KR101953652B1 - Ashes powdered crystals and a method of manufacturing the same - Google Patents
Ashes powdered crystals and a method of manufacturing the same Download PDFInfo
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Abstract
본 발명은, 낮은 온도에서 단시간에 외관이 미려하고 장기간이 지나도 천연의 다양한 색상과 광택 등이 그대로 보존되게 고강도로 성형하는 골분결정체 및 그 제조방법에 관한 것이다.
이와 같은 본 발명에 따른 골분결정체 및 그 제조방법은, 분쇄하고 불순물을 제거한 후 수분함량이 7~10중량%로 되게 건조하는 골분조성단계(10)와, 상기 조성된 골분 50~60중량%에 리튬 22~25중량%와 나노산화세륨 6~8중량%와 콜라겐 8~10중량% 및 붕소·붕사·붕산들 중 어느 하나의 4~7중량%를 혼합하는 제1혼합단계(20)와, 상기 1차 골분혼합물 90~95중량%에 규소 또는 알루미나 5~10중량%를 혼합하는 제2혼합단계(30)와, 상기 2차 골분혼합물 93~96중량%에 녹차분말·홍차분말·송진분말·황토분말·해초분말들 중 어느 하나 또는 복수를 4~7중량% 혼합하는 제3혼합단계(40) 및 상기 3차 골분혼합물을 성형판에 형성된 성형홈들에 각각 충전하고 가열로 넣어 1000~1050℃에서 5~10분 동안 가열용융한 후 인출냉각하는 성형단계(50)를 포함하여 이루어지는 것을 특징으로 하는 것이다.[0001] The present invention relates to a bone fragile crystal to be molded with high strength so that various natural hues and luster are preserved even if the appearance is good at a low temperature in a short time and after a long period of time, and a manufacturing method thereof.
The bone fragrance crystal and the method for producing the same according to the present invention are characterized by comprising a bone fragrance forming step (10) of pulverizing and drying impurities after removing moisture to have a moisture content of 7 to 10% by weight, A first mixing step (20) of mixing 22 to 25% by weight of lithium, 6 to 8% by weight of cerium oxide, 8 to 10% by weight of collagen and 4 to 7% by weight of any one of boron, borax and boric acid, A second mixing step (30) in which 90 to 95% by weight of the primary bone meal mixture is mixed with 5 to 10% by weight of silicon or alumina, and 93 to 96% by weight of the secondary bone meal mixture are mixed with green tea powder, black tea powder, A third mixing step (40) of mixing 4 to 7 wt% of any one or more of loess powder and seaweed powder, and a third mixing step (40) And a molding step (50) for heating and melting at 1050 ° C for 5 to 10 minutes, followed by drawing and cooling The.
Description
본 발명은 골분결정체 및 그 제조방법에 관한 것으로서, 더욱 상세하게는 낮은 온도에서 단시간에 외관이 미려하고 장기간이 지나도 천연의 다양한 색상과 광택 등이 그대로 보존되게 고강도로 성형하는 골분결정체 및 그 제조방법에 관한 것이다.More particularly, the present invention relates to a bone fragile crystal which is molded into a high strength so that various natural hues and luster are preserved even if the appearance is good in a short time at a low temperature for a long period of time, .
종래에는, 유골을 분쇄하여 만든 골분을 세라믹 용해로에 투입하고 소량의 탄산바륨과 석회를 투입한 후 450℃~ 550℃의 화염을 가해 골분의 표면에 막을 형성시킨 다음 막이 형성된 골분에 900℃~1000℃의 화염을 8~13분 동안 가해 골분을 덩어리로 응집시키고, 응집된 골분에 1700℃~2000℃의 화염을 15 ~ 25분 동안 가해 용융시켜 얻는 액상의 골분을 낙하시키면서 타격하여 미립화 된 액상의 골분이 진동판 위에 낙하하여 구형의 결정체로 형성하는 화장 후 남은 유골로부터 결정체를 만드는 방법(특허등록 제10-0407145호)이 있었다.Conventionally, the bone fragments obtained by crushing ashes are put into a ceramic melting furnace, a small amount of barium carbonate and lime are added thereto, and a film is formed on the surface of the bone fragments by applying a flame at 450 ° C to 550 ° C. ° C flame for 8 to 13 minutes to agglomerate the bone fragments into a mass, and applying a flame of 1700 ° C to 2000 ° C for 15 to 25 minutes to the aggregated bone fragments to melt and melt the liquid bone fragments, There is a method (patent registration No. 10-0407145) for making crystals from ash after the make-up formed by spherical crystals falling from the bone fragments on the diaphragm.
