KR101668319B1 - Manufacturing Method for Mixed Power Comprising Red Ginseng or Ginseng Extract - Google Patents
Manufacturing Method for Mixed Power Comprising Red Ginseng or Ginseng Extract Download PDFInfo
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- KR101668319B1 KR101668319B1 KR1020160028110A KR20160028110A KR101668319B1 KR 101668319 B1 KR101668319 B1 KR 101668319B1 KR 1020160028110 A KR1020160028110 A KR 1020160028110A KR 20160028110 A KR20160028110 A KR 20160028110A KR 101668319 B1 KR101668319 B1 KR 101668319B1
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- ginseng
- red ginseng
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/01—Instant products; Powders; Flakes; Granules
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L21/00—Marmalades, jams, jellies or the like; Products from apiculture; Preparation or treatment thereof
- A23L21/20—Products from apiculture, e.g. royal jelly or pollen; Substitutes therefor
- A23L21/25—Honey; Honey substitutes
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L31/00—Edible extracts or preparations of fungi; Preparation or treatment thereof
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/20—Natural extracts
- A23V2250/21—Plant extracts
- A23V2250/2124—Ginseng
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/10—Drying, dehydrating
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/14—Extraction
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/50—Concentrating, enriching or enhancing in functional factors
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Medicines Containing Plant Substances (AREA)
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Abstract
The present invention relates to a method for producing a mixed ginseng containing red ginseng or ginseng, comprising concentrating red ginseng or ginseng extract to prepare a red ginseng or ginseng concentrate; Concentrating the natural raw material extract to prepare a concentrated natural raw material; Mixing the red ginseng or ginseng concentrate with the natural raw material concentrate to prepare a mixed concentrate; Vacuum drying the mixed concentrate to prepare a powder; Pulverizing the powder; And shaping or pulverizing the coarse pulverized powder.
The method of preparing mixed ginseng containing red ginseng or ginseng according to the present invention can solve problems such as denaturation, browning and carbonization which occur during the pulverization process by employing the vacuum drying method, It is possible to provide a mixed regimen containing red ginseng or ginseng without any deterioration in quality due to the drying process of the natural raw material.
Description
More particularly, the present invention relates to a method for preparing a mixed concentrate by vacuum drying a mixed concentrate consisting of a concentrate of red ginseng or ginseng and a concentrate of a natural raw material will be.
Ginseng or red ginseng extract has higher contents of ginsenoside and more than general ginseng or red ginseng. These red ginseng extracts can be taken by dissolving in water or by ingesting directly into water.
Such red ginseng regeneration is disclosed in Korean Patent Publication No. 10-0470463 by adding water, protease and cellulase to red ginseng powder and honey, and concentrating and distilling in vacuo, then supplementing nutrients necessary for yeast growth, fermenting and aging, And Korean Patent Registration No. 10-1295549 discloses a method for preparing fermented beverage using red ginseng powder and honey. In Korean Patent Registration No. 10-1295549, mixed ginseng oil, pumpkin, pine sprout, safflower seed, ganoderma mushroom and sugar are mixed with red ginseng, A method of preparing a diluted solution by adding water to a fermentation broth and drying and pulverizing the diluted solution while spraying the diluted solution, thereby improving the flavor and mixing with other raw materials so as to be processed into various processed foods Powder.
In the case of preparing red ginseng syrup without mixing with other raw materials, red ginseng syrup is used as a raw material when processed into granules in Korean Patent Publication Nos. 10-1405109 and 10-1102013, and Korean Patent Registration No. 10-1069665 Is used as a raw material for red ginseng seeds in the production of red ginseng tablets, and red ginseng seeds are applied to the production of various types of foods.
However, when preparing the red ginseng extract by using the conventional method, the red ginseng extract is spray-dried using a spray dryer or the like.
This general method of preparing purified ginseng extract is disclosed in Korean Patent Publication No. 10-1343819 by spray-drying with a nozzle atomizing spray drying device to prepare red ginseng concentrate powder. In addition, Korean Patent Laid-Open Publication No. 10-2015-0113724 discloses that a top-spray method can be used in addition to the spray drying method. However, this is a kind of spray drying method, There is no.
The method of directly powdering red ginseng or ginseng, which is not red ginseng or ginseng extract, can take various forms other than spray drying. For example, Korean Patent Registration No. 10-0855897 discloses a process for pulverizing a red ginseng powder into an ultrafine powder using a jet mill.
