KR102229855B1 - 제올라이트 재료의 제조 방법 - Google Patents

제올라이트 재료의 제조 방법 Download PDF

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KR102229855B1
KR102229855B1 KR1020207003773A KR20207003773A KR102229855B1 KR 102229855 B1 KR102229855 B1 KR 102229855B1 KR 1020207003773 A KR1020207003773 A KR 1020207003773A KR 20207003773 A KR20207003773 A KR 20207003773A KR 102229855 B1 KR102229855 B1 KR 102229855B1
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mww
zeolite
zeolite material
weight
het
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KR20200019765A (ko
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울리히 뮐러
안드레이 니콜라에 파르불레스쿠
제프 양
한스 위르겐 루첼
게오르크 우흘
슈테판 둠저
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바스프 에스이
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026—After-treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/86—Borosilicates; Aluminoborosilicates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0027—Powdering
    • B01J37/0045—Drying a slurry, e.g. spray drying
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/12—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the replacing atoms being at least boron atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/22—After treatment, characterised by the effect to be obtained to destroy the molecular sieve structure or part thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/08—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the aluminium atoms being wholly replaced

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
KR1020207003773A 2012-02-07 2013-02-05 제올라이트 재료의 제조 방법 Active KR102229855B1 (ko)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
EP12154169 2012-02-07
EP12154169.2 2012-02-07
EP12189035.4 2012-10-18
EP12189035 2012-10-18
PCT/EP2013/052224 WO2013117537A1 (en) 2012-02-07 2013-02-05 Process for the preparation of a zeolitic material

Related Parent Applications (1)

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KR1020147025190A Division KR102079792B1 (ko) 2012-02-07 2013-02-05 제올라이트 재료의 제조 방법

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Publication Number Publication Date
KR20200019765A KR20200019765A (ko) 2020-02-24
KR102229855B1 true KR102229855B1 (ko) 2021-03-19

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KR1020147025190A Active KR102079792B1 (ko) 2012-02-07 2013-02-05 제올라이트 재료의 제조 방법

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EP (2) EP3326973B1 (enExample)
JP (1) JP6367118B2 (enExample)
KR (2) KR102229855B1 (enExample)
CN (2) CN104302577A (enExample)
BR (1) BR112014019483B1 (enExample)
ES (2) ES2935820T3 (enExample)
HU (1) HUE060651T2 (enExample)
MX (1) MX365892B (enExample)
MY (2) MY169244A (enExample)
RU (1) RU2619685C2 (enExample)
SG (2) SG11201404651YA (enExample)
WO (1) WO2013117537A1 (enExample)
ZA (1) ZA201406464B (enExample)

