KR102432908B1 - Very fine powder recovery device and very fine powder recovery system - Google Patents

Abstract

The present invention relates to a fine powder recovery device and a fine powder recovery system capable of collecting and recovering fine powder contained in an impregnated gas, which is formed in a hollow cylindrical shape, and the fine powder contained in the impregnated gas flows while the impregnated gas flows. A body in which a collecting space in which powder can be collected is formed, a gas inlet formed at one side of the main body so that the impregnated gas can be introduced into the collecting space, and the impregnated gas flowing in the collecting space is provided in the collecting space and a gas outlet formed adjacent to the gas inlet on one side of the main body so as to be discharged to the outside of the body, and the main body has a temperature difference in the collecting space to prevent the vortex of the impregnated gas In order to induce induction, the gas outlet may be divided into a plurality of regions having different temperatures, and the gas outlet may be formed in a tubular shape so that at least a portion thereof extends from one side of the main body to the inside of the collection space.

Description

Fine powder recovery device and fine powder recovery system {Very fine powder recovery device and very fine powder recovery system}

The present invention relates to a fine powder recovery device and a fine powder recovery system, and to a fine powder recovery device and a fine powder recovery system capable of collecting and recovering fine powder contained in an impregnated gas.

Multi Layer Ceramic Capacitor (MLCC) is a chip-type capacitor that temporarily charges electricity or removes noise in an electronic circuit. is a part In modern times, the multilayer ceramic capacitor is in high demand enough to be called the rice of the electronics industry, for example, about 1,000 pieces are needed for a personal computer or smart phone, and about 2000 pieces are needed for a television.

In such a multilayer ceramic capacitor, it is necessary to reduce the size of the MLCC and increase the storage capacity. To this end, the multilayer ceramic capacitor has a structure in which about 500 ceramic layers and nickel electrode layers are alternately stacked therein. A multilayer ceramic capacitor includes a molding process of forming a ceramic sheet on a release film, a printing process of forming an electrode pattern on the ceramic sheet, and cutting the ceramic sheet and removing the release film, and then laminating the ceramic sheet and the nickel electrode layer It is formed by a lamination process. An important technique in the multilayer ceramic capacitor is to make the nickel electrode layer as thin as possible and stack a lot of it, and to form it without cracking at a high temperature of 1000° C. or more.

The nickel electrode layer of the multilayer ceramic capacitor may be formed using nickel powder manufactured by a powder synthesis process using a chemical reaction. In general, in the nickel powder manufacturing process using the powder synthesis process, after the synthesis process of nickel powder is made by a chemical reaction in the synthesis device, the generated nickel powder is discharged as a gas-containing gas from the synthesis device together with the residual gas remaining after the reaction, and , a process of collecting and recovering nickel powder contained in the impregnated gas in a fine powder recovery device using a bag filter.

However, in this conventional fine powder recovery device, a differential pressure is generated in the bag filter during collection for a certain period of time, and in order to solve this, the bag filter needs to be regenerated using a jet or the like after the process is stopped to solve the problem, thereby lowering productivity. Accordingly, a method of reducing the load on the bag filter by installing a cyclone in front of the bag filter is also used, but the cyclone is a device that separates fine powder and coarse powder, and it is not easy to remove fine powder, so the effect is large in reducing the load on the bag filter There was a problem that it wasn't.

In addition, a method of collecting and recovering fine powder by thermophoresis by cooling using a cold trap has been proposed, but this also has poor efficiency, so a helical structure or multi-stage structure is used to maximize the cooling surface. By using a structure or the like, there is a problem in that it is not easy to recover the fine powder collected in the complicated flow path formed in the cold trap.

The present invention is to solve various problems including the above problems, and it is possible to reduce the load on the bag filter by recovering not only the coarse powder but also some fine powder in advance in front of the bag filter, and the fine powder produced and collected using a simple structure An object of the present invention is to provide a fine powder recovery device and a fine powder recovery system for easy recovery of However, these problems are exemplary, and the scope of the present invention is not limited thereto.

According to an embodiment of the present invention, a fine powder recovery device is provided. The device for recovering fine powder includes: a body having a hollow cylindrical shape, wherein a collecting space is formed in which the fine powder contained in the impregnated gas can be collected while the impregnated gas flows; a gas inlet formed on one side of the body so that the impregnated gas can be introduced into the collection space; and a gas outlet formed adjacent to the gas inlet on one side of the body so that the impregnated gas flowing in the collecting space can be discharged to the outside of the collecting space. It is divided into a plurality of regions having different temperatures so that a temperature deviation is formed to induce a vortex of the impregnated gas, and the gas outlet is formed in a tubular shape, so that at least a portion is one side of the body It may be formed to extend long into the collection space from the

According to an embodiment of the present invention, the gas inlet is formed at a position spaced a predetermined distance from the central axis of the main body on one side of the main body, and the gas outlet is a pipe having the same central axis as the central axis of the main body. In a shape, it may be formed to extend from one side of the body to the inside of the collection space.

