KR102103568B1 - Tablet shaped feminine cleanser and manufacturing method thereof - Google Patents

Tablet shaped feminine cleanser and manufacturing method thereof Download PDF

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KR102103568B1
KR102103568B1 KR1020180151476A KR20180151476A KR102103568B1 KR 102103568 B1 KR102103568 B1 KR 102103568B1 KR 1020180151476 A KR1020180151476 A KR 1020180151476A KR 20180151476 A KR20180151476 A KR 20180151476A KR 102103568 B1 KR102103568 B1 KR 102103568B1
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송운서
이차율
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주식회사 라이프 투게더
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    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
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    • A61K36/25Araliaceae (Ginseng family), e.g. ivy, aralia, schefflera or tetrapanax
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    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
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    • A61K36/70Polygonaceae (Buckwheat family), e.g. spineflower or dock
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    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/82Theaceae (Tea family), e.g. camellia
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K9/20Pills, tablets, discs, rods
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P15/00Drugs for genital or sexual disorders; Contraceptives
    • A61P15/02Drugs for genital or sexual disorders; Contraceptives for disorders of the vagina
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P31/00Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
    • A61P31/04Antibacterial agents
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2300/00Mixtures or combinations of active ingredients, wherein at least one active ingredient is fully defined in groups A61K31/00 - A61K41/00

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Abstract

The present invention relates to a tablet-type feminine cleanser and a method of preparing the same, wherein the method comprises the steps of: (a) with respect to 100 parts by weight of purified water, mixing 0.5-5.0 parts by weight of a clove extract and 0.5-1.5 parts by weight of a pine needle extract, stirring the same, and settling the mixture for 10-12 hours to prepare a feminine cleanser base; (b) with respect to 100 parts by weight of purified water, mixing 50-65 parts by weight of the feminine cleanser base, 2-5 parts by weight of a red ginseng extract, and 1-1.2 parts by weight of camellia oil; and (c) with respect to 100 parts by weight of the purified water in step (b), mixing 3-4.5 parts by weight of a natural medicinal herb extract with the mixture, settling the mixture for 10-15 hours, and then aging the same at 10-13°C for 60-75 days, to prepare a primary feminine cleanser. Thus, the feminine cleanser capable of maintaining a potent antibacterial effect and sufficient moisturization for a long time can be prepared in large quantities.

Description

타블릿 제형의 여성 청결제 및 이의 제조방법 {Tablet shaped feminine cleanser and manufacturing method thereof}Tablet-formed feminine cleanser and manufacturing method thereof

본 발명은 타블릿 제형의 여성 청결제 및 이의 제조방법에 관한 것이다.The present invention relates to a female cleansing agent for a tablet formulation and a method for manufacturing the same.

대한민국 등록특허 제1651530호(등록일자: 2016.8.22., 발명의 명칭: 약초추출물을 이용한 여성청결제 제조방법)는 알란토인, 멘톨을 계량한 후 혼합하여 제 1혼합물을 제조하는 제 1단계; 상기 제 1혼합물을 용해하는 제 2단계; 하이드록시에칠셀룰로오스, 피브이피, 발효주정, 베타인, 피피지-25-부테스-26, 피이지-40하이드로제네이티드캐스터오일, 알로에베라추출물을 혼합하여 제 2혼합물을 제조하는 제 3단계; 상기 제 2혼합물을 블렌더를 이용하여 용해하는 제 4단계; 정제수, 녹차추출물, 프로필렌글라이콜, 1,2-헥산디올을 혼합하여 제 3혼합물을 제조하는 제 5단계; 상기 제 3혼합물을 블렌더를 이용하여 용해하는 제 6단계; 상기 제 4단계의 제 2혼합물에 상기 제 6단계의 제 3혼합물, 상기 제 2단계의 제 1혼합물을 순차적으로 혼합하여 청결제 베이스를 제조하는 제 7단계; 상기 청결제 베이스에 디소듐이디티에이, 디포타슘글리시리제이트, 시트릭애씨드, 기능성약초추출물을 혼합한 다음 2일 내지 3일간 숙성하는 제 8단계;를 포함하되, 상기 기능성약초추출물은 한련초추출물 02중량부, 황칠추출물 02중량부, 마치현추출물 02중량부, 고장초추출물 02중량부, 산죽추출물 02중량부, 사자발추출물 02중량부, 비파추출물 02중량부를 혼합하여 제조한 것을 특징으로 하는 약초추출물을 이용한 여성청결제 제조방법이 개시되어 있다.Republic of Korea Registered Patent No. 1661530 (Registration Date: 2016.8.22., Name of the invention: a method for manufacturing a female cleansing agent using herbal extracts) is a first step of preparing a first mixture by weighing and mixing allantoin and menthol; A second step of dissolving the first mixture; The third step of preparing a second mixture by mixing hydroxyethylcellulose, fib, fermentation alcohol, betaine, sebum-25-butes-26, sesame-40hydrogenated castor oil, and aloe vera extract ; A fourth step of dissolving the second mixture using a blender; A fifth step of preparing a third mixture by mixing purified water, green tea extract, propylene glycol, and 1,2-hexanediol; A sixth step of dissolving the third mixture using a blender; A seventh step of sequentially mixing the second mixture of the fourth step with the third mixture of the sixth step and the first mixture of the second step to prepare a cleaner base; The cleanser base is mixed with disodium LED, dipotassium glyceride, citric acid, and functional herbal extracts, followed by aging for 2 to 3 days; 8, including, but the functional herbal extracts are Chinese herbal extracts 02 parts by weight, Hwangchil extract 02 parts by weight, Machihyeon extract 02 parts by weight, Jasper herb extract 02 parts by weight, mountain porridge extract 02 parts by weight, lion's foot extract 02 parts by weight, non-extract extract 02 parts by weight Disclosed is a method for manufacturing a female cleansing agent using.

이러한 종래 기술은, 여성청결제 제조 시 혼합함으로써 약초의 기능성이 부가된 여성청결제를 제공하는 효과가 있다고 주장하는 반면, 제조 공정이 복합한 단점이 있었다.While this prior art claims to have the effect of providing a female cleanser with added functionality of herbal medicines by mixing in the manufacture of a female cleanser, there was a disadvantage in that the manufacturing process was complex.

또한, 대한민국 등록특허 제1870780호(등록일자: 2018.6.19., 발명의 명칭: 다마스크 장미꽃오일 및 프로폴리스 추출물을 유효성분으로 포함하는 여성용 청결제 조성물)는 다마스크 장미꽃오일; 및 금잔화꽃수, 라벤더꽃수, 홍차 추출물 및 프로폴리스 추출물;을 유효성분으로 포함하되, 상기 다마스크 장미꽃오일은 발효오일이고, 상기 발효오일은 슈도지마 츄쿠밴시스(Pseudozyma tsukubaensis)를 접종하여 수득한 여성용 청결제 조성물이 개시되어 있다.In addition, the Republic of Korea Patent No. 1870780 (date of registration: 2018.6.19., The name of the invention: damask rose oil and propolis extract as a active ingredient for female cleaning agent composition) is damask rose oil; And marigold flowers, lavender flowers, black tea extract and propolis extract; as an active ingredient, the damask rose oil is fermented oil, and the fermented oil is obtained by inoculating Pseudozyma tsukubaensis Feminine cleansing compositions are disclosed.

