KR102012217B1 - Method for Manufacturing Allium hookeri Sap - Google Patents
Method for Manufacturing Allium hookeri Sap Download PDFInfo
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- KR102012217B1 KR102012217B1 KR1020170176077A KR20170176077A KR102012217B1 KR 102012217 B1 KR102012217 B1 KR 102012217B1 KR 1020170176077 A KR1020170176077 A KR 1020170176077A KR 20170176077 A KR20170176077 A KR 20170176077A KR 102012217 B1 KR102012217 B1 KR 102012217B1
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- 238000000034 method Methods 0.000 title claims abstract description 16
- 238000004519 manufacturing process Methods 0.000 title abstract description 9
- 241001513212 Allium hookeri Species 0.000 title description 2
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/09—Mashed or comminuted products, e.g. pulp, purée, sauce, or products made therefrom, e.g. snacks
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L21/00—Marmalades, jams, jellies or the like; Products from apiculture; Preparation or treatment thereof
- A23L21/10—Marmalades; Jams; Jellies; Other similar fruit or vegetable compositions; Simulated fruit products
- A23L21/12—Marmalades; Jams; Jellies; Other similar fruit or vegetable compositions; Simulated fruit products derived from fruit or vegetable solids
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/20—Natural extracts
- A23V2250/21—Plant extracts
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Molecular Biology (AREA)
- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
Abstract
본 발명은 자극적인 맛과 향을 지니는 삼채를 물, 에탄올 또는 이들의 혼합액에서 가열추출하는 방법과 당침 방법을 조합하여 순화시킴으로써, 삼채의 유용성분 손실을 최소화하면서 섭취의 거부감을 줄일 수 있는 삼채 진액의 제조방법에 관한 것이다.
본 발명은 삼채를 물, 에탄올 또는 이들의 혼합액에서 가열추출하여 항균 및 항산화 활성이 높은 삼채 추출액을 제조하고 여기에 삼채를 당침하여 삼채의 강한 맛과 향을 순화시킨 삼채 당침액을 혼합하여 삼채 진액을 제조하므로, 높은 항균 및 항산화 활성으로 인하여 삼채 진액을 장기간 저장하여도 쉽게 변질되지 않고 맛과 향이 순화되어 섭취시 거부감을 줄이면서 삼채가 가진 본래의 효능을 유지할 수 있다.The present invention is purified by combining a method of heating and extracting water and ethanol or a mixture of them and acupuncture method of the three flavors having a pungent taste and aroma, to reduce the rejection of intake while minimizing the loss of useful components of the three It relates to a manufacturing method of.
In the present invention, three extracts are heated and extracted from water, ethanol or a mixture thereof to prepare three extracts having high antimicrobial and antioxidant activity, and the three extracts are mixed with three sugar extracts, which have three strong flavors and aromas, and three extracts. Because of the high antibacterial and antioxidant activity, the three extracts are not easily deteriorated even after long-term storage, the taste and aroma are purified, reducing the rejection of ingestion while maintaining the original efficacy of the three.
Description
본 발명은 자극적인 맛과 향을 지니는 삼채를 물, 에탄올 또는 이들의 혼합액에서 가열추출하는 방법과 당침 방법을 조합하여 순화시킴으로써, 삼채의 유용성분 손실을 최소화하면서 섭취의 거부감을 줄일 수 있는 삼채 진액의 제조방법에 관한 것이다.The present invention is purified by combining a method of heating and extracting water and ethanol or a mixture of them and acupuncture method of the three flavors having a pungent taste and aroma, to reduce the rejection of intake while minimizing the loss of useful components of the three It relates to a manufacturing method of.
뿌리부추라고도 불리는 삼채(Allium hookeri)는 백합과의 여러해살이풀로서, 단맛, 매운맛, 쓴맛의 세 가지 맛이 나서 삼채(三菜)라는 이름이 붙여졌으며, 삼채의 잎과 뿌리에는 각각 필수 아미노산인 발린(valine), 이소류신(isoleucine), 메티오닌(methionine), 트레오닌(threonine), 라이신(lysine), 페닐알라닌(phenylalanine), 트립토판(tryptophan), 히스티딘(histidine) 등이 함유되어 있고 비타민 A와 C, 질소, 인산, 철분, 망간 및 아연의 함유량이 높으며, 특히 유황과 사포닌(saponin) 성분이 많이 함유되어 있다. Allium hookeri , also called root leek, is a perennial herb of the family Liliaceae, and it has three flavors of sweet, spicy, and bitter, and is named Samchae (三 菜). Contains valine, isoleucine, methionine, threonine, threonine, lysine, phenylalanine, tryptophan, histidine, vitamins A, C, nitrogen High in phosphoric acid, iron, manganese and zinc, especially sulfur and saponin.
삼채의 식이유황 성분은 통상 마늘보다 더 많이 함유되어 있다고 알려져 있으며, 유황냄새 때문에 동물들도 피해간다고 하여 노지재배시 울타리를 치지 않아도 야생동물의 피해를 받지 않는다.It is known that three kinds of dietary sulfur components are contained more than garlic, and because of the smell of sulfur, animals are also avoided, so they are not harmed by wild animals even when they are not fenced.
식이유황은 종류에 따라 알파 및 감마(향정신성 질환: 치매, 정신박약), 베타(암 또는 만성질환: 당뇨, 고혈압, 저혈압), 델타(피부질환: 고엽제, 건선피부, 아토피 알레르기), 람다 및 뮤(면역체계 강화) 효능과 더불어 간기능 개선 및 해독작용과 밀접한 관계가 있는데, 인삼류에는 베타 황 성분만 포함되어 있으나 삼채에는 상기 6 가지 황이 모두 함유되어 있는 것으로 알려져 있다.Depending on the type of dietary sulfur, alpha and gamma (psychiatric disorders: dementia, psychosis), beta (cancer or chronic diseases: diabetes, hypertension, hypotension), delta (skin diseases: defoliants, psoriasis skin, atopic dermatitis), lambda and mu (Immune System Enhancement) In addition to the efficacy of liver function and detoxification is closely related to the ginseng, it contains only the beta sulfur component, it is known that all three of the three sulfur contained.
유황은 인체를 구성하는 8 대 영양소 중의 하나로서, 뼈의 골밀도를 높여주어 골다공증을 예방하고 류마티스 관절염을 개선하는 효능을 나타내며, 피부의 조직을 서로 결집하는 접착제 역할을 하여 피부의 탄력을 유지시키고 세포 조직의 활성화로 검버섯과 기미 등이 엷어지며 피부 미백효과가 뛰어나 피부가 깨끗해지는 효능을 나타낸다.Sulfur is one of the eight nutrients that make up the human body, which increases bone density in bones, prevents osteoporosis, improves rheumatoid arthritis, and acts as an adhesive that binds skin tissues together to maintain skin elasticity and cells. By activating the tissues, black mushrooms and blemishes become thinner, and the skin whitening effect is excellent.
또한, 유황은 혈관벽을 좁히는 주원인이 되는 콜레스테롤과 과산화지질을 분해하는 기능을 가지고 있어서 고지혈증, 동맥경화 및 혈전증에 효과가 있으며, 항산화활성이 높아서 체내 염증 제거와 살균효과를 나타내고 이뇨작용과 함께 변비를 억제하는 작용을 가지는 것으로 알려져 있다.In addition, sulfur has the function of decomposing cholesterol and lipid peroxide, which is the main cause of narrowing blood vessel wall, and it is effective in hyperlipidemia, arteriosclerosis and thrombosis, and it has high antioxidant activity to remove inflammation and sterilization in the body and constipation with diuretic effect. It is known to have an inhibitory effect.