그러나, 이러한 방법은 골분을 세라믹 용해로에 투입하고 450℃~550℃의 화염을 가해 골분의 표면에 막을 형성한 후 900℃~1000℃의 화염을 8~13분 동안 가해 골분을 덩어리로 응집시킨 다음에 고온인 1700℃~2000℃의 화염을 15~25분 동안 가해 용융시켜서 얻는 액상의 골분으로 결정체를 제조하는 것이므로, 액상의 골분을 얻기 위한 과정이 매우 복잡하고 많은 시간이 소요되기 때문에 생산성이 저하되는 문제점은 물론 에너지의 사용량이 많아 생산비용이 상승하게 되는 등의 문제점도 있었다.However, in such a method, a bone meal is put into a ceramic melting furnace, a flame of 450 ° C to 550 ° C is applied to form a film on the surface of the bone meal, and a flame of 900 ° C to 1000 ° C is added for 8-13 minutes to agglomerate the bone meal into a mass Since the process for producing a crystal is made from a liquid bone meal obtained by adding a flame at a high temperature of 1,700 ° C to 2,000 ° C for 15 to 25 minutes to obtain a liquid crystal bone meal, the process for obtaining a liquid bone meal is very complicated and takes a long time, There is a problem that the production cost is increased due to a large amount of energy used.
또한, 골분에 소량의 탄산바륨과 석회만을 혼합하여 용해시켜 제조하는 것이므로, 결정체의 색상이 비취 빛으로 한정되기 때문에 장식효과가 반감되는 등의 문제점도 있었다.In addition, since it is produced by mixing only a small amount of barium carbonate and lime in the bone fragrance and dissolving it, there is also a problem that the decorative effect is reduced by half because the hue of the crystal is limited to jade light.
본 발명은 종래의 이러한 점들을 감안하여 발명된 것으로서, 그 목적은 골분결정체를 낮은 온도에서 단시간에 외관이 미려하고 장기간이 지나도 천연의 다양한 색상과 광택 등이 그대로 보존되게 고강도로 성형함으로써 생산성의 상승과 에너지의 절감효과는 물론 장식효과를 더욱 향상시켜 주는 골분결정체 및 그 제조방법을 제공하는 것이다.SUMMARY OF THE INVENTION The present invention has been made in view of such conventional points, and an object of the present invention is to provide a method and a device for molding a bone fragrant crystal with high strength so as to preserve various natural hues and luster even after a long period of time, The present invention also provides a method of manufacturing a bone fragrant crystal and a method of manufacturing the same.