However, in order to apply such a jet mill method to red ginseng or ginseng extract, a step of solidifying the extract is required, resulting in a decrease in process efficiency. Therefore, spray drying, which is a conventional powdering method, is generally used.
Such conventional spray drying is a typical drying method of pulverizing a liquid material, but the drying condition must be high temperature (180 ° C or higher). Therefore, in the case of red ginseng or ginseng extract, the drying, (Yield reduction). In particular, when applied to a health functional food, there is a problem of a change in an indicator component and a fear of loss.
Particularly, when mixing raw materials of other raw materials and red ginseng or ginseng seeds for the purpose of improving flavor and food production, the mixed powder is dried under the same drying conditions, so that the control of denaturation, Therefore, it is generally manufactured by preparing red ginseng or ginseng roots and other raw materials, and then mixing them.
Therefore, it is necessary to develop a method of producing a regimen which does not deteriorate the quality of the raw material due to the drying process while preparing the mixed regeneration from the mixed raw materials, and maintains a large amount of the ginsenoside component contained in the red ginseng extract or ginseng extract, You will be able to get a regression.
Disclosure of the Invention The present invention has been conceived in order to solve the problems of the prior art as described above, and it is an object of the present invention to provide a method for producing a ginseng or ginseng extract by pulverizing a concentrated concentrate of a red ginseng or a ginseng extract, It is an object of the present invention to provide a method for producing mixed powders of various natural raw materials while solving the problems of denaturation, galling, carbonization, and loss ratio (yield reduction) occurring in the pulverization process.
It is another object of the present invention to provide a method for producing a mixed regimen containing red ginseng or ginseng roots having a significantly reduced change and loss of an indicator component before and after a pulverizing step by employing a vacuum drying method.
In order to solve the above-mentioned problems, the present invention provides a method for preparing mixed ginseng containing red ginseng or ginseng, comprising concentrating red ginseng or ginseng extract to prepare red ginseng or ginseng concentrate; Concentrating the natural raw material extract to prepare a concentrated natural raw material; Mixing the red ginseng or ginseng concentrate with the natural raw material concentrate to prepare a mixed concentrate; Vacuum drying the mixed concentrate to prepare a powder; Pulverizing the powder; And shaping or pulverizing the coarse pulverized powder.
At this time, the natural raw materials are characterized by being one or more of honey, mushrooms, herbs, and herbal medicines.
The red ginseng extract or the ginseng extract may be obtained by extracting a raw material of red ginseng or ginseng using water, ethanol or a mixed solvent thereof and having a solids content of 40 wt% or more.
The vacuum drying is performed until the moisture content of the mixed concentrate reaches 10% by weight or less, and is performed at a temperature of 85 ° C or lower.
In addition, in the step of preparing the powder, the raw material loss rate is 3% or less, and the ginsenoside content loss rate of the mixed red ginseng or ginseng extract is 10% or less.
The method of preparing mixed ginseng containing red ginseng or ginseng according to the present invention can solve problems such as denaturation, browning and carbonization which occur during the pulverization process by employing the vacuum drying method, It is possible to provide a mixed regimen containing red ginseng or ginseng without any deterioration in quality due to the drying process of the natural raw material.
1 is a flow chart showing a process for producing a mixed ginseng containing red ginseng or ginseng according to the present invention.
2 is a photograph of an aqueous solution of 1% (w / w) solids of the spray dried red ginseng solution (a) and the vacuum drying solution (b).
FIG. 3 is a photograph of a mixed regent (a) of red ginseng and honey prepared according to the production method of the present invention and a mixed regent (b) prepared by spray drying.
4 is a photograph of a 1% w / w aqueous solution (a) of a mixed concentrate of red ginseng concentrate, honey and calcium powder and a 1% w / w aqueous solution (b) of a mixed concentrate obtained by vacuum drying the mixed concentrate .
Fig. 5 is a graph showing the results of a 1% w / w aqueous solution (a) of a mixed concentrate of a red ginseng concentrate and a plant extract consisting of jujube, ginger, licorice root, / w aqueous solution (b).
Hereinafter, the present invention will be described in detail.
The mixed regeneration comprising the red ginseng or the ginseng according to the present invention is produced according to the process sequence as shown in Fig.
That is, the mixed regeneration comprises concentrating red ginseng or ginseng extract to prepare a red ginseng or ginseng concentrate; Concentrating the natural raw material extract to prepare a concentrated natural raw material; Mixing the red ginseng or ginseng concentrate with the natural raw material concentrate to prepare a mixed concentrate; Vacuum drying the mixed concentrate to prepare a powder; Pulverizing the powder; And shaping or pulverizing the coarse pulverized powder.