상기와 같이 인체에 필요한 유황은 체내에서 생산되지 않으므로 음식물 등을 통하여 섭취해야 하나 식사를 통한 섭취량은 통상 일일 섭취권장량에 미치지 못하며, 유황제제 또는 유황이 풍부하게 함유된 식재료를 원료로 한 기능성 식품 등이 시중에 유통되고 있으나 유황을 법제화하거나 유황함유 식품으로 가공하여도 유황 본래의 강한 약성으로 인하여 섭취시 위에 강한 자극을 주어 속을 쓰리게 하는 단점이 있어서 유황함유 건강기능성 식품이 널리 보급되는데 걸림돌로 작용하고 있다.As mentioned above, the sulfur required by the human body is not produced in the body, so it should be ingested through food or the like, but the intake amount through meals usually does not reach the recommended daily intake, and it is a sulfur-containing or functional food made from sulfur-rich foods. Although it is distributed in the market, even though sulfur is legalized or processed into sulfur-containing foods, sulfur has a disadvantage of causing strong stomach irritation when ingested due to the strong weakness of sulfur. It's working.
이러한 문제를 해결하기 위하여, 한국등록특허공보 제1645337호에서는 아스퍼르길러스 오리자애(Aspergillus Oryzae), 사카로마이세스 엘립소이더스(Saccharomyces ellipsoideus) 및 사카로마이세스 세레비시애(Saccharomyces cerevisiae) 중 하나 이상의 효모를 배양한 농축분말과 과일효소 농축액으로 삼채를 발효시킨 후 숙성 및 건조하여 삼채의 비린 냄새와 역겨운 맛을 개선하고자 하였다.In order to solve this problem, Korean Patent Publication No. 1653537 describes Aspergillus orizaae. Oryzae ), Saccharomyces ellipsoideus and Saccharomyces cerevisiae , one or more yeasts grown from concentrated powders and fruit enzyme concentrates, and then aged and dried. To improve the fishy smell and disgusting taste.
상기 발명은 발효기법을 사용하여 삼채의 비린 냄새와 역겨운 맛을 개선하고 효소-효모 복합체를 사용하여 삼채에 함유된 배당체 성분을 비당체로 변화시킴으로써 유효성분의 항산화활성을 높이고 장내 흡수를 촉진시키는 효과를 제공한다.The present invention improves the anti-oxidant activity of the active ingredient and promotes intestinal absorption by improving fermentation techniques and improving the fishy smell and disgusting taste of the three, and by changing the glycosides contained in the three into non-saccharides using the enzyme-yeast complex To provide.
또한, 한국공개특허공보 제2016-0013389호에서는 삼채 분쇄물을 고온에서 가열한 후 김치에서 추출한 유산균을 접종하여 발효시킴으로써 삼채의 강한 맛을 순화시켜 섭취의 거부감을 줄이고 발효에 의해 삼채에 함유된 유용성분의 추출량을 증가시키면서 삼채에 함유된 사포닌의 인체흡수율을 향상시키는 효과를 제공한다.In addition, Korean Laid-Open Patent Publication No. 2016-0013389 discloses the three flavors are heated at a high temperature and then fermented by inoculating with lactic acid bacteria extracted from kimchi to purify the strong taste of the three, reducing the rejection of ingestion, and containing the three contained in the three by fermentation. It provides an effect of improving the human absorption rate of the saponin contained in the three while increasing the extraction amount of the ingredients.
그런데 식이유황은 항균력이 있어서 효모나 유산균의 발효를 억제하므로 삼채의 강한 맛을 발효기법으로 감소시키기가 쉽지 않고, 또한 식이유황은 술포닐(sulfonyl)기에 2 개의 메틸(methyl)기가 붙어있는 형태인데 발효에 의해 식이유황의 유기물이 분해되어 식이유황으로서의 효능이 저하될 수 있다.However, since sulfur susceptible to fermentation of yeast or lactic acid bacteria due to its antibacterial activity, it is not easy to reduce three strong flavors by fermentation technique. In addition, sulfur is a form in which sulfonyl group has two methyl groups. Fermentation may decompose the organic matter of sulfur in sulfur, and may reduce the efficacy as sulfur.
따라서 삼채를 발효시키면 식물세포의 유기물이 분해되어 발효생성물의 마스킹 효과로 인한 식이유황의 강한 맛을 감추는 효과를 얻을 수는 있으나 이러한 효과 정도로는 삼채의 강한 맛을 순화시키기에 부족하고, 발효에 의해 식이유황의 효과가 저하되는 단점이 있다.Therefore, fermentation of three vegetables can decompose the organic matter of plant cells and conceal the strong taste of dietary sulfur due to the masking effect of fermentation products. However, this effect is insufficient to purify the three strong tastes. There is a disadvantage that the effect of dietary sulfur is reduced.
본 발명은 상기의 문제를 해결하기 위한 것으로서, 삼채에 함유된 식이유황의 효능을 유지하면서 식이유황에 의한 강한 맛과 향을 순화시킬 수 있는 삼채 진액의 제조방법을 제공하는 것이다.The present invention has been made to solve the above problems, to provide a method for producing three extracts that can purify the strong taste and aroma by dietary sulfur while maintaining the efficacy of the dietary sulfur contained in the three.
상기 과제를 해결하기 위하여, 본 발명은 삼채를 세척한 후 10~30 분간 증숙하고 잎과 뿌리를 분리하는 단계; 상기 분리한 삼채의 잎과 뿌리를 각각 50~60 ℃의 온도에서 건조하면서 건조 도중에 물을 10~30 초간 분무하는 단계; 물, 에탄올 또는 이들의 혼합액 100 중량부에 상기 건조된 삼채 잎 1~10 중량부, 건조된 삼채 뿌리 1~10 중량부 및 쌀 1~3 중량부를 혼합하여 혼합물을 준비하는 단계; 상기 혼합물을 90~100 ℃에서 100~150 분간 가열한 후 여과하여 고형물이 제거된 삼채 추출액을 제조하는 단계; 삼채 전초를 세척한 후 식초에 50~100 초간 침지하고 건져내는 단계; 상기 식초에 침지하여 건져낸 삼채 전초 100 중량부에 당 80~120 중량부를 혼합하고 밀봉상태에서 숙성시킨 후 여과하여 고형물을 제거하되, 상기 숙성은 삼채 전초에 상기 당 혼합량의 40~60 중량%를 혼합하고 40~60 일간 숙성시킨 후 당 혼합량의 나머지를 혼합하고 40~60 일간 숙성시키는 과정으로 삼채 당침액을 제조하는 단계; 및 상기 삼채 추출액 100 중량부에 삼채 당침액 80~120 중량부를 혼합하는 단계;를 포함하는 삼채 진액의 제조방법을 제공한다.In order to solve the above problems, the present invention comprises the steps of steaming for 10-30 minutes after washing three and separating leaves and roots; Spraying the separated leaves and roots at a temperature of 50-60 ° C., respectively, for 10-30 seconds while drying the three leaves; Preparing a mixture by mixing 1 to 10 parts by weight of the dried three leaves, 1 to 10 parts by weight of dried three roots and 1 to 3 parts by weight of rice, to 100 parts by weight of water, ethanol or a mixture thereof; Heating the mixture at 90 to 100 ° C. for 100 to 150 minutes and then filtering to prepare three extracts from which solids are removed; Washing three outposts and soaking in vinegar for 50-100 seconds and scooping out; 80-120 parts by weight of sugar is added to 100 parts by weight of the three outposts immersed in the vinegar and aged in a sealed state, and then filtered to remove solids. The ripening is mixed with 40-60% by weight of the sugar mixture in three outposts. And then aged for 40 to 60 days to prepare the three sugar solution in the process of mixing the remainder of the sugar mixture and aged for 40 to 60 days; And mixing 80 to 120 parts by weight of the three sugar acupuncture to 100 parts by weight of the three extracts.
