KR101804877B1 - 침강 실리카의 신규 제조 방법, 신규 침강 실리카, 및 특히 중합체 보강을 위한 그의 용도 - Google Patents

침강 실리카의 신규 제조 방법, 신규 침강 실리카, 및 특히 중합체 보강을 위한 그의 용도 Download PDF

Info

Publication number
KR101804877B1
KR101804877B1 KR1020157007619A KR20157007619A KR101804877B1 KR 101804877 B1 KR101804877 B1 KR 101804877B1 KR 1020157007619 A KR1020157007619 A KR 1020157007619A KR 20157007619 A KR20157007619 A KR 20157007619A KR 101804877 B1 KR101804877 B1 KR 101804877B1
Authority
KR
South Korea
Prior art keywords
precipitated silica
silica
filter cake
silicate
acid
Prior art date
Application number
KR1020157007619A
Other languages
English (en)
Korean (ko)
Other versions
KR20150046289A (ko
Inventor
세드릭 부아뱅
로랑 기
에릭 페랭
킬라니 라미리
Original Assignee
로디아 오퍼레이션스
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 로디아 오퍼레이션스 filed Critical 로디아 오퍼레이션스
Publication of KR20150046289A publication Critical patent/KR20150046289A/ko
Application granted granted Critical
Publication of KR101804877B1 publication Critical patent/KR101804877B1/ko

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/126Preparation of silica of undetermined type
    • C01B33/128Preparation of silica of undetermined type by acidic treatment of aqueous silicate solutions
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/187Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
    • C01B33/193Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/18Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20Oxides; Hydroxides
    • C08K3/22Oxides; Hydroxides of metals
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/34Silicon-containing compounds
    • C08K3/36Silica
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00Use of organic ingredients
    • C08K5/04Oxygen-containing compounds
    • C08K5/09Carboxylic acids; Metal salts thereof; Anhydrides thereof
    • C08K5/092Polycarboxylic acids
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00Use of pretreated ingredients
    • C08K9/02Ingredients treated with inorganic substances
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00Use of pretreated ingredients
    • C08K9/04Ingredients treated with organic substances
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09CTREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28Compounds of silicon
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09CTREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28Compounds of silicon
    • C09C1/30Silicic acid
    • C09C1/3045Treatment with inorganic compounds
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09CTREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28Compounds of silicon
    • C09C1/30Silicic acid
    • C09C1/3063Treatment with low-molecular organic compounds
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09CTREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/06Treatment with inorganic compounds
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09CTREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/08Treatment with low-molecular-weight non-polymer organic compounds
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/16Pore diameter
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/18Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20Oxides; Hydroxides
    • C08K3/22Oxides; Hydroxides of metals
    • C08K2003/2227Oxides; Hydroxides of metals of aluminium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Inorganic Chemistry (AREA)
  • Silicon Compounds (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
KR1020157007619A 2012-08-31 2013-09-02 침강 실리카의 신규 제조 방법, 신규 침강 실리카, 및 특히 중합체 보강을 위한 그의 용도 KR101804877B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR1202349A FR2994962B1 (fr) 2012-08-31 2012-08-31 Nouveau procede de preparation de silices precitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres
FR1202349 2012-08-31
PCT/EP2013/068106 WO2014033301A1 (fr) 2012-08-31 2013-09-02 Nouveau procede de preparation de silices precipitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres

Publications (2)

Publication Number Publication Date
KR20150046289A KR20150046289A (ko) 2015-04-29
KR101804877B1 true KR101804877B1 (ko) 2017-12-06

Family

ID=47710212

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020157007619A KR101804877B1 (ko) 2012-08-31 2013-09-02 침강 실리카의 신규 제조 방법, 신규 침강 실리카, 및 특히 중합체 보강을 위한 그의 용도

Country Status (15)

