KR102179757B1 - Method for Preparing a Forming Bone - Google Patents
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- KR102179757B1 KR102179757B1 KR1020200055423A KR20200055423A KR102179757B1 KR 102179757 B1 KR102179757 B1 KR 102179757B1 KR 1020200055423 A KR1020200055423 A KR 1020200055423A KR 20200055423 A KR20200055423 A KR 20200055423A KR 102179757 B1 KR102179757 B1 KR 102179757B1
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Abstract
Description
본 발명은 사람의 시신을 처리하는 화장장에서 발생하는 유골을 성형하는 방법에 관한 것으로, 보다 상세하게는 유골을 분말 상태로 하여 이에 경화제만 소량 첨가하여 낮은 온도와 낮은 압력만으로 성형하는 방법에 관한 것이다. 여기에 유골이 더 잘 보존될 수 있도록 처리 속도를 신속히 하고 진공상태로 성형함으로써 유골의 DNA 등의 변형을 최소화하는 방법에 대한 것이다.The present invention relates to a method of molding ashes generated in a crematorium that treats a human body, and more particularly, to a method of molding the ashes in a powder state and adding only a small amount of a curing agent thereto at low temperature and low pressure. . Here, it is about a method of minimizing the modification of DNA of the ashes by speeding up the processing speed so that the ashes can be better preserved and molding in a vacuum state.
종래의 화장문화는 시신을 화장하여 유골을 용기에 넣고 납골당에 보관하는 것인데, 인산칼슘이 주성분인 유골이 습기를 강하게 흡수하는 성질을 가져 조금만 관리를 소홀히 하면 부패하여 악취를 발생시키며 해충의 침입으로 훼손되는 문제점이 있었다. In the conventional cremation culture, the body is cremated and the ashes are put in a container and stored in the crypt.The ashes, the main component of calcium phosphate, have the property of strongly absorbing moisture, so if little care is neglected, it will decay and generate an odor. There was a problem of being damaged.
이러한 문제점을 해결하기 위하여 (i) 유골을 고온에서 용융하여 서서히 냉각하여 결정체로 제조하거나, (ii) 규석(SiO2), 고령토, 운모, 제올라이트, 탄산칼슘 등을 유골분에 첨가하여, 고온전기로 안의 탄소 틀에 넣고 700℃~900℃의 고온에서 구워 유골을 성형하는 방법 (iii) 유골을 분쇄하여 1000Kbar 이상의 고압으로 압축성형하는 방법을 사용해 왔다.In order to solve this problem, (i) the ashes are melted at high temperature and gradually cooled to form crystals, or (ii) silica stone (SiO2), kaolin, mica, zeolite, calcium carbonate, etc. are added to the remains, and a high-temperature electric furnace The method of molding ashes by putting them in a carbon frame inside and baking them at a high temperature of 700℃~900℃.
(iii)의 제법은 가압을 이용한 제법으로 (ii)의 단점을 보완하였지만 고압 프레스 장치의 설치비용이 고가이고 성형시간이 1시간 정도로 오래 걸리는 단점이 있다. 또한 고압으로 성형하기 때문에 다양한 형태로 성형할 수 없고 구형이거나 뭉툭하고 단순한 형태 외에는 성형할 수 없다는 단점이 있으며, 유골의 DNA 등이 변형되는 단점이 있다.The manufacturing method of (iii) supplemented the disadvantage of (ii) with a manufacturing method using pressurization, but the installation cost of the high pressure press device is expensive, and the molding time is long, as long as 1 hour. In addition, since it is molded at high pressure, it cannot be molded into various shapes, and there is a disadvantage that it cannot be molded except for a spherical or blunt and simple shape, and the DNA of the remains is deformed.
상기와 같은 문제를 해결하기 위해 본 출원인은 대한민국 등록특허 제10-1389607호와 같은 기술을 제안한 바 있다.In order to solve the above problem, the present applicant has proposed a technology such as Korean Patent Registration No. 10-1389607.