이때, 상기 건조는 삼채 잎을 18~22 시간 건조하고 삼채 뿌리를 20~25 시간 건조하는 것이 바람직하다.At this time, the drying is preferably dried for three to three hours and three to three roots for 20 to 25 hours.
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본 발명은 삼채를 물, 에탄올 또는 이들의 혼합액에서 가열추출하여 항균 및 항산화 활성이 높은 삼채 추출액을 제조하고 여기에 삼채를 당침하여 삼채의 강한 맛과 향을 순화시킨 삼채 당침액을 혼합하여 삼채 진액을 제조하므로, 높은 항균 및 항산화 활성으로 인하여 삼채 진액을 장기간 저장하여도 쉽게 변질되지 않고 맛과 향이 순화되어 섭취시 거부감을 줄이면서 삼채가 가진 본래의 효능을 유지할 수 있다.In the present invention, three extracts are heated and extracted from water, ethanol or a mixture thereof to prepare three extracts having high antimicrobial and antioxidant activity, and the three extracts are mixed with three sugar extracts, which have three strong flavors and aromas, and three extracts. Because of the high antibacterial and antioxidant activity, the three extracts are not easily deteriorated even after long-term storage, the taste and aroma are purified, reducing the rejection of ingestion while maintaining the original efficacy of the three.
본 발명은 삼채의 잎과 뿌리를 건조하여 물, 에탄올 또는 이들의 혼합액에서 가열추출한 삼채 추출액과 삼채를 당류와 혼합하여 숙성시킨 삼채 당침액을 혼합하는 과정으로 삼채 진액을 제조한다.The present invention prepares three extracts by drying three leaves and roots, and mixing three extracts heated and extracted from water, ethanol or a mixture thereof with three sugars and aged three sugar salivate.
먼저, 삼채를 깨끗이 세척하고 잎과 뿌리를 분리하여 각각 건조한 후 이들 건조된 잎과 뿌리를 혼합하여 물, 에탄올 또는 이들의 혼합액에서 가열추출한다.First, three washes are clean, and the leaves and roots are separated and dried, respectively, these dried leaves and roots are mixed and extracted by heating in water, ethanol or a mixture thereof.
삼채에는 유용성분뿐만 아니라 이미(異味)와 이취(異臭)가 강하여 삼채를 취식하기 위해서는 이미와 이취를 감소시킬 필요가 있으며, 삼채의 이미와 이취는 주로 삼채에 함유된 휘발성 화합물에 의해 유발되고 휘발성분은 가열에 의해 제거되므로, 본 발명에서는 삼채를 먼저 건조하여 이미를 감소시키고 이취를 제거한다.In addition to the useful components, three already strong and already off-flavor (취) is necessary to reduce the odor and off-flavor in order to eat the three, the three is already caused by the volatile compounds contained in the three are volatile Since the powder is removed by heating, in the present invention, the three are first dried to reduce the odor and to remove odor.
상기 건조는 삼채의 유용성분이 파괴되지 않도록 50~60 ℃의 저온에서 건조하며, 건조된 잎과 뿌리의 수분함량을 균일하게 하기 위하여 얇은 삼채 잎은 18~22 시간 건조하고 상대적으로 두꺼운 삼채 뿌리는 20~25 시간 건조하는 것이 바람직하다.The drying is dried at a low temperature of 50 ~ 60 ℃ so as not to destroy the useful components of the three, in order to make the moisture content of the dried leaves and roots thin, the three leaves are dried for 18 to 22 hours, the relatively thick three roots 20 It is preferable to dry for ˜25 hours.
삼채의 잎과 뿌리에는 사포닌과 폴리페놀의 기능성 성분이 많이 함유되어 있고 이들 성분들은 건조하는 동안 열에 의해 파괴되기 쉬우므로 50~60 ℃의 낮은 온도에서 건조하여 성분 파괴를 방지하고, 삼채 뿌리에 비하여 삼채 잎에 상기 기능성 성분이 좀 더 많이 함유되어 있으므로 얇은 삼채 잎을 두꺼운 삼채 뿌리보다 좀 더 짧은 시간동안 건조한다.Three leaves and roots contain many functional ingredients of saponins and polyphenols, and these components are easily destroyed by heat during drying, so they are dried at a low temperature of 50-60 ℃ to prevent component destruction. Since the three leaves contain more of the functional ingredient, the thin three leaves are dried for a shorter time than the thick three roots.
삼채의 이미와 이취를 좀 더 감소시키기 위하여 건조하기 전에 삼채의 잎과 뿌리를 증숙하는 것이 바람직하고, 10~30 분간 증숙하는 것이 더욱 바람직하며, 얇은 삼채 잎은 10~20 분간 증숙하고 두꺼운 삼채 뿌리는 20~30 분간 증숙하는 것이 가장 바람직한데, 삼채를 증숙하면 100 ℃의 수증기가 삼채의 조직을 이완시키고 섬유질을 풀어헤친 후 고온의 열과 증발하는 증기에 동반하여 이미와 이취가 제거되며, 증숙에 의해 조직이 이완된 상태에서 건조하면 삼채 내부의 이미와 이취 성분이 더욱 제거될 수 있다.It is preferable to steam three leaves and roots before drying in order to further reduce the odor and odor of the three, more preferably steaming for 10 to 30 minutes, thin three leaves steaming and thick three roots for 10 to 20 minutes. It is most preferable to steam for 20 to 30 minutes. When steaming three steams, steam at 100 ℃ relaxes the three tissues, releases the fibers, and removes odor and odor accompanied by high temperature heat and evaporating steam. When the tissue is relaxed in a dry state, the nutrients and odors of the three insides may be further removed.
삼채에 함유된 식이유황은 메틸 설포닐 메탄(methyl sulfonyl methane)의 유기유황으로서 녹는점이 109 ℃이므로 증숙과정에서 100 ℃의 수증기에 의해 용해되지 않아서 증숙에 의해 손실되지 않으며, 세척한 삼채를 증숙한 후 잎과 뿌리를 분리하거나 또는 삼채의 잎과 뿌리를 분리한 후 증숙하는 방법 모두 선택 가능하다.The dietary sulfur contained in the three is an organic sulfur of methyl sulfonyl methane, which has a melting point of 109 ° C. Therefore, it is not dissolved by steam at 100 ° C during steaming and is not lost by steaming. After separating the leaves and roots or separating the three leaves and roots, steaming can be selected.
