KR102514942B1 - A cosmetic composition using a herbal medicine extract obtained by mixing nano bubbles and a herbal medicine extract prepared by mixing the nano bubble - Google Patents

Abstract

The present invention relates to a cosmetic composition using a herbal medicine extract mixed with nanobubbles and an apparatus for manufacturing a cosmetic composition using a herbal medicine extract mixed with the nanobubbles. According to the cosmetic composition using the herbal medicine extract mixed with nanobubbles and the manufacturing apparatus for the cosmetic composition using the herbal medicine extract mixed with the nanobubbles according to one aspect of the present invention, the cosmetic composition using the herbal medicine extract mixed with the nanobubbles An apparatus for manufacturing a cosmetic composition using the herbal medicine extract mixed with the nanobubbles and using the herbal medicine extract mixed with the nanobubbles includes the storage tank, the nanobubble generating member, the moving member, and the storage tank-side moving member. According to the inclusion, there is an advantage that the efficacy can be continued for a long time by improving the permeability of the skin while using the herbal medicine extract, which is a natural substance.

Description

A cosmetic composition using a herbal medicine extract obtained by mixing nano bubbles and a herbal medicine extract prepared by mixing the nano bubble}

The present invention relates to a cosmetic composition using a herbal medicine extract mixed with nanobubbles and an apparatus for manufacturing the cosmetic composition using a herbal medicine extract mixed with the nanobubbles.

In modern society, the level of income has risen relatively, but stress has increased proportionally and environmental pollution has become serious, so modern people have a lot of concerns about their health. ) culture was formed.

In addition, since modern people are accustomed to the well-being culture from their youth, they have become highly interested in health and beauty even in their old age. A cosmetics market for aging is being formed.

In order to satisfy the desire of consumers who want such well-aging, functional cosmetics, cosmetics based on the concept of naturalism, and oriental oriental herbal cosmetics are growing as major areas of the cosmetics industry, and various research and development are being conducted accordingly. It is being done.

What can be presented as an example of the invention of these cosmetics are those of the patent documents presented below.

However, cosmetic compositions using conventional natural substances, including the patent documents below, have active ingredients for skin diseases and skin improvement, but have a problem in that their efficacy lasts for a short time due to relatively poor permeability of the skin. .

Registered Patent No. 10-1192629, Registration date: 2012.10.12. Title of invention: Composition for preventing and treating atopic dermatitis derived from domestic native plants Registered Patent No. 10-0585444, Registration Date: 2006.05.24. Title of Invention: Cosmetics for preventing skin aging and improving acne using herbal medicines

The present invention is a cosmetic composition using herbal medicine extract mixed with nanobubbles, which can improve skin permeability while using herbal medicine extract, which is a natural substance, so that the effect can last for a long time, and manufacture of a cosmetic composition using herbal medicine extract mixed with nanobubbles One object is to provide a device.

Cosmetic composition using a herbal medicine extract mixed with nanobubbles according to an aspect of the present invention is a herbal medicine extract extracted by applying heat after supplying herbal medicine to an extraction solvent in which lava seawater and ethanol are mixed at a ratio of 60: 40 by volume It is obtained by mixing nano bubbles, and the herbal medicine is made by mixing dandelion sheath and loquat leaf, and the herbal medicine extract is added to the herbal medicine by 1.2 times the extraction solvent compared to the volume of the herbal medicine and 20 to 25 ° C. Extracted for 20 to 30 hours and then concentrated under reduced pressure to obtain a crude extract, and the crude extract obtained was firstly fractionated using water and butanol, and secondarily fractionated using hexane, followed by water and ethanol Characterized in that, after tertiary fractionation using polar solvent (15% aqM, aqueous methanol) mixed in a ratio of 15: 85 based on the volume, the polar solvent layer fraction dissolved in the polar solvent is extracted by concentrating under reduced pressure. do.