이러한 종래 기술은, 우수한 항염, 항균 활성을 가지고 외음부 질세정, 냉, 가려움 및 악취제거에 우수한 효과가 있으며, 종래의 여성용 질세정 성분에 비해 질염 개선 효과가 우수한 반면, 균주에 의한 발효오일 제조가 용이하지 못한 단점이 있었다.These prior arts have excellent anti-inflammatory and antibacterial activity, and have an excellent effect on vaginal vaginal cleansing, cold, itching, and odor removal, and have an excellent effect of improving vaginitis compared to conventional feminine vaginal cleansing ingredients, while producing fermented oil by strain There were disadvantages that were not easy.

상기와 같은 문제점을 해결하고자 창출된 본 발명의 목적은, 천연 재료로부터 항균성이 양호하고 보습 효과가 양호한 타블릿 제형의 여성 청결제 및 이의 제조방법을 제공하는 데 있다.The object of the present invention, created to solve the above problems, is to provide a feminine cleanser and a method for manufacturing the tablet formulation having good antibacterial properties and good moisturizing effect from natural materials.

이러한 본 발명의 목적은, (a) 정제수 100 중량부에 대하여, 정향추출물 0.5 ~ 5.0 중량부 및 솔잎추출물 0.5 ~ 1.5 중량부를 혼합하여 교반한 후 10 ~ 12시간 정치하여 여성청결제 베이스를 제조하는 단계와; (b) 정제수 100 중량부에 대하여, 여성청결제 베이스 50 ~ 65 중량부, 홍삼추출물 2 ~ 5 중량부 및 동백오일 1 ~ 1.2 중량부를 혼합하는 단계와; (c) 상기 (b)단계의 정제수 100 중량부에 대하여, 천연 한약추출물 3 ~ 4.5 중량부를 혼합한 다음 10 ~ 15시간 정치한 후 10 ~ 13℃에서 60 ~ 75일간 숙성하여 초벌 여성청결제를 제조하는 단계로 이루어지되, 상기 (c)단계의 천연 한약추출물은, 감초추출물 100 중량부에 대하여, 관화육종용추출물 50 ~ 75 중량부, 익모초추출물 10 ~ 15 중량부, 고삼추출물 15 ~ 27 중량부, 하수오추출물 4 ~ 6 중량부 및 애엽추출물 1 ~ 2 중량부로 조성되는 것을 특징으로 하는 여성청결제 제조방법에 의해 달성될 수 있다.The object of the present invention, (a) 100 parts by weight of purified water, 0.5 to 5.0 parts by weight of clove extract and 0.5 to 1.5 parts by weight of pine needle extract, stirred and left for 10 to 12 hours to prepare a female cleanser base Wow; (b) mixing with respect to 100 parts by weight of purified water, 50 to 65 parts by weight of a female cleanser base, 2 to 5 parts by weight of red ginseng extract and 1 to 1.2 parts by weight of camellia oil; (c) Mixing 3 to 4.5 parts by weight of a natural herbal extract with respect to 100 parts by weight of purified water in the step (b), and then standing for 10 to 15 hours, and then aged at 10 to 13 ° C for 60 to 75 days to prepare a first female cleanser The natural herbal extract of step (c) is 50 to 75 parts by weight of the extract for mandarinous sarcoma, 10 to 15 parts by weight of motherwort extract, 15 to 27 parts by weight of ginseng extract, It can be achieved by a method for producing a female cleanser characterized in that it is composed of 4 to 6 parts by weight of sewage extract and 1 to 2 parts by weight of cotyledon extract.

바람직하게는, 본 발명의 상기 (a)단계의 여성청결제 베이스 제조시 온도를 10 ~ 35℃로 유지하기 위하여, 상기 (a)단계의 정제수 100 중량부에 대하여 -15℃ ~ -5℃로 냉각된 스테인레스 볼 10 ~ 15 중량부를 투입하는 (a)-1단계를 더 포함하는 것을 특징으로 한다.Preferably, in order to maintain a temperature of 10 to 35 ° C when manufacturing the female cleanser base of step (a) of the present invention, cooling to -15 ° C to -5 ° C with respect to 100 parts by weight of purified water in step (a) Characterized in that it further comprises (a) -1 step of adding 10 to 15 parts by weight of the stainless steel ball.

바람직하게는, 본 발명의 상기 (a)단계의 정향추출물은, ① 정향 100 중량부에 대하여, 정제수 30 ~ 45 중량부를 혼합한 후 10 ~ 15분간 증숙한 다음 14 ~ 20시간 그늘에서 자연 건조하는 단계와; ② 정제수 100 중량부에 대하여, 증숙건조된 정향 300 ~ 350 중량부, 천일염 5 ~ 7 중량부, 자몽씨추출물 0.3 ~ 0.7 중량부, 비타민 C 1 ~ 3 중량부를 혼합한 다음 180 ~ 240℃에서 30 ~ 45분간 가열한 후 5 ~ 10℃로 급냉하는 단계와; ③ 원심 분리한 후 상등수를 분리한 후 여과하여 10 ~ 15℃에서 보관하는 단계로 제조되고, 상기 (c)단계의 감초추출물은, ⓐ 정제수 100 중량부에 대하여, 감초 50 ~ 75 중량부, 말린 대추 5 ~ 10 중량부, 현미 분말 0.5 ~ 1.5 중량부 및 천일염 3 ~ 5 중량부를 혼합한 다음 80 ~ 85℃에서 240 ~ 270분간 가열한 후 서냉하는 단계와; ⓑ 상기 ⓐ단계의 정제수 100 중량부에 대하여, 편백수 10 ~ 12 중량부를 더 혼합한 후 교반하는 단계와; ⓒ 원심 분리한 후 상등수를 분리한 후 여과하여 10 ~ 15℃에서 보관하는 단계로 제조되는 것을 특징으로 한다.Preferably, the clove extract of the step (a) of the present invention, ① with respect to 100 parts by weight of clove, 30 to 45 parts by weight of purified water and then steamed for 10 to 15 minutes, and then dried naturally in the shade for 14 to 20 hours Step and; ② With respect to 100 parts by weight of purified water, 300 to 350 parts by weight of dried and dried cloves, 5 to 7 parts by weight of sea salt, 0.3 to 0.7 parts by weight of grapefruit seed extract, and 1 to 3 parts by weight of vitamin C, and then 30 at 180 to 240 ° C Rapidly heating to 5-10 ° C. after heating for 45 minutes; ③ After centrifugation, the supernatant is separated, filtered and stored at 10 to 15 ° C. The licorice extract of step (c) is ⓐ 50 to 75 parts by weight of licorice, dried Mixing 5-10 parts by weight of jujube, 0.5-1.5 parts by weight of brown rice powder and 3-5 parts by weight of sea salt, and then heating at 80-85 ° C for 240-270 minutes, followed by slow cooling; Ⓑ with respect to 100 parts by weight of purified water in step ⓐ, mixing 10 to 12 parts by weight of cypress water, followed by stirring; Ⓒ After centrifugation, supernatant is separated, filtered and stored at 10 ~ 15 ℃.