그런데 건조하는 동안 수분이 기화되어 빠져나가면서 삼채 조직이 다시 수축되어 삼채의 이미와 이취의 제거속도가 느려질 수 있는데, 이를 방지하기 위하여 건조하는 도중에 삼채의 잎과 뿌리에 물을 10~30 초간 분무하여 수분을 공급한 후 계속해서 건조하는 것이 바람직하며, 수분은 건조된 삼채 조직에 스며들어 조직을 이완시킨 후 건조 열에 의해 증발하면서 삼채의 이미와 이취 성분을 동반하여 제거하게 된다.However, as the moisture vaporizes and escapes during drying, the three tissues may contract again, slowing down the removal of three already and off-flavors.To prevent this, spray water on three leaves and roots during drying for 10-30 seconds. It is preferable to continue drying after supplying moisture, and the moisture penetrates into the dried three tissues, relaxes the tissues, and then removes them with the three already and off-flavor components while evaporating by dry heat.
다음은 물, 에탄올 또는 이들의 혼합액 100 중량부에 상기 건조된 삼채 잎 1~10 중량부와 건조된 삼채 뿌리 1~10 중량부를 혼합하고 90~100 ℃의 온도로 100~150 분간 가열한 후 여과하여 고형물이 제거된 삼채 추출액을 제조한다.Next, 1 to 10 parts by weight of the dried three leaves and 1 to 10 parts by weight of the dried three roots are mixed with 100 parts by weight of water, ethanol or a mixture thereof, and heated at a temperature of 90 to 100 ° C. for 100 to 150 minutes, followed by filtration. To prepare three extracts from which solids were removed.
삼채에 함유된 식이유황은 법제유황과 비교하여 독성이 없고 소화흡수율이 높으며 강력한 항산화물질로서 DNA 손상을 예방하고 항염·항균작용으로 인하여 면역력 증진에 도움을 주나 자극성의 맛과 향으로 인하여 섭취시 소비자의 거부감을 유발하는 단점이 있다.The dietary sulfur contained in the three is not toxic compared to the legal sulfur, has a high digestive absorption rate, and is a powerful antioxidant that prevents DNA damage and improves immunity due to its anti-inflammatory and antibacterial effects, but it can be consumed by consumers due to its irritating taste and flavor. It has the disadvantage of causing a sense of rejection.
이러한 단점을 해소하기 위하여 가열추출시 쌀(쌀알)을 첨가하는 것이 바람직하며, 쌀을 넣고 가열추출하면 쌀이 물속에서 가열되면서 쌀뜨물이 우러나오고 쌀뜨물은 흡착하는 성질이 있어서 식이유황의 자극성 맛과 향을 흡착하고 쌀뜨물의 구수한 맛으로 강한 맛과 향을 상쇄시켜 기호도를 향상시킨다.In order to solve this disadvantage, it is preferable to add rice (rice grains) during heat extraction, and when the rice is heated and extracted, the rice is heated while the rice is heated and the rice water is adsorbed. It adsorbs the fragrance and improves the taste by offsetting the strong taste and aroma with the gentle taste of rice water.
또한, 가열에 의해 물 또는 에탄올의 분자운동이 활발해지고 쌀 또한 물 또는 에탄올 분자의 움직임에 따라 활발히 운동하므로 물 또는 에탄올 입자보다 질량이 큰 쌀이 삼채에 좀 더 충격을 가하여 삼채에 함유된 유용성분이 물 또는 에탄올에 빨리 용출될 수 있다.In addition, the molecular movement of water or ethanol is active by heating, and the rice is also actively moving in accordance with the movement of water or ethanol molecules. It can quickly elute in water or ethanol.
상기 쌀은 물, 에탄올 또는 이들의 혼합액 100 중량부 기준 쌀 1~3 중량부 첨가하는 것이 바람직하며, 쌀의 첨가량이 1 중량부 미만이면 쌀뜨물의 생성이 부족하여 삼채 추출액에 삼채의 강한 맛과 향이 많이 잔존하고 3 중량부를 초과하면 쌀뜨물의 생성이 과도하여 삼채 추출액이 탁해지고 맛이 깔끔하지 못하여 상품성이 저하되며, 쌀은 추출 후 여과하는 과정에서 삼채 고형물과 함께 제거된다.The rice is preferably added 1 to 3 parts by weight of water, ethanol or 100 parts by weight of a mixture of them, if the addition amount of the rice is less than 1 part by weight of the production of the rice water is insufficient, three strong flavors in three extracts and When the amount of fragrance remains much and exceeds 3 parts by weight, the production of rice water is excessive, the three extracts become turbid and the taste is not clear, and the marketability is lowered. The rice is removed together with the three solids in the process of extraction and filtration.
다음은 삼채 전초(잎과 뿌리)를 깨끗이 세척한 후 당과 혼합하고 밀봉상태에서 숙성시켜 삼채 당침액을 제조하며, 삼채 전초 100 중량부에 당 80~120 중량부를 혼합한 다음 80 일 이상, 바람직하게는 80~120 일간 숙성시키는데, 당 함량이 80 중량부 미만이거나 숙성기간이 80일 미만이면 삼채의 유용성분이 당침액에 충분히 용출되지 못하고 당 함량이 120 중량부를 초과하면 당침액의 당도가 너무 높아져 진액이 너무 단맛이 나게되므로 바람직하지 않다.Next, the three outposts (leaves and roots) are washed thoroughly, mixed with sugars, and aged in a sealed state to prepare three-dough sap solution, 80-120 parts by weight per 100 parts by weight of three outposts are mixed, and then 80 days or more. Preferably aged 80 to 120 days, when the sugar content is less than 80 parts by weight or the maturation period is less than 80 days, three of the useful components are not sufficiently eluted in the sugar solution, sugar content of the sugar solution is too high if the sugar content exceeds 120 parts by weight It is undesirable because the juice becomes too sweet.
삼채를 당과 혼합하여 숙성시키면 삼채의 유황성분이 당의 유기물과 반응하여 펜타티온산(pentathionic acid)을 생성하고, 펜타티온산은 살균작용을 가지므로 유황의 항균작용과 함께 삼채 당침액의 항균력이 증가하는 효과를 얻을 수 있다.When three vegetables are mixed with sugar and matured, the sulfur content of the three reacts with the organic substance of the sugar to produce pentathione acid.The pentathione acid has a bactericidal action. You can get the effect.
삼채에는 잡균 등의 여러 미생물이 묻어있고 삼채를 깨끗이 세척하여도 먼지와 같은 이물질은 제거되나 미생물은 잔류할 수 있으며, 이러한 미생물은 당침과정에서 이상발효를 일으키거나 또는 최종 제품인 삼채 진액에 함유되어 삼채 진액을 밀봉포장하여도 포장지 내에서 발효 또는 부패를 일으켜 포장제품이 부풀어오르는 제품불량을 유발할 수 있다.Three microbes contain various microorganisms such as various bacteria, and even if the three washes clean, foreign substances such as dust are removed, but microorganisms may remain. These microorganisms cause abnormal fermentation during the acupuncture process or are contained in the final product three samchae juice. Sealing and packing the essences may also cause fermentation or decay in the packaging, resulting in swelling of the packaged product.