본 발명은 이러한 목적을 달성하기 위해, 화장하고 남은 뼈를 입자가 미세한 분말로 되게 분쇄한 다음 불순물을 선별제거하고 수분함량이 7~10중량%로 되게 건조하여 순수한 골분을 조성하는 골분조성단계와; 상기 골분조성단계에서 조성된 골분 50~60중량%에 리튬 22~25중량%와, 나노산화세륨 6~8중량%와, 콜라겐 8~10중량% 및 붕소·붕사·붕산들 중 어느 하나의 4~7중량%를 혼합하여 1차 골분혼합물을 얻는 제1혼합단계와; 상기 1차 골분혼합물 90~95중량%에 규소 또는 알루미나 5~10중량%를 혼합하여 2차 골분혼합물을 얻는 제2혼합단계와: 상기 2차 골분혼합물 93~96중량%에 천연색상을 갖는 물질인 녹차분말·홍차분말·송진분말·황토분말·해초분말들 중 어느 하나 또는 하나 이상의 복수를 4~7중량% 혼합하여 3차 골분혼합물을 얻는 제3혼합단계 및 상기 3차 골분혼합물을 성형판에 함몰형성되는 성형홈들에 각각 충전하고, 가열로에 넣어 1000~1050℃에서 5~10분 동안 가열하여 용융시킨 후 인출 냉각시켜 골분결정체를 얻는 성형단계를 포함하여 이루어져 쉽게 파손되지 않는 고강도로 성형됨과 동시에 외관이 미려하고 장기간이 지나도 천연의 색상과 광택 등이 원형 그대로 보존되기 때문에 장기간 보관할 수 있도록 하는 골분결정체 및 그 제조방법을 제공하는 것이다.In order to accomplish this object, the present invention provides a method for preparing a bone meal, comprising the steps of: crushing the make-up remaining bone into fine powder, screening and removing the impurities, drying the beef to a moisture content of 7 to 10 wt% ; The bone fragments formed in the bone fragrance composition step may contain 22 to 25% by weight of lithium, 6 to 8% by weight of cerium oxide, 8 to 10% by weight of collagen, and 4 to 10% by weight of boron, borax and boric acid in 50 to 60% To 7% by weight of a bone meal to obtain a primary bone meal mixture; A second mixing step of mixing 90 to 95% by weight of the primary bone meal mixture with 5 to 10% by weight of silicon or alumina to obtain a secondary bone meal mixture; and 93 to 96% by weight of the secondary bone meal mixture, A green tea powder, a black tea powder, a rosin powder, a loess powder, and a seaweed powder to obtain a third bone meal mixture by mixing 4 to 7 wt% And a shaping step of filling the shaping recesses formed in the recesses into a heating furnace, heating the compacts at 1000 to 1050 DEG C for 5 to 10 minutes to melt them, And the natural color and gloss are preserved in the original form even after a long period of time, so that they can be stored for a long period of time, and a method for producing the same.
이와 같은 본 발명에 따른 골분결정체의 제조방법 및 그에 따라 제조되는 골분결정체는, 성형하는 시간의 단축과 저온에서의 용융에 따른 에너지사용량의 대폭적인 절감 및 생산성을 상승시켜 주는 등의 효과는 물론 색상이 선명하게 표현됨에 따라 외관이 미려하고 장기간이 지나도 천연의 색상과 광택 등이 변형되거나 변질이 되지 않고 원형 그대로 보존되는 특징도 있다.The method of manufacturing a bone fragrance crystal according to the present invention and the bone fragrance crystal produced by the method according to the present invention are effective not only in shortening the molding time but also remarkably reducing the energy consumption amount due to melting at low temperature and raising the productivity, The appearance is beautiful and the natural color and gloss are not deformed or deteriorated even after a long period of time and are preserved in a circular shape.
도 1은 본 발명 실시 예에 따른 골분결정체 제조방법의 공정도BRIEF DESCRIPTION OF THE DRAWINGS FIG.
이하, 본 발명에 따른 골분결정체 및 그 제조방법을 첨부된 도면에 의거하여 상세하게 설명하면 다음과 같다.DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS Hereinafter, the present invention will be described in detail with reference to the accompanying drawings.
