KR101788791B1 - Manufacturing method of bio cellulous sheet having curcumin - Google Patents
Manufacturing method of bio cellulous sheet having curcumin Download PDFInfo
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- KR101788791B1 KR101788791B1 KR1020150166508A KR20150166508A KR101788791B1 KR 101788791 B1 KR101788791 B1 KR 101788791B1 KR 1020150166508 A KR1020150166508 A KR 1020150166508A KR 20150166508 A KR20150166508 A KR 20150166508A KR 101788791 B1 KR101788791 B1 KR 101788791B1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A45—HAND OR TRAVELLING ARTICLES
- A45D—HAIRDRESSING OR SHAVING EQUIPMENT; EQUIPMENT FOR COSMETICS OR COSMETIC TREATMENTS, e.g. FOR MANICURING OR PEDICURING
- A45D44/00—Other cosmetic or toiletry articles, e.g. for hairdressers' rooms
- A45D44/002—Masks for cosmetic treatment of the face
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- A—HUMAN NECESSITIES
- A45—HAND OR TRAVELLING ARTICLES
- A45D—HAIRDRESSING OR SHAVING EQUIPMENT; EQUIPMENT FOR COSMETICS OR COSMETIC TREATMENTS, e.g. FOR MANICURING OR PEDICURING
- A45D44/00—Other cosmetic or toiletry articles, e.g. for hairdressers' rooms
- A45D44/22—Face shaping devices, e.g. chin straps; Wrinkle removers, e.g. stretching the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The present invention is in the field of cosmetics, and in particular, discloses a process for producing bio-cellulose containing a sulfur component. In the method for producing a bio-cellulose containing a sulfur component of the present invention, since a mask pack is produced using turmeric which is effective for skin moisturization and anti-aging, there is no need for a separate decolorization and deodorization process, Because it is a manufacturing method using natural materials, there is no side effect to the human body.
Description
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for producing a bio-cellulose sheet, and more particularly, to a method for producing a bio-cellulose sheet containing turmeric.
In general, in the field of cosmetics, a sheet type pack is a product which can obtain a moisturizing and cleansing effect by attaching a sheet made of a specific shape to a human body without needing to hand it. The sheet type pack has a supporter capable of supporting the emulsion for a long time to act on the skin as compared with general makeup emulsion. Due to the occlusive effect provided by the supporter, the skin penetration effect of the skin effect ingredient is enhanced It is a cosmetic product with excellent moisturizing effect and skin care effect.
Generally, the cosmetic sheet is a plant cellulose fiber obtained from cotton or pulp, or a nonwoven fabric made of synthetic fibers, which is used as a fresh water body or a mask-like support of cosmetic lotion. In addition to the fibrous nonwoven fabric, diverse and unique supports can be used as the fresh water body of the cosmetic lotion, and they are differentiated in terms of feel, fit, and efficacy. Various materials researches have been attempted.
On the other hand, bio cellulose produced using microorganisms is a natural material, so it has no side effects and does not cause environmental pollution. Unlike plant celluloses, it is an ultrafine fiber and has excellent physical strength, harmless biodegradability, The material is attracting attention because. Because of its physical and chemical properties, it is used as an industrial material for foods, medical care, and the like. At present, a process for dewatering and compressing a bio-cellulose sheet is a process for producing a sheet of a small amount (1 to 10 sheets) at a time in a manner of pressing using a towel or a sponge or by using centrifugal separation to obtain several sheets Method is used. Biocellulose produced through microorganisms requires deodorization and decolorization due to odor and coloring peculiar to the culture medium.
Korean Patent Publication No. 2010-0135455 discloses a bio-cellulose mask pack sheet using co-cultivation of acetobactor xylenol and yeast. However, this takes a long time to deodorize the bio-cellulose produced.
Therefore, development of a bio-cellulose sheet which is easier to manufacture and economical is required.
Disclosure of Invention Technical Problem [8] Accordingly, the present invention has been made keeping in mind the above problems occurring in the prior art, and an object of the present invention is to provide a method for producing a bio-cellulose sheet which is easy to produce and has a moisturizing effect and an anti-aging effect.
In order to solve the above problems, the inventors of the present invention have found a method for producing a bio-cellulose mask pack sheet containing a sulfur component and exhibiting a moisturizing effect and an anti-aging effect, thereby completing the present invention.