According to an embodiment of the present invention, the main body may be a first region portion having a first temperature, and the gas outlet may be a second region portion having a second temperature lower than the first temperature.

According to an embodiment of the present invention, the first region portion is formed at the first temperature higher than the temperature of the impregnated gas flowing into the collection space so as to be formed as a high temperature portion, and the second region portion is a low temperature portion It may be formed at the second temperature lower than the temperature of the impregnated gas flowing into the collection space so as to be formed as a .

According to an embodiment of the present invention, the first temperature of the first region may be formed at a temperature of 550K to 650K, and the second temperature of the second region may be formed at a temperature of 250K to 350K. .

According to an embodiment of the present invention, the gas outlet may be a first region portion having a first temperature, and the body may be a second region portion having a second temperature lower than the first temperature.

According to an embodiment of the present invention, the gas inlet is formed on one side of the main body at a position spaced apart from the central axis of the main body by a predetermined distance, and the gas outlet is, based on the central axis of the main body, the gas inlet and Conversely, it may be formed to extend from one side of the main body to the inside of the collection space in a tubular shape having a central axis spaced apart by a predetermined distance.

According to an embodiment of the present invention, the main body, based on a virtual cross-section passing through the central axis of the main body, the first region formed on one side of the inner wall surface of the main body and having a first temperature; and a second region portion formed on the other side of the inner wall surface of the body to face the first region portion based on the virtual cross-section and having a second temperature lower than the first temperature.

According to an embodiment of the present invention, the first region portion is formed at a position corresponding to the position where the gas inlet is formed in the body, and the second region portion is formed at a position corresponding to the position where the gas outlet is formed in the main body. may be formed at the location.

According to an embodiment of the present invention, the first region portion is formed at a position corresponding to the position where the gas outlet is formed in the body, and the second region portion is formed at a position corresponding to the position where the gas inlet is formed in the body. may be formed at the location.

According to an embodiment of the present invention, the body further includes a heat insulating portion formed along a boundary portion between the first region having the first temperature and the second region having the second temperature. can do.

According to an embodiment of the present invention, the main body may be formed in a cylindrical shape extending long in a horizontal direction perpendicular to the direction of gravity.

According to an embodiment of the present invention, the main body may be formed in a cylindrical shape extending long in a vertical direction parallel to the gravity direction.

According to another embodiment of the present invention, a fine powder recovery system is provided. The fine powder recovery system includes: a synthesizing device for synthesizing fine powder through a powder synthesizing process using a chemical reaction; a fine powder recovery device that primarily collects and recovers the fine powder contained in the impregnated gas discharged from the synthesis device; and a bag filter device for secondarily collecting and recovering the fine powder contained in the impregnated gas discharged from the fine powder recovery device.

According to another embodiment of the present invention, it further includes a connector for connecting the synthesizing device and the fine powder recovery device, wherein the connector is formed in a tubular shape and is formed to extend in a straight line from the synthesizing device. first part; and a second portion formed in a tubular shape and inclined at a predetermined angle from one end of the first portion to connect one end of the first portion and the gas inlet of the fine powder recovery device.

According to another embodiment of the present invention, the second part is divided into a plurality of regions having different temperatures so as to induce a vortex phenomenon of the impregnated gas flowing in the internal space by forming a temperature difference in the internal space. can be partitioned.

According to another embodiment of the present invention, a first collection port installed in the connection part of the second part of the connection pipe and the fine powder recovery device, the fine powder collected in the second part is collected; and a second collection port installed on one side of the fine powder recovery device to collect the fine powder collected in the fine powder recovery device.

According to an embodiment of the present invention made as described above, a temperature difference is formed by arranging a high temperature part and a low temperature part on the body in which the collection space of the fine powder is formed, and the buoyancy force in the impregnated gas containing the fine powder flowing in the collection space By inducing a vortex phenomenon by generating an effect, it is possible to increase the residence time of the impregnated gas, thereby securing sufficient time for the fine powder particles included in the impregnated gas to move beyond the mean free path. Accordingly, the fine powder colliding with each other in the collection space and the agglomerated coarse powder can be recovered by falling to the floor by its own weight. In addition, the temperature deviation formed in the collection space causes thermophoresis, so that fine powder can also be collected and recovered by the cold wall.

Accordingly, by reducing the load on the bag filter by efficiently reducing the load on the bag filter by pre-recovering some fine powder as well as the coarse powder contained in the impregnated gas in front of the bag filter, the regeneration process of the bag filter for resolving the differential pressure is reduced, thereby reducing the time to stop the process. , it is possible to implement a fine powder recovery device and a fine powder recovery system having the effect of increasing the productivity of the overall fine powder recovery process. Of course, the scope of the present invention is not limited by these effects.