The ginsengs used in the present invention include ginseng, ginseng, taegeuk ginseng and white ginseng. Red ginsengs include red ginseng, black ginseng, In the present invention, the extract is obtained from the ginseng root or red ginseng as a raw material, and then the extract is prepared by using the same.
In addition, the above natural raw materials are any one or more of honey, mushrooms, herbs and herbal medicines, and a concentrate obtained by concentrating the extracts of these natural raw materials is used as a raw material for the preparation of the regeneration.
Examples of the mushroom include throat mushroom, white throat mushroom, mushroom mushroom, mushroom mushroom, mushroom mushroom, mushroom mushroom, matsutake mushroom, shiitake mushroom, mushroom mushroom, mushroom mushroom, mushroom mushroom, scaly mushroom, mushroom mushroom, In addition to the mushroom, any mushroom can be used as the edible mushroom.
As to the foods that can supply nutrients by using mushroom and red ginseng mixture, the utility is well known as disclosed in Korean Patent Publication Nos. 10-0615604 and 10-2006-0001848.
In addition, as for the food for enhancing the immunity and intensifying the nourishment through mixing of red ginseng and honey, as disclosed in Korean Patent Publication No. 10-1148838, Korean Patent Laid-Open Nos. 10-2014-0103668, 10-2015-0064829, The utility is known.
In addition, the improvement of the taste and aroma of red ginseng products by mixing red ginseng and herbal ginseng is also well known in Korean Patent Publication No. 10-1185961.
In the present invention, examples of the medicinal herbs include jujube, gingko, gingen, angelica, gingia, licorice, astragalus, baekbokryeong, hwanggi, hassooo and bokbunja. One or more of these may be used. The production of foods such as beverages by mixing red ginseng with herbal medicines is well known in Korean Registered Patent No. 10-0833208.
In addition, the mixed tablet of the present invention may be prepared by adding various nutrients such as calcium, minerals, and vitamins, if necessary, for application to the production of various foods.
The inventors of the present invention have found that by preparing mixed ginseng mixed with red ginseng or ginseng and natural ingredients on the basis of these known techniques, it is possible to produce red ginseng, health functional foods, liquor, confectionery, tea, biscuit, chocolate, sausage, candy, The present invention has been accomplished to provide a method for producing a mixed tablet which can be easily applied as a raw material for various processed foods such as tea, drink, alcoholic beverage, bread, beverage or vitamin complex.
In general, the methods used in the drying process in the field of food include natural drying, hot air drying, spray drying (S / D), vacuum drying (V / D), freeze drying, F / D).
Natural drying is not suitable for mass production because it carries out the drying process in a state exposed to the external environment, which is problematic in terms of hygiene and process efficiency is lowered.
In addition, hot air drying can cause physico-chemical changes such as taste and flavor of food caused by heat, and thus can not be applied to all foods.
Spray drying is the same as hot air drying in that it is dried under heating conditions, but since it is dried through spray spraying, it can be pulverized at the same time as it is dried and widely used. However, most of the drying conditions are at a high temperature of 180 ° C or more, so that problems such as denaturation, tarnishing, carbonization, etc. may occur due to high temperatures. Therefore, there is a limit to the use of the food according to the kind of the food as in the case of the hot air drying.
Particularly, in foods such as ginseng and red ginseng, in which the content of ginsenoside and changes in color and taste after pulverization are closely related to the quality of the product, the powdering by spray drying is not limited to the product deterioration due to the high temperature But the loss of essential nutrients, especially heat-sensitive components, of ginsenosides, contained in the raw materials.
In addition, when the mixed ginseng and red ginseng is mixed with other ingredients to prepare mixed ginseng, the high temperature stability and the degree of deterioration depending on the materials are different. Therefore, it is very difficult to produce high quality mixed ginseng through one process.
Therefore, drying and pulverization using vacuum drying or freeze drying is expected to be advantageous in view of such problems.
Nevertheless, the reason for using spray drying in most processes is that process optimization is easy and is beneficial for pulverization. Especially, it is not easy to control various process parameters such as vacuum condition, drying time, drying amount per batch, etc., in vacuum drying, which is considered to be advantageous in comparison with spray drying.