그런데 상기의 종래 기술은 유골 변질 방지를 위한 제산, 제습제, 방충제를 첨가하므로 유골 성형의 처리속도가 느리고, 환경오염의 가능성이 있는 문제가 있었다.However, in the prior art, since an antacid, a dehumidifying agent, and an insect repellent are added to prevent the ashes from deteriorating, the processing speed of the ashes molding is slow, and there is a possibility of environmental pollution.
이와 같은 종래의 기술에서 발생하는 문제점을 해결하기 위하여 본 발명은 경화제만을 낮은 온도(섭씨42도씨)에서 낮은 압력으로도 유골의 DNA 등의 변형 없이 유골을 유족이 원하는 모양대로 다양한 모양으로 성형하는데 그 목적이 있다. In order to solve the problems that occur in the prior art, the present invention molds the remains into various shapes as desired by the bereaved family without modification of the DNA of the remains even at low pressure at a low temperature (42 degrees Celsius). There is a purpose.
또한, 낮은온도(섭씨42도씨)와 낮은 압력에서 경화제만을 사용하여 종래에 유골을 성형하는 데서 발생할 수 있는 유골의 변질을 막기 위해 사용한 다양한 화공 약품을 배제하고 처리속도를 단축시키며 사용한 용매를 99% 회수하여 친환경 유골성형을 지향하는데 목적이 있다.In addition, using only the hardener at low temperature (42 degrees Celsius) and low pressure, various chemicals used to prevent the deterioration of the remains that may occur in the conventional molding of the ashes are excluded, the processing speed is shortened, and the solvent used is 99. The purpose is to aim for eco-friendly ashes by recovering %.
또한, 본 발명은 1회 분쇄, 저온, 저압에 의한 성형으로 성형시간을 최대한 단축시키고 소요되는 전력을 절감하여 비용을 낮추는 데 그 목적이 있다. In addition, an object of the present invention is to reduce the cost by shortening the molding time as much as possible by one-time grinding, molding by low temperature and low pressure, and reducing power required.
본 발명은 상술한 목적들을 달성하기 위하여 다음과 같은 수단을 사용한다. The present invention uses the following means to achieve the above objects.
본 발명은 (a) 유골 분말에 불포화 폴리에스테르 수지(경화제)를 넣고 교반하는 단계; (b) 상기 교반된 유골 분말에 저온(42℃)에서 1kbar 정도의 압력을 가해 성형체를 얻는 단계를 포함하여 유골 성형물을 제조하여, 유골 분말을 경화제인 불포화 폴리에스테르 수지(멜라민 수지 등)를 사용하여 성형함으로서 저온(42℃)에서 1kbar 정도의 낮은 압력에서도 성형이 가능하도록 하는 데 특징이 있다. 이때 경화제의 안정제를 추가 투입 없이 바로 교반한다. The present invention comprises the steps of (a) adding and stirring an unsaturated polyester resin (curing agent) to the ashes powder; (b) preparing a molded ashes including the step of obtaining a molded body by applying a pressure of about 1 kbar to the stirred ashes powder at a low temperature (42°C), and using an unsaturated polyester resin (melamine resin, etc.) as a curing agent for the ashes powder It is characterized in that it enables molding at low temperature (42℃) at a pressure as low as 1kbar. At this time, the stabilizer of the curing agent is immediately stirred without additional addition.
또한, 본 발명은 상기 단계에 (a) 활성탄과 유골 분말과 아세톤을 넣고 교반하는 단계; 및 (b) 교반 후에 분별증류를 통해 아세톤을 99% 회수하는 단계를 추가로 포함하여, 유골 성형물이 자체적으로 제산 및 제습 기능을 가지도록 하면서도 용매로 사용된 아세톤을 회수하여 유골의 변형을 최소화하는 데 특징이 있다. 이때 활성탄은 불순물을 흡착하는 효과를 가진다.In addition, the present invention comprises the steps of (a) adding activated carbon, ashes powder, and acetone to the above step and stirring; And (b) further comprising the step of recovering 99% of acetone through fractional distillation after stirring, while minimizing the deformation of the remains by recovering acetone used as a solvent while allowing the molded remains to have its own antacid and dehumidifying functions. There are features. At this time, activated carbon has an effect of adsorbing impurities.
