minimal, and if it exceeds 30 wt%, there is no special effect, resulting in an economic loss.

In late fall, the flower of the Japanese pine is like a tower, with small white flowers that grow in the shape of spikes. During the winter, the long, thin leaves lose their traces and instead form a rosette filled with short, hard leaves and overwinter. Small, short leaves form a rosette. It appears in various forms depending on the growing conditions. It is rich in physiologically active substances and helps relieve skin irritation and stress. If the amount of Wasong is less than 1 wt% compared to the total weight of the third mixture, it may not be able to help relieve skin irritation, and if it exceeds 30 wt%, it has no special effect, so it is preferable to use it in a limited range.

More specifically, a third mixture was prepared by mixing 20 wt% of Cheongung, 20 wt% of Baekbokryeong, 20 wt% of Angelica, 10 wt% of elm bark, 10 wt% of black garlic, 10 wt% of lotus root, and 10 wt% of Japanese pine. do.

After mixing 30 wt% of the third mixture with 70 wt% of distilled water, the third extract was prepared by shaking extraction for 15 hours at 70°C and 200 rpm.

The third extract was centrifuged at 9,000 rpm for 30 minutes in a centrifuge, and then the supernatant was filtered and the filtrate was concentrated under reduced pressure with a vacuum rotation evaporator for 5 hours under conditions of 0.1 to 0.3 mPA. Prepare 3 ampoule composition.

[Step of preparing the final ampoule composition (S4)]

90 to 95 wt% of the first ampoule composition; 1 to 5 wt% of the second ampoule composition; and 1 to 5 wt% of the third ampoule composition; to prepare the final ampoule composition.

More specifically, 95 wt% of the first ampoule composition and 2.5 wt% of the second ampoule composition; and 2.5 wt% of the third ampoule composition; to prepare the final ampoule composition.

[Step of going through high pressure emulsification process (S5)] I [Step of aging (S6)]

After stirring the final ampoule composition at 2,000 to 3,000 rpm for 2 to 3 minutes, the stirred liquid is subjected to a high pressure emulsification process 2 to 3 times under conditions of 700 to 1,100 bar using a high pressure emulsifier.

More specifically, the final ampoule composition is stirred at 3,000 rpm for 3 minutes, and then the stirred liquid is subjected to a high-pressure emulsification process twice at 1000 bar using a high-pressure emulsifier.

After cooling the final ampoule composition that has undergone the high-pressure emulsification process, it is aged at room temperature for 30 to 40 hours to prepare the lifting ampoule of Example 1, which improves skin elasticity and wrinkles according to the present invention.

In addition, the method of using the lifting ampoule of the present invention is that after use, the user spreads an appropriate amount on the face and washes it off with lukewarm water after 20 minutes when it has elasticity.

Additionally, Example 2 is characterized in that it may contain more conchiolin powder compared to Example 1.

,

The conchiolin powder,

Pearl powder is manufactured by crushing pearls using a crushing machine,

A mixture of 20 to 30 wt% of the pearl powder and 70 to 80 wt% of distilled water is pulverized through a grinding machine, and the moisture is evaporated to prepare pearl powder,

After mixing 1 to 10 wt% of the pearl powder with 90 to 99 wt% of acetic acid, the mixture was decalcified by stirring at 37 to 39°C for 8 to 14 hours, and then the mixture was stirred for 5 to 15 minutes for 10 to 15 hours. Centrifuge at 7000 rpm at ℃ to generate precipitate,

Conchiolin powder was prepared by washing 30 to 40 wt% of the resulting precipitate with 60 to 70 wt% of distilled water and freeze-drying,

It is characterized in that it is manufactured by adding 20 to 30 wt% of citric acid solution to 70 to 80 wt% of the conchiolin powder into a grinding machine, stirring for 10 to 15 minutes at 34 to 37°C, and then freeze-drying again.