도 1은 본 발명 실시 예에 따른 골분결정체 제조방법의 공정도이다,BRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 is a process diagram of a method of manufacturing a bone fragrant crystal according to an embodiment of the present invention;
도 1의 본 발명에 따른 골분결정체 제조방법은, 유골(동물뼈)로 골분을 조성하는 골분조성단계(10)와, 상기 조성된 골분에 리튬·나노산화세륨·콜라겐과, 붕소·붕사·붕산들 중 어느 하나를 혼합하여 1차 골분혼합물을 얻는 제1혼합단계(20)와, 상기 1차 골분혼합물에 규소나 알루미나 중 어느 하나를 혼합하여 2차 골분혼합물을 얻는 제2혼합단계(30)와, 상기 2차 골분혼합물에 녹차분말·홍차분말·송진분말·황토분말·해초분말들 중 어느 하나를 혼합하여 3차 골분혼합물을 얻는 제3혼합단계(40)와, 상기 3차 골분혼합물을 탄소 판으로 되는 형판에 형성된 다수 성형홈에 각각 충전하고 가열용융시킨 후 냉각하여 성형하는 골분결정체의 성형단계(50)로 이루어지는 것을 특징으로 한다.The method for producing bone fragrance according to the present invention as shown in FIG. 1 comprises the steps of forming bone fragments (10) for forming bone fragments from ashes (animal bones), and adding lithium ions, cerium oxide collagens, boron borax, boric acid A second mixing step (30) for obtaining a primary bone meal mixture by mixing any one of silicon and alumina in the primary bone meal mixture, And a third mixing step (40) of mixing the secondary bone meal mixture with any one of green tea powder, black tea powder, rosin powder, loess powder and seaweed powder to obtain a tertiary bone meal mixture, and a third mixing step (40) A molding step (50) of filling a plurality of molding grooves formed in a mold plate made of a carbon plate, filling each of the molding grooves, heating and melting, and then cooling and molding.
골분조성단계(10)는, 화장을 하고 남은 유골이나 동물뼈를 입자가 미세한 분말로 되게 분쇄한 다음 불순물을 선별제거하고 수분함량이 7~10중량%로 되게 건조하여 순수한 골분을 조성하는 단계이다.The bone
이러한 골분조성단계(10)는 일반적인 분쇄기와 선별기 및 건조기를 사용하여 이루어지는 것이며, 조성된 골분은 미세한 입자의 분말로 됨과 동시에 수분함량이 최소화되기 때문에 후술하는 바와 같이 성형단계(50)에서 신속하게 용융되어 단시간에 골분결정체를 성형할 수 있게 된다.The bone
제1혼합단계(20)는, 골분조성단계(10)에서 조성된 골분 50~60중량%에 리튬 22~25중량%와 나노산화세륨 6~8중량%와 콜라겐 8~10중량% 및 붕소·붕사·붕산들 중 어느 하나의 4~7중량%를 혼합하여 1차 골분혼합물을 얻는 단계이다.In the
이와 같이 1차 골분혼합물에 혼합되는 리튬은 용제로 골분의 용융점을 낮춰주므로 저온에서 신속하게 용융되도록 하며, 나노산화세륨은 성형단계(50)에서 골분혼합물을 형판의 다수 성형홈에 각각 충전하고 가열용융시킨 후 냉각하여 골분결정체를 성형할 때 골분결정체가 성형홈에 부착되는 현상이 전혀 발생하지 않도록 작용함으로써 원형손상이 없이 분리되게 한다.Lithium mixed in the primary bone meal mixture melts rapidly at a low temperature because it lowers the melting point of the bone meal with a solvent. In the forming
또한, 콜라겐은 골분결정체의 색상이 선명하게 표현되도록 하는 작용을 하며, 붕소나 붕사 또는 붕산은 살균 작용과 방부성이 있기 때문에 장기간이 지나도 미생물에 의한 골분결청체의 부패가 초래되는 현상이 발생하지 않도록 한다.In addition, since collagen has a function of expressing the color of the bone fragile crystal clearly, boron, borax or boric acid has a sterilizing action and anticorrosive property so that the phenomenon of causing the decay of the bone fragments caused by the microorganism does not occur even after a long period of time do.