1 and 2 are a front view and a side view schematically showing an apparatus for recovering fine powder according to an embodiment of the present invention.
3 is a front view schematically showing a fine powder recovery apparatus according to another embodiment of the present invention.
4 and 5 are images showing the results of analyzing the flow of the impregnated gas in the collection space depending on whether or not a temperature deviation occurs in the fine powder recovery device.
6 and 7 are a front view and a side view schematically showing an apparatus for recovering fine powder according to another embodiment of the present invention.
8 is a front view schematically showing an apparatus for recovering fine powder according to another embodiment of the present invention.
9 and 10 are images showing the results of analyzing the flow of the impregnated gas in the collection space depending on whether or not a temperature deviation occurs in the fine powder recovery device.
11 is a process diagram schematically illustrating a fine powder recovery system to which a fine powder recovery device is applied.

Hereinafter, several preferred embodiments of the present invention will be described in detail with reference to the accompanying drawings.

Examples of the present invention are provided to more completely explain the present invention to those of ordinary skill in the art, and the following examples may be modified in various other forms, and the scope of the present invention is as follows It is not limited to an Example. Rather, these embodiments are provided so as to more fully and complete the present disclosure, and to fully convey the spirit of the present invention to those skilled in the art. In addition, in the drawings, the thickness or size of each layer is exaggerated for convenience and clarity of description.

DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS Hereinafter, embodiments of the present invention will be described with reference to the drawings schematically illustrating ideal embodiments of the present invention. In the drawings, variations of the illustrated shape can be envisaged, for example depending on manufacturing technology and/or tolerances. Accordingly, embodiments of the inventive concept should not be construed as limited to the specific shape of the region shown in the present specification, but should include, for example, changes in shape caused by manufacturing.

1 and 2 are a front view and a side view schematically showing a fine powder recovery device 100 according to an embodiment of the present invention, and FIG. 3 is a fine powder recovery device 100 according to another embodiment of the present invention. It is a schematic front view. And, FIGS. 4 and 5 are images showing the results of analyzing the flow of the impregnated gas in the collection space according to whether or not a temperature deviation occurs in the fine powder recovery apparatus 100 .

First, as shown in FIG. 1 , the fine powder recovery apparatus 100 according to an embodiment of the present invention may largely include a body 110 , a gas inlet 120 , and a gas outlet 130 . have.

As shown in FIGS. 1 and 2 , the body 110 is formed in a hollow tubular shape, and a collection space is formed in which the fine powder contained in the impregnated gas can be collected while the impregnated gas flows therein. can

For example, the body 110 may be formed in a hollow cylindrical shape, and the gas inlet 120 and the gas outlet 130 may be formed to be spaced apart from each other by a predetermined distance on one side.

More specifically, the gas inlet 120 is formed on one side of the main body 110 so that the impregnated gas can be introduced into the collecting space inside the main body 110 , and the gas outlet 130 is the collecting space. The gas inlet 120 and the gas inlet 120 on one side of the main body 110 so that the impregnated gas flowing in can be discharged to the outside of the collection space may be formed adjacently spaced apart from each other.

In addition, the impregnated gas introduced into the collection space of the body 110 through the gas inlet 120 is not directly discharged through the gas outlet 130 formed adjacent to the gas inlet 120, but is sufficiently in the collection space. After flowing, the gas outlet 130 may be formed in a tubular shape so as to be discharged through the gas outlet 130, at least a portion of which may be formed to extend from one side of the body 110 to the inside of the collection space. have.

For example, the gas inlet 120 is formed at a position spaced apart from the central axis A of the main body 110 by a predetermined distance d on one side of the main body 110 , and the gas outlet 130 is the main body 110 . A tubular shape having the same central axis as the central axis (A) of the body 110 may be formed to extend from one side of the body 110 to the inside of the collection space.

Accordingly, the gas inlet 120 and the gas outlet 130 are located adjacent to one side of the body 110, but the gas outlet 130 is formed to extend long into the inside of the collection space in a tubular shape, the gas outlet Since the inlet 130 is formed deeply adjacent to the other side of the body 110 inside the collection space, the gas inlet 120 and the gas outlet 130 may be substantially separated from each other.

However, the positions of the gas inlet 120 and the gas outlet 130 are not necessarily limited to Figs. 1 and 2, so that the impregnated gas can be discharged after sufficient flow in the collection space of the body 110, The gas inlet 120 is formed in the center of the main body 110 , and the gas outlet 130 may be formed to be spaced apart from the central axis A of the main body 110 by a predetermined distance, and the gas outlet 130 is not the gas outlet 130 . The inlet 120 may be formed to extend long into the collection space in a tubular shape.

In addition, as shown in FIG. 1 , the main body 110 is divided into a plurality of regions having different temperatures so that a temperature deviation is formed in the collection space to induce a vortex of the impregnated gas. can be

For example, the body 110 formed in a cylindrical shape extending long in a horizontal direction perpendicular to the direction of gravity to form the collection space is formed of a first region portion 111 having a first temperature, and The gas outlet 130 formed in a tubular shape inside the collection space may be formed as a second region portion 112 having a second temperature lower than the first temperature. Accordingly, by forming the body 110 and the gas outlet 130 at different temperatures with the collecting space interposed therebetween, a temperature difference may be formed in the collecting space.