바람직하게는, 본 발명의 상기 (c)단계 이후에 (d)단계를 더 포함하되, 상기 (d)단계는 상기 초벌 여성청결제 100 중량부에 대하여, 냉이 발효추출물 0.5 ~ 1.0 중량부, 달래 발효추출물 0.5 ~ 1.0 중량부 및 원추리 발효추출물 0.5 ~ 1.0 중량부를 혼합하는 단계를 더 포함하되, 상기 냉이 발효추출물은 냉이 100 중량부에 대하여, 설탕 100 ~ 150 중량부 및 감초 10 ~ 15 중량부를 밀폐용기에 충전하여 6 ~ 9개월 발효한 후 원심분리하여 상등수를 분리하여 제조되고, 상기 달래 발효추출물은 달래 구군 100 중량부에 대하여, 설탕 100 ~ 150 중량부, 양조식초 10 ~ 15 중량부 및 감초 10 ~ 15 중량부를 밀폐용기에 충전하여 6 ~ 9개월 발효한 후 원심분리하여 상등수를 분리하여 제조되고, 상기 원추리 발효추출물은 원추리 뿌리 100 중량부에 대하여, 설탕 10 ~ 15 중량부 및 감초 10 ~ 15 중량부를 밀폐용기에 충전하여 6 ~ 9개월 발효한 후 원심분리하여 상등수를 분리하여 제조되는 것을 특징으로 한다.Preferably, the step (d) after the step (c) of the present invention further comprises a step (d), the step (d) with respect to 100 parts by weight of the first female cleanser, wasabi fermentation extract 0.5 ~ 1.0 parts by weight, soothing fermentation Further comprising the step of mixing 0.5 to 1.0 parts by weight of the extract and 0.5 to 1.0 parts by weight of the fermented extract of the original, the horseradish fermented extract is 100 to 150 parts by weight of sugar, 100 to 150 parts by weight of sugar and 10 to 15 parts by weight of licorice in a sealed container The fermentation extract is prepared by separating the supernatant by centrifugation after fermentation for 6 to 9 months, and the soothing fermentation extract is 100 to 150 parts by weight of sugar, 10 to 15 parts by weight of brewed vinegar, and licorice 10 ~ 15 parts by weight is filled in a sealed container, fermented for 6 to 9 months, and then centrifuged to separate the supernatant, and the original fermented extract is 10 to 15 parts by weight of sugar and 10 to 15 parts of licorice for 100 parts by weight of the root of the original medium It is characterized by being produced by separating the supernatant by centrifugation after fermentation for 6 to 9 months by filling the amount in a sealed container.

본 발명의 다른 목적은, 위의 방법들 중 어느 한 방법에 의해 제조되며, 고형제인 마그네슘 스테아레트, 결합제인 하이드록시에칠셀룰로오스, 금속이온 붕쇄제인 디소듐이디티에이, 알라토인 및 멘톨을 함유하는 타블릿 제형의 여성청결제에 의해 달성될 수 있다.Another object of the present invention is prepared by any one of the above methods, solid magnesium stearate as a binder, hydroxyethyl cellulose as a binder, disodium disodium, a metal ion disintegrating agent, alatoin and menthol It can be achieved by a feminine cleanser of the tablet formulation containing.

이상과 같은 본 발명은 강력한 항균 효과와 충분한 보습을 장시간 유지할 수 있는 여성청결제를 대량 생산할 수 있는 효과가 있다.The present invention as described above has an effect that can produce a large amount of a female cleanser that can maintain a strong antibacterial effect and sufficient moisturization for a long time.

이하, 본 발명의 실시예를 참조하여 설명하기로 한다.Hereinafter, it will be described with reference to embodiments of the present invention.

1. 여성청결제 베이스 만들기1. Creating a female cleanser base

먼저, 여성청결제 베이스는 정제수 100 중량부에 대하여, 정향추출물 0.5 ~ 5.0 중량부 및 솔잎추출물 0.5 ~ 1.5 중량부를 혼합하여 제조한다.First, the female cleanser base is prepared by mixing 0.5 to 5.0 parts by weight of clove extract and 0.5 to 1.5 parts by weight of pine needle extract with respect to 100 parts by weight of purified water.

여기서, 정향추출물은 주성분인 정향오일이 민감하며 특히, 45℃ 이상에서는 정향오일의 산폐가 급속하게 진전되기 때문에 이를 방지하기 위하여 여성청결제 베이스의 제조시 온도를 10 ~ 35℃로 유지하여야 하며, 최적 온도는 12 ~ 15℃이다.Here, the clove extract is sensitive to clove oil, which is the main component. Especially, at 45 ° C or higher, the clogging of clove oil is rapidly developed. To prevent this, the temperature of the cleanser base should be maintained at 10 to 35 ° C. The temperature is 12-15 ℃.

본 실시예에서는 여성청결제 베이스 제조시 온도를 10 ~ 35℃로 유지하기 위하여, 정제수 100 중량부에 대하여 -15℃ ~ -5℃로 냉각된 스테인레스 볼(Stainless balls) 10 ~ 15 중량부를 투입한다. 본 실시예에서 냉각된 스테인레스 볼을 사용하는 이유는 별도의 냉각장치를 구비하지 않아도 간편하고 용이하게 최적 온도를 유지할 수 있고 제조되는 여성청결제 베이스에 유해한 영향을 미치지 않기 때문이다.In this embodiment, 10 to 15 parts by weight of stainless balls cooled to -15 ° C to -5 ° C with respect to 100 parts by weight of purified water are added in order to maintain the temperature at 10 to 35 ° C when manufacturing the female cleanser base. The reason for using the cooled stainless ball in this embodiment is that it is simple and easy to maintain the optimum temperature without having a separate cooling device, and does not adversely affect the manufactured female cleanser base.

정향은 정향나무의 꽃봉오리로서, 분말이나 정향유를 식용, 약용하며 방부제로도 사용한다. 특히, 정향은 위가 차가워서 생기는 구토, 위암, 복통, 소화불량과 성기능 증대, 잇몸염증 및 잇몸통증 등에 쓰인다. 약리작용으로 위액분비촉진, 진통, 항경련, 항염, 항산화, 항혈전, 항균, 구충, 혈압강하작용 등이 보고되었다.Clove is a bud of a clove tree, edible, medicinal, or used as a preservative. In particular, clove is used for vomiting, stomach cancer, abdominal pain, indigestion and increased sexual function, gum inflammation and gum pain caused by cold stomach. As a pharmacological action, gastric secretion promotion, analgesic, anticonvulsant, anti-inflammatory, antioxidant, antithrombotic, antibacterial, anthelmintic and hypotensive effects have been reported.