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US9371239B2 (en) * 2012-11-05 2016-06-21 Basf Se Tin-containing zeolitic material having an MWW-type framework structure
ES2621510T3 (es) * 2012-11-05 2017-07-04 Basf Se Un material zeolítico que contiene estaño que tiene una estructura de marco de tipo MWW
JP6526689B2 (ja) 2013-11-05 2019-06-05 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ Ｍｗｗ型の骨格構造を有するスズ含有のゼオライト材料
US9999878B2 (en) 2013-11-05 2018-06-19 Basf Se Tin-containing zeolitic material having a BEA framework structure
CN104709919B (zh) * 2013-12-16 2017-03-08 中国科学院大连化学物理研究所 一种具有mww拓扑结构的含锡分子筛及其制备和应用
DE102014008081A1 (de) 2014-05-30 2015-11-19 Basf Se Verfahren zur Herstellung von Acrylsäure unter Verwendung eines alkali- und erdalkalifreien zeolithischen Materials
DE102014008080A1 (de) 2014-05-30 2015-11-12 Basf Se Verfahren zur Herstellung von Acrylsäure unter Verwendung eines aluminiumfreien zeolithischen Materials
DE102014017804A1 (de) 2014-12-02 2016-04-21 Basf Se Verfahren zur Herstellung von Acrylsäure
JP2018522009A (ja) 2015-07-15 2018-08-09 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ アリールプロペンの調製方法
BR112018000519A2 (pt) 2015-07-15 2018-09-11 Basf Se processo para preparar um composto, e, uso de um catalisador poroso sólido
JP7039472B2 (ja) * 2015-12-08 2022-03-22 ビーエーエスエフ ソシエタス・ヨーロピア Ｂｅａ骨格構造を有するスズ含有ゼオライト材料
EP3554694B1 (en) * 2016-12-13 2024-02-14 Basf Se A process for the preparation of a titanium-containing zeolite
KR102503496B1 (ko) * 2016-12-20 2023-02-23 바스프 에스이 골격 타입 mww를 갖는 티타늄 함유 제올라이트 물질을 포함하는 압출성 조성물의 제조 방법
RU2762171C2 (ru) * 2017-01-18 2021-12-16 Басф Се Способ получения формованного изделия, содержащего цинк и титансодержащий цеолит
CN108398422B (zh) * 2018-01-30 2019-12-10 北京联合大学 同时测定空气中硫化氢、苯和三甲胺的敏感材料
EP3749611A4 (en) * 2018-02-06 2022-02-23 Basf Se PROCESS FOR PRODUCTION OF A ZEOLITE MATERIAL WITH RTH FRAME STRUCTURE
FR3081345B1 (fr) * 2018-05-24 2023-11-10 Ifp Energies Now Procede de synthese d'une zeolithe de type structural afx de tres haute purete en presence d'un structurant organique azote
US20220403207A1 (en) 2019-10-24 2022-12-22 Basf Se Removal of monomeric aliphatic diisocyanate in an aliphatic polyisocyanate using scavengers
CN110668463B (zh) * 2019-11-06 2021-04-02 中国天辰工程有限公司 一种含钛高硅铝比丝光沸石的制备方法
BR112022018861A2 (pt) 2020-03-23 2022-11-22 Basf Se Material zeolítico, composto contendo ti, uso de um composto contendo ti, processos para preparar um material zeolítico e para oxidar um composto orgânico, moldagem, uso de uma moldagem, e, óxido de propileno
WO2022029076A1 (en) 2020-08-03 2022-02-10 Basf Se A polyester molding having a low outgassing of volatile organic compounds
CN114180594B (zh) * 2020-09-14 2023-05-02 中国石油化工股份有限公司 一种ith分子筛的制备方法
KR102408100B1 (ko) * 2021-05-31 2022-06-15 충북대학교 산학협력단 메탄의 건식 개질 반응용 2차원 니켈 실리케이트 분자체 촉매의 제조방법 및 이에 따라 제조된 메탄의 건식 개질 반응용 2차원 니켈 실리케이트 분자체 촉매
KR102773001B1 (ko) * 2023-07-27 2025-02-27 동우 화인켐 주식회사 유기용매 정제 방법 및 탈수 시스템

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JP6367118B2 (ja) 2018-08-01
HUE060651T2 (hu) 2023-04-28
ES2683376T3 (es) 2018-09-26
CN104302577A (zh) 2015-01-21
RU2619685C2 (ru) 2017-05-17
KR102079792B1 (ko) 2020-02-20
EP2812282A1 (en) 2014-12-17
KR20200019765A (ko) 2020-02-24
RU2014136174A (ru) 2016-04-10
JP2015506332A (ja) 2015-03-02
SG11201404651YA (en) 2014-09-26
KR20140133564A (ko) 2014-11-19
BR112014019483A2 (enExample) 2017-06-20
EP3326973B1 (en) 2022-10-26
MY195237A (en) 2023-01-11
EP2812282B1 (en) 2018-05-09
BR112014019483B1 (pt) 2021-04-20
EP3326973A1 (en) 2018-05-30
MX2014009271A (es) 2014-09-22
MX365892B (es) 2019-06-19
WO2013117537A1 (en) 2013-08-15
ES2935820T3 (es) 2023-03-10
CN108264053A (zh) 2018-07-10
SG10201606435XA (en) 2016-09-29
BR112014019483A8 (pt) 2017-07-11
ZA201406464B (en) 2015-12-23
MY169244A (en) 2019-03-19

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