또한, 본 발명은 상기 유골 분말에 추가적인 약품의 투입을 배제하고 교반후 유골성형물의 처리를 가속함으로 유골성형물 안을 진공상태로 함으로써 유골 성형물이 자체적으로 방충력을 가질 수 있도록 하는 데 특징이 있다. In addition, the present invention is characterized in that the injection of additional chemicals to the ashes powder is excluded and the processing of the ashes after stirring is accelerated, so that the inside of the ashes is in a vacuum state, so that the ashes can have insect repellency by itself.
본 발명은 다음과 같은 우수한 효과 있다.The present invention has the following excellent effects.
먼저 본 발명에 의하면, 경화제만을 사용하여 유골을 성형하므로 성형에 적합한 유골 분말의 크기가 종래보다 커도 무방하다. 따라서, 종래에는 통상 2회의 분쇄가 필요했지만 본 발명에서는 1회의 분쇄로도 충분하여 시간이 적게 들고, 투입되는 에너지가 적다.First, according to the present invention, since the ashes are molded using only the curing agent, the size of the ashes powder suitable for molding may be larger than the conventional one. Therefore, conventionally, two pulverization was normally required, but in the present invention, one pulverization is sufficient, which takes less time and less energy to be input.
또한, 종래에는 1시간 동안 1000Kbar의 가압이 필요했지만 본 발명에 의하면 경화제를 사용하여 유골을 성형하므로 유골 분말을 1kbar의 압력을 1분간 가하는 것으로도 성형이 가능하다.In addition, conventionally, 1000Kbar of pressure was required for 1 hour, but according to the present invention, since the ashes are molded using a curing agent, it is possible to mold the ashes powder by applying a pressure of 1kbar for 1 minute.
또한, 본 발명에 의하면, 경화제를 사용함으로써 종래보다 더 정교한 성형이 가능하다.In addition, according to the present invention, more sophisticated molding is possible than before by using a curing agent.
또한 본 발명에 의하면 유골을 진공상태로 처리함으로써 유골이 습기나 산에 의해 변질되는 것을 막을 수 있다.In addition, according to the present invention, by treating the ashes in a vacuum state, it is possible to prevent the ashes from being deteriorated by moisture or acid.
또한 본 발명에 의하면 유골을 진공상태로 처리함으로써 해충에 의해 훼손되는 것을 막을 수 있다.Further, according to the present invention, it is possible to prevent damage by pests by treating the ashes in a vacuum state.
또한, 본 발명에 의하면 용매로 사용한 아세톤을 회수함으로써, 유골의 변형을 막을 수 있다.In addition, according to the present invention, by recovering acetone used as a solvent, it is possible to prevent deformation of the ashes.
도 1은 본 발명의 바람직한 실시예에 따른 유골을 이용한 성형체를 제조하는 과정을 나타낸 순서도이다.1 is a flow chart showing a process of manufacturing a molded body using ashes according to a preferred embodiment of the present invention.
본 발명에서 사용되는 용어는 가능한 현재 널리 사용되는 일반적인 용어를 선택하였으나, 특정한 경우는 출원인이 임의로 선정한 용어도 있는데 이 경우에는 단순한 용어의 명칭이 아닌 발명을 실시하기 위한 구체적인 내용에 기재되거나 사용된 의미를 고려하여 그 의미가 파악되어야 할 것이다. As for terms used in the present invention, general terms that are currently widely used are selected, but in certain cases, some terms are arbitrarily selected by the applicant. In this case, the meanings described or used in the specific contents for carrying out the invention are not just the names of terms. The meaning should be grasped in consideration of.
먼저, 본 발명에 사용되는 시약의 명칭과 화학식 및 각 시약의 용도는 다음과 같다. First, the names and chemical formulas of the reagents used in the present invention and the uses of each reagent are as follows.