According to an aspect of the present invention, an apparatus for manufacturing a cosmetic composition using a herbal medicine extract mixed with nanobubbles supplies herbal medicine to an extraction solvent in which lava seawater and ethanol are mixed at a ratio of 60: 40 by volume, and then extracted by applying heat. To prepare a cosmetic composition using the herbal medicine extract mixed with the nano bubbles obtained by mixing the nano bubbles in the herbal medicine extract to be, a storage tank in which the herbal medicine extract is stored; Nano-bubble generation member for generating nano-bubbles in the herbal medicine extract; a moving member for moving the herbal medicine extract stored in the storage tank to the nano bubble generating member so that the nano bubbles are generated in the herbal medicine extract; And the nano-bubble generating member and the storage tank are connected, and the nano-bubble generated by the nano-bubble generating member is mixed to move the cosmetic composition using the herbal medicine extract mixed with the nano-bubble to the storage tank. A moving member on the storage tank side to do so, wherein the nano-bubble generating member includes a plurality of nano-bubble generating bodies in which the herbal medicine extract moved through the moving member is accommodated, and the nano-bubble generating body accommodated in each of the nano-bubble generating bodies A plurality of injection nozzle parts for spraying herbal medicine extracts, and the herbal medicine extract sprayed from each injection nozzle part and the herbal medicine extract mixed with the nano bubbles formed by mixing the nano bubbles generated while being sprayed from each injection nozzle part It includes a housing portion in which a cosmetic composition using is accommodated, and the spray nozzle portion is formed in a spiral shape converging toward the direction in which the herbal extract is sprayed, so that the herbal extract is sprayed in a radial form from the spray nozzle portion, and a plurality of the nano The bubble-generating body and the injection nozzle part are positioned while being spaced apart so that a certain portion of the herbal medicine extract sprayed in a radial form from each injection nozzle part crosses, and a part of the herbal medicine extract is sprayed so as to cross each other to cause collision, thereby causing a collision. The housing portion is characterized in that the cosmetic composition using the herbal medicine extract mixed with the nanobubbles can be accommodated.

According to the cosmetic composition using the herbal medicine extract mixed with nanobubbles and the manufacturing apparatus for the cosmetic composition using the herbal medicine extract mixed with the nanobubbles according to one aspect of the present invention, the cosmetic composition using the herbal medicine extract mixed with the nanobubbles An apparatus for manufacturing a cosmetic composition using the herbal medicine extract mixed with the nanobubbles and using the herbal medicine extract mixed with the nanobubbles includes the storage tank, the nanobubble generating member, the moving member, and the storage tank-side moving member. According to the inclusion, there is an effect that the efficacy can be continued for a long time by improving the permeability of the skin while using the herbal medicine extract, which is a natural substance.

1 is a view showing the extraction amount of the extract of dandelion sheath according to the extraction solvent conditions among the herbal extracts constituting the cosmetic composition using the herbal extract mixed with nanobubbles according to the first embodiment of the present invention.
Figure 2 is a view showing the extraction amount of the extract of bipayeop according to the extraction solvent conditions among the herbal medicine extracts constituting the cosmetic composition using the herbal medicine extract mixed with nano bubbles according to the first embodiment of the present invention.
Figure 3 is a view showing the appearance of the manufacturing apparatus of the cosmetic composition using the herbal medicine extract nanobubbles are mixed according to the first embodiment of the present invention.
4 is an enlarged view of part A of FIG. 3;
5 is a view showing the appearance of a nano-bubble generating member constituting the manufacturing apparatus of a cosmetic composition using a herbal medicine extract in which nano-bubbles are mixed according to a second embodiment of the present invention.

Hereinafter, with reference to the drawings, a cosmetic composition using a herbal medicine extract mixed with nanobubbles according to embodiments of the present invention and an apparatus for manufacturing a cosmetic composition using a herbal medicine extract mixed with nanobubbles will be described.

1 is a view showing the extraction amount of the extract of dandelion sentinel according to the extraction solvent conditions among the herbal extracts constituting the cosmetic composition using the herbal extract mixed with nanobubbles according to the first embodiment of the present invention, Figure 2 is the present invention 3 is a view showing the extraction amount of the extract of loquat leaf according to the extraction solvent conditions among the herbal medicine extracts constituting the cosmetic composition using the herbal medicine extract mixed with nano bubbles according to the first embodiment of the present invention. It is a view showing the appearance of a manufacturing apparatus for a cosmetic composition using a herbal medicine extract mixed with nano-bubbles according to, and FIG. 4 is an enlarged view of part A of FIG.

1 to 4 together, the cosmetic composition using the herbal medicine extract mixed with nanobubbles according to the present embodiment is obtained by supplying the herbal medicine to the extraction solvent in which lava seawater and ethanol are mixed at a ratio of 60: 40 based on volume It is obtained by mixing nano bubbles in herbal medicine extract extracted by applying heat.

The lava seawater is water naturally filtered by volcanic bedrock and seeped into the land, and Jeju lava seawater may be suggested as an example.

Unlike general seawater, that is, general seawater, the lava seawater is not exposed to the external environment and contains relatively less harmful components such as organic matter and pathogens than the general seawater.

