KR102195134B1 - processof manufacturing of composition - Google Patents

Abstract

The present invention relates to a method of manufacturing an agent for preventing damages by viral diseases and insects and promoting plant growth, which includes a porous nanoparticle carrier and flaxseed powder, and more particularly, to a method of manufacturing an agent for preventing damages by viral diseases and insects and promoting plant growth, which includes a porous nanoparticle carrier and flaxseed powder, in which a porous nanoparticle carrier and flaxseed powder liquid is sprayed onto roots or leaves of plants, so that prevention of plant root rot, prevention of agglomeration of soil attached to plant roots, prevention of damages by diseases and insects, prevention of mold reproduction, virus sterilization, inhibition of virus reproduction, inhibition of germ reproduction, and inhibition of insect reproduction are achieved. The method includes: preparing a porous carrier; preparing porous nanoparticle carrier powder; preparing porous nanoparticle flaxseed powder; and preparing a porous nanoparticle carrier and flaxseed powder liquid.

Description

Method of manufacturing a plant growth accelerator and virus disease prevention agent consisting of nanoparticle porous carrier and flaxseed powder {processof manufacturing of composition}

The present invention relates to a method for preparing a viral pest prevention and plant growth accelerator comprising a nanoparticle porous carrier and flaxseed powder, and more particularly, to a plant root rot by spraying a nanoparticle porous carrier and flaxseed powder solution onto the roots or leaves of a plant. Prevention, prevention of soil clogging attached to plant roots, disease and pest prevention, fungal growth prevention, bacteria sterilization, virus growth inhibition, microbial growth inhibition, and virus pest prevention and plant growth consisting of nanoparticle porous carrier and flax seed powder It relates to a method of manufacturing an accelerator.

Rural migration is accelerating due to rapid industrialization and urbanization.Therefore, agricultural work is difficult due to the aging and women of the rural labor force.Many researches are being developed and distributed to reduce the labor force, and eco-friendly agricultural development research is also conducted for stable production of agricultural products. It has been continuously promoted.

Although many farms are actively participating in this by the chemical fertilizer reduction policy, it is a reality that most farms still use fast-acting fertilizers to maintain the existing level of fertilization, and the efficiency of fertilizers decreases because fast-acting fertilizers are easily lost. In order to reduce the labor required for fertilization, as well as increase the labor force for fertilization and various environmental pollution, sustained-release fertilizer products are being produced and distributed.

Sustained release fertilizer uses a variety of materials derived from petrochemical products.Since the manufacturing method goes through many processes, not only the production cost is high compared to the efficiency, but also secondary soil environmental pollution problems are emerging, and the soil physical properties of the cultivated land are maintained. It is suitable for cultivated crops considering the benefits such as economic use of moisture, weeding suppression effect, and improvement of the crop rooting environment, and the concentration of inorganic nutrients required during the entire growth period of the crop can be maintained at a certain level, and ideal cleanliness considering the amount of labor input. Slow-release fertilizer is required.

Efforts are being made to develop natural zeolite, which has the effect of improving environmental friendliness and environmental pollution, as a functional material with the performance of a sustained-release fertilizer, and the use of zeolite in the agricultural sector is to increase the cation exchange capacity of the soil in the field to be used. As it is limited to increase it, it is used as a simple soil improvement agent or soil environment improvement agent with low added value rather than development as a sustained-release fertilizer.

The present inventors have functionalized the fine pores of a plant growth accelerator composed of nanoparticle porous carrier powder and flaxseed powder as a carrier, and use it as a high efficiency plant growth component and as a substitute for complex fertilizers. The accelerator was developed.

The present inventor uses a plant growth accelerator composed of nanoparticle porous carrier powder and flaxseed powder, and has 2 to 4 times superior effect compared to the plant growth accelerator composed of nanoparticle porous carrier powder used in Patent Publication 10-2020-8879. Was developed.

The present invention sprays a nanoparticle porous carrier and flaxseed powder solution onto the roots or leaves of plants to prevent plant root rot, prevent soil agglomeration attached to plant roots, prevent pests, prevent fungal growth, sterilize bacteria, inhibit virus propagation, and It is an object of the present invention to provide a method for preventing viral diseases and pests and producing a plant growth accelerator composed of a nanoparticle porous carrier and flaxseed powder for inhibiting reproduction and inhibiting the reproduction of insects.