따라서 삼채에 포함될 수 있는 미생물을 완전히 살균할 필요가 있으며, 삼채 추출액은 제조과정에서 고온으로 가열하므로 자동 살균되나 삼채 당침액에는 미생물이 잔존할 수 있으므로 당침액 제조시 살균을 위하여 세척한 삼채를 식초에 침지한 후 건져내어 당과 혼합하는 것이 바람직하다.Therefore, it is necessary to completely sterilize the microorganisms that can be included in the three vegetables, and the three extracts are automatically sterilized because they are heated to high temperature during the manufacturing process. After dipping in, it is preferable to take out and mix with sugar.
식초는 살균기능이 있어서 미생물을 사멸시키고 더불어 삼채를 식초에 침지하면 삼채의 세포막이 용해되거나 연해져서 당침 시간이 단축될 수 있고, 더불어 식초는 삼채의 강한 맛과 향을 순화시키는 효과를 부여한다.Vinegar has a bactericidal function and kills microorganisms, and immersing three in vinegar can shorten the acupuncture time by dissolving or softening the three cell membranes. In addition, vinegar gives the effect of purifying the strong taste and aroma of the three.
상기 침지는 50~100 초간 실시하는 것이 바람직하며, 50 초 미만이면 미생물이 충분히 사멸되지 않을 수 있고 100 초를 초과하면 삼채가 너무 물러져 식초에서 건져내는 중에 식초에 남아서 모두 회수하지 못할 수 있으며, 또한 삼채의 유효성분이 식초에 용출되어 손실될 우려가 있다.The immersion is preferably carried out for 50 to 100 seconds, less than 50 seconds, the microorganisms may not be sufficiently killed, and if more than 100 seconds, the three may be so receded that the remaining in the vinegar may not be recovered, In addition, there is a fear that the three active ingredients are eluted in vinegar and lost.
더불어, 가열추출시 쌀을 첨가할 경우 삼채 추출액에 용해된 쌀뜨물이 식초의 향을 흡착하여 식초향을 싫어하는 취식자도 거부감없이 섭취할 수 있다.In addition, when added to the rice during heating extraction, the rice water dissolved in the three extracts adsorb the scent of vinegar can be eaten without a sense of rejection of vinegar.
숙성 중에는 당이 완전히 녹을 때까지 수시로 섞어주고 이후 간헐적으로 용기를 흔들어주어 삼채의 유용성분이 삼투압 현상에 의해 용액 중에 충분히 용출되도록 하며, 숙성이 완료되면 여과하여 고형물을 제거함으로써 삼채 당침액이 제조된다.During ripening, the sugar is often mixed until it is completely dissolved, and then the container is intermittently shaken so that the three useful components are sufficiently eluted in the solution by osmotic pressure. When the ripening is completed, the three sugar solution is prepared by removing solids by filtration.
삼채 당침액의 제조에는 80 일 이상의 많은 숙성시간이 소요되어 삼채 진액의 제조과정 중에서 가장 많은 시간을 소비하므로 숙성시간을 단축시켜 전체 제조기간을 단축할 필요가 있으며, 이를 위하여 삼채 당침액 제조시 혼합되는 당을 반분하여 2 회에 나누어 삼채와 혼합하는 것이 바람직하다.It is necessary to shorten the maturation time by shortening the maturation time, because it takes a lot of aging time of 80 days or more for the production of three sugar acupuncture solution. It is preferable to divide the sugar to be divided into two and mix with three.
즉, 당 혼합량의 40~60 중량%를 먼저 삼채와 혼합하고 밀봉상태에서 40~60 일간 정치하면서 간헐적으로 섞어준 후 여기에 다시 당 혼합량의 나머지(40~60 중량%)를 혼합하고 밀봉상태에서 40~60 일간 정치하면서 간헐적으로 용기를 흔들어주어 삼채 당침액을 제조한다.In other words, 40 to 60% by weight of the sugar mixture is first mixed with three, and then mixed intermittently while standing in the sealed state for 40 to 60 days, and then mixed with the rest of the sugar content (40 to 60% by weight) again in the sealed state. While still standing for 40 to 60 days, shake the container intermittently to prepare three sugar solution.
상기와 같이 당류를 반분하여 삼채를 예비 당침하면 삼투압 현상에 의해 삼채 내부로부터 외부로 삼채액이 흘러나오고 상대적으로 적게 혼합된 당류는 삼채액에 모두 녹아서 용액상태로 되며, 여기에 당류 혼합량의 나머지 당류를 혼합하면 후첨가된 당류가 삼채 당액 중에서 빠르게 용액상태가 되어 삼채의 유용성분을 용액 중에 신속히 추출하므로 삼채 당침액의 제조기간을 단축할 수 있다.As described above, when the three sugars are preliminarily immersed in three sugars, the three liquids flow out from the inside of the three liquids by osmotic pressure, and the relatively less mixed sugars are dissolved in the three liquids to form a solution. After mixing, the added sugar becomes a solution in three sugar liquids rapidly, and extracts three useful components in the solution quickly, thereby reducing the production period of three sugar solution.
당침액 중에 미생물이 완전히 사멸되지 않을 수도 있으므로 제조된 삼채 당침액을 끓여서 균을 확실하게 사멸시킬 수도 있다.Since the microorganisms may not be completely killed in the sap solution, the prepared three sap solution may be boiled to reliably kill the bacteria.
삼채 당침액 중에 생성된 펜타티온산은 가열되면 서서히 분해하여 살균력을 상실하게 되므로, 본 발명에서는 장시간 가열과정을 거치는 삼채 추출액 제조시 당을 첨가하지 않고 가열과정을 거치지 않는 당침액 제조시 당을 첨가하여 펜타티온산을 생성시킨 후 삼채 추출액과 혼합하므로 삼채 진액 중에 펜타티온산이 분해되지 않고 유지되어 진액의 저장성이 높으며, 잡균 제거를 위하여 당침액을 끓일 경우 가능한 한 짧은 시간 내에 끓여서 펜타티온산의 분해를 최소화하는 것이 바람직하고 열을 가하지 않는 자외선 살균법 또는 고주파 살균법을 이용하여 당침액의 잡균을 제거하는 것이 더욱 바람직하다.The pentathiic acid produced in the three sugar acupuncture solution is gradually decomposed when heated and loses sterilizing power. In the present invention, by adding sugar in the preparation of the sugar acupuncture solution which does not undergo a heating process without adding sugar in the three- extraction extract which is subjected to a long heating process Since the pentathiic acid is produced and mixed with three extracts, the pentathiic acid is maintained without being decomposed in the three extracts, and the shelf life of the extract is high.When boiling the salivary solution for removing bacteria, it is boiled within the shortest time to decompose It is preferable to minimize and it is more preferable to remove the germs of sugar solution liquid by using ultraviolet sterilization or high frequency sterilization without heat.
다음은 상기 제조된 삼채 추출액 100 중량부에 삼채 당침액 80~120 중량부를 혼합하여 삼채 진액을 제조한다.Next, the three extracts 80 to 120 parts by weight of the three extracts were prepared in 100 parts by weight of the three extracts prepared above to prepare the three extracts.