However, the arrangement of the first region portion 111 and the second region portion 112 is not necessarily limited to FIG. 1 , and the gas outlet 130 is formed of the first region portion 111 having the first temperature. , the main body 110 may be formed of a second region portion 112 having the second temperature lower than the first temperature.

In addition, as shown in FIG. 3 , the main body 110 may be formed in a cylindrical shape extending in a vertical direction parallel to the direction of gravity. As such, even when the body 110 is formed in the vertical direction, the first region 111 and the second region 112 may be formed separately from the body 110 and the gas outlet 130 . have.

However, the arrangement of the first region part 111 and the second region part 112 in the fine powder recovery apparatus 100 is not necessarily limited to the above-described embodiment, and the gas inlet 120 rather than the gas outlet 130 is disposed. ) is formed to extend long into the collection space in a tubular shape, the first region portion 111 and the second region portion 112 may be formed separately from the body 110 and the gas inlet 120 . may be

At this time, the first region part 111 is formed at the first temperature higher than the temperature of the impregnated gas flowing into the collection space so as to be formed as a high temperature part, and the second region part 112 is formed as a low temperature part. To be formed, the second temperature may be lower than the temperature of the impregnated gas flowing into the collection space.

For example, when the temperature of the impregnated gas flowing into the collection space of the main body 110 is 400K, the first temperature of the first region part 111 is formed at a temperature of 550K to 650K, and the second region part The second temperature of 112 may be formed at a temperature of 250K to 350K, and more preferably, the first temperature of the first region part 111 is formed as a high temperature part of 600K, and the second region part The second temperature of 112 may be formed as a low temperature part of 300K.

Accordingly, in the fine powder recovery device 100, the first region 111, which is a high temperature part of 600 K, and the second region part 112, which is a low temperature part, which is 300 K, have the body 110 and the gas outlet ( 130) to induce a temperature deviation in the collecting space, thereby inducing a vortex phenomenon of the impregnated gas flowing in the collecting space.

For example, as shown in the analysis result of FIG. 4 , when a temperature deviation is not formed in the collecting space, the impregnated gas introduced through the gas inlet 120 passes through the collecting space in a straight line and then the gas outlet It was confirmed that a slight flow was observed only near the inlet of 130 and immediately discharged through the tubular gas outlet 130 .

However, as shown in the analysis result of FIG. 5 , the main body 110 formed of the first region part 111 or the second region part 112 and the second region part 112 or the first region part ( 111), when a temperature deviation is formed in the collection space by the gas outlet 130 formed of It was confirmed that it was discharged through the tubular gas outlet 130 while flowing in multiple directions.

Therefore, according to the fine powder recovery device 100 according to an embodiment of the present invention, the tubular shape formed at a different temperature from the body 110 inside the body 110 in which the collection space of the fine powder is formed. By installing the gas outlet 130 and arranging a high temperature part and a low temperature part in the collection space to form a temperature difference, a buoyancy effect is generated in the impregnated gas containing the fine powder flowing in the collection space to induce a vortex phenomenon. can do.

Therefore, by increasing the residence time of the impregnated gas in the collecting space to secure sufficient time for the fine powder particles included in the impregnated gas to move beyond the mean free path, the fine powder in the collecting space The colliding and agglomerated coarse powder can be recovered by falling to the floor by its own weight, and the temperature deviation formed in the collection space causes thermophoresis, so that the fine powder deposited on the cold wall can also be collected and recovered.

6 and 7 are a front view and a side view schematically showing a fine powder recovery device 100 according to another embodiment of the present invention, and FIG. 8 is a fine powder recovery device 100 according to another embodiment of the present invention. ) is a schematic front view. And, FIGS. 9 and 10 are images showing the results of analyzing the flow of the impregnated gas in the collection space according to whether or not a temperature deviation occurs in the fine powder recovery apparatus 100 .

As shown in FIGS. 6 and 7 , in the fine powder recovery apparatus 100 according to another embodiment of the present invention, the impregnated gas introduced into the collection space of the body 110 through the gas inlet 120 . The gas outlet 130 is not directly discharged through the gas outlet 130 formed adjacent to the gas inlet 120, but is discharged through the gas outlet 130 after sufficiently flowing in the collection space. It is formed in a shape, and at least a portion may be formed to extend from one side of the main body 110 to the inside of the collection space.

For example, the gas inlet 120 is formed at a position spaced apart from the central axis A of the main body 110 by a predetermined distance d on one side of the main body 110 , and the gas outlet 130 is the main body 110 . In a tubular shape having a central axis spaced apart from the gas inlet 120 by a predetermined distance (d) with respect to the central axis (A) of .

Accordingly, the gas inlet 120 and the gas outlet 130 are located adjacent to one side of the body 110, but the gas outlet 130 is formed to extend long into the inside of the collection space in a tubular shape, the gas outlet Since the inlet 130 is formed deeply adjacent to the other side of the body 110 inside the collection space, the gas inlet 120 and the gas outlet 130 may be substantially separated from each other.