In particular, drying and pulverization of ginseng and red ginseng extracts containing a large amount of liquid components by vacuum drying, unlike the case of drying solid ginseng and ginseng products, is not easy to optimize the process conditions . Furthermore, when the liquid component and the liquid component of the natural component for producing the mixed regimen are mixed, the process condition becomes more complicated and the reproducibility is decreased.
Therefore, the spray drying process is practically applied to the powdering of ginseng and red ginseng extracts, as well as ginseng and red ginseng itself, especially in the prior art. In addition, when the mixed regeneration is manufactured, a finished product can be obtained by further performing a step of preparing each regeneration and mixing thereof, which complicates the process and increases the cost.
In view of the problems of the prior art, the present inventors have conducted continuous research on pulverization of mixed extracts of ginseng and red ginseng extracts and natural component extracts through vacuum drying, And a process for obtaining a mixed regent having the characteristics of the present invention has been developed.
When the drying and pulverization process is carried out through vacuum drying, the drying process is performed at a relatively low temperature of 85 ° C or less, preferably 50 to 70 ° C as compared with spray drying. Therefore, the red ginseng extract or the ginseng extract The loss of the surface element (ginsenoside) is greatly reduced. It was also found that changes in taste, color, and flavor were minimized through the sensory evaluation of the manufactured stevens.
Further, it has been found that by applying the vacuum drying of the present invention, it is possible to inhibit the deterioration or denaturation of various natural ingredients contained in the mixed stabilizers by the drying process.
Recently, techniques for commercialization of chaga mushroom extract powder have been developed by vacuum drying at room temperature or vacuum drying at low temperature. However, in case of red ginseng or ginseng extract, the process efficiency is too low and the drying time is too long at room temperature or low temperature. Reproducibility and particle size uniformity are low. Therefore, it is important to carry out the drying process within a temperature range that does not cause carbonization or browning of red ginseng or ginseng extract and under conditions not too low.
Particularly, in the case of spray drying, the process loss rate is about 10% or more of the theoretical yield due to the regeneration that is not recovered due to the inside of the drying chamber. In the present invention, when the drying and pulverizing process is performed through vacuum drying, The loss ratio is less than 3%, which shows that the yield is very high.
In case of vacuum drying, drying and pulverization processes are carried out in a state where a plurality of drying plates having a uniformly coated sample in a drying chamber are stacked and housed. Therefore, after the completion of the process, each drying plate is recovered, It is because it is possible to collect all just by scraping.
In addition, unlike spray drying, liquid components contained in the extract under vacuum drying conditions form a space while being naturally granulated (granulated).
In particular, the advantages of the drying process of the present invention can be confirmed through photographs comparing the aqueous solution of 1% (w / w) solids of the spray dried red ginseng solution (a) and the vacuum drying solution (b) . That is, the red ginseng extract (a) prepared by spray drying and the red ginseng extract (b) prepared by the production method of the present invention were prepared in a flask so as to be an aqueous solution of 1% (w / w) The red ginseng extract prepared by spray drying showed a black color, indicating that the browning and carbonization of the product occurred during the high temperature drying process.
In addition, it can be seen that when powdering by spray drying, a fine powder-form regimen is formed and a granulation process is required in a post-process, but the red ginseng regimen produced according to the preparation method of the present invention is .
In the case of the above-mentioned spray drying, since the caking phenomenon occurs, there is a problem in the packaging of the product, and if left in the air, the water is absorbed to cause aggregation and flowability. Therefore, granulation process should be additionally performed for commercialization.
That is, the red ginseng syrup prepared by spray drying has a relatively low particle size of about 200 mesh, resulting in low charging efficiency when filled in pouches or containers due to caking and low flowability. Due to these problems, additional processes such as granulation are required.
On the other hand, the red ginseng syrup prepared through the vacuum drying of the present invention can be formed into a particle size of 20 to 50 meshes and exhibits excellent flowability and solubility due to the granulation phenomenon in which the surface area of the powder is widened during the vacuum process No separate granulation process is required.
Therefore, the regeneration of the red ginseng or ginseng extract prepared according to the method of the present invention can be easily dissolved by mixing with cold water or hot water, and can be used as a tea drink, and can be produced as a product which can be ingested without user's discomfort even if it is ingested as it is.
In addition, according to the production method of the present invention, it is possible to complete the product by simply collecting the dried powder and then pulverizing it with a general pulverizer and granulating it using a sizing machine, The process efficiency is significantly increased compared to the spray drying which additionally includes the process and the granulation process, which is advantageous in terms of energy consumption.