In addition, since the lava seawater is based on the general seawater, mineral components such as magnesium (Mg) and calcium (Ca) are similar to those of the general seawater, but zinc (Zn) useful for the human body while permeating inland by the volcanic bedrock layer ), minerals such as vanadium (V) and germanium (Ge) are contained in a relatively large amount compared to the general seawater.

Since the lava seawater permeates the land, it can be developed at a relatively low cost compared to purifying the general seawater.

The herbal medicine is made of a mixture of dandelion outpost and loquat leaves, which are natural products grown in nature.

In the herbal medicine, it is preferable that the dandelion sheath and the loquat leaves are mixed in the same weight ratio.

The dandelion outpost refers to a plant belonging to the Asteraceae (compositase), which is a perennial herb.

The loquat leaf is a dried leaf of a loquat (Eriobotrya japonica lindley) tree, which is a plant in the rosaceae family.

The herbal medicine extract is extracted from the herbal medicine mixed with the extraction solvent and the dandelion sheath and the loquat leaf.

In detail, the herbal extract is (a) added to the herbal medicine in which 50 g of the dandelion spruce and loquat leaves were mixed with 1.2 times the extraction solvent compared to the herbal medicine volume, extracted at 20 to 25 ° C. for 20 to 30 hours, and then reduced pressure. Concentrate to obtain a crude extract, (b) first fractionate the crude extract obtained in step (a) using water and butanol, (c) among the crude extract obtained, (b) ), the fraction remaining after the primary fractionation in step is secondarily fractionated using hexane, and water and ethanol are mixed with 15:85 by volume for the fraction remaining after the secondary fractionation in step (c) among the crude extracts obtained in (d). After tertiary fractionation using a polar solvent (15% aqM, aqueous methanol) mixed at a ratio of (e) extraction by concentrating the polar solvent layer fraction separated in step (d) and dissolved in the polar solvent under reduced pressure do.

In the step (a), the lava seawater and the ethanol are mixed in a volume ratio of 60:40 as the extraction solvent, and the mixing ratio of the lava seawater and the ethanol is determined after measuring the extraction amount according to the extraction solvent conditions. do.

In detail, when the lava seawater and the ethanol were mixed in a ratio of 60:40 by volume (60% lava seawater) and when the lava seawater and the ethanol were mixed in a ratio of 40:60 by volume (40% lava seawater). seawater) and distilled water instead of the lava seawater, but the distilled water and the ethanol are mixed in a volume ratio of 60:40 (60% distilled water), and the distilled water and the ethanol are mixed in a volume ratio of 40:60 As a result of measuring the extraction amount of the extract extracted from the dandelion outpost for the case of mixing (40% distilled water), as shown in FIG. You can see the big one.

In addition, when the lava seawater and the ethanol are mixed in a ratio of 60:40 by volume (60% lava seawater) and when the lava seawater and the ethanol are mixed in a ratio of 40:60 by volume (40% lava seawater) seawater) and distilled water instead of the lava seawater, but the distilled water and the ethanol are mixed in a volume ratio of 60:40 (60% distilled water), and the distilled water and the ethanol are mixed in a volume ratio of 40:60 As a result of measuring the extraction amount of the extract extracted from the loquat leaves for the case of mixing (40% distilled water), as shown in FIG. can confirm that

The herbal medicine extract contains caffeic acid and ferulic acid extracted from the dandelion sheath.

On the other hand, the apparatus 100 for manufacturing a cosmetic composition using the herbal medicine extract mixed with the nano bubbles is extracted by applying heat after supplying the herbal medicine to an extraction solvent in which lava seawater and ethanol are mixed at a ratio of 60: 40 by volume To prepare a cosmetic composition using a herbal medicine extract mixed with nano bubbles obtained by mixing nano bubbles in a herbal medicine extract, a storage tank 110, a nano bubble generating member 120, and a moving member ( 130), and a storage tank-side moving member 135.

The storage tank 110 has an empty space formed therein to store the herbal medicine extract.

The nano-bubble generating member 120 generates nano-bubbles in the herbal medicine extract, and includes a plurality of nano-bubble generating bodies 121, a plurality of spray nozzle parts 122, and a housing part 124.

The plurality of nano-bubble generating bodies 121 accommodate the herbal medicine extract moved through the moving member 130 therein.

The nano-bubble generating body 121 becomes the entrance of the nano-bubble generating member 120, and the oriental medicine extract where the nano-bubbles are to be formed is kept for a certain period of time.

The plurality of spray nozzle parts 122 are accommodated in the storage tank 110 and are moved through the moving member 130 to spray the herbal medicine extract accommodated in each nano-bubble generating body 121.