In addition, as shown in FIG. 6 , the main body 110 is divided into a plurality of regions having different temperatures so that a temperature deviation is formed in the collection space to induce a vortex of the impregnated gas. can be

For example, the body 110 is formed in a cylindrical shape extending long in the horizontal direction perpendicular to the direction of gravity to form the collection space, based on an imaginary cross section passing through the central axis A of the body 110, the main body ( The first region 111 formed on one side of the inner wall surface of the body 110 and having a first temperature and the other side of the inner wall surface of the body 110 to face the first region 111 based on the imaginary cross-section It may include a second region portion 112 formed and having a second temperature lower than the first temperature.

In this case, the first region 111 is formed at a position corresponding to the position where the gas outlet 130 is formed in the body 110 , and the second region 112 is formed at the gas inlet 120 in the body 110 . ) may be formed at a position corresponding to the formed position.

However, the arrangement of the first region part 111 and the second region part 112 is not necessarily limited to that shown in FIG. 6 , and the first region part 111 is positioned at the position where the gas inlet 120 is formed in the body 110 . It is formed at a corresponding position, and the second region part 112 may be formed at a position corresponding to the position where the gas outlet 130 is formed in the body 110 .

In addition, as shown in FIG. 8 , the main body 110 may be formed in a cylindrical shape extending in a vertical direction parallel to the direction of gravity. As such, even when the body 110 is formed in the vertical direction, the first region 111 and the second region 112 have the virtual cross-section passing through the central axis A of the body 110 . It may be formed to bisect the body 110 based on the .

At this time, the first region part 111 is formed at the first temperature higher than the temperature of the impregnated gas flowing into the collection space so as to be formed as a high temperature part, and the second region part 112 is formed as a low temperature part. To be formed, the second temperature may be lower than the temperature of the impregnated gas flowing into the collection space.

For example, when the temperature of the impregnated gas flowing into the collection space of the main body 110 is 400K, the first temperature of the first region part 111 is formed at a temperature of 550K to 650K, and the second region part The second temperature of 112 may be formed at a temperature of 250K to 350K, and more preferably, the first temperature of the first region part 111 is formed as a high temperature part of 600K, and the second region part The second temperature of 112 may be formed as a low temperature part of 300K.

At this time, heat conduction occurs between the first region portion 111, which is a high-temperature portion, and the second region portion 112, which is a low-temperature portion, and is generated in the body 110 by the first region portion 111 and the second region portion 112. Insulation along the boundary portion between the first region portion 111 having the first temperature and the second region portion 112 having the second temperature so as to prevent the temperature deviation from disappearing or the boundary thereof becoming ambiguous A portion 140 may be formed.

Accordingly, the heat insulating portion 140 thermally separates the first region portion 111 that is a high temperature portion and the second region portion 112 that is a low temperature portion, so that the first region portion 111 and the second region portion 112 are separated from each other. By effectively preventing heat conduction from occurring, it is possible to induce a temperature deviation to clearly occur in the collection space of the body 110 . Here, all kinds of heat insulating materials capable of preventing heat conduction between the first region part 111 and the second region part 112 may be applied to the heat insulating part 140 .

Accordingly, the main body 110 is formed such that the first region 111, which is a high temperature part of 600K, and the second region part 112, which is a low temperature part, of 300K bisect the body 110, so that the temperature deviation within the collection space is reduced. By inducing it, it is possible to induce a vortex phenomenon of the impregnated gas flowing in the collection space.

For example, as shown in the analysis result of FIG. 9 , when a temperature deviation is not formed in the body 110 , the impregnated gas introduced through the gas inlet 120 passes through the collection space in a substantially straight line. It was confirmed that the gas was directly discharged through the tubular gas outlet 130 .

However, as shown in the analysis result of FIG. 10 , a temperature deviation is formed in the collection space by the main body 110 divided into the first region 111 and the second region 112 having different temperatures. In this case, it is confirmed that a vortex phenomenon occurs in the impregnated gas introduced through the gas inlet 120 , and the impregnated gas flows in multiple directions within the collection space and is discharged through the tubular gas outlet 130 . it became

Therefore, according to the fine powder recovery apparatus 100 according to another embodiment of the present invention, by arranging a high temperature part and a low temperature part on the main body 110 in which the collection space of the fine powder is formed to form a temperature deviation, the collection space It is possible to induce a vortex phenomenon by generating a buoyancy effect in the impregnated gas containing the fine powder flowing in.

Therefore, by increasing the residence time of the impregnated gas in the collecting space to secure sufficient time for the fine powder particles included in the impregnated gas to move beyond the mean free path, the fine powder in the collecting space The colliding and agglomerated coarse powder can be recovered by falling to the floor by its own weight, and the temperature deviation formed in the collection space causes thermophoresis, so that the fine powder deposited on the cold wall can also be collected and recovered.

11 is a process diagram schematically showing the fine powder recovery system 1000 to which the fine powder recovery device 100 is applied.