The present invention is SiO ₂ 60 to 80 wt%, Al ₂ O ₃ 5 to 15 wt%, Fe ₂ O ₃ 1 to 5 wt%, CaO 1 to 5 wt%, Na ₂ O 1 to 5 wt%, K ₂ O A porous carrier composed of 1 to 5% by weight, MgO 01 to 1% by weight, and Ag ₂ O 0.5 to 10% by weight was mixed by stirring for 1 hour, and then added to a glass melting furnace at 1200 to 1550°C and melted for 30 hours. Preparing a porous carrier; Pulverizing the porous carrier into a nanoparticle shape to prepare a nanoparticle porous carrier powder; Pulverizing the flax seed powder into nanoparticles to prepare nanoparticle porous flaxseed powder; And 5 to 10 parts by weight of the nanoparticle porous carrier powder, 5 to 10 parts by weight of nanoparticle porous flaxseed powder, and 0.5 to 1 parts by weight of a dispersant for 2 hours to prepare a nanoparticle porous carrier and a flaxseed powder solution to 100 parts by weight of water. It consists of a nanoparticle porous carrier and flaxseed powder, characterized in that consisting of the step of.

The plant growth promoter of the present invention sprays a nanoparticle porous carrier and flaxseed powder solution onto the roots or leaves of plants to prevent plant root rot, prevent soil agglomeration attached to plant roots, prevent plant diseases and pests, prevent plant fungus propagation, and multiply plant bacteria It has the effect of suppressing and suppressing the reproduction of plant insects.

In the present invention, the nanoparticle porous carrier powder is uniformly dispersed in a water-soluble flaxseed oil and water mixture, and even if the powder is mixed in a state where the nanoparticle porous carrier powder is uniformly dispersed in a water-soluble flaxseed oil and water mixture, the powder is mixed without being entangled. , As a water-soluble flaxseed oil dispersant is added, the dispersion is smoothly mixed without clumping and even distribution of moisture is induced, so there is an effect of preventing the problem of poor quality uniformity due to a sudden decrease in dispersibility due to clumping, which is a conventional problem.

1 is a flow chart showing the steps of preparing a viral pest prevention and plant growth accelerator made of a nanoparticle porous carrier and flax seed powder of the present invention.

Advantages and features of the present invention, and a method of achieving them will become apparent with reference to the embodiments described below in detail. The present invention is not limited to the embodiments described herein and may be embodied in other forms. Rather, the embodiments introduced herein are intended to ensure that the disclosed content is thorough and complete, and the spirit of the present invention can be sufficiently conveyed to those skilled in the art. Is provided for. The terms used in the present application are only used to describe specific embodiments and are not intended to limit the present invention. Singular expressions include plural expressions unless the context clearly indicates otherwise. Unless otherwise defined, all terms used herein, including technical or scientific terms, have the same meaning as commonly understood by one of ordinary skill in the art to which the present invention belongs. Terms as defined in a commonly used dictionary should be construed as having a meaning consistent with the meaning of the related technology, and should not be interpreted as an ideal or excessively formal meaning unless explicitly defined in the present application.

The present invention is SiO ₂ 60 to 80 wt%, Al ₂ O ₃ 5 to 15 wt%, Fe ₂ O ₃ 1 to 5 wt%, CaO 1 to 5 wt%, Na ₂ O 1 to 5 wt%, K ₂ O A porous carrier composed of 1 to 5% by weight, MgO 01 to 1% by weight, and Ag ₂ O 0.5 to 10% by weight was mixed by stirring for 1 hour, and then added to a glass melting furnace at 1200 to 1550°C and melted for 30 hours. Preparing a porous carrier (S100); Pulverizing the porous carrier into a nanoparticle shape to prepare a nanoparticle porous carrier powder (S200);

Pulverizing the flaxseed powder into nanoparticles to prepare nanoparticle porous flaxseed powder (S300); And

5 to 10 parts by weight of the nanoparticle porous carrier powder, 5 to 10 parts by weight of the nanoparticle porous flaxseed powder, and 0.5 to 1 parts by weight of the dispersant are mixed for 2 hours to prepare a nanoparticle porous carrier and a flaxseed powder solution to 100 parts by weight of water. It relates to a method for preparing a viral pest prevention and plant growth accelerator consisting of a nanoparticle porous carrier and flaxseed powder, characterized in that consisting of step (S400).