As the plurality of spray nozzles 122 are formed in a spiral shape converging towards the direction in which the herbal medicine extract is sprayed, the herbal medicine extract is sprayed in a radial form from the spray nozzle part 122 .

In detail, the spray nozzle unit 122 is formed in a form in which a bar formed long in a predetermined length has a pitch of a predetermined length and is twisted in a spiral shape, and the direction in which the nano bubble generating body 121 is disposed As it extends toward the housing part 124, which is opposite to the direction, it is formed in the form of a spiral whose diameter becomes relatively small, and is formed in a whirlwind shape as a whole.

The interior of the spray nozzle unit 122 is formed as an empty space, and a communication space 123 communicating with the empty space inside the spray nozzle unit 122 is formed between twisted portions of the spray nozzle unit 122. do.

Then, the herbal medicine extract sprayed from the spray nozzle unit 122 is discharged in a radial form from the inside of the spray nozzle unit 122 through each communication space 123 as shown in FIG. As the nozzle part 122 is formed in a spiral shape with a relatively smaller diameter toward the lower side, the herbal medicine extract sprayed from each communication space 123 can be sprayed radially while having different diameters.

The housing part 124 is a herbal medicine mixed with the nano bubbles formed by mixing the herbal medicine extract sprayed from each spray nozzle part 122 and the nano bubbles generated while being sprayed from each spray nozzle part 122. A cosmetic composition using the extract is accepted.

The plurality of nano-bubble generating bodies 121 and the spray nozzle part 122 are spaced apart so that the herbal medicine extract sprayed in a radial form while having diameters of different sizes from each spray nozzle part 122 crosses a certain portion. While being positioned, some of the herbal medicine extracts sprayed from each spray nozzle part 122 are sprayed so that they cross each other so that a collision occurs between the herbal medicine extracts sprayed from each spray nozzle part 122, and thus the Since the nanobubbles are formed between the herbal medicine extracts, the cosmetic composition using the herbal medicine extracts mixed with the nanobubbles can be accommodated in the housing part 124 .

The moving member 130 moves the herbal medicine extract stored in the storage tank 110 to the nano-bubble generating member 120 so that the nano-bubbles are generated in the herbal medicine extract, and a pipe or the like may be presented as an example. there is.

The storage tank-side moving member 135 connects the nano-bubble generating member 120 and the storage tank 110, and is manufactured by mixing the nano-bubbles generated by the nano-bubble generating member 120. A pipe or the like may be suggested as an example of moving the cosmetic composition using the herbal medicine extract mixed with the nanobubbles to the storage tank 110.

Reference numeral 136 is an opening/closing valve for controlling the movement of the cosmetic preparation using the herbal medicine extract mixed with the nanobubbles through the moving member 135 on the storage tank side.

When the storage tank-side moving member 135 is connected to the storage tank 110, the herbal medicine extract stored in the storage tank 110 passes through the moving member 130 and the nano bubble generating member 120. After the cosmetic composition using the herbal medicine extract mixed with the nano bubbles is prepared, the cosmetic composition using the herbal medicine extract mixed with the nano bubbles is moved to the storage tank 110 through the storage tank side moving member 135 A process of mixing the cosmetic composition and the herbal medicine extract, which is moved and mixed with the herbal medicine extract stored in the storage tank 110, is performed, and the storage tank 110, the moving member 130, and the nano bubble generating member 120 ), and the mixing process of the cosmetic composition and the herbal extract is repeatedly performed by connecting the storage tank 110 side moving member 130 and the storage tank 110, so that the initially formed nanobubbles are mixed Compared to the number of nanobubbles in the cosmetic composition using the herbal extract, the number of nanobubbles in the cosmetic composition using the herbal extract mixed with the repeatedly circulated nanobubbles gradually increases.

Hereinafter, the operation of the apparatus 100 for manufacturing a cosmetic composition using the herbal medicine extract mixed with the nanobubbles according to the present embodiment will be described with reference to the drawings.

First, after supplying the herbal medicine to the lava seawater, heat is applied to extract the herbal medicine extract.

Then, the herbal medicine extract is stored in the storage tank 110.

Then, the herbal medicine extract stored in the storage tank 110 is moved to the nano bubble generating member 120 through the moving member 130 .

Then, the nanobubbles are formed between the herbal medicine extracts, and the cosmetic composition using the herbal medicine extracts mixed with the nanobubbles is prepared and then stored in the housing part 124 .