제2혼합단계(30)는, 1차 골분혼합물 90~95중량%에 규소 또는 알루미나를 5~10중량% 혼합하여 2차 골분혼합물을 얻는 단계이다.The second mixing
이렇게 혼합되는 규소 또는 알루미나는, 골분혼합물의 결합력과 강도를 높여주어 골분결정체가 고강도로 성형되어 쉽게 파손 또는 변질이 발생하지 않도록 함으로써 원형이 장기간 그대로 보존되게 한다.The silicon or alumina mixed in this way enhances the binding force and strength of the mixture of bone fragments, so that the fragments of the bone fragments are formed into a high strength so that breakage or alteration does not occur easily, thereby preserving the original shape for a long period of time.
제3혼합단계(40)는, 2차 골분혼합물 93~96중량%에 녹차분말·홍차분말·송진분말·황토분말·해초분말 등과 같은 천연색상을 갖는 물질들 중 어느 하나 또는 필요에 따라 하나 이상의 복수를 4~7중량% 혼합하여 3차 골분혼합물을 얻는 단계이다.The third mixing
이러한 3차 골분혼합물에 혼합되는 녹차분말·홍차분말·송진분말·황토분말·해초분말들은, 각각 그 천연의 색상에 의해 골분결정체를 원하는 색상으로 성형할 수 있게 된다.Green tea powder, black tea powder, rosin powder, loess powder, and seaweed powder mixed in the mixture of the third bone fractions can be molded into a desired color by the natural color of each of them.
즉, 골분혼합물에 녹차분말을 혼합하여 성형하면 녹색의 골분결정체를 얻게 되며, 또한, 홍차분말은 붉은색의 골분결정체를 송진분말은 노란색의 골분결정체를 얻게 된다.That is, when the green tea powder is mixed with the bone meal mixture, green bone powder crystals are obtained. In addition, the red powder of the black tea powder and the yellow powder of the rosin powder are obtained.
한편, 골분결정체의 색상 선택은 반드시 녹차분말·홍차분말·송진분말·황토분말·해초분말들에만 한정되는 것은 아니며, 이들 이외에도 원하는 색상을 표현할 수 있는 천연물질이라면 어떠한 것이라도 사용할 수 있는 것으로서 이러한 경우에도 발명의 범위에 속하게 되는 것임은 물론이다.On the other hand, the selection of the color of the bone crumb crystal is not limited to the green tea powder, the black tea powder, the rosin powder, the loess powder and the seaweed powder, and any natural substance which can express a desired color may be used. Of course, fall within the scope of the invention.
성형단계(50)는, 성형판에 종횡일정간격으로 내면이 곡면으로 되게 소정깊이로 함몰형성되는 성형홈들에 각각 3차 혼합물을 충전하고, 가열로 넣어 1000~1050℃에서 5~10분 동안 가열하여 용융시킨 후 인출하여 냉각시켜 이루어진다.In the forming
이러한 성형단계(50)는, 골분혼합물에 혼합된 리튬에 의해 골분혼합물의 용융점이 크게 낮아져 1000~1050℃의 저온에서 단시간에 용융이 완료된다.In this
이렇게 용융되는 골분혼합물은 나노산화세륨의 작용에 따라 각 성형홈에 구 형태를 이루고 있게 되며, 이에 따라 냉각시키면 구슬모양으로 됨과 동시에 성형홈에 극히 일부분이라도 부착되는 현상이 전혀 발생하지 않고 분리되기 때문에 깨끗한 골분결정체를 얻게 된다.The mixture of molten bone fractions is spherical in the shape of each groove according to the action of the nano-ceria, so that it becomes a bead shape when cooled, and at the same time, even a small part of the groove is adhered to the groove A clear bone fragrance crystal is obtained.