The present invention relates to a method for producing a bio-cellulose sheet containing a sulfur component,
The method comprises the steps of: inoculating a sterilized culture with Acetobactor Xylinum, a strain of bio-cellulose production; Culturing the produced strain at 30 ° C. for 8 to 12 days to produce bio-cellulose; Collecting and slicing the bio-cellulose, and washing the bio-cellulose; Forming a bio-cellulosic laminate in which 50 to 200 slices of the sliced bio-cellulose are stacked in a mesh bag; Stacking a plurality of mesh bags including the bio-cellulose laminate in a vertical direction, compressing the bag at a predetermined weight to dewater, and adjusting a thickness of the bio-cellulosheet; Subjecting the dehydrated and thickness-adjusted bio-cellulose to a preservation treatment and grounding the non-woven fabric or paper; And sterilizing the bio-cellulose which has undergone the molding step using a gamma ray after sealing, wherein the culture liquid contains 60 to 80% by weight of a coconut solution, 0.1 to 30% by weight of a sulfuric acid and 0.05 to 0.1% by weight of an additive Wherein the solution contains a sulfur component. The present invention also provides a method for producing a bio-cellulose sheet.
The present invention also provides a method for producing a bio-cellulose sheet containing a sulfur component, wherein the culture broth is sterilized at 100 DEG C for 30 minutes.
The present invention also relates to the above-mentioned preservative treatment, wherein said at least one substance selected from the group consisting of phenoxy ethanol, methyl paraben, ethyl paraben, propyl paraben, butyl paraben and 1,2- 0.3 wt%, and the immersion is carried out for 2 to 30 hours. The present invention also provides a method for producing a bio-cellulose sheet containing sulfur components.
The present invention also provides a method for producing a bio-cellulose sheet containing a sulfur component, wherein the predetermined weight is 0.8 to 1.2 tons and the thickness is adjusted to 0.1 to 0.6 mm.
The present invention also provides a bio-cellulose sheet containing a sulfur component.
The present invention also provides a bio-cellulose mask pack containing a sulfur component produced using a bio-cellulose sheet containing a sulfur component.
The present invention also provides a biocellulose mask pack containing a sulfur component, wherein the mask pack further comprises a cosmetic ingredient.
In the method for producing a bio-cellulose containing a sulfur component of the present invention, since a mask pack is produced using turmeric which is effective for skin moisturization and anti-aging, there is no need for a separate decolorization and deodorization process, Because it is a manufacturing method using natural materials, there is no side effect to the human body.
BRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 is a photograph of a bio-cellulose prepared from a culture solution containing a sulfur component according to an embodiment of the present invention. FIG.
FIG. 2 is a mask pack prepared by processing bio-cellulose produced from a culture solution containing a sulfur component according to an embodiment of the present invention.
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS Hereinafter, preferred embodiments of the present invention will be described in detail with reference to the accompanying drawings.
In one embodiment, the present invention provides a method for producing a bio-cellulose sheet containing a sulfur component, comprising the steps of: inoculating a sterilized culture with Acetobactor Xylinum, a strain producing bio-cellulose; Culturing the produced strain at 30 ° C. for 8 to 12 days to produce bio-cellulose; Collecting and slicing the bio-cellulose, and washing the bio-cellulose; Forming a bio-cellulosic laminate in which 50 to 200 slices of the sliced bio-cellulose are stacked in a mesh bag; Stacking a plurality of mesh bags including the bio-cellulose laminate in a vertical direction, compressing the bag at a predetermined weight to dewater, and adjusting a thickness of the bio-cellulosheet; Subjecting the dehydrated and thickness-adjusted bio-cellulose to a preservation treatment and grounding the non-woven fabric or paper; And sterilizing the bio-cellulose having undergone the molding step using a gamma ray after sealing.
The biocellulose of the present invention is a cellulose made by culturing a microorganism and may be referred to as a microbial cellulose, and is used as a material for an image processor or a mask pack for medicines. Bio-cellulose is a polymer in which glucose is bonded with? -1,4, like cellulose obtained from plants, but its fiber width is much smaller than that of plant celluloses and has a three-dimensional network structure and excellent water retention. When used in a cosmetic mask, it can give a soft texture like a hydrogel mask and a smooth fit, and it has excellent adhesion. The bio-cellulose of the present invention uses a turmeric extract, a fruit juice containing sugar and acetic acid, such as coconut, as a culture solution, and microorganisms belonging to various classes are used to achieve the effect of the present invention.