In the present invention, the dispersant is a water-soluble linseed oil dispersion, polyacrylate, acrylic polymer emulsion, and sulfonated polystyrene.

In the present invention, the nanoparticle porous carrier flaxseed powder solution is sprayed onto the roots or leaves of plants to prevent plant root rot, prevent soil coagulation attached to plant roots, prevent pests, prevent fungal growth, sterilize bacteria, inhibit virus propagation, and It is characterized in that the reproduction inhibition and multiply insect reproduction inhibition.

In the present invention, when the nanoparticle porous carrier powder is dissolved in water, the nanomineral components SiO ₂ , Al ₂ O ₃ , Fe ₂ O ₃ , CaO, Na ₂ O, K ₂ O, MgO and Ag ₂ O components are slowly dissolved. Nano-mineral water is generated, a nano-mineral balance is formed, and the mineral balance of Ca, Na, K, and Mg, which are essential components of plant growth, is maintained.

MO + OH ^- → MO- + MOH

In the above formula, M represents the metal component of Al ₂ O ₃ , Fe ₂ O ₃ , CaO, Na ₂ O, K ₂ O, MgO and Ag ₂ O. In the present invention, the metal components of Al ₂ O ₃ , Fe ₂ O ₃ , CaO, Na ₂ O, K ₂ O, MgO and Ag ₂ O, which are nanoparticle porous carrier powder components, are converted into ionic forms in a weak alkaline atmosphere. The ions of the metal oxide generated in the above reaction formula cause the modification of amino acids constituting the protein of the microorganism or bacteria, destroying the cell membrane of the bacteria, causing a perforation in the cell membrane, thereby exhibiting a sterilizing effect. Therefore, the nanoparticle porous carrier powder of the present invention can be used as an antibacterial or disinfectant.

The nanoparticle porous carrier powder of the present invention is used as a freshness preservative for maintaining the freshness of pine mushrooms, strawberries, grapes, and vegetables, and in this case, it is preferably used as a spray product. In addition, it is preferable to spray matsutake mushrooms, strawberries, grapes, and vegetables with the nanoparticle porous carrier powder water of the present invention and then sell them as plastic packaging products. In addition, the nanoparticle porous carrier powder of the present invention is used as an antifungal agent, an antibacterial agent, an odor remover, an agent for preventing rot of plant roots, and the like.

The nanoparticle porous carrier powder of the present invention is a kind of artificially synthesized zeolite and has the excellent effects of zeolite as it is. Zeolite is a fine, nano-sized microporous material generated by the rapid action of volcanic ash in the Cenozoic 3rd base layer. It absorbs physical adsorption (90% to 95%, respectively, such as nitrogen and potassium phosphate) and gas, supplies minerals, and absorbs moisture. It has the effect of preventing soft stool and water stool.

Zeolite is an aluminosilicate mineral containing alkaline earth metals such as sodium and potassium and alkaline earth metals such as calcium, and crystal water. Unlike general structural water, zeolite crystal water exists as water molecules. The island structure is not destroyed, and the water molecules remain intact and become a porous structure like a sponge, and moisture or gas is adsorbed to return to the original state. So, soil improvers, fertilizer mixtures, pesticide extenders, soil mixtures, etc. Agricultural, marine pollution prevention agent, prevention of red tide

For fishery, such as odor and carp feed, odor remover, diarrhea treatment for livestock, water purification, feed additives, livestock, paper filler, wastewater treatment agent, drying agent, ceramic raw material, pharmaceutical raw material, landscaping agent, construction agent, tobacco filter It has been widely known for its properties and uses, such as industrial use, and has excellent stability so that it is used to purify water and is used as a raw material for various pharmaceuticals.

Zeolite is a crystalline aluminosilicate containing alkali metals and alkaline earth metals [SiO ₄ ] and [AlO ₄ ] by crosslinking oxygen atoms to form unique shapes and uniformly sized pores, while regularly forming different geometric arrangements. It forms a three-dimensional skeletal structure. The zeolite water has a slight difference depending on the physical condition and health condition of a person, but after 10 to 30 minutes after drinking 200cc, it has the effect of adsorbing impurities in the body with excellent absorption. Since wastes and debris generated from are discharged smoothly, blood circulation in the body is smooth.