Then, after the cosmetic composition using the herbal medicine extract mixed with the nano bubbles is moved from the housing part 124 to the storage tank 110 through the storage tank-side moving member 135, the storage tank ( 110), a mixing process of the herbal medicine extract mixed with the nanobubbles mixed with the herbal medicine extract stored in the herbal medicine extract is performed.

The process of mixing the herbal medicine extract with the nanobubbles and the herbal medicine extract as described above is repeatedly performed.

Then, the number of nanobubbles formed by the mixing process of the herbal medicine extract mixed with the nanobubbles is relative to the number of nanobubbles formed in the composition using the herbal medicine extract mixed with the nanobubbles initially formed. will increase to

As described above, the apparatus 100 for manufacturing a cosmetic composition using the herbal medicine extract in which the nano bubbles are mixed includes the storage tank 110, the nano bubble generating member 120, the moving member 130, and the storage tank 110. By including the tank-side moving member 135, while using the herbal medicine extract, which is a natural substance, the permeability of the skin is improved so that the effect can last for a long time.

Hereinafter, a skin permeability test (franz cell test) for the case where the nanobubbles are not mixed with the herbal medicine extract and the case where the nanobubbles are mixed will be described.

In the skin permeability test, concentrated under reduced pressure is applied based on the condition that the caffeic acid and the ferrolic acid contained in the dandelion sheath among the herbal extracts are extracted in a relatively large amount.

The herbal medicine extract according to the present invention contains other ingredients such as taraxinic acid or dihydrotaraxinic acid in addition to the caffeic acid and the ferulic acid, and in the skin permeability test of this embodiment, several Among the eggplant components, the caffeic acid and the ferulic acid were selected as reference components for comparative analysis, but the present invention is not limited to the caffeic acid and the ferulic acid components.

The caffeic acid and the ferulic acid are dissolved in the polar solvent, and the polar solvent layer fraction is dried under reduced pressure, and then the mixed solvent in which the methanol and the water are mixed (the methanol and the water are 50: 50, 60: 40, 70: 30, 80:20, 90:10, and 100:0 sequentially) to perform reverse-phase column chromatography and separate into six fractions according to polarity to secure a polar fraction.

The active ingredient is separated from the polar fraction by using a mixed solvent of methanol and water and performing reverse-phase high-speed reduced pressure chromatography (YMC-Pack ODS-A, 10 x 250 mm, elution rate: 1.0 ml/min).

Among the six polar fractions separated as described above, 60aqM (a polar solvent in which water and ethanol were mixed at a ratio of 60:40 based on volume), which is a condition for confirming that the caffeic acid was the main component, was applied.

In the skin permeability test, the degree of permeation was measured after adding a cosmetic composition using a herbal medicine extract mixed with a predetermined concentration of the nanobubbles to a mist. The filter used at this time becomes a Start-M Membrane filter similar to the actual skin condition.

Caffeic acid permeation amount and permeation increase amount over time time (hr) No application of nano bubbles (mg) Application of nano bubbles (mg) Penetration increase (%) 2 0 0 0 4 1.07 1.82 70.1 6 1.12 2.02 80.4 8 1.21 3.02 149.6 12 4.25 8.91 109.6 16 11.1 11.1 0

As a result of testing the increase in permeation of caffeic acid over time for the case where the nanobubbles were not applied and the case where the nanobubbles were applied, there was no permeation and permeation increase until 2 hours had elapsed, but after 8 hours The amount of increase in permeability increased to 149.6%, then decreased again, and no difference in permeability was observed after 16 hours.

Ferulic acid permeation amount and permeation increase over time time (hr) No application of nano bubbles (mg) Application of nano bubbles (mg) Penetration increase (%) 2 0 0 0 4 1.12 1.65 47.3 6 1.15 2.05 78.3 8 1.31 2.23 70.2 12 3.95 7.53 90.6 16 10.1 10.3 2.0

As a result of testing the permeation increase of the ferulic acid over time for the case where the nanobubbles were not applied and the case where the nanobubbles were applied, there was no permeation and permeation increase until 2 hours had elapsed, but after 12 hours The amount of increase in permeation increased to 90.6% and then decreased again. Hereinafter, the results of the moisturizing persistence test and the skin elasticity improvement test result performed on the mist prepared with the cosmetic composition using the herbal extracts mixed with the nano bubbles will be described. First, the moisture retention test selects 22 study subjects, and after applying a sample of 2 mg / cm ² to the study subjects, a moisture meter (corneometer) is used at 1 hour, 3 hours, 6 hours, and 24 hours Moisture content was measured.

The moisture meter is a device for indirectly measuring the moisture content by using the property that the capacitance of the skin increases in proportion to the moisture content.