More specifically,

Purified water 10 ~ 70 wt%, sodium polystyrene sulfonate 10 ~ 70 wt%, polysorbate 20 0.05 ~ 0.15 wt%, ammonium acryloyl dimethyl taurate/V picopolymer 1 ~ 5 wt%, xanthan gum 0.5 ~ 1 wt%, polyvinyl alcohol 0.2 ~ 0.3 wt%, butylene glycol 5 ~ 10 wt%, ethylhexylglycerin 1 ~ 5 wt%, disodium EDTA 0.01 ~ 0.05 wt%, propanediol 2 ~ 5 wt% , 1-2 hexanediol 0.01 ~ 0.02 wt%, camellia flower extract 0.2 ~ 1 wt%, black mulberry fruit extract 0.2 ~ 1 wt%, propolis extract 0.2 ~ 1 wt%, rosehip fruit extract 0.2 ~ 1 wt% , Vitamin tree fruit extract 0.2 ~ 1 wt%, Cerolta cherry tree flower extract 0.2 ~ 1 wt%, Aspen tree flower extract 0.2 ~ 1 wt%, Royal jelly extract 0.2 ~ 1 wt%, Port marigold flower extract 0.2 ~ 1 wt %, fragrance 0.01 ~ 0.02 wt%, sodium acetate 0.1 ~ 0.5 wt%, linalool 0.01 ~ 0.02 wt%, hexylcinnamal 0.01 ~ 0.02 wt%, alpha-isomethyl ionone 0.01 ~ 0.02 wt%, and adenosine 0.01 ~ 1 A first ampoule composition prepared by adding the first mixture of wt% to a stirrer (HOMO MIXER) and stirring it at 5,000 to 6,000 rpm for 3 to 8 minutes;

Lotus leaf 1 ~ 30 wt%, hydrangea leaf 1 ~ 30 wt%, pine needle 1 ~ 30 wt%, banana leaf 1 ~ 30 wt%, moringa leaf 1 ~ 30 wt%, dill leaf 1 ~ 30 wt%, amaranth leaf 1 ~ 30 wt% of the second mixture of 30 wt%, 1 ~ 30 wt% of ramie leaves, 1 ~ 30 wt% of okra leaves, and 1 ~ 30 wt% of arrowroot leaves was mixed with 60 ~ 70 wt% of distilled water. Then, a second extract was prepared by shaking extraction for 10 to 15 hours at 30 to 70°C and 140 to 200 rpm, and the second extract was centrifuged in a centrifuge at 7,000 to 9,000 rpm for 10 to 30 minutes. A second ampoule composition prepared by filtering the supernatant and concentrating the filtrate under reduced pressure with a vacuum rotation evaporator for 5 to 7 hours under conditions of 0.1 to 0.3 mPA;

Cheongung 1 ~ 30 wt%, Baekbokryeong 1 ~ 30 wt%, Angelica 1 ~ 30 wt%, Elm bark 1 ~ 30 wt%, Black garlic 1 ~ 30 wt%, Lotus root 1 ~ 30 wt%, and Wasong 1 ~ 30 wt% After adding 30 to 40 wt% of the third mixture mixed with 60 to 70 wt% of distilled water, the third extract was prepared by shaking extraction for 10 to 15 hours under conditions of 30 to 70 ℃ and 140 to 200 rpm. After centrifuging the third extract for 10 to 30 minutes at 7,000 to 9,000 rpm in a centrifuge, the supernatant was filtered and the filtrate was evaporated under vacuum rotation evaporator for 5 to 7 hours under conditions of 0.1 to 0.3 mPA. ) The third ampoule composition prepared by concentration under reduced pressure;

90 to 95 wt% of the first ampoule composition; 1 to 5 wt% of the second ampoule composition; and 1 to 5 wt% of the third ampoule composition to prepare the final ampoule composition,

After stirring 99 wt% of the final ampoule composition and 1 wt% of conchiolin powder for 3 minutes at 3,000 rpm, the stirred liquid was subjected to a high-pressure emulsification process three times at 1,100 bar using a high-pressure emulsifier,

After cooling the final ampoule composition that underwent the high-pressure emulsification process, it was aged at room temperature for 40 hours to prepare the lifting ampoule of Example 2.

The lifting ampoule of Example 2 may further include the conchiolin powder to maximize skin moisturizing and elasticity effects.

Hereinafter, we will look at specific test examples according to Example 3.

[Example 3]

First, 31.95 wt% of purified water, 40 wt% of sodium polystyrene sulfonate, 0.05 wt% of polysorbate 20, 1 wt% of ammonium acryloyl dimethyl taurate/Vpicopolymer, 0.5 wt% of xanthan gum, 0.3 wt of polyvinyl alcohol. %, butylene glycol 10 wt%, ethylhexylglycerin 5 wt%, disodium EDTA 0.01 wt%, propanediol 2 wt%, 1-2 hexanediol 0.01 wt%, camellia flower extract 1 wt% , black mulberry fruit extract 1 wt%, propolis extract 1 wt%, rosehip fruit extract 1 wt%, vitamin tree fruit extract 1 wt%, serolta cherry tree flower extract 1 wt%, peach tree flower extract 1 wt%, royal jelly Extract 1 wt%, port marigold flower extract 1 wt%, fragrance 0.01 wt%, sodium acetate 0.1 wt%, linalool 0.01 wt%, hexylcinnamal 0.01 wt%, alpha-isomethyl ionone 0.01 wt% and adenosine 0.04 The first ampoule composition mixed by wt% is put into a stirrer (HOMO MIXER) and stirred at 5,000 rpm for 8 minutes to prepare a first ampoule composition.