Turmeric, Curcuma longa ) is a perennial plant belonging to the ginger family. It is mainly cultivated in tropical and subtropical areas, mainly in India. It is used for stem and root for edible and medicinal purposes. The major component is curcuminoid pigment, and the curative effect of curcumin, which is a physiologically active substance that constitutes about 73% of cucuminoids, is known, and antioxidant, antibacterial, blood circulation improvement, hemostasis and detoxification, atopic dermatitis, And a variety of studies have been actively carried out, including effects on androgenetic alopecia or acne. In the present invention, a turmeric component is added to the culture broth to produce bio-cellulose. The turmeric can be distinguished from the conventional mask pack by being used as a raw material for the mask pack due to the effects of skin moisturization and anti-aging effects. In one embodiment, the culture is a solution comprising 60 to 80 wt.% Of a coconut solution, 5 to 20 wt.% Of a cyanide and 0.05 to 0.1 wt.% Of an additive. In the production method of the present invention, the color of the bio-cellulose produced when the sulfur component is added to the culture liquid becomes yellowish as shown in FIG. 1, and the green body is aesthetically pleasing. In addition, it is not necessary to take a deodorizing process to eliminate the incense of the culture medium itself due to the unique flavor of turmeric. The manufacturing cost and the manufacturing time can be reduced by manufacturing the mask pack without the need for the separate decoloring and deodorizing process. In addition, since it is a manufacturing method using a natural substance, there is no side effect to the human body.
The microorganism inoculated into the culture medium may be a microorganism using at least one microorganism selected from the group consisting of Acetobacter sp., Rhizobium sp., And Agrobacterium sp. (Acetobactor Xylinum). The culturing conditions of the microorganisms are incubated at 20 ° C to 40 ° C for 5 to 10 days in order to maintain optimal growth of the microorganisms producing the bio-cellulose. If the temperature of the microorganism is lowered to below 20 캜, the temperature is too low to grow the microorganism well, which makes it difficult to produce the desired bio-cellulose. Even if the temperature exceeds 40 캜, the temperature is too high to adversely affect microbial growth It becomes difficult to produce the intended bio-cellulose. In the embodiment of the present invention, the bio-cellulose is produced using the acetobactor xylenol.
In the present invention, in order to facilitate the adjustment of the thickness of the bio-cellulose sheet, the bio-cellulose culture container is cultured in a container having a size of, for example, 30 cm to 35 cm and a length of 30 cm to 35 cm to produce 0.5 to 2.0 mm thick bio- . The produced bio-cellulose is stacked in a mesh bag for 50 to 200 sheets, and a plurality of mesh bags including the bio-cellulose laminate are vertically stacked. The mesh bag laminate is compressed to a weight of 0.8 to 1.2 ton to be dehydrated, and the thickness of the bio-cellulose sheet can be adjusted to 0.1 mm to 0.6 mm through weight control. If necessary, the bio-cellulose sheet can be washed several times using purified water.
The method for producing a bio-cellulose sheet containing a sulfur component of the present invention includes an embedding treatment step. Due to the nature of bio-cellulose, it is easily contaminated and decayed due to contamination from the outside, so it is subjected to a preservative treatment process to be used as a mask pack sheet for cosmetics. In one embodiment, the resulting bio-cellulose sheet is washed three or more times with purified water, and then subjected to a preservative treatment process. Wherein the preservative treatment is one or more selected from the group consisting of phenoxy ethanol, methyl paraben, ethylparaben, propylparaben, butylparaben and 1,2-hexanediol, and the at least one substance is added to purified water The bio-cellulose sheet is immersed and treated. In one embodiment, the aqueous solution contains 0.1 to 0.3% by weight, and the immersion is conducted for 2 to 30 hours. The bio-cellulose sheet completed through the preservation treatment can be stored for a long time, and various cosmetic materials can be applied.
The cosmetics applicable to the bio-cellulose sheet according to the present invention are not particularly limited and may include conventional additives such as antioxidants, stabilizers, solubilizers, vitamins, pigments and / or perfumes. The bio-cellulose containing the sulfur component of the present invention can be processed into a mask form using a molding machine or the like to produce a mask pack for a face (FIG. 2). In one embodiment, the papermaking and nonwoven fabrics are respectively grounded on both sides of the plate-type bio-cellulose and compressed to about 0.3 mm to remove 90% moisture of the bio-cellulose. Folding, inserting, filling and packaging processes, and gamma-ray irradiation for sterilization are performed for the production of cosmetic mask packs.
Hereinafter, embodiments are provided to facilitate understanding of the present invention. However, the following examples are provided only for the purpose of easier understanding of the present invention, and the present invention is not limited to the following examples.