11 , the fine powder recovery system 1000 according to an embodiment of the present invention may largely include a synthesis device 200 , a fine powder recovery device 100 , and a bag filter device 300 . can

11 , the synthesizing apparatus 200 may synthesize fine powder through a powder synthesizing process using a chemical reaction. For example, when the fine powder synthesized in the synthesizing apparatus 200 is nickel nanopowder, the synthesizing apparatus 200 nucleates nickel particles by a reduction reaction using a reducing gas from a nickel salt introduced into the interior by a carrier gas. and growing to form the nickel nanopowder.

In this way, the fine powder synthesized in the synthesis device 200 may be discharged as the impregnated gas together with the residual gas after the chemical reaction, and the fine powder recovery device 100 may be discharged from the synthesis device 200 . The fine powder contained in the impregnated gas may be primarily collected and recovered.

Here, the connection pipe 400 connecting the synthesis apparatus 200 and the fine powder recovery apparatus 100 is formed in a tubular shape and extends in a straight line from the synthesis apparatus 200 , a first part 410 and Formed in a tubular shape and inclined at a predetermined angle (a) from one end of the first portion 410 to connect one end of the first portion 410 and the gas inlet 120 of the fine powder recovery device 100 It may include two parts 420 .

At this time, the first part 410 of the connection pipe 400 is the impregnated gas discharged from the synthesis apparatus 200 so that the high-temperature impregnated gas discharged from the synthesis apparatus 200 can be cooled to a predetermined temperature. It can be formed at a lower temperature. Although not shown, the first part 410 may be a cooling unit in which a cooling passage is formed along an inner or outer circumferential surface and is cooled in a water cooling manner by cooling water flowing along the cooling passage.

In addition, the second part 420 may be divided into a plurality of regions having different temperatures so as to induce a vortex phenomenon of the impregnated gas flowing in the internal space by forming a temperature difference in the internal space.

For example, the upper portion 421 with respect to the central axis of the second portion 420 having a circular tubular shape has a first temperature lower than the temperature of the impregnated gas cooled to the predetermined temperature in the first portion 410 . is formed as a low-temperature portion, and the lower portion 422 may be formed at a second temperature higher than the temperature of the impregnated gas to be formed as a high-temperature portion.

The upper part 421 of the second part 420 may be formed as a low temperature part by a water cooling method or an air cooling method, and the lower part 422 may be formed as a high temperature part by a heating method by a hot wire. In addition, the upper portion 421 of the second portion 420 may be formed as a high temperature portion and the lower portion 422 may be formed as a low temperature portion, but in order to induce a smooth vortex of the impregnated gas, the upper portion 421 is It may be most preferable that the lower portion 422 is formed of the low temperature portion and that the lower portion 422 is formed of the high temperature portion.

Accordingly, of the impregnated gas passing through the second portion 420, the impregnated gas flowing through the lower portion 422, which is a high-temperature part, is heated and has an upward airflow, and the impregnated gas flowing through the upper part 421, which is a low-temperature part, is cooled. By having a downstream air flow, a vortex phenomenon can occur.

Due to the above-described vortex phenomenon, the fine powder contained in the impregnated gas collides with each other, and the agglomerated powder can be recovered by falling to the bottom surface by its own weight, and thermophoresis induced by the temperature difference between the high temperature part and the low temperature part. The unreacted residual precursor contained in the fine powder may be precipitated and recovered by the cold wall surface.

In this way, the coarse powder and the precipitated residual precursor recovered from the second part 420 of the connection pipe 400 are separated from the second part 420 of the connection pipe 400 and the fine powder recovery device 100 . It may be collected by the first collection port 500 installed in the connection part. The first collection port 500 may include a wet cleaning port to wet the shell layer of the precipitated residual precursor.

Accordingly, in the fine powder recovery system 1000 of the present invention, the impregnated gas through the connection pipe 400 before the fine powder recovery device 100 that primarily collects and recovers the fine powder contained in the impregnated gas. In the process of flowing, by recovering in advance at least a portion of the fine powder included in the impregnated gas, it is possible to further increase the recovery efficiency of the fine powder.

Subsequently, as shown in FIG. 11 , the impregnated gas flowing into the fine powder recovery device 100 through the connection pipe 400 has a buoyancy effect generated by a temperature deviation formed in the fine powder recovery device 100 . The vortex phenomenon is induced by the vortex, and the fine powder contained in the impregnated gas collides with each other in the collection space of the fine powder recovery device 100, and the agglomerated coarse powder falls to the floor by its own weight and can be recovered. , the unreacted residual precursor contained in the fine powder may be precipitated and recovered on the cold wall by thermophoresis induced by the temperature difference between the high temperature part and the low temperature part.

Here, the fine powder recovery device 100 includes the components and the configuration of the fine powder recovery device 100 according to various embodiments of the present invention shown in FIGS. 1 to 3 and 6 to 8 described above. and roles may be the same. Therefore, detailed description is omitted.

