KR102135558B1 - 혼합 디바이스를 포함하는 다층 하향류 반응기, 상기 반응기의 용도, 및 혼합 방법 - Google Patents

혼합 디바이스를 포함하는 다층 하향류 반응기, 상기 반응기의 용도, 및 혼합 방법 Download PDF

Info

Publication number
KR102135558B1
KR102135558B1 KR1020157012014A KR20157012014A KR102135558B1 KR 102135558 B1 KR102135558 B1 KR 102135558B1 KR 1020157012014 A KR1020157012014 A KR 1020157012014A KR 20157012014 A KR20157012014 A KR 20157012014A KR 102135558 B1 KR102135558 B1 KR 102135558B1
Authority
KR
South Korea
Prior art keywords
discharge
ejection
vector
vertical axis
nozzles
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
KR1020157012014A
Other languages
English (en)
Korean (ko)
Other versions
KR20150067330A (ko
Inventor
수자타 데갈레산
베노이트 비트캄프
Original Assignee
쉘 인터내셔날 리써취 마트샤피지 비.브이.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 쉘 인터내셔날 리써취 마트샤피지 비.브이. filed Critical 쉘 인터내셔날 리써취 마트샤피지 비.브이.
Publication of KR20150067330A publication Critical patent/KR20150067330A/ko
Application granted granted Critical
Publication of KR102135558B1 publication Critical patent/KR102135558B1/ko
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/004Sparger-type elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/26Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/002Nozzle-type elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0492Feeding reactive fluids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0496Heating or cooling the reactor
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G49/00Treatment of hydrocarbon oils, in the presence of hydrogen or hydrogen-generating compounds, not provided for in a single one of groups C10G45/02, C10G45/32, C10G45/44, C10G45/58 or C10G47/00
    • C10G49/002Apparatus for fixed bed hydrotreatment processes
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G65/00Treatment of hydrocarbon oils by two or more hydrotreatment processes only
    • C10G65/02Treatment of hydrocarbon oils by two or more hydrotreatment processes only plural serial stages only
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G65/00Treatment of hydrocarbon oils by two or more hydrotreatment processes only
    • C10G65/02Treatment of hydrocarbon oils by two or more hydrotreatment processes only plural serial stages only
    • C10G65/12Treatment of hydrocarbon oils by two or more hydrotreatment processes only plural serial stages only including cracking steps and other hydrotreatment steps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00327Controlling the temperature by direct heat exchange
    • B01J2208/00336Controlling the temperature by direct heat exchange adding a temperature modifying medium to the reactants
    • B01J2208/00353Non-cryogenic fluids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00327Controlling the temperature by direct heat exchange
    • B01J2208/00336Controlling the temperature by direct heat exchange adding a temperature modifying medium to the reactants
    • B01J2208/00353Non-cryogenic fluids
    • B01J2208/00362Liquid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00327Controlling the temperature by direct heat exchange
    • B01J2208/00336Controlling the temperature by direct heat exchange adding a temperature modifying medium to the reactants
    • B01J2208/00353Non-cryogenic fluids
    • B01J2208/00371Non-cryogenic fluids gaseous
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796Details of the reactor or of the particulate material
    • B01J2208/00823Mixing elements
    • B01J2208/00831Stationary elements
    • B01J2208/00849Stationary elements outside the bed, e.g. baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796Details of the reactor or of the particulate material
    • B01J2208/00893Feeding means for the reactants
    • B01J2208/00902Nozzle-type feeding elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796Details of the reactor or of the particulate material
    • B01J2208/00893Feeding means for the reactants
    • B01J2208/00911Sparger-type feeding elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/02Processes carried out in the presence of solid particles; Reactors therefor with stationary particles
    • B01J2208/023Details
    • B01J2208/027Beds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00119Heat exchange inside a feeding nozzle or nozzle reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0449Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
    • B01J8/0453Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being superimposed one above the other

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
KR1020157012014A 2012-10-10 2013-10-08 혼합 디바이스를 포함하는 다층 하향류 반응기, 상기 반응기의 용도, 및 혼합 방법 Active KR102135558B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP12187887 2012-10-10
EP12187887.0 2012-10-10
PCT/EP2013/070972 WO2014056935A1 (en) 2012-10-10 2013-10-08 Multiple-bed downflow reactor comprising a mixing device, use of said reactor, as well as mixing method