불포화 폴리에스테르 수지(멜라닌 수지 등) - 경화제Unsaturated polyester resin (melanine resin, etc.)-hardener
활성탄(C) - 불순물제거Activated carbon (C)-remove impurities
아세톤 Dimethyl Ketone : CH3COCH3 - 용매 Acetone Dimethyl Ketone: CH 3 COCH 3 -Solvent
디메틸에테르 Diethyl ether : C2H50C2H5 - 세척제Diethyl ether: C 2 H 5 0C 2 H 5 -Cleaner
본 발명은 유골 분말을 경화제인 불포화 폴리에스테르 수지(멜라닌 수지 등)만을 사용하여 낮은 온도, 낮은 압력에서 빠른 속도로 유골 분말의 성형이 가능하도록 하는 데 기술적 특징이 있다. The present invention has a technical feature in enabling the ashes powder to be molded at a high speed at a low temperature and low pressure using only an unsaturated polyester resin (melanine resin, etc.) as a curing agent.
불포화 폴리에스테르 수지는 불포화기를 가진 선 모양의 폴리에스테르와 비닐 단위체의 혼성 중합에 의하여 얻어지는 열경화성 수지로, 용액 상태의 불포화 폴리에스테르 수지에 반응 개시제를 가하여 틀에 넣으면 혼성 중합 가교 반응으로 용해·용융 되지 않는 성형물이 된다. 불포화 폴리에스테르 수지는 상온, 상압에서도 성형되는 장점이 있다. Unsaturated polyester resin is a thermosetting resin obtained by hybrid polymerization of a linear polyester with unsaturated groups and a vinyl unit.When a reaction initiator is added to the solution-state unsaturated polyester resin and placed in a frame, it cannot be dissolved or melted through a cross-linking reaction. It becomes a molded product that does not work. Unsaturated polyester resin has the advantage of being molded at room temperature and pressure.
또한, 본 발명은, 상기 경화제만을 용매인 아세톤과 함께 교반하여 처리 시간을 단축시키고 유골 분말의 변형을 최소화할 수 있다. In addition, in the present invention, only the curing agent may be stirred with acetone as a solvent to shorten the processing time and minimize the deformation of the ashes powder.
또한 빠른 가압시간으로 성형체 내부를 진공상태로 함으로써 자체적으로 방충, 방염을 가능하게 하였고, 보존 기간을 최대한 연장시켰다.In addition, by making the inside of the molded body in a vacuum state with a quick pressurization time, it is possible to self-insect and flame retardant, and the preservation period is extended as much as possible.
이하, 첨부한 도 1에 도시된 본 발명의 바람직한 바람직한 실시 예를 참조하여 본 발명의 기술적 구성을 상세하게 설명한다.Hereinafter, the technical configuration of the present invention will be described in detail with reference to a preferred embodiment of the present invention shown in FIG. 1.
먼저 유골을 분쇄 및 건조한다.(S41)First, the ashes are crushed and dried (S41).
이때, 분쇄된 유골 분말의 크기가 0.1mm이하가 되어야 하는데, 본 발명은 경화제를 사용하여 유골을 성형하므로, 1회 분쇄로 충분하다.At this time, the size of the pulverized ashes powder should be 0.1mm or less, but since the present invention molds the ashes using a hardener, one pulverization is sufficient.
그 다음 유골 분말 100g 당 아세톤 용매 약 10ml, 디메틸에테르 20ml, 제충국 추출물을 교반 후 분별 증류로 용매를 회수, 세척제인 디메틸에테르는 여과로 회수한다.(S42)Then, about 10 ml of acetone solvent, 20 ml of dimethyl ether, and pyrethrum extract per 100 g of the ashes powder are stirred, and the solvent is recovered by fractional distillation, and dimethyl ether, a detergent, is recovered by filtration (S42).
상기 제충국 추출물은 살충 성분이 포함된 국화의 일종인 제충국에서 추출한 것으로 특히 꽃 부분의 "피레트린"을 유기용매에 의해 추출하여 피레트린을 포함한 추출물로 해충의 접근을 방지하나 인체에는 무해한 특징을 갖는다.The pyrethrum extract is extracted from pyrethrum, which is a kind of chrysanthemum containing insecticidal ingredients. In particular, "pyrethrin" in the flower part is extracted with an organic solvent to prevent access to pests, but harmless to the human body. .
이때, 활성탄을 추가적으로 투입하여 유골 분말과 아세톤 용매와 디메틸에테르와 같이 교반하여 활성탄이 불순물을 흡착하도록 할 수 있다.At this time, the activated carbon may be additionally added and stirred with the ashes powder, acetone solvent, and dimethyl ether to allow the activated carbon to adsorb impurities.