Table 3 is a mist prepared from a cosmetic composition using herbal medicine extracts mixed with the nanobubbles as a test group, the applicant's general mist (Miaesu Rose Blossom Soothing Mist) as a positive control group, and moisture for no application as a negative control group It is the result value of measuring the content, and this result value becomes the average value of the 22 study subjects.

Moisture content of skin by time period (measurement value is arbitrary unit (using Arbitrary Unit, A.U.)) test group positive control negative control Test group improvement rate (%) before application 25.70 25.32 26.66 - 1 hour after application 52.28 28.05 26.36 107.04 3 hours after application 43.58 27.97 27.83 72.00 6 hours after application 41.69 27.67 27.57 64.51 24 hours after application 36.76 29.44 31.12 44.83

The improvement rate of skin moisture content in the test area was confirmed to be 107.04% and 72.00% after 1 hour and 3 hours of application, respectively, and 64.15% and 44.83% after 6 hours and 24 hours of application, respectively. From the measured values in Table 3, it can be seen that the skin moisture content of the test group continuously increased after application of the samples compared to before application. In addition, the skin moisture content of the test group was statistically significant compared to the other two control groups (P < 0.05) was found to be high.

The skin elasticity improvement test for the mist prepared with a cosmetic composition using herbal extracts mixed with nanobubbles selected 20 research subjects, and after the subjects used themselves on the face twice a day in the morning and evening, a skin measuring instrument (cutometer) ) to measure skin elasticity.

The skin measuring device is a device capable of measuring the extensibility and elasticity of the skin through the viscoelastic property of the skin.

Table 4 is a result of measuring skin elasticity for a mist prepared with a cosmetic composition using a herbal medicine extract mixed with the nanobubbles as a test group and a general mist (Miaesu Rose Blossom Soothing Mist) of the present applicant as a control group, This result is the average of the 20 study subjects.

Skin elasticity measurement result (measurement value is an arbitrary unit (using Arbitrary Unit, A.U.)) division Measures Improvement rate (%) test group before exam 0.4957 - 2 weeks after exam 0.5291 7.02 4 weeks after exam 0.5706 16.64 control group before exam 0.4953 - 2 weeks after exam 0.4831 -2.22 4 weeks after exam 0.4922 0.52

The R7 (Ur/Uf) measured value (A.U.) representing the skin elasticity of the test group increased to 7.02% after 2 weeks of the test and 16.64% after 4 weeks of the test compared to before the test, respectively, while R7 representing the skin elasticity of the control group. (Ur/Uf) measured values (A.U.) decreased by 2.22% after 2 weeks of testing compared to before testing, and increased by 0.52% after 4 weeks of testing compared to before testing. The skin elasticity of the test group was statistically higher than that of the control group. It was confirmed that it was significantly high (P<0.05). Hereinafter, the results of the moisturizing durability test and the skin elasticity improvement test result performed on the toner prepared from the cosmetic composition using the herbal medicine extract mixed with the nanobubbles will be described.

First, the moisturizing persistence test selected 22 study subjects, applied a sample of 2mg / cm ² to the study subjects, and then measured the moisture with a moisture meter (corneometer) at 1 hour, 3 hours, 6 hours, and 24 hours. content was measured.

Table 5 shows a toner prepared from a cosmetic composition using a herbal medicine extract mixed with the nanobubbles as a test group, the applicant's general toner (Miaesu Perfect Pure Seed Toner) as a positive control group, and moisture for no application as a negative control group. It is the result of measuring the content, and this result becomes the average value of the 22 study subjects.

Moisture content of skin by time period (measurement value is in arbitrary unit (using Arbitrary Unit, A.U.)) test group positive control negative control Test group improvement rate (%) before application 32.23 32.48 30.58 - 1 hour after application 65.39 59.89 35.43 116.44 3 hours after application 49.30 47.55 30.66 58.67 6 hours after application 46.19 43.64 31.30 49.98 24 hours after application 40.12 39.66 32.49 31.89

The improvement rate of skin moisture content in the test area was confirmed to be 116.44% and 58.67% after 1 hour and 3 hours of application, respectively, and 49.98% and 31.89% after 6 hours and 24 hours of application, respectively. From the measured values in Table 5, it can be seen that the skin moisture content of the test group continuously increased after application of the samples compared to before application. In addition, the skin moisture content of the test group was statistically significant compared to the other two control groups (P < 0.05 ) was found to be high.