Publications (2)

Publication Number Publication Date
KR20150067330A KR20150067330A (ko) 2015-06-17
KR102135558B1 true KR102135558B1 (ko) 2020-07-21

Family

ID=47010375

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020157012014A Active KR102135558B1 (ko) 2012-10-10 2013-10-08 혼합 디바이스를 포함하는 다층 하향류 반응기, 상기 반응기의 용도, 및 혼합 방법

Country Status (6)

Country Link
US (1) US10076736B2 (enExample)
KR (1) KR102135558B1 (enExample)
CA (1) CA2887392C (enExample)
IN (1) IN2015DN02809A (enExample)
RU (1) RU2643041C2 (enExample)
WO (1) WO2014056935A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102903575B1 (ko) * 2025-04-07 2025-12-24 주식회사 티앨씨 합성 반응기

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SG10201805893PA (en) 2015-12-15 2018-08-30 Saudi Arabian Oil Co Supercritical reactor systems and processes for petroleum upgrading
US10066176B2 (en) 2015-12-15 2018-09-04 Saudi Arabian Oil Company Supercritical water upgrading process to produce high grade coke
US10577546B2 (en) 2017-01-04 2020-03-03 Saudi Arabian Oil Company Systems and processes for deasphalting oil
US10815434B2 (en) 2017-01-04 2020-10-27 Saudi Arabian Oil Company Systems and processes for power generation
US10589244B1 (en) 2019-02-07 2020-03-17 Uop Llc Hydroprocessing reactor internals having reduced height
US10668442B1 (en) 2019-02-07 2020-06-02 Uop Llc Hydroprocessing reactor internals having reduced height
RU198299U1 (ru) * 2019-12-17 2020-06-30 Федеральное государственное бюджетное образовательное учреждение высшего образования "Волгоградский государственный технический университет" (ВолгГТУ) Многослойный каталитический реактор
US11207650B1 (en) 2020-09-30 2021-12-28 Uop Llc Hydroprocessing reactor internals having reduced height

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1276457A (en) 1969-03-18 1972-06-01 Chemie Linz Ag Improvements in or relating to the temperature regulation of high pressure synthesis reactions
US4960571A (en) 1988-12-14 1990-10-02 Exxon Research And Engineering Company Quench assembly design
US20070248510A1 (en) 2006-04-25 2007-10-25 Dean Anne M Dual gas-liquid spargers for catalytic processing units

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2632692A (en) * 1949-01-18 1953-03-24 Hydrocarbon Research Inc Multiple bed catalyst apparatus
US3787189A (en) * 1971-12-17 1974-01-22 Standard Oil Co Apparatus for mixing fluids in a vessel between beds of solids
EP0716881B1 (en) * 1994-08-23 1998-06-03 Shell Internationale Researchmaatschappij B.V. Distributor device for multiple-bed downflow reactors
US5635145A (en) * 1994-08-23 1997-06-03 Shell Oil Company Multi-bed downflow reactor
US6486371B1 (en) * 2000-11-28 2002-11-26 Fina Technology, Inc. Multistage reaction system with interstage sparger systems
US7112312B2 (en) * 2001-04-02 2006-09-26 Tai-Sheng Chou Quench box for a multi-bed, mixed-phase cocurrent downflow fixed-bed reactor
US7074371B2 (en) * 2003-05-16 2006-07-11 Exxonmobil Research And Engineering Company Multiphase mixing device with improved quench injection
US7074372B2 (en) 2003-05-16 2006-07-11 Exxonmobil Research And Engineering Company Multiphase mixing device with improved quench injection for inducing rotational flow
DK1846150T3 (da) * 2005-01-21 2010-11-29 Morten Mueller Ltd Aps Fordelingsindretning til beholdere med tofaset, samtidig nedstrømning samt fordelingsfremgangsmåde
DE102006054415A1 (de) * 2006-11-16 2008-05-21 Uhde Gmbh Verfahren und Vorrichtung zum Eindüsen von Sauerstoff in ein einen Synthesereaktor durchströmendes Reaktionsgas
DE102009002592A1 (de) * 2009-04-23 2010-10-28 Evonik Röhm Gmbh Dosierring
RU2417246C1 (ru) * 2009-08-03 2011-04-27 Открытое акционерное общество "Славнефть-Ярославнефтеоргсинтез" Способ каталитического крекинга углеводородного сырья