본 실시예의 정향추출물은 열수 추출방법에 의해 추출된다.The clove extract of this embodiment is extracted by a hot water extraction method.

① 정향 100 중량부에 대하여, 정제수 30 ~ 45 중량부를 혼합한 후 10 ~ 15분간 증숙한 다음 14 ~ 20시간 그늘에서 자연 건조한다.① For 100 parts by weight of cloves, mix 30 to 45 parts by weight of purified water, boil for 10 to 15 minutes, and then dry naturally in the shade for 14 to 20 hours.

여기서, 정향을 증숙하는 이유는 정향 표면의 불순물을 제거하기 쉽도록 함과 동시에 유효성분을 농축하기 위함이다.Here, the reason for steaming cloves is to make it easy to remove impurities on the cloves surface and to concentrate the active ingredients.

② 정제수 100 중량부에 대하여, 증숙건조된 정향 300 ~ 350 중량부, 천일염 5 ~ 7 중량부, 자몽씨추출물 0.3 ~ 0.7 중량부, 비타민 C 1 ~ 3 중량부를 혼합한 다음 180 ~ 240℃에서 30 ~ 45분간 가열한 후 5 ~ 10℃로 급냉한다.② With respect to 100 parts by weight of purified water, 300 to 350 parts by weight of dried and dried cloves, 5 to 7 parts by weight of sea salt, 0.3 to 0.7 parts by weight of grapefruit seed extract, and 1 to 3 parts by weight of vitamin C, and then 30 at 180 to 240 ° C After heating for ~ 45 minutes, it is rapidly cooled to 5 ~ 10 ℃.

여기서, 천일염, 자몽씨추출물 및 비타민 C는 정향의 부패를 방지하고 잡균의 증식을 미연에 방지하기 위하여 제공된 것이다.Here, the sun salt, grapefruit seed extract and vitamin C are provided to prevent spoilage of cloves and prevent the growth of various germs.

③ 그런 다음, 원심 분리한 후 상등수를 분리한 후 여과하여 완성한다.③ Then, after centrifugation, the supernatant is separated and filtered to complete.

이렇게 추출된 정향추출물은 10 ~ 15℃에서 보관한다.The clove extract thus extracted is stored at 10 ~ 15 ℃.

솔잎은 상록침엽의 교목인 소나무의 잎이자 향신료로, 초록색에 바늘과 같이 얇고 길쭉한 생김새를 가지고 있으며 그 향은 상쾌하고 쓴맛이 난다. 특히, 솔잎에는 비타민 A, C, K가 함유되어 있어 혈액 순환을 돕고 피부 미용, 피로 해소, 면역력 개선 등에 도움을 주며 그밖에 위장 질환 예방 등의 효과가 있는 것으로 보고되었다.Pine needles are the leaves and spices of evergreen coniferous trees, green and have a thin, elongated appearance like needles, and the fragrance has a refreshing and bitter taste. In particular, pine needles contain vitamins A, C, and K to help blood circulation, help skin beauty, relieve fatigue, and improve immunity, and have been reported to have other effects such as preventing gastrointestinal diseases.

본 실시예의 솔잎추출물은 발효추출 방법에 의해 추출된다.The pine needle extract of this embodiment is extracted by a fermentation extraction method.

① 정제수 100 중량부에 대하여, 솔잎 10,000 ~ 15,000 중량부를 혼합한 후 120 ~ 150℃에서 3 ~ 5분간 증숙한 다음 14 ~ 20시간 그늘에서 자연 건조한다.① With respect to 100 parts by weight of purified water, mix 10,000 to 15,000 parts by weight of pine needles, steam for 3 to 5 minutes at 120 to 150 ℃, and then dry naturally in the shade for 14 to 20 hours.

여기서, 솔잎을 증숙하는 이유는 유효성분을 농축하기 위함이다.Here, the reason for steaming pine needles is to concentrate the active ingredient.

② 정제수 100 중량부에 대하여, 증숙건조된 솔잎 3,500 ~ 4,000 중량부, 설탕 3,500 ~ 5,000 중량부 및 자몽씨추출물 0.3 ~ 0.7 중량부를 밀폐용기에 충전한 후 30 ~ 35℃에서 6 ~ 9개월 발효한다.② For 100 parts by weight of purified water, 3,500 to 4,000 parts by weight of dried pine needles, 3,500 to 5,000 parts by weight of sugar, and 0.3 to 0.7 parts by weight of grapefruit seed extract are filled in a sealed container and fermented at 30 to 35 ℃ for 6 to 9 months. .

여기서, 자몽씨추출물은 솔잎의 부패를 방지하고 잡균의 증식을 미연에 방지하기 위하여 제공된 것이다.Here, the grapefruit seed extract is provided to prevent the decay of pine needles and prevent the growth of various germs.

③ 그런 다음, 원심 분리한 후 여과하여 완성한다.③ Then, after centrifugation, filtration is completed.

이렇게 추출된 솔잎추출물은 10 ~ 15℃에서 보관한다.The pine needle extract extracted in this way is stored at 10 ~ 15 ℃.

2. 피부 보습제 첨가2. Add skin moisturizer

정제수 100 중량부에 대하여, 여성청결제 베이스 50 ~ 65 중량부, 홍삼추출물 2 ~ 5 중량부 및 동백오일 1 ~ 1.2 중량부를 혼합한다.With respect to 100 parts by weight of purified water, 50 to 65 parts by weight of a female cleanser base, 2 to 5 parts by weight of red ginseng extract and 1 to 1.2 parts by weight of camellia oil are mixed.

본 실시예의 홍삼추출물 및 동백오일은 피부 보습제이다.The red ginseng extract and camellia oil of this embodiment are skin moisturizers.

3. 위 2단계의 정제수 100 중량부에 대하여, 천연 한약추출물 3 ~ 4.5 중량부를 혼합한 다음 10 ~ 15시간 정치한 후 10 ~ 13℃에서 60 ~ 75일간 숙성하여 초벌 여성청결제를 제조한다.3. With respect to 100 parts by weight of purified water in the above step 2, 3 to 4.5 parts by weight of a natural herbal extract is mixed and left for 10 to 15 hours, then aged at 10 to 13 ° C for 60 to 75 days to prepare a first female cleanser.

또한, 여성청결제 베이스 100 중량부에 대하여, 편백오일 1 ~ 1.2 중량부를 더 혼합한다. 본 실시예의 편백오일은 소취제이다. 여기서, 편백오일이 0.8 중량부 이하인 경우에는 소취 기능이 현저히 저하되고 1.4 중량부 이상인 경우에는 불쾌한 냄새가 날 수 있기 때문에 함량에 특히 주의하여야 한다.In addition, 1 to 1.2 parts by weight of cypress oil is further mixed with respect to 100 parts by weight of the female cleanser base. Cypress oil in this example is a deodorant. Here, if the cypress oil is 0.8 parts by weight or less, the deodorizing function is remarkably lowered, and if it is 1.4 parts by weight or more, special attention should be paid to the content, since an unpleasant odor may be generated.