The skin elasticity improvement test for the toner prepared from a cosmetic composition using a herbal medicine extract mixed with the nanobubbles selected 20 research subjects, and after the subjects used themselves on the face twice a day in the morning and evening, the skin measuring instrument ( The elasticity of the skin was measured with a cutometer).

Table 6 is a result of measuring skin elasticity for a toner prepared with a cosmetic composition using a herbal medicine extract mixed with the nanobubbles as a test group and a general toner (Miaesu Perfect Pure Seed Toner) of the present applicant as a control group, This result is the average of the 20 study subjects.

Skin elasticity measurement result (measurement value is an arbitrary unit (using Arbitrary Unit, A.U.)) division Measures Improvement rate (%) test group before exam 0.4655 - 2 weeks after exam 0.4950 6.87 4 weeks after exam 0.5206 12.7 control group before exam 0.4695 - 2 weeks after exam 0.4514 -3.04 4 weeks after exam 0.4595 -1.40

The R7 (Ur/Uf) measured value (A.U.) representing the skin elasticity of the test group increased to 6.87% after 2 weeks and 12.7% after 4 weeks of the test compared to before the test, respectively, while R7 representing the skin elasticity of the control group. (Ur/Uf) measured values (A.U.) decreased to 3.04% after 2 weeks of testing and 1.40% after 4 weeks of testing compared to before the test. The skin elasticity of the test group was statistically significant compared to the control group (P < 0.05) was found to be high.

Hereinafter, with reference to the drawings, a cosmetic composition using a herbal medicine extract mixed with nanobubbles according to other embodiments of the present invention and an apparatus for manufacturing the cosmetic composition using a herbal medicine extract mixed with nanobubbles will be described.

In carrying out this description, descriptions overlapping with those already described in the first embodiment of the present invention are replaced therewith, and will be omitted here.

5 is a view showing the appearance of a nano-bubble generating member constituting the manufacturing apparatus of a cosmetic composition using a herbal medicine extract in which nano-bubbles are mixed according to a second embodiment of the present invention.

Referring to FIG. 5, in this embodiment, an apparatus for manufacturing a cosmetic composition using a herbal medicine extract in which nano bubbles are mixed includes a storage tank, a nano bubble generating member 220, a moving member, and a storage tank side moving member. do.

The storage tank is to store the herbal medicine extract therein.

The nano-bubble generating member 220 generates nano-bubbles in the herbal medicine extract, and includes a nano-bubble generating body 221, a plurality of injection nozzle parts 222, a housing part, and a herbal medicine extract spraying body 225. And, it includes a spray hole 226.

The moving member moves the herbal medicine extract stored in the storage tank to the nano bubble generating member 220 so that the nano bubbles are generated in the herbal medicine extract.

The storage tank-side moving member connects the nano-bubble generating member 220 and the storage tank, and the nano-bubbles produced by mixing the nano-bubbles generated by the nano-bubble generating member 220 are mixed. The cosmetic composition using the herbal extract is moved to the storage tank.

The herbal medicine extract spraying body 225 constituting the nano-bubble generating member 220 is formed while tilting in a form in which a plurality of nano-bubble generating bodies 221 open each other, and is accommodated in the nano-bubble generating body 221. When the herbal medicine extract is sprayed through the injection nozzle part 222, a part of the herbal medicine extract accommodated in the nano-bubble generating body 221 flows into it.

The herbal medicine extract injection body 225 is made of an elastic material and is normally contracted, but is inflated when the herbal medicine extract flows.

The spray hole 226 is formed through a plurality of spaced apart from the side facing the spray nozzle unit 222 of the herbal medicine extract spray body 225.

The injection hole 226 is formed in plurality to discharge the herbal medicine extract flowing toward the herbal medicine extract injection body 225 toward the spray nozzle part 222 and the herbal medicine extract sprayed from the spray nozzle part 222. .

When configured as above, the herbal medicine extract accommodated in the nano bubble generating body 221 is sprayed together through the spray hole 226 and the spray nozzle part 222, and the herbal medicine extract spraying body 225 By being disposed relatively higher than the spray nozzle part 222, the herbal medicine extract is sprayed from the spray nozzle part 222 and then hits the outside of the spray nozzle part 222 due to a phenomenon such as the spray nozzle Splashing to the outside of the unit 222 can be prevented by the extract jet.

Although the present invention has been shown and described in relation to specific embodiments above, those skilled in the art may modify the present invention in various ways without departing from the spirit and scope of the present invention described in the claims below. And it will be appreciated that it can be changed. However, it should be clearly stated that all of these modifications and variations are included within the scope of the present invention.