As such, the coarse powder and the precipitated residual precursor recovered by the fine powder recovery device 100 may be collected by the second collection port 600 installed on one side of the fine powder recovery device 100 . The second collection port 600 may include a wet cleaning port so that the shell layer of the precipitated residual precursor can be wet removed.

Subsequently, as shown in FIG. 11 , the impregnated gas in which the fine powder is primarily collected in the fine powder recovery device 100 is another connection pipe connected to the gas outlet 130 of the fine powder recovery device 100 ( 800), the bag filter device 300 may collect and recover the fine powder contained in the impregnated gas secondarily.

For example, the bag filter chamber 310 of the bag filter device 300 is formed in a cylindrical shape as a whole so as to accommodate at least one bag filter 330 therein, and is formed in the lower portion where the fine powder outlet 321 is formed. At least a portion may be formed in an inverted cone shape whose cross-sectional area gradually decreases toward the bottom. At this time, the bag filter chamber 310 is configured to recover only the fine powder of high purity from the impregnated gas recovered by precipitating the residual precursor in the process of first collecting the fine powder in the fine powder recovery device 100 . , may be heated to a temperature equal to or higher than the second temperature as a high-temperature part. However, the temperature of the bag filter chamber 310 is not necessarily limited to the second temperature or higher, and a wide variety of temperatures at which the fine powder can be easily recovered may be applied.

Accordingly, the impregnated gas introduced into the impregnated gas inlet 311 formed on one side of the lower end of the bag filter chamber 310 passes through the bag filter 330 installed in the bag filter chamber 310, and the bag filter It may be discharged to the outside through the impregnated gas discharge unit 313 formed on one side of the upper end of the chamber 310 . In this way, the fine powder remaining in the impregnated gas may be collected in the bag filter 330 while the impregnated gas passes through the bag filter 330 .

In addition, at an upper portion of the bag filter 330 installed in the bag filter chamber 310 , the high-pressure air storage unit 321 , the high-pressure air supply pipe 322 , and at least one of at least one installed at a position corresponding to the bag filter 330 . A high-pressure air injection unit 320 including a high-pressure air injection nozzle 323 may be installed.

Accordingly, when a certain level of the fine powder is collected in the bag filter 330 , a differential pressure is generated, and high-pressure air is supplied to the bag filter 330 through the high-pressure air injection nozzle 323 installed on the top of the bag filter 330 . When sprayed, the fine powder collected in the bag filter 330 may fall and accumulate in the lower portion of the bag filter chamber 310 . Then, the fine powder may be collected by the collection container 700 by opening the fine powder outlet 321 formed at the bottom of the bag filter chamber 310 .

In this high-pressure air injection process according to the differential pressure generation of the bag filter 330 , the fine powder recovery device 100 primarily recovers the coarse powder and the residual precursor contained in the impregnated gas, so that the conventional Compared to the fine powder recovery system, it can be performed with a longer cycle.

Therefore, according to the fine powder recovery device 100 and the fine powder recovery system 1000 including the same according to an embodiment of the present invention, it contains the unreacted residual precursor as well as the coarse powder included in the impregnated gas in front of the bag filter. By efficiently reducing the load on the bag filter by recovering some of the fine powder in advance, the regeneration process of the bag filter for resolving the differential pressure is reduced, reducing the time to stop the process, and increasing the productivity of the overall fine powder recovery process. can

Although the present invention has been described with reference to the embodiments shown in the drawings, which are merely exemplary, those skilled in the art will understand that various modifications and equivalent other embodiments are possible therefrom. Therefore, the true technical protection scope of the present invention should be determined by the technical spirit of the appended claims.

100: fine powder recovery device
110: body
111: first area part
112: second area part
120: gas inlet
130: gas outlet
140: insulation
200: synthesizing device
300: bag filter device
310: bag filter chamber
320: high-pressure air injection unit
330: bag filter
400: connector
410: first part
420: second part
500: first collection port
600: second collection port
700: collection vessel
800: connector
1000: fine powder recovery system

Claims (17)