여기서, 천연 한약추출물은 감초추출물(Glycyrrhiza Extract) 100 중량부에 대하여, 관화육종용추출물(C.tubulosa Extract) 50 ~ 75 중량부, 익모초추출물(Motherwort Extract) 10 ~ 15 중량부, 고삼추출물(Sophora Flavescens Root Extract) 15 ~ 27 중량부, 하수오추출물(Polygonaceae Extract) 4 ~ 6 중량부 및 애엽추출물(Artemisia princeps leaves Extract) 1 ~ 2 중량부로 조성되어 있다.Here, natural herbal extracts are 100 to 100 parts by weight of licorice extract (Glycyrrhiza Extract), 50 to 75 parts by weight of C. tubulosa extract, Motherwort Extract (10 to 15 parts by weight), and high ginseng extract (Sophora Flavescens) Root Extract) 15 ~ 27 parts by weight, 4 ~ 6 parts by weight of Polygonaceae Extract, and 1 ~ 2 parts by weight of Artemisia princeps leaves Extract.

감초추출물은 글리실리진산 50.0% 미만을 함유하고 있으며, 감초 또는 동속식물의 뿌리 및 줄기를 추출하여 농축한 것으로 감미의 주성분은 백색 또는 무색의 결정성 분말인 글리실리진산이다. 이중 감초정제물에는 천연에서 존재하는 염형과 염형을 탈염한 산형이 있는데 백-황색의 결정 또는 분말형태이거나 황-갈색의 분말, 얇은 조각, 알갱이, 덩어리, 페이스트상 또는 액상의 물질이다. 특히, 감초추출물은 독소 제거 효능이 있으며 다른 약재의 유효성분을 배가시키는 상승 작용이 있다.The licorice extract contains less than 50.0% of glycylic acid, and is concentrated by extracting the roots and stems of licorice or a common plant, and the main component of the sweetness is glycylic acid, a white or colorless crystalline powder. Among the licorice tablets, there are salt forms and salt forms that demineralize salt forms existing in nature. They are white-yellow crystals or powders, or yellow-brown powders, thin flakes, granules, lumps, pastes, or liquid substances. In particular, the licorice extract has the effect of removing toxins and has a synergistic effect of doubling the active ingredients of other medicines.

본 실시예의 감초추출물은 열수 추출방법에 의해 추출된다.The licorice extract of this embodiment is extracted by a hot water extraction method.

ⓐ 정제수 100 중량부에 대하여, 감초 50 ~ 75 중량부, 말린 대추 5 ~ 10 중량부, 현미 분말 0.5 ~ 1.5 중량부 및 천일염 3 ~ 5 중량부를 혼합한 다음 80 ~ 85℃에서 240 ~ 270분간 가열한 후 서냉한다.Ⓐ For 100 parts by weight of purified water, 50 to 75 parts by weight of licorice, 5 to 10 parts by weight of dried jujube, 0.5 to 1.5 parts by weight of brown rice powder, and 3 to 5 parts by weight of sea salt are mixed, and then heated at 80 to 85 ° C for 240 to 270 minutes After cooling slowly.

여기서, 말린 대추는 이뇨, 강장, 완화 효능으로 감초추출물의 독소 제거 효능을 배가시키고, 현미 분말은 천연 점증제이며, 천일염은 부패 방지를 위해 제공된 것이다.Here, the dried jujube doubles the toxin removal effect of the licorice extract with diuretic, tonic, and relieving effects, and the brown rice powder is a natural thickener, and the sea salt is provided to prevent spoilage.

ⓑ 정제수 100 중량부에 대하여, 편백수 10 ~ 12 중량부를 더 혼합한 후 교반한다.Ⓑ For 100 parts by weight of purified water, 10 to 12 parts by weight of cypress water is further mixed and stirred.

ⓒ 그런 다음, 원심 분리한 후 상등수를 분리한 후 여과하여 완성한다.Ⓒ Then, after centrifugation, supernatant is separated and filtered to complete.

이렇게 추출된 감초추출물은 10 ~ 15℃에서 보관한다.The licorice extract thus extracted is stored at 10 ~ 15 ℃.

관화육종용추출물은 한의학(중의학)에서 강장제 및 만성 신질환, 발기부전, 여성불임, 노인성 변비 등의 치료에 사용되는 관화육종용을 스팀처리하여 수용성분을 추출한 것이다.The extract for mandarinous sarcoma is an extract of water-soluble components by steam treatment of mandarin sarcoma used in the treatment of tonic and chronic renal diseases, erectile dysfunction, female infertility, and senile constipation in Oriental Medicine (Chinese Medicine).

익모초은 중국 한방 약용 식물 기본 50가지에 들어가는 식물로 꽃, 잎, 열매, 줄기, 뿌리 등 모든 부위를 약용으로 활용한다. 여기서, 익모초추출물은 자궁 수축작용, 지혈작용, 혈압 낮춤작용, 강심작용, 이뇨작용, 항암작용이 있으며, 부인들의 월경과다, 산후출혈, 생리통, 생리불순, 산후에 배가 아플 때 산전산후의 허약증 등에 널리 사용된다. 특히, 익모초추출물은 여성의 생리불순을 해소하며, 혈액 순환을 자극하여 어혈을 풀어주고 혈전 생성을 억제하는 효과가 있다.Ikmocho is a plant that belongs to 50 basic Chinese herbal medicinal plants and utilizes all parts such as flowers, leaves, fruits, stems, and roots for medicinal purposes. Here, motherwort extract has uterine contraction, hemostasis, blood pressure lowering, strong heart, diuretic, and anti-cancer effects. Excessive menstruation, postpartum hemorrhage, menstrual cramps, menstrual irregularities, postpartum postpartum weakness when the stomach hurts, etc. Widely used. In particular, motherwort extract has the effect of resolving women's menstrual irregularities, stimulating blood circulation, releasing blood and restraining clots.

고삼추출물은 고삼의 뿌리에서 추출한 것으로, 강력한 항염, 항균작용이 있으며, 항알러지 작용을 함과 동시에 피부 가려움증을 완화시켜주고 열독을 제거시켜주는 효능이 있다. 본 실시예의 고삼추출물은 산화 방지제로 사용되고 있다.High ginseng extract is extracted from the roots of high ginseng, has strong anti-inflammatory and anti-bacterial effects, and has an anti-allergic effect, at the same time, relieves skin itching and removes heat poison. The ginseng extract of this example is used as an antioxidant.