That is, as shown in FIG. 3, in the case of the mixed regimen (a) of red ginseng and honey produced through the drying process in the production method of the present invention, granulated regenerated fraction can be obtained, (b), since only the powdered stabilized powder can be obtained, when the powder is used for food processing as it is, problems such as generation of loss of regular powder and scattering occur, and the granulation step must be further performed.
In one embodiment, a mixed regimen was prepared from a mixed concentrate consisting of red ginseng extract, honey extract, and calcium powder.
In order to prepare red ginseng extract, red ginseng was extracted with water, ethanol (or alcohol) or a mixed solvent thereof. The extraction solvent is adjusted to be 5 times or more of the raw material, and extracted at 70 to 100 ° C over 3 to 120 hours to produce red ginseng extract.
The red ginseng extract preferably has a solid content of 40 wt% or more. Therefore, the extracted red ginseng extract is subjected to a preliminary concentration and concentration process to increase the solid content.
The reason why the solids content should be 40 wt% or more is to make the content of the indicator substance (ginsenoside) contained in the prepared regeneration to be such that the product can be released. When the extract having a lower solid content is dried and accumulated, a sufficient amount of the indicator substance required as the product can be secured, but the drying process takes a long time and the economic efficiency is lowered. In particular, since the viscosity of the extract applied to the drying vessel is low, it is impossible to apply a sufficient amount of the extract to the drying vessel, so that not only the process efficiency is reduced but also the drying degree depending on the position of the dried drying vessel is changed, .
The red ginseng extract extracted with the above extraction solvent is firstly filtered through a filter net of 100 to 200 mesh, and then filtered using a 10 to 20 탆 filter to remove impurities.
Separately, a honey extract can be prepared through the above process. The mixing ratio of each ingredient may be varied depending on the daily intake of the indicator ingredients for health functional foods or for sensual reasons. In one embodiment, the red ginseng extract, the honey extract, and the calcium powder were mixed at a weight ratio of 20: 79.5: 0.5 to prepare a mixed extract.
The mixed extract prepared by removing and mixing the impurities is subjected to a preliminary concentration step of concentrating the mixture to a solid content of 15 to 30% by weight under a vacuum condition of not less than 700 mbar and 50 ° C or more, and removing the insoluble component using an ultrafast centrifuge . The insoluble component causes the drying efficiency to be lowered during vacuum drying, so it is preferable to remove the insoluble component by centrifugation. At this time, centrifugation is preferably carried out for 5 to 30 minutes under the condition of 9,000 rpm or more.
The extract solution which has been removed from the insoluble components by centrifugation is secondarily concentrated under vacuum conditions of not less than 700 mbar and 50 캜 or more to make the solid content not less than 40% by weight.
The resulting mixed concentrate is concentrated in a vacuum drier and dried to be pulverized. The concentrate is thinly and broadly applied to a plate for drying, and the thickness of the coating is preferably about 1 cm or less.
Drying in a vacuum dryer at a pressure of 800 mbar or more and a vacuum condition of 50 ° C or higher for 4 to 48 hours to carry out drying and pulverization. Such vacuum drying conditions can be flexibly adjusted depending on the state of the sample, the throughput, and the type of the sample. However, as an index of the drying process, the moisture content after drying is used, and the moisture content after the pulverization process should be 10% by weight or less, preferably 3% by weight or less.
During the vacuum drying, liquid components such as moisture contained in the concentrated liquid are removed and a space is formed, resulting in drying in the form of agglomerates of particles.
Therefore, the sieved powder obtained through the pulverization process can be pulverized in a pulverizer regardless of the particle size, and then put into a sieving machine to uniformize the particle size, so that a commercial granular sieving can be obtained.
Further, when the coarse pulverized powder is commercialized as a fine powder, a pulverization process may be further performed to obtain a modified powder having a fine powder form.
The mixed regeneration produced according to the preparation method of the present invention showed a loss of ginsenoside content of 10% or less, preferably 5% or less, more preferably 1% or less as compared with the mixed extract. It can be understood that the loss rate of the indicator component is greatly improved as compared with the loss rate of the ginsenoside content of the regenerated solution prepared by conventional spray drying is 10 to 20%. In the present invention, the ginsenoside content as an indicator component is the total sum of the contents of ginsenosides Rg1, Rb1, and Rg3.
The results of the analysis of the regression of the red ginseng extract prepared according to the preparation method of the present invention are shown in Table 1 (in Table 1, the index component is the total sum of ginsenosides Rg1, Rb1, and Rg3). Table 1 shows the results of analysis of the regression of red ginseng extracts extracted with a mixed solvent of water and alcohol at a weight ratio of 3: 7.