Example
Example One Bio-cellulose Manufacture of sheet
end. Preparation of Culture Strain
400 ml of a vessel (pH 3-4) in which 1% (v / v) acetic acid was added to the stock solution of coconut extract was inoculated into a 1 L Erlenmeyer flask and inoculated with Acetobacter xylinum BRC5 and shaken at 30 ° C and 150 rpm for 3 days Lt; / RTI >
I. Bio-cellulose production
The turmeric was used as a turmeric extract by filtration with a mixer. In order to control the shape of the produced bio-cellulose, a plastic container having a width of 32 cm and a length of 33 cm was used. The culture liquid was coconut (100 g) containing 1% (v / v) acetic acid, 10% Extract. The culture broth according to Example 1 (a) was inoculated at 5% (v / v) and cultured at 30 ° C for 10 days to produce bio-cellulose having a thickness of 10 to 15 mm. The broth was sliced A translucent gel-state microbial cellulose having a thickness of about 3 mm was obtained.
100 of the sliced bio-celluloses were stacked in a mesh bag. 50 mesh bags containing the bio-cellulosic laminate were prepared and dehydrated and compressed at a weight of 1 ton to prepare a 0.15-0.5 mm bio-cellulose sheet. This can simultaneously produce 1000 to 10000 sheets of bio-cellulose sheets, thus saving manufacturing cost and time.
All. Compression and molding
The nonwoven fabric was attached to one surface of each bio-cellulose sheet produced and processed according to the above example, and the other surface was coated with paper, followed by compressing to remove moisture of 90% or more, and then a face mask pack sheet was completed using a molding machine . In order to prevent the secondary contamination of the completed mask pack sheet, the package was sealed with vinyl, and then gamma ray was irradiated to sterilize it.
While the present invention has been described in connection with what is presently considered to be the preferred embodiments, it is to be understood that the invention is not limited to the disclosed embodiments, but, on the contrary, .
All technical terms used in the present invention are used in the sense that they are generally understood by those of ordinary skill in the relevant field of the present invention unless otherwise defined. The contents of all publications referred to herein are incorporated herein by reference.
Claims (7)
The method comprises the steps of: inoculating a sterilized culture with Acetobactor Xylinum, a strain of bio-cellulose production;
Culturing the produced strain at 30 ° C. for 8 to 12 days to produce bio-cellulose;
Collecting the bio-cellulose and slicing and washing the slice with a thickness of 3 mm;
Forming a bio-cellulosic laminate in which 50 to 200 slices of the sliced bio-cellulose are stacked in a mesh bag;
Stacking a plurality of mesh bags including the bio-cellulose laminate in a vertical direction, compressing the bag at a predetermined weight to dewater, and adjusting a thickness of the bio-cellulose sheet;
Treating the dehydrated and thickness-regulated bio-cellulose, grounding the non-woven fabric or papermaking, removing 90% of the moisture, and molding; And
Sterilizing the bio-cellulose which has undergone the molding step by sealing and then using gamma ray,
The culture solution is a solution containing 60 to 80% by weight of a coconut solution, 0.1 to 30% by weight of a sulfuric acid and 0.05 to 0.1% by weight of an additive,
The preservative treatment may include 0.1% to 0.3% by weight of at least one substance selected from the group consisting of phenoxy ethanol, methyl paraben, ethyl paraben, propyl paraben, butyl paraben and 1,2-hexane diol Lt; / RTI > for 2 to 30 hours,
The predetermined weight is 0.8 to 1.2 tons,
Wherein the thickness adjustment is adjusted to 0.1 mm to 0.6 mm.
A method for producing a bio-cellulose sheet containing a sulfur component.
The culture broth is sterilized at 100 DEG C for 30 minutes.
A method for producing a bio-cellulose sheet containing a sulfur component.
Bio-cellulose mask pack containing turmeric ingredients.
Bio-cellulose mask pack containing turmeric ingredients.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR102069443B1 (en) * | 2018-08-31 | 2020-01-22 | (주)대한뷰티산업진흥원 | Biocellulose containing Curcuma longa L., Beta vulgaris and Raphanus sativus L. extract and method for their preparation |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR102039415B1 (en) * | 2017-08-22 | 2019-11-01 | 에이치앤비 주식회사 | Manufacturing method of decolorization inhibiting color bio-cellulose |
| KR102049406B1 (en) * | 2017-08-31 | 2019-11-28 | (주)화니핀코리아 | Cosmetic composition of high viscosity cream type and mask pack using the same |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2011173851A (en) * | 2010-02-25 | 2011-09-08 | Kazki International:Kk | Patch for beautification |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JP2011173851A (en) * | 2010-02-25 | 2011-09-08 | Kazki International:Kk | Patch for beautification |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR102069443B1 (en) * | 2018-08-31 | 2020-01-22 | (주)대한뷰티산업진흥원 | Biocellulose containing Curcuma longa L., Beta vulgaris and Raphanus sativus L. extract and method for their preparation |
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