그 다음 상기 혼합물에 불포화 폴리에스테르 수지(멜라민수지 등) 약 0.1g을 넣고 섭씨 42도에서 약 1분간 교반한다.(S43)Then, about 0.1 g of an unsaturated polyester resin (melamine resin, etc.) is added to the mixture and stirred for about 1 minute at 42 degrees Celsius. (S43)
상기와 같은 온도와 교반시간은 혼합물 내에 공기가 없이 진공상태로 되도록 한다.The above temperature and stirring time are made to be in a vacuum state without air in the mixture.
그 다음 성형 틀에 상기 혼합물을 넣고 섭씨42도에서 1kbar 정도의 낮은 압력을 혼합물에 2초~3초간 가한 후 성형물을 수득한다.(S44)Then, the mixture was put in a molding mold, and a low pressure of about 1 kbar at 42 degrees Celsius was applied to the mixture for 2 to 3 seconds, and a molded product was obtained (S44).
상기의 과정에 의해 성형물은 내부가 진공상태로 고형화된다.By the above process, the inside of the molded product is solidified in a vacuum state.
그 다음 디메틸에테르 용매에 1회 10초 담궈 불순물을 제거하고 자연건조시키면 유골성형체가 완성된다.(S45)Then, it is immersed in a dimethyl ether solvent for 10 seconds to remove impurities and air-dried to complete the ashes (S45).
이때, 상기 성형물이 자연건조된 후 습도지시약을 자연건조된 상기 성형물의 표면 일부에 도포하는 단계를 더 포함하게 할 수 있다. 상기 습도지시약은 염화코발트 등 습도가 높아지면 색상이 나타나는 물질을 포함하는 지시약으로 부패가 발생할 수 있는 상대습도 65% 이상에서는 발색되는 종류인 것이 바람직하며, 성형물의 부패가능성을 사용자가 알 수 있도록 하는 역할을 한다.In this case, after the molding is naturally dried, a step of applying a humidity indicator to a part of the surface of the naturally dried molding may be further included. The humidity indicator is an indicator containing a substance that appears color when the humidity increases, such as cobalt chloride, and is preferably a type that develops color at a relative humidity of 65% or more, which can cause decay, and allows the user to know the possibility of decay of the molded product. Plays a role.
또한 상기 성형물이 자연건조된 후 방수코팅제를 자연건조된 상기 성형물의 표면 전체에 도포하는 단계를 더 포함하도록 하여 성형물이 침수 등에 의해 부패되는 것을 2중으로 방지할 수 있다. 이때 방수코팅제는 투명한 것이 바람직하며, 시중에서 널리 사용되는 우레탄 방수 코팅제 등 다양한 방수코팅제가 사용될 수 있다.In addition, after the molding is naturally dried, the step of applying a waterproof coating agent to the entire surface of the naturally dried molding may be further included, so that the molded product can be prevented from being spoiled by immersion. At this time, the waterproof coating agent is preferably transparent, and various waterproof coating agents such as urethane waterproof coating agents widely used in the market may be used.
이상에서 살펴본 바와 같이 본 발명은 바람직한 실시 예를 들어 도시하고 설명하였으나, 상기한 실시 예에 한정되지 아니하며 본 발명의 정신을 벗어나지 않는 범위 내에서 당해 발명이 속하는 기술분야에서 통상의 지식을 가진 자에 의해 다양한 변경과 수정이 가능하다 할 것이다.As described above, the present invention has been illustrated and described with a preferred embodiment, but is not limited to the above-described embodiment, and within the scope of the spirit of the present invention, those of ordinary skill in the art It will be said that various changes and modifications are possible.