After that, lotus leaves 20 wt%, hydrangea leaves 20 wt%, pine needles 20 wt%, banana leaves 10 wt%, moringa leaves 1 wt%, dill leaves 1 wt%, amaranth leaves 5 wt%, ramie leaves 21 wt%, okra A second mixture is prepared by mixing 1 wt% of leaves and 1 wt% of arrowroot leaves.

30 wt% of the second mixture is mixed with 70 wt% of distilled water, and then extracted by shaking for 15 hours at 70°C and 200 rpm to prepare the second extract.

After centrifuging the second extract in a centrifuge at 7,000 rpm for 30 minutes, the supernatant was filtered and the filtrate was concentrated under reduced pressure with a vacuum rotation evaporator for 7 hours under conditions of 0.1 to 0.3 mPA to produce a second ampoule. A composition is prepared.

Afterwards, 20 wt% of Cheongung, 20 wt% of Baekbokryeong, 20 wt% of Angelica, 10 wt% of elm bark, 10 wt% of black garlic, 10 wt% of lotus root, and 10 wt% of Japanese pine were mixed to prepare a third mixture.

After mixing 30 wt% of the third mixture with 70 wt% of distilled water, the third extract was prepared by shaking extraction for 15 hours at 70°C and 200 rpm.

The third extract was centrifuged at 9,000 rpm for 30 minutes in a centrifuge, and then the supernatant was filtered and the filtrate was concentrated under reduced pressure with a vacuum rotation evaporator for 5 hours under conditions of 0.1 to 0.3 mPA. Prepare 3 ampoule composition.

Afterwards, 95 wt% of the first ampoule composition and 2.5 wt% of the second ampoule composition; and 2.5 wt% of the third ampoule composition; to prepare the final ampoule composition.

Thereafter, the final ampoule composition is stirred at 3,000 rpm for 3 minutes, and then the stirred liquid is subjected to a high-pressure emulsification process twice at 1000 bar using a high-pressure emulsifier.

Afterwards, the final ampoule composition that had undergone the high-pressure emulsification process was cooled and aged at room temperature for 30 hours to prepare the lifting ampoule of Example 3.

Test example 1

Among 40 women aged 30, 20 used the lifting ampoule of Example 3, and 20 used the lifting ampoule of Company A, which is commonly sold on the market.

The method of use in Example 3 was to apply a thin layer to the skin once a day for 30 days after washing the face every evening, and then repeat washing after 20 minutes. The degree of improvement in the skin condition after 30 days was measured by tube. The results are shown in Table 1. appeared in

In the comparative example, the method of use of company A's lifting ampoule was followed, and the degree of improvement in skin condition after 30 days was measured by tube, and the results are shown in Table 1.

division Improved skin condition Number of people
Example
very good 15 good night 3 is average 2 no effect at all 0 Comparison example


very good 10 good night 2 is average 6 no effect at all 2

As shown in Table 1, the lifting ampoule of the present invention was evaluated as having a generally excellent skin improvement effect, but in the case of Company A's ampoule, some had no effect, so the lifting ampoule of the present invention was judged to be generally superior.

In addition, after using the lifting ampoule of Example 3 of the present invention, among the 20 subjects, the women who showed particularly excellent results are shown in Figure 1.

The present invention adds skin elasticity within 20 minutes after application to the face, allowing the user to feel an immediate effect, and can positively improve the user's skin texture, wrinkles, freckles, skin tone, etc. overall, making it an industrial application. The possibility is very high.

Claims (5)