하수오추출물은 하수오의 뿌리에서 추출한 것으로, 신장 기능을 튼튼하게 하여 정력을 높이고 머리칼을 검게 하며 장수에 도움이 되며, 특히 간장의 기능을 좋게 하여 피곤함을 제거함은 물론, 살결을 곱게 하며, 뼈와 근육을 튼튼하게 만든다고 하여 옛부터 사용되어 왔으며, 최근 들어 강심 효과와 불면증에도 효과가 있는 것으로 확인되었다.Sewage extract is extracted from the roots of sewage, which strengthens kidney function, enhances stamina, darkens hair, and helps longevity. In particular, it improves the function of soy sauce, removes fatigue, fines the bones and muscles It has been used since ancient times to make it strong, and recently it was confirmed that it has an effect on angina and insomnia.

애엽추출물은 말린 약쑥의 잎에서 추출한 것으로, 성질이 온화한 쑥은 예로부터 몸을 따뜻하게 하며 부인병, 위장병, 간질환, 호흡기 질환 등에 좋은 것으로 알려져 있으며, 또한 혈관을 깨끗하게 해 심혈관 질환을 예방 개선한다.The cotyledon extract is extracted from the leaves of dried wormwood, and wormwood with mild properties has long been known to warm the body and is known to be good for gynecological diseases, gastrointestinal diseases, liver diseases, respiratory diseases, etc., and also prevents and improves cardiovascular disease by cleaning blood vessels.

이상의 조성으로 만들어진 초벌 여성청결제는 에센스와 유사한 액상 제형으로 펌핑 용기에 충전하여 사용되며, 사용시 2 ~ 3회 펌핑한 후 외음부를 따라 부드럽게 마사지하듯이 문지르고 30 ~ 40℃의 미온수로 잔여물이 남지 않도록 헹구어 사용한다.The first female cleanser made with the above composition is used as a liquid formulation similar to the essence, which is used by filling it into a pumping container. When used, it is pumped 2-3 times and rubbed like a gentle massage along the vulva so that no residue remains with lukewarm water at 30 to 40 ℃. Rinse and use.

4. 발효산나물 추출물 혼합하기4. Mixing fermented acid extract

초벌 여성청결제 100 중량부에 대하여, 냉이 발효추출물 0.5 ~ 1.0 중량부, 달래 발효추출물 0.5 ~ 1.0 중량부 및 원추리 발효추출물 0.5 ~ 1.0 중량부를 혼합한다.With respect to 100 parts by weight of the first female cleansing agent, 0.5 to 1.0 parts by weight of the fermented horseradish extract, 0.5 to 1.0 parts by weight of the soothing fermentation extract and 0.5 to 1.0 parts by weight of the fermentation extract from the native root are mixed.

여기서, 본 실시예의 발효산나물 추출물은 모두 식용으로 섭취가 가능한 국내산 산나물을 이용한 것이며, 부인병에 효과가 좋으며 항암 성분이 다량 함유된 것으로 연구 보고되었다.Here, all of the fermented acid herb extracts of this example are made using domestic wild herbs that can be consumed for food, and have been reported to be effective in gynecological diseases and contain large amounts of anti-cancer ingredients.

냉이는 숙취 해소와 간 기능 회복에 우수하며, 중국의 '신농본초경'에는 지방간을 막아준다고 적혀있다. 또한, 냉이는 간경변, 당뇨, 고혈압, 정력감퇴, 불감증, 복막염, 해열, 안질, 두통, 해독, 산후출혈 등에 두루 효과가 있으며, 특히 비장과 간장에 좋은 것으로 알려져 있고, '본초강목'과 '동의보감'에는 동맥경화를 예방하며 변비를 완화한다는 효능이 기재되어 있다.Horseradish is excellent for relieving hangover and restoring liver function, and in China's 'New Nongbo Carbide', it is said to prevent fatty liver. In addition, horseradish is effective for cirrhosis, diabetes, high blood pressure, degeneration, insensitivity, peritonitis, fever, eye disease, headache, detoxification, and postpartum hemorrhage. It is known to be particularly good for spleen and liver, and it is known as 'primary strength' and 'consent' In ', the efficacy of preventing arteriosclerosis and alleviating constipation is described.

냉이 발효추출물은 냉이 100 중량부에 대하여, 설탕 100 ~ 150 중량부 및 감초 10 ~ 15 중량부를 밀폐용기에 충전하여 6 ~ 9개월 발효한 후 원심분리하여 상등수를 분리하여 제조된다.The horseradish fermentation extract is prepared by filling 100 to 150 parts by weight of sugar and 10 to 15 parts by weight of licorice in a sealed container, fermenting for 6 to 9 months, and centrifuging to separate the supernatant.

달래는 백합과의 여러해살이 구근식물로서 '동의보감'에 비장과 신장에 작용해 소화를 돕으며 토사곽란에 좋다고 효능이 기재되어 있다. 또한, 달래는 위장병, 월경불순, 신경 안정에 효과에 있으며, 마늘과 함께 알리움(Allium) 속으로 관상동맥의 흐름을 좋게 해 심장병을 예방하는 동시에, 항소양 성능이 다량 함유된 것으로 보고되어 있다.The soothing lily of the perennial plant is a bulbous plant that acts on the spleen and kidneys in 'Dongui Bogam' to help digestion and is said to be good for sedimentation. In addition, soothing is effective in gastrointestinal diseases, menstrual disorders, and nerve stabilization, and it has been reported that it prevents heart disease by improving the flow of coronary arteries into Allium along with garlic, and also contains a large amount of anti-pruritic performance.

달래 발효추출물은 달래 구군 100 중량부에 대하여, 설탕 100 ~ 150 중량부, 양조식초 10 ~ 15 중량부 및 감초 10 ~ 15 중량부를 밀폐용기에 충전하여 6 ~ 9개월 발효한 후 원심분리하여 상등수를 분리하여 제조된다. 여기서, 달래는 구근만을 사용하며 발효시 양조식초를 첨가하는 이유는 달래의 주성분인 베타카로틴의 추출을 용이하게 하기 위함이다.The soothing fermentation extract is filled with 100 to 150 parts by weight of sugar, 100 to 150 parts by weight of sugar, 10 to 15 parts by weight of brewed vinegar and 10 to 15 parts by weight of licorice in a sealed container, fermented for 6 to 9 months, and then centrifuged to obtain supernatant. It is manufactured separately. Here, only soybean bulb is used, and the reason why brewed vinegar is added during fermentation is to facilitate extraction of the main component of beta-carotene.

원추리는 훤초, 망우초, 금침채, 황화채로도 불리우며 폐결핵, 종양, 궤양, 황달에 약효가 있는 것으로 알려져 있다. 또한, 원추리의 뿌리는 결석, 수종, 불면증, 월경불순, 대하, 변비 등과 젖이 나오지 않는 부인병이 좋은 것으로 알려져 있다.Wonchuri is also known as astringent, mango, gold, and yellow flowers, and is known to be effective in pulmonary tuberculosis, tumors, ulcers, and jaundice. In addition, the root of the cone is known to be good for absenteeism, tree species, insomnia, dysmenorrhea, larvae, constipation, etc.