Country Link
US (1) US9862810B2 (ja)
EP (1) EP2890638B1 (ja)
JP (1) JP5996807B2 (ja)
KR (1) KR101804877B1 (ja)
CN (1) CN104603055B (ja)
BR (1) BR112015004241B1 (ja)
CA (1) CA2881281C (ja)
ES (1) ES2711573T3 (ja)
FR (1) FR2994962B1 (ja)
MX (1) MX360563B (ja)
PL (1) PL2890638T3 (ja)
RU (1) RU2673521C2 (ja)
TR (1) TR201902111T4 (ja)
TW (1) TWI508919B (ja)
WO (1) WO2014033301A1 (ja)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL3105180T3 (pl) * 2014-02-14 2019-10-31 Rhodia Operations Sposób otrzymywania strąconych krzemionek, strącane krzemionki i ich zastosowania, zwłaszcza do wzmacniania polimerów
TR201810851T4 (tr) * 2014-02-14 2018-08-27 Rhodia Operations Çöktürülmüş silikanın hazırlanması prosesi, çöktürülmüş silika ve özellikle polimerlerin takviyeleri için kullanımı.
FR3018070B1 (fr) * 2014-02-28 2017-09-15 Rhodia Operations Nouveau procede de preparation de silices precipitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres
FR3018072B1 (fr) * 2014-02-28 2019-10-25 Rhodia Operations Nouveau procede de preparation de silices precipitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres
US10487213B2 (en) * 2014-03-05 2019-11-26 Rhodia Operations Process for the preparation of precipitated silicas, precipitated silicas and their uses, in particular for the reinforcement of polymers
US20180215895A1 (en) * 2015-06-12 2018-08-02 Bridgestone Corporation Rubber composition and tire
EP3717278A1 (en) * 2017-11-29 2020-10-07 Pirelli Tyre S.p.A. Microbeads comprising silicate fibres with needle-shaped morphology of nanometric size, preparation thereof, elastomeric compositions and tyres for vehicles comprising them
EP3820816A1 (en) * 2018-07-13 2021-05-19 Rhodia Operations Precipitated silica with improved processing properties
WO2021186210A1 (en) * 2020-03-16 2021-09-23 Bridgestone Europe Nv/Sa Rubber composition, rubber product and tyre

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100244062B1 (ko) * 1994-06-07 2000-02-01 로디아 쉬미 침강 실리카의 제조 방법, 알루미늄을 함유하는침강 실리카 및 이의 엘라스토머 강화용 용도
JP2008542163A (ja) * 2005-05-27 2008-11-27 ロディア・シミ 沈降シリカの製造方法、それにより得られる沈降シリカ、特にシリコン母材において充填剤としての使用

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1420000A1 (ru) * 1986-01-02 1988-08-30 Предприятие П/Я В-2609 Полимерна композици
FR2627176B1 (fr) 1988-02-11 1990-06-15 Rhone Poulenc Chimie Suspension aqueuse stable de silice de precipitation
FR2732331B1 (fr) * 1995-03-29 1997-06-20 Rhone Poulenc Chimie Nouveau procede de preparation de silice precipitee, nouvelles silices precipitees contenant du zinc et leur utilisation au renforcement des elastomeres
FR2732328B1 (fr) * 1995-03-29 1997-06-20 Rhone Poulenc Chimie Nouveau procede de preparation de silice precipitee, nouvelles silices precipitees contenant de l'aluminium et leur utilisation au renforcement des elastomeres
FR2732351B1 (fr) * 1995-03-29 1998-08-21 Michelin & Cie Composition de caoutchouc pour enveloppe de pneumatique renfermant de la silice dopee aluminium a titre de charge renforcante
FR2732329B1 (fr) 1995-03-29 1997-06-20 Rhone Poulenc Chimie Nouveau procede de preparation de silice precipitee, nouvelles silices precipitees contenant de l'aluminium et leur utilisation au renforcement des elastomeres
FR2819246B1 (fr) * 2000-12-27 2003-10-03 Rhodia Chimie Sa Suspensions de silice precipitee, dopee et de faible granulometrie et leur application comme charge pour papier
FR2833937B1 (fr) * 2001-12-26 2004-11-12 Rhodia Chimie Sa Silices a faible reprise en eau
EP1674520A1 (en) * 2004-12-23 2006-06-28 Rhodia Chimie Elastomeric composition comprizing functionalized butadienic elastomers and high dispersible aluminium-based silica
FR2994963B1 (fr) 2012-08-31 2014-10-03 Rhodia Operations Nouveau procede de preparation de silices precipitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres
FR2994961B1 (fr) 2012-08-31 2014-10-03 Rhodia Operations Nouveau procede de preparation de silices precipitee, nouvelles silices precipitees et leur utilisations, notamment pour le renforcement de polymeres