Claims (3)
(b) 상기 분쇄된 유골 분말에 유골 분말 100g 당 아세톤 용매 10ml, 디메틸에테르 20ml, 제충국 추출물 교반 후 분별 증류로 용매를 회수, 세척제인 디메틸에테르는 여과로 회수하는 단계; 및
(c) 상기 단계를 거친 유골 분말에 불포화 폴리에스테르 수지 0.1g을 넣고 섭씨 42도에서 1분간 공기가 없이 진공상태로 교반하는 단계; 및
(d) 성형 틀에 상기 혼합물을 넣고 섭씨42도에서 1kbar의 낮은 압력을 혼합물에 2초~3초간 가한 후 성형물을 수득하는 단계; 및
(e) 상기 성형물을 디메틸에테르 용매에 1회 10초 담궈 불순물을 제거하고 자연건조시키면 유골성형체가 완성하는 단계를 포함하는 유골 성형물의 제조 방법. (a) grinding and drying the ashes; And
(b) recovering the solvent by fractional distillation after stirring the pulverized ashes powder per 100 g of the ashes powder, 10 ml of acetone solvent, 20 ml of dimethyl ether, and pyrethrum extract, and recovering the dimethyl ether as a detergent by filtration; And
(c) adding 0.1 g of an unsaturated polyester resin to the ashes powder passed through the above step and stirring in a vacuum state without air at 42 degrees Celsius for 1 minute; And
(d) placing the mixture in a molding mold and applying a low pressure of 1 kbar at 42 degrees Celsius to the mixture for 2 to 3 seconds to obtain a molded product; And
(e) a method for producing a molded ashes comprising the step of immersing the molded product in a dimethyl ether solvent for 10 seconds to remove impurities and then naturally drying the molded product to complete the ashes.
상기(b)단계에서 분쇄된 유골 분말에 흡착을 위한 활성탄을 첨가하여 교반하는 것을 특징으로 하는 유골 성형물의 제조 방법.The method of claim 1,
A method for producing an ashes molded article, characterized in that the activated carbon for adsorption is added to the bone powder pulverized in step (b) and stirred.
상기(e)단계에서 상기 성형물이 자연건조된 후 습도지시약을 자연건조된 상기 성형물의 표면 일부에 도포하는 단계를 더 포함하는 유골 성형물의 제조 방법.
The method of claim 1,
The method of manufacturing a molded ashes further comprising the step of applying a humidity indicator to a part of the surface of the naturally dried molded product after the molded product is naturally dried in step (e).
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20060076124A (en) * | 2004-12-29 | 2006-07-04 | (주)지피엔이 | The producing method of cobalt-free humidity indicating agent and its application |
| JP2009275021A (en) * | 2008-05-19 | 2009-11-26 | Sumika Life Tech Co Ltd | Insecticidal composition comprising pyrethrum extract |
| KR20110000774A (en) * | 2009-06-29 | 2011-01-06 | 김상안 | Ceramic type ball using skeletal powder and thereof composition component |
| KR20140035108A (en) * | 2012-09-13 | 2014-03-21 | 한규선 | Method for preparing a forming bone |
| KR20180058382A (en) * | 2016-11-24 | 2018-06-01 | 채의수 | Insecitcide Composition with the Extract of Tanacetum cinerariifolium, and Agastache rugosa |
| KR20190123916A (en) * | 2018-04-25 | 2019-11-04 | 한규선 | Method for Preparing a Forming Bone |
-
2020
- 2020-05-08 KR KR1020200055423A patent/KR102179757B1/en active IP Right Grant
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20060076124A (en) * | 2004-12-29 | 2006-07-04 | (주)지피엔이 | The producing method of cobalt-free humidity indicating agent and its application |
| JP2009275021A (en) * | 2008-05-19 | 2009-11-26 | Sumika Life Tech Co Ltd | Insecticidal composition comprising pyrethrum extract |
| KR20110000774A (en) * | 2009-06-29 | 2011-01-06 | 김상안 | Ceramic type ball using skeletal powder and thereof composition component |
| KR20140035108A (en) * | 2012-09-13 | 2014-03-21 | 한규선 | Method for preparing a forming bone |
| KR20180058382A (en) * | 2016-11-24 | 2018-06-01 | 채의수 | Insecitcide Composition with the Extract of Tanacetum cinerariifolium, and Agastache rugosa |
| KR20190123916A (en) * | 2018-04-25 | 2019-11-04 | 한규선 | Method for Preparing a Forming Bone |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR102418368B1 (en) * | 2022-03-28 | 2022-07-06 | 한규선 | Method for Preparing a Forming Bone |
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