원추리 발효추출물은 원추리 뿌리 100 중량부에 대하여, 설탕 10 ~ 15 중량부 및 감초 10 ~ 15 중량부를 밀폐용기에 충전하여 6 ~ 9개월 발효한 후 원심분리하여 상등수를 분리하여 제조된다. 여기서, 원추리 뿌리만을 사용하는 이유는 본 실시예에서의 월경불순, 대하 등에 중요 약리성분이 뿌리에 집중되어 있기 때문이며, 설탕을 10 ~ 15 중량부으로 적게 사용하는 이유는 원추리 자체가 4.4%의 당질을 함유하기 있기 때문에 많은 설탕이 필요하지 않기 때문이다.Fermentation extract of Wonchuri is prepared by filling 10 to 15 parts by weight of sugar and 10 to 15 parts by weight of licorice in a sealed container, fermenting for 6 to 9 months, and centrifuging to separate supernatant water. Here, the reason for using only the root of the original root is because important pharmacological components in the present embodiment are concentrated in the root, such as menstrual impurity, daeha, and the reason for using less sugar in 10-15 parts by weight is that the original root itself has a 4.4% sugar content. This is because it does not require a lot of sugar.

5. 타블릿 제형으로 제조5. Tablet formulation

또한, 본 실시예의 여성청결제는 보관이나 지참을 용이하도록 타블릿 제형으로 제조될 수 있다.In addition, the female cleansing agent of this embodiment may be prepared in a tablet formulation to facilitate storage or bringing.

여기서, 여성청결제는 고형제인 마그네슘 스테아레트(Magnesium Stearate)를 첨가하여 타블릿 제형으로 제조되며, 결합제인 하이드록시에칠셀룰로오스(하이드록시에틸셀룰로스)(Hydroxyethylcellulose), 금속이온 붕쇄제인 디소듐이디티에이(Disodium EDTA), 알라토인(Allantoin), 멘톨(Menthol) 등이 첨가될 수 있다.Here, the female cleaning agent is prepared in a tablet formulation by adding magnesium stearate, a solid agent, and a binder, hydroxyethylcellulose (Hydroxyethylcellulose), disodium LED, which is a metal ion disintegrating agent. (Disodium EDTA), allantoin, menthol (Menthol), etc. may be added.

이러한 타블릿 제형의 여성청결제의 제조방법이나 첨가되는 성분들은 공지 기술에 불과하기 때문에 이에 대한 상세한 설명은 생략하기로 한다.Since the method for manufacturing a female cleanser of the tablet formulation or the ingredients added is only a known technique, detailed description thereof will be omitted.

본 실시예의 타블릿 제형의 여성청결제는 깨끗한 미온수(35 ~ 38℃)로 외음부를 씻은 후 타블릿 1 ~ 2정을 온수(38 ~ 42℃)에 10 ~ 15분간 녹여 외음부를 부드럽게 마사지하듯 문지른 다음 물로 헹구지 않고 물기를 그대로 말려 사용한다.The female cleansing agent of the tablet formulation of this embodiment washes the vulva with clean lukewarm water (35 ~ 38 ℃), and then dissolves 1-2 tablets in hot water (38 ~ 42 ℃) for 10-15 minutes, rubs the vulva gently as if massaging, then rinses with water. It is used without drying.

이상과 같은 액상 제형이나 타블릿 제형의 여성청결제는 일반적인 여성청결제와 동일하거나 유사한 세정력을 나타내며 특히, 본 실시예의 특수한 추출공정에 의해 제조된 정향추출물, 감초추출물 및 홍삼추출물로 인해 사용후 불쾌한 냄새가 남지않고 은은하며 그윽한 향기가 일정 시간(10 ~ 24시간) 지속되는 것으로 확인되었다.Women's cleansers in the above liquid formulations or tablet formulations show the same or similar cleaning power as the general women's cleansers, and in particular, unpleasant odors remain after use due to the clove extract, licorice extract and red ginseng extract prepared by the special extraction process of this embodiment. It was confirmed that the subtle scent did not last for a certain period of time (10 to 24 hours).

이상과 같은 본 발명은 일 실시예에 한정되어 설명되었으나, 이에 한정되지 않고 본 발명의 기술적 사상을 토대로 변형되는 실시예들은 모두 본 발명의 권리범위에 속함이 분명하다.The present invention as described above has been described limited to one embodiment, but is not limited thereto, and the embodiments modified based on the technical spirit of the present invention are all within the scope of the present invention.

Claims (5)