The dispersant used in the present invention is added to prevent poor quality uniformity due to a sudden decrease in dispersibility due to agglomeration of the nanoparticle porous carrier powder due to the nature of the nanoparticle porous carrier powder. It has the advantage of inducing even distribution.

The dispersant used in the present invention is added in an amount of 0.5 to 1 parts by weight relative to the total nanoparticle porous carrier powder, and if it is added in an amount of 0.5 parts by weight or less relative to the total nanoparticle porous carrier powder, the effect is insufficient and the dispersibility of the nanoparticle porous carrier powder In the present invention, it is preferable that 0.5 to 1 part by weight of the dispersant is added relative to the total nanoparticle porous carrier powder.

Water-soluble flaxseed oil is very effective as a dispersant for dispersing the nanoparticle porous carrier powder in the present invention. The dispersant used in the nanoparticle porous carrier powder of the present invention is preferably composed of 0,5 to 1 parts by weight of water-soluble flaxseed oil.

The water-soluble flaxseed oil used in the present invention is heated flaxseeds at 100°C for 20 minutes to remove moisture from flaxseeds, then rapidly cooled, put the rapidly cooled flaxseeds into a milking machine, and milked at a temperature of 100℃ in the milking machine, and then at 200 mesh. Filtrated flaxseed oil was obtained, and the filtered flaxseed oil was naturally precipitated for 20 days, and then purified flaxseed oil was obtained through a process of recovering the upper layer to prepare flaxseed oil, and 50 g of the flaxseed oil and 25 g of water were added. After mixing, 5 g of Tween 60 is added and coated while rotating at high speed at 3000 rpm to use water-soluble flaxseed oil.

[The water-soluble flaxseed oil used in the present invention is added in an amount of 0.1 to 1 part by weight relative to the total nanoparticle porous carrier powder. If it is added in an amount of 0.1 parts by weight or less relative to the total nanoparticle porous carrier powder, the effect is insufficient. In the present invention, it is preferable that the water-soluble flaxseed oil is 0.1 to 1 weight compared to the nanoparticle porous carrier powder because the dispersibility of the nanoparticles is lowered and the production cost is increased when 1 part by weight or more is added to the total nanoparticle porous carrier powder.

In the present invention, the nanoparticle porous carrier powder is uniformly dispersed in a water-soluble flaxseed oil and water mixture, and nanoparticles are mixed even if the nanoparticle porous carrier powder is uniformly dispersed in a water-soluble flaxseed oil and water mixture. Porous carrier powder is mixed without being entangled, and a water-soluble flaxseed oil dispersant is added so that the dispersion is smoothly mixed in the mixture without agglomeration and even distribution of moisture is induced, so the uniformity of quality is poor due to a sudden decrease in dispersibility due to agglomeration. There is an effect that can prevent.

When used as another dispersant in the present invention, any one dispersant selected from among the dispersant polyacrylate, acrylic polymer emulsion, and sulfonated polystyrene 0.5 to 1 compared to the entire nanoparticle porous carrier powder It is preferable to add and use parts by weight.

Example 1

SiO ₂ 60 to 80 wt%, Al ₂ O ₃ 5 to 15 wt%, Fe ₂ O ₃ 1 to 5 wt%, CaO 1 to 5 wt%, Na ₂ O 1 to 5 wt%, K ₂ O 1 to 5 After mixing by stirring the porous carrier composed of wt%, MgO 0.1 to 1 wt% and Ag ₂ O 0.5 to 10 wt% for 0.5 to 1 hour, it is added to a glass melting furnace at 1200 to 1550°C and melted for 19 to 30 hours To prepare a porous carrier and pulverize the porous carrier into a nanoparticle shape to prepare a nanoparticle porous carrier powder, and pulverize the flaxseed powder into a nanoparticle shape to prepare a nanoparticle porous flaxseed powder, and then add the nanoparticle porosity to 100g of water. 10 g of a carrier powder, 10 g of flaxseed powder, and 1 g of a water-soluble flaxseed oil dispersion were mixed for 2 hours to prepare a nanoparticle porous carrier powder solution.