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100244062B1 (ko) * 1994-06-07 2000-02-01 로디아 쉬미 침강 실리카의 제조 방법, 알루미늄을 함유하는침강 실리카 및 이의 엘라스토머 강화용 용도
JP2008542163A (ja) * 2005-05-27 2008-11-27 ロディア・シミ 沈降シリカの製造方法、それにより得られる沈降シリカ、特にシリコン母材において充填剤としての使用

Also Published As

Publication number Publication date
US9862810B2 (en) 2018-01-09
US20150247022A1 (en) 2015-09-03
TW201425225A (zh) 2014-07-01
FR2994962B1 (fr) 2014-12-26
TWI508919B (zh) 2015-11-21
BR112015004241A2 (pt) 2017-07-04
EP2890638B1 (fr) 2018-11-14
JP5996807B2 (ja) 2016-09-21
MX2015002581A (es) 2015-06-22
CN104603055A (zh) 2015-05-06
CN104603055B (zh) 2016-10-26
ES2711573T3 (es) 2019-05-06
CA2881281A1 (fr) 2014-03-06
FR2994962A1 (fr) 2014-03-07
RU2673521C2 (ru) 2018-11-27
EP2890638A1 (fr) 2015-07-08
RU2015111246A (ru) 2016-10-20
WO2014033301A1 (fr) 2014-03-06
JP2015529625A (ja) 2015-10-08
CA2881281C (fr) 2020-10-27
TR201902111T4 (tr) 2019-03-21
BR112015004241B1 (pt) 2021-09-21
MX360563B (es) 2018-11-07
KR20150046289A (ko) 2015-04-29
PL2890638T3 (pl) 2019-05-31

Similar Documents

Publication Publication Date Title
KR101804876B1 (ko) 침강 실리카의 신규 제조 방법, 신규 침강 실리카, 및 특히 중합체 보강을 위한 그의 용도
KR101804877B1 (ko) 침강 실리카의 신규 제조 방법, 신규 침강 실리카, 및 특히 중합체 보강을 위한 그의 용도
KR102150435B1 (ko) 침강 실리카의 신규 제조 방법, 신규 침강 실리카, 및 특히 중합체 보강을 위한 그의 용도
KR102397679B1 (ko) 침강 실리카의 신규 제조 방법, 신규 침강 실리카, 및 특히 중합체 강화를 위한 이의 용도
KR102398810B1 (ko) 침강 실리카의 신규 제조 방법, 신규 침강 실리카, 및 특히 중합체 강화를 위한 이의 용도
KR102397678B1 (ko) 침강 실리카의 제조 방법, 침강 실리카, 및 특히 중합체 보강을 위한 이의 용도
JP6564388B2 (ja) 沈澱シリカの新規製造方法、新規沈澱シリカおよび、特にポリマーを強化するための、それらの使用
EP3110760B1 (en) Process for the preparation of precipitated silicas, precipitated silicas and their uses, in particular for the reinforcement of polymers
TWI658991B (zh) 製備沈澱二氧化矽之新穎方法,新穎沈澱二氧化矽及其用途,尤其是用於增強聚合物
KR102398816B1 (ko) 침강 실리카의 제조 방법, 침강 실리카, 및 특히 중합체 보강을 위한 이의 용도
KR102398812B1 (ko) 침강 실리카의 제조 방법, 침강 실리카, 및 특히 중합체 보강을 위한 이의 용도
EP3105183B1 (en) Process for the preparation of precipitated silica, precipitated silica and its uses, in particular for the reinforcement of polymers

Legal Events

Date Code Title Description
A201 Request for examination
E902 Notification of reason for refusal
E701 Decision to grant or registration of patent right