delete Purified water 10 ~ 70 wt%, sodium polystyrene sulfonate 10 ~ 70 wt%, polysorbate 20 0.05 ~ 0.15 wt%, ammonium acryloyl dimethyl taurate/V picopolymer 1 ~ 5 wt%, xanthan gum 0.5 ~ 1 wt%, polyvinyl alcohol 0.2 ~ 0.3 wt%, butylene glycol 5 ~ 10 wt%, ethylhexylglycerin 1 ~ 5 wt%, disodium EDTA 0.01 ~ 0.05 wt%, propanediol 2 ~ 5 wt% , 1-2 hexanediol 0.01 ~ 0.02 wt%, camellia flower extract 0.2 ~ 1 wt%, black mulberry fruit extract 0.2 ~ 1 wt%, propolis extract 0.2 ~ 1 wt%, rosehip fruit extract 0.2 ~ 1 wt% , Vitamin tree fruit extract 0.2 ~ 1 wt%, Cerolta cherry tree flower extract 0.2 ~ 1 wt%, Aspen tree flower extract 0.2 ~ 1 wt%, Royal jelly extract 0.2 ~ 1 wt%, Port marigold flower extract 0.2 ~ 1 wt %, fragrance 0.01 ~ 0.02 wt%, sodium acetate 0.1 ~ 0.5 wt%, linalool 0.01 ~ 0.02 wt%, hexylcinnamal 0.01 ~ 0.02 wt%, alpha-isomethyl ionone 0.01 ~ 0.02 wt%, and adenosine 0.01 ~ 1 A first ampoule composition prepared by adding the first mixture of wt% to a stirrer (HOMO MIXER) and stirring it at 5,000 to 6,000 rpm for 3 to 8 minutes;

Lotus leaf 1 ~ 30 wt%, hydrangea leaf 1 ~ 30 wt%, pine needle 1 ~ 30 wt%, banana leaf 1 ~ 30 wt%, moringa leaf 1 ~ 30 wt%, dill leaf 1 ~ 30 wt%, amaranth leaf 1 ~ A second mixture was prepared by mixing 30 wt%, 1 to 30 wt% of ramie leaves, 1 to 30 wt% of okra leaves, and 1 to 30 wt% of arrowroot leaves, and 30 to 40 wt% of the second mixture was mixed with 60 wt% of distilled water. After mixing at ~70 wt%, a second extract was prepared by shaking extraction for 10 to 15 hours at 30 to 70°C and 140 to 200 rpm, and the second extract was centrifuged at 7,000 to 9,000 rpm. A second ampoule composition prepared by centrifuging for 10 to 30 minutes, filtering the supernatant, and concentrating the filtrate under reduced pressure with a vacuum rotation evaporator for 5 to 7 hours under conditions of 0.1 to 0.3 mPA;

Cheongung 1 ~ 30 wt%, Baekbokryeong 1 ~ 30 wt%, Angelica 1 ~ 30 wt%, Elm bark 1 ~ 30 wt%, Black garlic 1 ~ 30 wt%, Lotus root 1 ~ 30 wt%, and Wasong 1 ~ 30 wt% % was mixed to prepare a third mixture, and 30 to 40 wt% of the third mixture was added to 60 to 70 wt% of distilled water, and then heated at 30 to 70°C and 140 to 200 rpm for 10 to 15 hours. A third extract was prepared by shaking extraction, the third extract was centrifuged in a centrifuge at 7,000 to 9,000 rpm for 10 to 30 minutes, and the supernatant was filtered and the filtrate was centrifuged for 5 to 7 minutes under conditions of 0.1 to 0.3 mPA. A third ampoule composition prepared by concentrating under reduced pressure with a vacuum rotation evaporator for a period of time;

90 to 95 wt% of the first ampoule composition, 1 to 5 wt% of the second ampoule composition; and 1 to 5 wt% of the third ampoule composition to prepare the final ampoule composition,
After stirring the final ampoule composition at 2,000 to 3,000 rpm for 2 to 3 minutes, the stirred liquid was subjected to a high pressure emulsification process 2 to 3 times under conditions of 700 to 1,100 bar using a high pressure emulsifier,
A lifting ampoule composition that improves skin elasticity and wrinkles, produced by cooling the final ampoule composition that has undergone the high-pressure emulsification process and then aging it at room temperature for 30 to 40 hours.
Purified water 10 ~ 70 wt%, sodium polystyrene sulfonate 10 ~ 70 wt%, polysorbate 20 0.05 ~ 0.15 wt%, ammonium acryloyl dimethyl taurate/V picopolymer 1 ~ 5 wt%, xanthan gum 0.5 ~ 1 wt%, polyvinyl alcohol 0.2 ~ 0.3 wt%, butylene glycol 5 ~ 10 wt%, ethylhexylglycerin 1 ~ 5 wt%, disodium EDTA 0.01 ~ 0.05 wt%, propanediol 2 ~ 5 wt% , 1-2 hexanediol 0.01 ~ 0.02 wt%, camellia flower extract 0.2 ~ 1 wt%, black mulberry fruit extract 0.2 ~ 1 wt%, propolis extract 0.2 ~ 1 wt%, rosehip fruit extract 0.2 ~ 1 wt% , Vitamin tree fruit extract 0.2 ~ 1 wt%, Cerolta cherry tree flower extract 0.2 ~ 1 wt%, Aspen tree flower extract 0.2 ~ 1 wt%, Royal jelly extract 0.2 ~ 1 wt%, Port marigold flower extract 0.2 ~ 1 wt %, fragrance 0.01 ~ 0.02 wt%, sodium acetate 0.1 ~ 0.5 wt%, linalool 0.01 ~ 0.02 wt%, hexylcinnamal 0.01 ~ 0.02 wt%, alpha-isomethyl ionone 0.01 ~ 0.02 wt%, and adenosine 0.01 ~ 1 A step (S1) of preparing a first ampoule composition by adding the first mixture mixed by wt% to a stirrer (HOMO MIXER) and stirring it at 5,000 to 6,000 rpm for 3 to 8 minutes,