According to the cosmetic composition using the herbal medicine extract mixed with the nanobubbles and the apparatus for manufacturing the cosmetic composition using the herbal medicine extract mixed with the nanobubbles according to one aspect of the present invention, the skin permeability is improved while using the herbal medicine extract, which is a natural substance. It can be improved and its efficacy can last for a long time, so it can be said that its industrial applicability is high.

100: Apparatus for manufacturing a cosmetic composition using a herbal medicine extract mixed with nano bubbles
110: storage tank
120: absence of nanobubbles
121: nano bubble generating body
122: injection nozzle unit
123: communication space
124: housing part
130: moving member
135: storage tank side moving member

Claims (5)

It is obtained by supplying herbal medicine to an extraction solvent in which lava seawater and ethanol are mixed at a ratio of 60: 40 by volume, and then mixing nano bubbles in the herbal medicine extract extracted by applying heat,
The herbal medicine is made of a mixture of dandelion outpost and loquat leaves,
The herbal medicine extract is
The herbal medicine was added with 1.2 times the extraction solvent compared to the volume of the herbal medicine, extracted at 20 to 25 ° C. for 20 to 30 hours, concentrated under reduced pressure to obtain a crude extract, and the obtained crude extract was mixed with water and butanol. After primary fractionation using hexane, secondary fractionation using hexane, and tertiary fractionation using a polar solvent (15%aqM, aqueous methanol) mixed with water and ethanol in a volume ratio of 15:85, , Cosmetic composition using a herbal medicine extract mixed with nanobubbles, characterized in that extracted by concentrating the polar solvent layer fraction dissolved in the polar solvent under reduced pressure. delete According to claim 1,
In the herbal extract,
A cosmetic composition using a herbal medicine extract mixed with nanobubbles, characterized in that it contains caffeic acid and ferulic acid extracted from the dandelion sheath. After supplying herbal medicines to an extraction solvent in which lava seawater and ethanol are mixed at a ratio of 60:40 by volume, herbal medicine extracts with nano bubbles obtained by mixing nano bubbles with herbal medicine extracts extracted by applying heat As for preparing a cosmetic composition using,
a storage tank in which the herbal medicine extract is stored;
Nano-bubble generation member for generating nano-bubbles in the herbal medicine extract;
a moving member for moving the herbal medicine extract stored in the storage tank to the nano bubble generating member so that the nano bubbles are generated in the herbal medicine extract; and
Connecting the nano-bubble generating member and the storage tank, and moving the cosmetic composition using the herbal medicine extract mixed with the nano-bubbles prepared by mixing the nano-bubbles generated by the nano-bubble generating member to the storage tank Including; storage tank side moving member,
The nano-bubble generating member
A plurality of nano-bubble generating bodies in which the herbal medicine extract moved through the moving member is accommodated;
A plurality of injection nozzle parts for injecting the herbal medicine extract accommodated in each of the nano-bubble generating bodies;
A housing portion accommodating a cosmetic composition using the herbal medicine extract mixed with the nano bubbles formed by mixing the herbal medicine extract sprayed from each spray nozzle part and the nano bubbles generated while spraying from each spray nozzle part,
The injection nozzle portion is formed in a spiral shape converging towards the spraying side of the herbal medicine extract, so that the herbal medicine extract is injected in a radial form from the injection nozzle portion,
The plurality of nano-bubble generating bodies and the spray nozzle parts are spaced apart so that a certain portion of the herbal medicine extract sprayed in a radial form from each spray nozzle part crosses, and some of the herbal medicine extracts are sprayed so as to cross each other so that a collision occurs. And, accordingly, the housing unit manufacturing apparatus of a cosmetic composition using a herbal medicine extract mixed with nano bubbles, characterized in that the cosmetic composition using the herbal medicine extract mixed with the nano bubbles can be accommodated. According to claim 4,
The nano-bubble generating member
The inside communicates with the inside of the nano-bubble generating body, and a plurality of them are coupled to the nano-bubble generating body while being spaced apart from each other, and the herbal medicine extract injection body is formed inclined in a form that widens each other as the distance from the nano-bubble generating body increases. and,
Further comprising a plurality of spray holes formed through the spraying body so that a plurality of pieces are spaced apart from the side facing the spray nozzle part of the herbal medicine extract spraying body,
When the herbal medicine extract accommodated in the nano-bubble generating body is sprayed through the spray nozzle part, a portion of the herbal medicine extract sprayed through the spray nozzle part is discharged through the spray hole toward the spray nozzle part. Apparatus for producing a cosmetic composition using a herbal extract mixed with nanobubbles, characterized in that the spray range can be limited.

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