Example 2

The nanoparticle porous carrier and flaxseed powder solution prepared in Example 1 were sprayed onto the roots or leaves of potatoes to observe whether plant growth was promoted.

In the case of general soil, the roots are clumped by prolonging water retention or preventing the movement of oxygen, causing suffocation to cause plant death, but the plant growth accelerator of the present invention has the effect of solving the problem of root rot. In particular, compared to the plant growth accelerator made of nanoparticle porous carrier powder used in Patent Publication 10-2020-8879, the effect was excellent 2 to 4 times.

Example 3

The nanoparticle porous carrier and flaxseed powder solution prepared in Example 1 were sprayed onto the roots or leaves of strawberries to observe whether plant growth was promoted.

When the plant growth accelerator of the present invention is present between the clay attached to the plant roots, the cohesiveness of the soil is reduced to prevent the agglomeration of the soil and the phenomenon of the agglomeration of the roots is improved, thereby supplying oxygen smoothly and occurring in the soil. Noxious gas is easily discharged and the problem of rotting roots is solved. In particular, compared to the plant growth accelerator made of nanoparticle porous carrier powder used in Patent Publication 10-2020-8879, the effect was excellent 2 to 4 times.

Example 4

The nanoparticle porous carrier and flaxseed powder solution prepared in Example 1 were sprayed onto the roots or leaves of pepper to observe whether plant growth was promoted.

Pests gather as odors and excess fertilizers remain on the leaves as food for pests. The plant growth promoter of the present invention removes nutrient sources, which are food for pests, and acts bacteriostatic to reduce pests and diseases. In particular, compared to the plant growth accelerator made of nanoparticle porous carrier powder used in Patent Publication 10-2020-8879, the effect was excellent 2 to 4 times.

Example 5

The nanoparticle porous carrier and flaxseed powder solution prepared in Example 1 were sprayed onto the roots or leaves of pepper to observe whether plant growth was promoted.

The plant growth accelerator of the present invention has an adsorption function that restricts the respiration activity of various bacteria or insects, making it difficult to supply and supply nutrients, inhibit reproduction, and reduce density. The plant growth accelerator of the present invention is porous and smooth oxygen supply proliferates effective bacteria and prevents the propagation of various bacteria. In particular, compared to the plant growth accelerator made of nanoparticle porous carrier powder used in Patent Publication 10-2020-8879, the effect was excellent 2 to 4 times.

S100: preparing a porous carrier by melting
S200: preparing a nanoparticle porous carrier powder

Claims (3)

SiO ₂ 80 wt%, Al ₂ O ₃ 15 wt%, Fe ₂ O ₃ 5 wt%, CaO 5 wt%, Na ₂ O 5 wt%, K ₂ O 5 wt%, MgO 1 wt% and Ag ₂ O 10 A step of preparing a porous carrier by stirring and mixing the porous carrier composed of wt% for 1 hour, and then adding it to a glass melting furnace at 1550° C. and melting for 30 hours; Pulverizing the porous carrier into a nanoparticle shape to prepare a nanoparticle porous carrier powder;
Pulverizing the flax seed powder into nanoparticles to prepare nanoparticle porous flaxseed powder;
10 parts by weight of the nanoparticle porous carrier powder, 10 parts by weight of nanoparticle porous flaxseed powder, and water-soluble flaxseed in 100 parts by weight of water so that the nanoparticle porous carrier powder is uniformly dispersed by the water-soluble flaxseed oil dispersion and can be absorbed by the roots of plants It consists of a step of preparing a nanoparticle porous carrier and flaxseed powder by mixing 1 part by weight of the oil dispersion for 2 hours,
The nanoparticle porous carrier powder and the nanoparticle porous flaxseed powder are uniformly dispersed by a water-soluble flaxseed oil dispersion to be absorbed by the roots of plants to prevent plant root rot, prevent soil agglomeration attached to plant roots, prevent disease and pests, prevent mold growth, A method of producing a viral pest prevention and plant growth accelerator comprising a porous carrier and flaxseed powder, characterized in that bacteria sterilization, virus propagation inhibition, various germ propagation inhibition, and multi-insect propagation inhibition.













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