이와 같이 제조되는 골분결정체는, 이물질이 선별제거된 골분에 리튬·나노산화세륨·콜라겐과, 붕소·붕사·붕산들 중 어느 하나를 혼합한 후 규소 또는 알루미나 중 어느 하나를 혼합하고 천연색상을 갖는 천연물질인 녹차분말·홍차분말·송진분말·황토분말·해초분말들 중 어느 하나를 혼합한 골분혼합물을 탄소 판으로 되는 형판의 성형홈들에 각각 충전하여 단시간에 가열하여 용융시켜 냉각하여 성형하는 것이므로, 골분결정체를 성형하는 시간의 단축과 저온에서의 용융에 따른 에너지사용량의 대폭적인 절감 및 생산성을 상승시켜 주는 등의 효과도 있다.The bone fragrant crystals thus produced are prepared by mixing lithium, nano-oxide cerium, collagen, boron, borax, boric acid, or the like mixed with silicon or alumina, The mixture of bone powder mixed with any one of green tea powder, black tea powder, rosin powder, loess powder and seaweed powder, which is a natural substance, is charged into the molding grooves of a plate made of a carbon plate, and the mixture is heated and melted for a short time, It is possible to shorten the time required for molding the bone crushed crystal, drastically reduce the amount of energy consumed due to melting at low temperature, and increase the productivity.
또한, 색상이 선명하게 표현됨에 따라 외관이 미려하여 장식효과를 더욱 향상시켜 줌과 동시에 장기간이 지나도 변형되거나 변질이 되지 않고 원형이 그대로 보존되는 골분결정체를 제공하게 되는 등의 특징이 있다.Further, since the color is expressed clearly, the appearance is so beautiful that the decoration effect is further improved, and at the same time, a bone fragrance is provided in which the original shape is preserved without being deformed or altered even after a long period of time.
10 : 골분조성단계 20 : 제1혼합단계
30 : 제2혼합단계 40 : 제3혼합단계
50 : 성형단계10: bone meal forming step 20: first mixing step
30: second mixing step 40: third mixing step
50: molding step
Claims (2)
상기 골분조성단계(10)에서 조성된 골분 50~60중량%에 리튬 22~25중량%와, 나노산화세륨 6~8중량%와, 콜라겐 8~10중량% 및 붕소·붕사·붕산들 중 어느 하나의 4~7중량%를 혼합하여 1차 골분혼합물을 얻는 제1혼합단계(20)와;
상기 1차 골분혼합물 90~95중량%에 규소 또는 알루미나 5~10중량%를 혼합하여 2차 골분혼합물을 얻는 제2혼합단계(30)와:
상기 2차 골분혼합물 93~96중량%에 천연색상을 갖는 물질인 녹차분말·홍차분말·송진분말·황토분말·해초분말들 중 어느 하나 또는 하나 이상의 복수를 4~7중량% 혼합하여 3차 골분혼합물을 얻는 제3혼합단계(40); 및
상기 3차 골분혼합물을 성형판에 함몰형성되는 성형홈들에 각각 충전하고, 가열로 넣어 1000~1050℃에서 5~10분 동안 가열하여 용융시킨 후 인출 냉각시켜 골분결정체를 얻는 성형단계(50)를 포함하여 이루어지는 것을 특징으로 하는 골분결정체 제조방법,(10) which comprises crushing the bone remaining to be made into a powder, selectively removing impurities, and drying the mixture to have a moisture content of 7 to 10% by weight to form bone fragments;
In the bone fragrance composition step 10, 22 to 25% by weight of lithium, 6 to 8% by weight of cerium oxide, 8 to 10% by weight of collagen, and boron, borax and boric acid are added to 50 to 60% A first mixing step (20) for obtaining a primary bone meal mixture by mixing 4 to 7% by weight of one;
A second mixing step (30) in which 90 to 95% by weight of the primary bone meal mixture is mixed with 5 to 10% by weight of silicon or alumina to obtain a secondary bone meal mixture;
The green tea powder, the black tea powder, the rosin powder, the loess powder, and the seaweed powder, which are natural coloring substances, are mixed with 93 to 96% by weight of the secondary bone meal mixture in an amount of 4 to 7 wt% A third mixing step (40) to obtain a mixture; And
A molding step (50) of filling the above-mentioned mixture of the third bone fractions into the molding grooves formed in the molding plate, heating the mixture at 1000 to 1050 ° C for 5 to 10 minutes to melt, A method of manufacturing a bone fragrant crystal,
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