삼채를 가열추출한 삼채 추출액은 삼채를 당과 혼합하여 숙성시킨 삼채 당침액보다 삼채의 맛과 향이 강한데, 본 발명과 같이 삼채 추출액에 삼채 당침액을 혼합하면 삼채 추출액의 강한 맛과 향이 삼채 당침액으로 인하여 연해지고 당침액의 단맛이 삼채에 함유된 식이유황의 아린맛을 상쇄하여 삼채 진액의 기호도를 높일 수 있다.Three extracts heated by three extracts have three flavors and aromas stronger than three sugars prepared by mixing the three with sugars. When the three extracts are mixed with the three extracts, the strong taste and aroma of the three extracts are the three extracts. Due to softening and sweetness of the sugar acupuncture can offset the arine taste of dietary sulfur contained in the three can increase the palatability of the three.
이하, 본 발명을 하기의 실시예, 비교예 및 시험예에 의거하여 좀더 상세하게 설명한다.Hereinafter, the present invention will be described in more detail based on the following Examples, Comparative Examples and Test Examples.
단, 하기의 실시예는 본 발명을 예시하기 위한 것일 뿐, 본 발명이 하기 실시예에 의해 한정되는 것이 아니고, 본 발명의 기술적 사상을 벗어나지 않는 범위 내에서 치환 및 균등한 타 실시예로 변경할 수 있음은 본 발명이 속하는 기술분야에서 통상의 지식을 가진 자에게 있어서 명백할 것이다.However, the following examples are only for illustrating the present invention, and the present invention is not limited to the following examples, and may be changed to other embodiments equivalent to substitutions and equivalents without departing from the technical spirit of the present invention. It will be apparent to those skilled in the art to which the present invention pertains.
<실시예 1> <Example 1>
삼채를 깨끗이 세척하고 잎과 뿌리를 분리한 다음 삼채 잎을 55 ℃에서 20 시간 건조하고 삼채 뿌리를 55 ℃에서 22 시간 건조하였다.Three leaves were washed thoroughly, the leaves and roots were separated, and the three leaves were dried at 55 ° C. for 20 hours and the three roots were dried at 55 ° C. for 22 hours.
가열용기에 물 15 ℓ와 상기 건조된 삼채 잎 500 g 및 건조된 삼채 뿌리 500 g을 넣고 95 ℃에서 2 시간 가열하여 열수추출한 후 고운 체(sieve)로 여과하여 고형물이 제거된 삼채 추출액을 제조하였다.15 liters of water, 500 g of the dried three leaves and 500 g of the dried three roots were put in a heating container, and heated at 95 ° C. for 2 hours to extract hot water, followed by filtration with a sieve to prepare solid extracts. .
삼채 전초(뿌리와 잎)를 깨끗이 세척하고 물기를 제거한 후 유리항아리에 3 ㎝ 정도 담고 그 위에 설탕을 넣었으며, 이 과정을 계속 반복하여 삼채 전초와 설탕이 켜켜이 적층되도록 하였고 제일 상부의 삼채 전초가 완전히 덮이도록 설탕을 다량 넣은 다음 뚜껑을 닫고 100 일간 정치(定置)하였으며, 사용된 삼채 전초와 설탕은 대략 동일 중량비가 되도록 하였다.The three outposts (roots and leaves) were washed clean and drained, and then 3 cm of glass jars were put in a glass jar and sugar was added to it. This process was repeated repeatedly so that the three outposts and sugar were stacked on top of each other. A large amount of sugar was added so that it was completely covered, and the lid was closed and settled for 100 days, and the three outposts and the sugar used were about the same weight ratio.
정치 후 처음 1 개월간은 막대기로 저어주면서 상하 뒤집어주었고 이후 유리항아리를 흔들어주어 삼채 전초와 설탕이 잘 혼합되도록 하였으며, 정치 100 일 후 상기 유리항아리의 내용물을 고운 체로 여과하여 고형물이 제거된 삼채 당침액을 제조하였다.The first one month after stationary, the mixture was stirred upside down with a stick, and then the glass jars were shaken so that the three outposts and sugar were well mixed. After 100 days, the contents of the glass jars were filtered with a fine sieve, and the solid solution was removed. Was prepared.
상기 삼채 추출액과 삼채 당침액을 동일 중량비로 혼합하여 삼채 진액을 제조하였다.The three extracts and three sugar solution were mixed in the same weight ratio to prepare the three extracts.
<실시예 2><Example 2>
찜솥에 물을 담고 받침을 받친 다음 받침 위에 깨끗이 세척한 삼채 전초를 올려놓고 뚜껑을 덮어서 가열하였으며, 증기가 올라오고 20 분간 경과시 삼채를 꺼내어 잎과 뿌리를 분리하였다.After putting the water in the steamer and supporting the saucer, three clean outposts were placed on the saucer and covered with a lid and heated. The steam was raised, and after 20 minutes, three leaves were taken out to separate leaves and roots.
상기 증숙한 삼채의 잎과 뿌리를 건조, 열수추출 및 여과하여 삼채 추출액을 제조한 것을 제외하고는, 상기 실시예 1과 동일한 방법으로 삼채 진액을 제조하였다.The three extracts were prepared in the same manner as in Example 1, except that the three extracts were prepared by drying, hot water extraction, and filtering the steamed three leaves and roots.
<실시예 3><Example 3>
상기 실시예 1에서, 삼채의 잎과 뿌리를 건조하는 도중에 건조시작 후 10 시간(삼채 잎) 및 11 시간(삼채 뿌리) 경과시 잎과 뿌리에 물을 20 초간 골고루 분무한 후 계속 건조한 것을 제외하고는, 상기 실시예 1과 동일한 방법으로 삼채 진액을 제조하였다.In Example 1, 10 hours after the start of drying (three leaves) and 11 hours (three roots) after the start of drying the leaves and roots evenly spraying the leaves and roots for 20 seconds, except that it continues to dry Was prepared in the same manner as in Example 1 three extract.
<실시예 4><Example 4>
상기 실시예 1에서, 열수추출시 물에 쌀알 300 g을 첨가하여 가열한 것을 제외하고는, 상기 실시예 1과 동일한 방법으로 삼채 진액을 제조하였다.In Example 1, three extracts were prepared in the same manner as in Example 1, except that 300 g of rice grains were added to water during hot water extraction.
<비교예 1>Comparative Example 1
상기 실시예 1에서, 삼채 당침액을 제조하지 않고 삼채 추출액만으로 제품화하였다.In Example 1, three sugar solution was prepared without producing only three extracts.
<비교예 2>Comparative Example 2
상기 실시예 1에서, 삼채 추출액을 제조하지 않고 삼채 당침액만으로 제품화하였다.In Example 1, three extracts were prepared and only three sugar solution was prepared.
<시험예 1> 항균활성 분석Test Example 1 Antibacterial Activity Analysis
상기 실시예 1~4 및 비교예 1, 2에서 제조된 삼채 진액, 추출액 및 당침액을 실온에서 3 일간 보관한 후 항균활성을 분석하였다.The three extracts, extracts and sugar solution prepared in Examples 1 to 4 and Comparative Examples 1 and 2 were stored at room temperature for 3 days and then analyzed for antimicrobial activity.
황색포도상구균(Staphylococcus aureus ATCC 6538)을 액체배지에 배양시킨 후 배양된 세균을 희석하여 초기 세균수가 105~106 CFU/㎖가 되도록 조정하여 시험에 사용하였다.The Staphylococcus aureus (Staphylococcus aureus ATCC 6538) is adjusted such that after incubation by diluting the initial bacterial culture bacteria number 10 5 ~ 10 6 CFU / ㎖ in the liquid medium was used for testing.