(a) 정제수 100 중량부에 대하여, 정향추출물 0.5 ~ 5.0 중량부 및 솔잎추출물 0.5 ~ 1.5 중량부를 혼합하여 교반한 후 10 ~ 12시간 정치하여 여성청결제 베이스를 제조하는 단계와;
(b) 정제수 100 중량부에 대하여, 여성청결제 베이스 50 ~ 65 중량부, 홍삼추출물 2 ~ 5 중량부 및 동백오일 1 ~ 1.2 중량부를 혼합하는 단계와;
(c) 상기 (b)단계의 정제수 100 중량부에 대하여, 천연 한약추출물 3 ~ 4.5 중량부를 혼합한 다음 10 ~ 15시간 정치한 후 10 ~ 13℃에서 60 ~ 75일간 숙성하여 초벌 여성청결제를 제조하는 단계로 이루어지되,
상기 (c)단계의 천연 한약추출물은,
감초추출물 100 중량부에 대하여, 관화육종용추출물 50 ~ 75 중량부, 익모초추출물 10 ~ 15 중량부, 고삼추출물 15 ~ 27 중량부, 하수오추출물 4 ~ 6 중량부 및 애엽추출물 1 ~ 2 중량부로 조성되는 것을 특징으로 하는 여성청결제 제조방법.
(a) mixing 100 parts by weight of purified water, 0.5 to 5.0 parts by weight of the clove extract and 0.5 to 1.5 parts by weight of the pine needle extract, followed by stirring for 10 to 12 hours to prepare a female cleanser base;
(b) mixing with respect to 100 parts by weight of purified water, 50 to 65 parts by weight of a female cleanser base, 2 to 5 parts by weight of red ginseng extract and 1 to 1.2 parts by weight of camellia oil;
(c) Mixing 3 to 4.5 parts by weight of the natural herbal extract with respect to 100 parts by weight of the purified water in the step (b), and then standing for 10 to 15 hours, and then aged at 10 to 13 ° C for 60 to 75 days to prepare the first female cleanser It consists of steps,
The natural herbal extract of step (c),
100 parts by weight of licorice extract, 50 to 75 parts by weight of extract for mandarinous sarcoma, 10 to 15 parts by weight of motherwort extract, 15 to 27 parts by weight of ginseng extract, 4 to 6 parts by weight of sewage extract and 1 to 2 parts by weight of cotyledon extract Method of manufacturing a female cleanser characterized in that.
제 1 항에 있어서,
상기 (a)단계의 여성청결제 베이스 제조시 온도를 10 ~ 35℃로 유지하기 위하여, 상기 (a)단계의 정제수 100 중량부에 대하여 -15℃ ~ -5℃로 냉각된 스테인레스 볼 10 ~ 15 중량부를 투입하는 (a)-1단계를 더 포함하는 것을 특징으로 하는 여성청결제 제조방법.
According to claim 1,
In order to maintain the temperature of 10 to 35 ° C when manufacturing the female cleanser base of step (a), 10 to 15 weight of stainless steel balls cooled to -15 ° C to -5 ° C with respect to 100 parts by weight of purified water in step (a) Method for producing a female cleanser further comprising the step (a) -1 of adding wealth.
제 1 항에 있어서,
상기 (a)단계의 정향추출물은,
① 정향 100 중량부에 대하여, 정제수 30 ~ 45 중량부를 혼합한 후 10 ~ 15분간 증숙한 다음 14 ~ 20시간 그늘에서 자연 건조하는 단계와;
② 정제수 100 중량부에 대하여, 증숙건조된 정향 300 ~ 350 중량부, 천일염 5 ~ 7 중량부, 자몽씨추출물 0.3 ~ 0.7 중량부, 비타민 C 1 ~ 3 중량부를 혼합한 다음 180 ~ 240℃에서 30 ~ 45분간 가열한 후 5 ~ 10℃로 급냉하는 단계와;
③ 원심 분리한 후 상등수를 분리한 후 여과하여 10 ~ 15℃에서 보관하는 단계로 제조되고,
상기 (c)단계의 감초추출물은,
ⓐ 정제수 100 중량부에 대하여, 감초 50 ~ 75 중량부, 말린 대추 5 ~ 10 중량부, 현미 분말 0.5 ~ 1.5 중량부 및 천일염 3 ~ 5 중량부를 혼합한 다음 80 ~ 85℃에서 240 ~ 270분간 가열한 후 서냉하는 단계와;
ⓑ 상기 ⓐ단계의 정제수 100 중량부에 대하여, 편백수 10 ~ 12 중량부를 더 혼합한 후 교반하는 단계와;
ⓒ 원심 분리한 후 상등수를 분리한 후 여과하여 10 ~ 15℃에서 보관하는 단계로 제조되는 것을 특징으로 하는 여성청결제 제조방법.
According to claim 1,
The clove extract of step (a),
① With respect to 100 parts by weight of cloves, after mixing 30 to 45 parts by weight of purified water, steam for 10 to 15 minutes, and then naturally dry in the shade for 14 to 20 hours;
② With respect to 100 parts by weight of purified water, 300 to 350 parts by weight of dried and dried cloves, 5 to 7 parts by weight of sea salt, 0.3 to 0.7 parts by weight of grapefruit seed extract, and 1 to 3 parts by weight of vitamin C, and then 30 at 180 to 240 ° C Rapidly heating to 5-10 ° C. after heating for 45 minutes;
③ After centrifugation, the supernatant is separated, filtered and stored at 10 ~ 15 ℃.
The licorice extract of step (c),
Ⓐ For 100 parts by weight of purified water, 50 to 75 parts by weight of licorice, 5 to 10 parts by weight of dried jujube, 0.5 to 1.5 parts by weight of brown rice powder, and 3 to 5 parts by weight of sea salt are mixed, and then heated at 80 to 85 ° C for 240 to 270 minutes And then slowly cooling;
Ⓑ with respect to 100 parts by weight of purified water in step ⓐ, mixing 10 to 12 parts by weight of cypress water, followed by stirring;
Ⓒ After centrifugation, the supernatant is separated, filtered and stored at 10 ~ 15 ℃ to produce a female cleanser.
제 1 항에 있어서,
상기 (c)단계 이후에 (d)단계를 더 포함하되,
상기 (d)단계는 상기 초벌 여성청결제 100 중량부에 대하여, 냉이 발효추출물 0.5 ~ 1.0 중량부, 달래 발효추출물 0.5 ~ 1.0 중량부 및 원추리 발효추출물 0.5 ~ 1.0 중량부를 혼합하는 단계를 더 포함하되,
상기 냉이 발효추출물은 냉이 100 중량부에 대하여, 설탕 100 ~ 150 중량부 및 감초 10 ~ 15 중량부를 밀폐용기에 충전하여 6 ~ 9개월 발효한 후 원심분리하여 상등수를 분리하여 제조되고,
상기 달래 발효추출물은 달래 구군 100 중량부에 대하여, 설탕 100 ~ 150 중량부, 양조식초 10 ~ 15 중량부 및 감초 10 ~ 15 중량부를 밀폐용기에 충전하여 6 ~ 9개월 발효한 후 원심분리하여 상등수를 분리하여 제조되고,
상기 원추리 발효추출물은 원추리 뿌리 100 중량부에 대하여, 설탕 10 ~ 15 중량부 및 감초 10 ~ 15 중량부를 밀폐용기에 충전하여 6 ~ 9개월 발효한 후 원심분리하여 상등수를 분리하여 제조되는 것을 특징으로 하는 여성청결제 제조방법.
According to claim 1,
After step (c), further comprising step (d),
The step (d) further comprises the step of mixing 0.5 to 1.0 parts by weight of the horseradish fermentation extract, 0.5 to 1.0 parts by weight of the soothing fermentation extract, and 0.5 to 1.0 parts by weight of the original fermentation extract, with respect to 100 parts by weight of the first female cleanser,
The horseradish fermentation extract is prepared by filling 100 to 150 parts by weight of sugar and 10 to 15 parts by weight of licorice in an airtight container, fermenting for 6 to 9 months, and centrifuging to separate supernatant water.
The soothing fermentation extract is filled with 100 to 150 parts by weight of sugar, 100 to 150 parts by weight of sugar, 10 to 15 parts by weight of brewed vinegar and 10 to 15 parts by weight of licorice in a sealed container, fermented for 6 to 9 months, and then centrifuged to obtain supernatant. It is prepared by separating,
The fermentation extract of the original root is prepared by separating the supernatant by centrifuging after fermenting for 6 to 9 months by filling 10 to 15 parts by weight of sugar and 10 to 15 parts by weight of licorice in a sealed container with respect to 100 parts by weight of the root of the original root. A method of manufacturing a female cleanser.
청구항 1 내지 청구항 4 중 어느 한 방법에 의해 제조되며 고형제인 마그네슘 스테아레트, 결합제인 하이드록시에칠셀룰로오스, 금속이온 붕쇄제인 디소듐이디티에이, 알라토인 및 멘톨을 함유하는 타블릿 제형의 여성청결제.A female cleansing agent for a tablet formulation prepared by any one of claims 1 to 4 and containing magnesium stearate as a solid agent, hydroxyethyl cellulose as a binder, disodium IDT as a metal ion disintegrating agent, alatoin and menthol .
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