Lotus leaf 1 ~ 30 wt%, hydrangea leaf 1 ~ 30 wt%, pine needle 1 ~ 30 wt%, banana leaf 1 ~ 30 wt%, moringa leaf 1 ~ 30 wt%, dill leaf 1 ~ 30 wt%, amaranth leaf 1 ~ A second mixture was prepared by mixing 30 wt%, 1 to 30 wt% of ramie leaves, 1 to 30 wt% of okra leaves, and 1 to 30 wt% of arrowroot leaves, and 30 to 40 wt% of the second mixture was mixed with 60 wt% of distilled water. After mixing at ~70 wt%, a second extract was prepared by shaking extraction for 10 to 15 hours at 30 to 70°C and 140 to 200 rpm, and the second extract was centrifuged at 7,000 to 9,000 rpm. After centrifuging for 10 to 30 minutes, the supernatant was filtered and the filtrate was concentrated under reduced pressure with a vacuum rotation evaporator for 5 to 7 hours under conditions of 0.1 to 0.3 mPA to prepare a second ampoule composition ( S2) Wow,

Cheongung 1 ~ 30 wt%, Baekbokryeong 1 ~ 30 wt%, Angelica 1 ~ 30 wt%, Elm Bark 1 ~ 30, Black Garlic 1 ~ 30 wt%, Lotus root 1 ~ 30 wt%, and Japanese Pine 1 ~ 30 wt%. Prepare a third mixture by mixing, add 30 to 40 wt% of the third mixture to 60 to 70 wt% of distilled water, and shake and extract for 10 to 15 hours at 30 to 70°C and 140 to 200 rpm. A third extract was prepared, and the third extract was centrifuged in a centrifuge at 7,000 to 9,000 rpm for 10 to 30 minutes, and then the supernatant was filtered and the filtrate was centrifuged for 5 to 7 hours under conditions of 0.1 to 0.3 mPA. A step (S3) of producing a third ampoule composition prepared by concentrating under reduced pressure with a vacuum rotation evaporator,

Preparing a final ampoule composition by mixing 90 to 95 wt% of the first ampoule composition, 1 to 5 wt% of the second ampoule composition, and 1 to 5 wt% of the third ampoule composition (S4);

After stirring the final ampoule composition at 2,000 to 3,000 rpm for 2 to 3 minutes, the stirred liquid is subjected to a high pressure emulsification process 2 to 3 times at 700 to 1,100 bar using a high pressure emulsifier (S5);

A lifting ampoule manufacturing method for improving skin elasticity and wrinkles, comprising the step of cooling the final ampoule composition that has undergone the high-pressure emulsification process and then maturing it at room temperature for 30 to 40 hours (S6).
In claim 3,
The final ampoule composition is,
Lifting ampoule manufacturing method for improving skin elasticity and wrinkles, characterized in that it may further contain conchiolin powder
In claim 4,
Conchiolin powder,
Pearl powder is manufactured by crushing pearls using a crushing machine,
A mixture of 20 to 30 wt% of the pearl powder and 70 to 80 wt% of distilled water is pulverized through a grinding machine, and the moisture is evaporated to prepare pearl powder,
After mixing 1 to 10 wt% of the pearl powder with 90 to 99 wt% of acetic acid, the mixture was decalcified by stirring at 37 to 39°C for 8 to 14 hours, and then the mixture was stirred for 5 to 15 minutes for 10 to 15 hours. Centrifuge at 7000 rpm at ℃ to generate precipitate,
Conchiolin powder was prepared by washing 30 to 40 wt% of the resulting precipitate with 60 to 70 wt% of distilled water and freeze-drying,
Skin elasticity product prepared by adding 20 to 30 wt% of citric acid solution to 70 to 80 wt% of the conchiolin powder into a grinding machine, stirring for 10 to 15 minutes at 34 to 37°C, and then freeze-drying again. and lifting ampoule manufacturing method to improve wrinkles