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1276457A (en) 1969-03-18 1972-06-01 Chemie Linz Ag Improvements in or relating to the temperature regulation of high pressure synthesis reactions
US4960571A (en) 1988-12-14 1990-10-02 Exxon Research And Engineering Company Quench assembly design
US20070248510A1 (en) 2006-04-25 2007-10-25 Dean Anne M Dual gas-liquid spargers for catalytic processing units

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102903575B1 (ko) * 2025-04-07 2025-12-24 주식회사 티앨씨 합성 반응기

Also Published As

Publication number Publication date
US20150258517A1 (en) 2015-09-17
WO2014056935A1 (en) 2014-04-17
KR20150067330A (ko) 2015-06-17
RU2015116415A (ru) 2016-12-10
RU2643041C2 (ru) 2018-01-30
US10076736B2 (en) 2018-09-18
CA2887392C (en) 2022-02-15
CA2887392A1 (en) 2014-04-17
CN104781002A (zh) 2015-07-15
IN2015DN02809A (enExample) 2015-09-11

Similar Documents

Publication Publication Date Title
KR102135558B1 (ko) 혼합 디바이스를 포함하는 다층 하향류 반응기, 상기 반응기의 용도, 및 혼합 방법
RU2542248C2 (ru) Устройство распределения потока текучей среды для каталитических реакторов с нисходящим потоком
US8597595B2 (en) Multiphase contact and distribution apparatus for hydroprocessing
CN103990393B (zh) 用于两相并行容器的具有切向入口的混合设备和混合方法
KR101869760B1 (ko) 수첨처리를 위한 다중상 접촉 및 분배 장치
US7988928B2 (en) Treatment or hydrotreatment reactor with a granular bed and an essentially liquid phase and an essentially gaseous phase flowing through the bed
WO2007121419A1 (en) A fluid distribution tray and method for the distribution of a highly dispersed fluid across a bed of contact material
KR102012629B1 (ko) 다층 하향류 반응기용 분배장치
US20150071834A1 (en) Inter-bed mixing in fixed bed reactors
JP2008528248A5 (enExample)
KR20140107561A (ko) 다층 하향류 반응기용 분배장치
JP7158412B2 (ja) 流動媒体を含むチャンバ内の多相混合物を分配するための新規な装置
CN104781002B (zh) 包括混合装置的多层床下流式反应器、所述反应器的使用方法、以及混合方法
AU2018288546A1 (en) Distributor tray for a fractionating column, comprising a compartment for distributing gas
US20140346086A1 (en) Distributor device for a multiple-bed downflow reactor
US20250091020A1 (en) Fluid distributor and up-flow reactors
CA2925339A1 (en) Inter-bed mixing in fixed bed reactors

Legal Events

Date Code Title Description
PA0105 International application

Patent event date: 20150507

Patent event code: PA01051R01D

Comment text: International Patent Application

PG1501 Laying open of application
PA0201 Request for examination

Patent event code: PA02012R01D

Patent event date: 20181005

Comment text: Request for Examination of Application

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

Comment text: Notification of reason for refusal

Patent event date: 20191003

Patent event code: PE09021S01D

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

Patent event code: PE07011S01D

Comment text: Decision to Grant Registration

Patent event date: 20200413

GRNT Written decision to grant
PR0701 Registration of establishment

Comment text: Registration of Establishment

Patent event date: 20200714

Patent event code: PR07011E01D

PR1002 Payment of registration fee

Payment date: 20200715

End annual number: 3

Start annual number: 1

PG1601 Publication of registration
PR1001 Payment of annual fee

Payment date: 20230615

Start annual number: 4

End annual number: 4

PR1001 Payment of annual fee

Payment date: 20240617

Start annual number: 5

End annual number: 5

PR1001 Payment of annual fee

Payment date: 20250616

Start annual number: 6

End annual number: 6