각 군별 시료 20 ㎖에 시험균액을 첨가하고 초기 세균수와 실온에 1 일간 정치하였을 때의 세균수를 측정하였으며, 최초 희석단계에서 D/E Neutralizing Broth(MB-D0862)를 이용하여 중화시키는 과정을 거쳤고 세균수의 측정은 TSA(triptic soy agar) 배지를 이용하여 실시하였다.The test bacteria were added to 20 ml of the sample in each group, and the number of bacteria at the initial bacterial count and at room temperature for 1 day was measured. The process of neutralization using D / E Neutralizing Broth (MB-D0862) at the initial dilution step was performed. The bacterial count was measured using a TSA (triptic soy agar) medium.
세균수 및 세균감소율을 하기의 식에 의거하여 계산하고 표 1에 나타내었다.The number of bacteria and the rate of bacterial reduction were calculated based on the following formula and shown in Table 1.
* 세균수=집락수×희석배수* Number of bacteria = colony × dilution
* 세균감소율(%)={(초기 세균수-1 일 경과 후 세균수)/초기 세균수}×100* Bacterial Reduction (%) = {(Initial Bacterial Count-Number of Bacteria after Day 1) / Initial Bacterial Count} × 100
(CFU/㎖)Early bacterial count
(CFU / mL)
(CFU/㎖)Number of bacteria after 1 day
(CFU / mL)
(%)Bacterial reduction rate
(%)
상기 표 1을 보면, 실시예 1~4 및 비교예 1의 세균감소율은 >99.9 %를 보였는데, 이는 삼채 진액과 삼채 추출액에 함유된 유황성분의 항균작용 및 삼채 진액 중의 펜타티온산의 살균작용에 기인한 것으로 판단된다.In Table 1, the bacterial reduction rate of Examples 1 to 4 and Comparative Example 1 was> 99.9%, which is the antibacterial activity of the sulfur components contained in the three extracts and the three extracts and the bactericidal action of pentathiate in the three extracts. It seems to be due to.
삼채 추출액으로만 구성된 비교예 1의 세균감소율이 실시예보다 좀 더 높게 측정되고 삼채 당침액으로만 구성된 비교예 2의 세균감소율이 가장 낮게 측정된 결과로부터, 삼채 당침액이 삼채 추출액에 비하여 항균효과가 낮은 것을 알 수 있고 이는 당침액에 펜타티온산의 살균력이 더해지나 당 성분으로 인하여 균의 배양이 촉진되어 전체적으로 항균력이 저하된 것으로 판단된다.The bactericidal rate of Comparative Example 1 composed only of three extracts was measured to be higher than that of Example, and the bacterial reduction rate of Comparative Example 2 composed only of three saucy solution was measured to be the lowest. It can be seen that this is added to the sterilizing power of pentathiic acid in the sugar solution, but the culture of the bacteria is promoted due to the sugar component is judged that the overall antimicrobial activity is reduced.
따라서 본 발명과 같이 삼채 추출액에 삼채 당침액을 혼합하면 세균감소율이 약간 낮아지나 99.9 % 이상의 높은 항균활성을 나타내면서 삼채를 당침함으로써 삼채의 강한 맛과 향이 어느 정도 순화될 것으로 예상된다.Therefore, when the three sugar solution is mixed with the three extracts as in the present invention, the bacterial reduction rate is slightly lowered, but the strong taste and aroma of the three are expected to be purified to some extent by showing the high antibacterial activity over 99.9%.
<시험예 2> 항산화활성 분석Test Example 2 Antioxidant Activity Analysis
상기 실시예 및 비교예에서 제조된 삼채 진액, 추출액 및 당침액을 3 일간 보관한 후 DPPH(1,1-diphenyl-2-picrylhydrazyl) 라디칼(radical) 소거능을 측정하여 항산화활성을 분석하였다.The three extracts, extracts and sugar solution prepared in Examples and Comparative Examples were stored for 3 days and then analyzed for antioxidant activity by measuring DPPH (1,1-diphenyl-2-picrylhydrazyl) radical scavenging ability.
각 군별 시료 0.2 ㎖에 60 μM DPPH(1,1-diphenyl-2-picryl hydrazyl) 메탄올 용액 2.6 ㎖를 혼합한 후 암소(暗所)에서 15 분간 반응시킨 다음 517 ㎚에서 흡광도를 측정하였다.After mixing 0.2 ml of 60 μM DPPH (1,1-diphenyl-2-picryl hydrazyl) methanol solution in 0.2 ml of each group, the reaction was carried out in a dark place for 15 minutes, and then the absorbance was measured at 517 nm.
공시험은 시료 대신에 70 vol.% 메탄올을 사용하여 동일한 방법으로 분석하였고 대조구는 DPPH 메탄올 용액 대신 70 vol.% 메탄올을 사용하여 흡광도를 측정하였으며, DPPH 라디칼 소거능을 하기의 식에 의거하여 계산하고 그 결과를 표 2에 나타내었다.For the blank test, 70 vol.% Methanol was used instead of the sample, and the control was measured for absorbance using 70 vol.% Methanol instead of DPPH methanol solution. DPPH radical scavenging ability was calculated according to the following equation. The results are shown in Table 2.
* DPPH 라디칼 소거능(%)={1-(시료의 흡광도-대조구의 흡광도)/공시험의 흡광도}×100* DPPH radical scavenging activity (%) = {1- (absorbance of sample-absorbance of control) / absorbance of blank test} × 100
상기 표 2에 나타난 바와 같이, 삼채 추출액으로만 구성된 비교예 1의 항산화활성이 가장 높고 삼채 당침액으로만 구성된 비교예 2의 항산화활성이 가장 낮았는데, 이러한 결과로부터 삼채를 당침하는 것보다 열수추출하는 것이 삼채의 황산화성분을 회수하는데 효과적임을 알 수 있다.As shown in Table 2, the antioxidant activity of Comparative Example 1 consisting of only three extracts was the highest and the antioxidant activity of Comparative Example 2 consisting only of three sap acupuncture was the lowest, from these results than hot water to beat three It can be seen that extraction is effective in recovering three sulfated components.
실시예 중에서는 열수추출시 물에 쌀알을 첨가하여 가열한 실시예 4가 높게 분석되어 쌀알이 끓는 물의 격한 운동에 따라 삼채에 충격을 가함으로써 삼채에 함유된 황산화성분의 용출을 촉진한 것으로 추정되고, 삼채를 증숙하여 열수추출한 실시예 2는 증숙과정에서 항산화 효능을 나타내는 성분이 수증기와 동반하여 일부 유실된 것으로 추정된다.Among the examples, Example 4, which was heated by adding rice grains to water during hot water extraction, was highly analyzed, and it was estimated that rice grains accelerated the dissolution of sulfated components contained in the three by impacting three mushrooms under vigorous movement of boiling water. In Example 2 of steaming three waters and extracting hot water, some components showing antioxidant efficacy during steaming were partially lost along with water vapor.