a body formed in a hollow tubular shape, and having a collecting space in which the fine powder contained in the impregnated gas can be collected while the impregnated gas flows;
a gas inlet formed on one side of the body so that the impregnated gas can be introduced into the collection space; and
It is formed in a tubular shape so that the impregnated gas flowing in the collecting space can be discharged to the outside of the collecting space, and at least a portion is formed to extend from one side of the main body to the inside of the collecting space, one side of the main body and a gas outlet formed adjacent to the gas inlet to
The body is
It is divided into a plurality of regions having different temperatures so that a temperature deviation is formed in the collection space to induce a vortex of the impregnated gas,
The gas inlet is
It is formed on one side of the main body at a position spaced a predetermined distance from the central axis of the main body,
The gas outlet is
It is formed in a tubular shape having the same central axis as the central axis of the main body to extend from one side of the main body to the inside of the collection space,
The body is a first region portion having a first temperature,
wherein the gas outlet is a second region portion having a second temperature lower than the first temperature. delete delete The method of claim 1,
The first area part,
It is formed at the first temperature higher than the temperature of the impregnated gas flowing into the collection space so as to be formed as a high-temperature part,
The second area part,
To be formed as a low-temperature part, the fine powder recovery device is formed at the second temperature lower than the temperature of the impregnated gas flowing into the collection space. 5. The method of claim 4,
The first temperature of the first region is formed at a temperature of 550K to 650K,
The second temperature of the second region portion is formed at a temperature of 250K to 350K, a fine powder recovery device. a body formed in a hollow tubular shape, and having a collecting space in which the fine powder contained in the impregnated gas can be collected while the impregnated gas flows;
a gas inlet formed on one side of the body so that the impregnated gas can be introduced into the collection space; and
It is formed in a tubular shape so that the impregnated gas flowing in the collecting space can be discharged to the outside of the collecting space, and at least a portion is formed to extend from one side of the main body to the inside of the collecting space, one side of the main body and a gas outlet formed adjacent to the gas inlet to
The body is
It is divided into a plurality of regions having different temperatures so that a temperature deviation is formed in the collection space to induce a vortex of the impregnated gas,
The gas inlet is
It is formed on one side of the main body at a position spaced a predetermined distance from the central axis of the main body,
The gas outlet is
It is formed in a tubular shape having the same central axis as the central axis of the main body to extend from one side of the main body to the inside of the collection space,
The gas outlet is a first region portion having a first temperature,
wherein the main body is a second region portion having a second temperature lower than the first temperature. a body formed in a hollow tubular shape, and having a collecting space in which the fine powder contained in the impregnated gas can be collected while the impregnated gas flows;
a gas inlet formed on one side of the body so that the impregnated gas can be introduced into the collection space; and
It is formed in a tubular shape so that the impregnated gas flowing in the collecting space can be discharged to the outside of the collecting space, and at least a portion is formed to extend from one side of the main body to the inside of the collecting space, one side of the main body and a gas outlet formed adjacent to the gas inlet to
The body is
It is divided into a plurality of regions having different temperatures so that a temperature deviation is formed in the collection space to induce a vortex of the impregnated gas,
The gas inlet is
It is formed on one side of the main body at a position spaced a predetermined distance from the central axis of the main body,
The gas outlet is
It is formed to extend from one side of the main body to the inside of the collection space in a tubular shape having a central axis spaced apart from the gas inlet by a predetermined distance with respect to the central axis of the main body,
The body is
a first region portion formed on one side of the inner wall surface of the main body and having a first temperature based on an imaginary cross section passing through the central axis of the main body; and
a second region portion formed on the other side of the inner wall surface of the body to face the first region portion based on the virtual cross-section and having a second temperature lower than the first temperature;
Including, a fine powder recovery device. delete 8. The method of claim 7,
The first region portion is formed at a position corresponding to the position where the gas inlet is formed in the body,
The second region portion is formed at a position corresponding to a position where the gas outlet is formed in the main body, the fine powder recovery device. 8. The method of claim 7,
The first region portion is formed at a position corresponding to the position where the gas outlet is formed in the body,
The second region portion is formed at a position corresponding to a position where the gas inlet is formed in the main body, the fine powder recovery device. 8. The method of claim 7,
The body is
a heat insulating portion formed along a boundary between the first region having the first temperature and the second region having the second temperature;
Further comprising, a fine powder recovery device. The method of claim 1,
The body is
A fine powder recovery device, which is formed in a cylindrical shape extending long in a horizontal direction perpendicular to the gravity direction. The method of claim 1,
The body is
A device for recovering fine powder, which is formed in a cylindrical shape elongated in a vertical direction parallel to the direction of gravity. a synthesizing device for synthesizing fine powder by a powder synthesizing process using a chemical reaction;
Claims 1, 4, 5, 6, 7, 9, 10, and claim 1 for collecting and recovering the fine powder contained in the impregnated gas discharged from the synthesis device. The apparatus for recovering fine powder according to any one of claims 11, 12 and 13; and
a bag filter device for secondarily collecting and recovering the fine powder contained in the impregnated gas discharged from the fine powder recovery device;
Including, fine powder recovery system. 15. The method of claim 14,
Further comprising; a connector connecting the synthesis device and the fine powder recovery device;
The connector is
a first portion formed in a tubular shape and extending in a straight line from the synthesizing device; and
a second portion formed in a tubular shape and inclined at a predetermined angle from one end of the first portion to connect one end of the first portion and the gas inlet of the fine powder recovery device;
Including, fine powder recovery system. 16. The method of claim 15,
The second part is
The fine powder recovery system, which is partitioned into a plurality of regions having different temperatures so as to induce a vortex phenomenon of the impregnated gas flowing in the internal space by forming a temperature deviation in the internal space. 16. The method of claim 15,
a first collection port installed in the connection part of the second part of the connection pipe and the fine powder recovery device to collect the fine powder collected in the second part; and
a second collection port installed on one side of the fine powder recovery device to collect the fine powder collected in the fine powder recovery device;
Further comprising a, fine powder recovery system.

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