삼채의 맛과 향이 강한 삼채 추출액에 삼채 당침액을 혼합하면 삼채의 강한 맛과 향이 순화되는 효과를 기대할 수 있고, 삼채 추출액의 높은 항산화활성이 당침액의 첨가로 인해 약간 저하되기는 하나, 열수추출시 물에 쌀알을 첨가(실시예 4)하거나 삼채를 건조하는 도중에 물을 분무(실시예 3)하는 방법으로 항산화 성분의 추출을 촉진하여 당침액의 첨가로 인한 항산화활성의 저하를 보완할 수 있을 것으로 판단된다.Mixing three sugars in three extracts with strong taste and aroma of three can be expected to have the effect of purifying the three strong tastes and aromas, while the high antioxidant activity of the three extracts is slightly lowered due to the addition of sugar solution. By adding rice grains to water (Example 4) or spraying water during drying three (Example 3), the extraction of antioxidant components may be promoted to compensate for the degradation of antioxidant activity due to the addition of sugar solution. Judging.
<시험예 3> 저장성 측정<Test Example 3> storage capacity measurement
상기 실시예 및 비교예에서 제조된 삼채 진액, 추출액 및 당침액을 상온에 보관하면서 부패가 발생하는 것을 육안 및 냄새로 관찰하여, 부패가 처음 관찰된 날을 하기 표 3에 나타내었다.The storage and storage of the three extracts, extracts and sugar solution prepared in Examples and Comparative Examples at room temperature was observed by the naked eye and odor, the day when the first corruption is shown in Table 3 below.
상기 표 3의 결과, 비교예 1에서 부패가 가장 늦게 발생하였고 비교예 2에서 부패가 가장 빨리 발생하였는데, 이 결과는 상기 시험예 1의 항균활성 분석결과와 동일한 이유로 판단된다.As a result of Table 3, the decay was the latest in Comparative Example 1 and the decay occurred the fastest in Comparative Example 2, this result is determined for the same reason as the antimicrobial activity analysis results of Test Example 1.
단지, 실시예 4의 경우 항균활성은 높으나 부패가 비교적 빨리 발생한 것은 열수추출 중에 쌀알로부터 용출된 전분성분이 부패를 촉진한 것으로 추정된다.However, in Example 4, the antibacterial activity was high, but the decay occurred relatively quickly, and it is estimated that the starch component eluted from the grains of rice during the hot water extraction promoted the decay.
전체적으로 저장성이 낮은 삼채 당침액(비교예 2)에 저장성이 높은 삼채 추출액(비교예 1)을 혼합하여 삼채 진액을 제조(실시예)함으로써 진액의 부패를 늦출 수 있음을 알 수 있다.It can be seen that the decay of the essences can be slowed down by mixing the three extracts (Comparative Example 1) with the highly storageable three immersion liquor (Comparative Example 2) and preparing the three essences (Example).
<시험예 4> 관능검사Test Example 4 Sensory Test
10 대에서 70 대까지의 남녀 각각 5 명씩 모두 70 명을 대상으로 상기 제조된 삼채 진액, 삼채 추출액 및 삼채 당침액의 맛, 향, 색상 및 전체적인 기호도를 5 점 척도법으로 측정하여 그 평균값을 하기 표 4에 나타내었다.Taste, aroma, color, and overall preference of the three extracts, three extracts, and three sugar acupuncture extracts of the three extracts, the three extracts, and the three sugar acupuncture extracts were analyzed using a five-point scale method. 4 is shown.
상기 표 4를 보면, 실시예 4의 맛과 향이 가장 우수하고 색상이 가장 낮은 평가를 받았는데, 쌀알로부터 우러나온 쌀뜨물이 식이유황의 자극성 맛과 향을 흡착하여 순화시킨 반면에 쌀뜨물의 뿌연 형상이 색상의 평가를 저하시킨 것으로 판단된다.In Table 4, the taste and aroma of Example 4 received the best evaluation and the lowest color. The rice water from rice grains was purified by adsorbing the irritating taste and aroma of dietary sulfur, while the cloudy shape of rice water. It is judged that the evaluation of this color was reduced.
비교예 1은 식이유황의 맛과 향, 삼채의 이미와 이취가 강하여 맛과 향의 평가가 낮았으나 색상은 선명하였고, 비교예 2는 단맛이 너무 강하다는 의견이 많았다.In Comparative Example 1, the taste and aroma of dietary sulfur, and the three flavors and smells of three were strong, the taste and aroma evaluation was low, but the color was clear, and Comparative Example 2 had a lot of opinion that the sweet taste was too strong.
전체적인 기호도에서는 삼채 추출액 및 당침액을 혼합한 실시예가 비교예보다 높게 평가되어 본 발명에 따른 삼채 진액의 상품성을 확인할 수 있었다.In the overall preference, the mixed example of the three extracts and the sugar solution was evaluated higher than the comparative example was able to confirm the commerciality of the three extracts according to the present invention.
Claims (7)
상기 분리한 삼채의 잎과 뿌리를 각각 50~60 ℃의 온도에서 건조하면서 건조 도중에 물을 10~30 초간 분무하는 단계;
물, 에탄올 또는 이들의 혼합액 100 중량부에 상기 건조된 삼채 잎 1~10 중량부, 건조된 삼채 뿌리 1~10 중량부 및 쌀 1~3 중량부를 혼합하여 혼합물을 준비하는 단계;
상기 혼합물을 90~100 ℃에서 100~150 분간 가열한 후 여과하여 고형물이 제거된 삼채 추출액을 제조하는 단계;
삼채 전초를 세척한 후 식초에 50~100 초간 침지하고 건져내는 단계;
상기 식초에 침지하여 건져낸 삼채 전초 100 중량부에 당 80~120 중량부를 혼합하고 밀봉상태에서 숙성시킨 후 여과하여 고형물을 제거하되, 상기 숙성은 삼채 전초에 상기 당 혼합량의 40~60 중량%를 혼합하고 40~60 일간 숙성시킨 후 당 혼합량의 나머지를 혼합하고 40~60 일간 숙성시키는 과정으로 삼채 당침액을 제조하는 단계; 및
상기 삼채 추출액 100 중량부에 삼채 당침액 80~120 중량부를 혼합하는 단계;를 포함하는 삼채 진액의 제조방법.Washing the three and steaming for 10-30 minutes and separating leaves and roots;
Spraying the separated leaves and roots at a temperature of 50-60 ° C., respectively, for 10-30 seconds while drying the three leaves;
Preparing a mixture by mixing 1 to 10 parts by weight of the dried three leaves, 1 to 10 parts by weight of dried three roots and 1 to 3 parts by weight of rice, to 100 parts by weight of water, ethanol or a mixture thereof;
Heating the mixture at 90 to 100 ° C. for 100 to 150 minutes and then filtering to prepare three extracts from which solids are removed;
Washing three outposts and soaking in vinegar for 50-100 seconds and scooping out;
80-120 parts by weight of sugar is added to 100 parts by weight of the three outposts immersed in the vinegar, aged in a sealed state, and filtered to remove solids. And then aged for 40 to 60 days to prepare the three sugar solution in the process of mixing the remainder of the sugar mixture and aged for 40 to 60 days; And
Mixing three to four sugar solution 80 ~ 120 parts by weight to 100 parts by weight of the three extract; three.
상기 건조는 삼채 잎을 18~22 시간 건조하고 삼채 뿌리를 20~25 시간 건조하는 것을 특징으로 하는 삼채 진액의 제조방법.The method according to claim 1,
The drying is a method of producing three extracts, characterized in that the three leaves are dried for 18 to 22 hours and the three roots are dried for 20 to 25 hours.
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