In Table 2, mixed solvent in which water and alcohol are mixed at a weight ratio of 8: 2, mixed solvent in which water and alcohol are mixed at a weight ratio of 7: 3 in Table 3, and water and alcohol in a mixing ratio of 5: The analytical results of the regression of each red ginseng extract extracted with one mixed solvent are described.
From the results of Tables 1 to 4, it was found that the mixed extracts obtained through various mixing ratios showed a yield of 99% or more and an index component yield of about 100% Was obtained.
For example, as shown in Table 1, the solid content after the concentration of the mixed extract was 63.3% by weight, and the content of the solid content was 95% by weight.
Also, the theoretical production per 100 kg was calculated as 66.3 kg, and the actual production amount was 66.0 kg, which is about the same amount as the theoretical production amount. This is a result of the fact that when the same product is spray dried, the production efficiency is greatly increased as compared with the actual production of 60 kg or less.
Particularly, regarding the total content of ginsenosides Rg1, Rb1, and Rg3 as the indicator components, it was found that the theoretical calculated content after drying of the concentrate containing 31.9 mg / g of ginsenoside, The side content was found to be equivalent, and it was confirmed that the loss rate of the surface component was 0% and the yield was 100% in the vacuum drying process.
It can be seen that the production method of the present invention is very effective in maintaining the yield of the indicator component in the pulverization process since the yield of the indicator component is 99% or more although the difference is somewhat different when the mixing ratio of the extraction solvent is different.
This is a result that when the same product is spray-dried, the effect is remarkably excellent when the ginsenoside loss is 10 to 20%.
It can be seen that the process efficiency of the production method of the present invention is much higher than that of the conventional spray drying in view of the same production yield and yield rate of the indicator component for various production conditions.
4, a 1% w / w aqueous solution (a) of a mixed concentrate of red ginseng concentrate, honey and calcium powder and a 1% w / w aqueous solution (b) of the mixed concentrate obtained by vacuum drying the mixed concentrate were compared It can be confirmed that there is almost no change in color visually. This means that the vacuum drying process of the present invention means that the concentrated concentrate is dried as it is without causing problems such as denaturation, browning and carbonization during the drying process.
Separately, in another embodiment, a mixed regimen was prepared from a concentrated mixture of a red ginseng concentrate and a plant extract consisting of jujubes, ginseng, gangrene, angelica, ginger, and licorice.
The results are shown in FIG. 5, and it can be seen from FIG. 5 that a 1% w / w aqueous solution (a) of a mixed concentrate of red ginseng concentrate and a plant extract consisting of jujube, (B) of 1% w / w aqueous solution of the mixed regent obtained by the method of the present invention, the vacuum drying process of the present invention can solve the problems such as denaturation, tarnishing and carbonization during the drying process It was confirmed that the concentrate was dried as it was without causing it.
The prepared red ginseng and honey mixture were dissolved in the same amount of water to prepare red ginseng tea and then tasted to 20 tasting participants. As a result, red ginseng prepared by spray drying and red ginseng The bitterness of the tea was strong, but the red ginseng tea prepared by the red ginseng method of the present invention was evaluated as having no bitter taste regardless of the concentration and maintaining the characteristic flavor of red ginseng.
Therefore, it was confirmed that the red ginseng liquid prepared according to the present invention has a problem that the problem caused by the high temperature treatment is solved and the quality of the product is greatly improved.
While the present invention has been particularly shown and described with reference to exemplary embodiments thereof, it is to be understood that the invention is not limited to the disclosed exemplary embodiments and that various changes and modifications may be made therein without departing from the spirit and scope of the invention. Change is possible. Such variations and modifications are to be considered as falling within the scope of the invention and the appended claims.
Claims (8)
A step;
Concentrating the natural raw material extract to prepare a concentrated natural raw material;
Mixing the red ginseng or ginseng concentrate with the natural raw material concentrate to prepare a mixed concentrate;
Vacuum drying the mixed concentrate to prepare a powder;
Pulverizing the powder;
Shaping or pulverizing the coarse pulverized powder;
/ RTI >
The natural raw material may be one or more of honey, mushroom, herb, and herb medicine,
The vacuum drying is carried out by applying the mixed concentrate to a plate for drying and drying in a dryer at a temperature of at least 800 mbar and a vacuum of 50 ° C or higher for 4 to 48 hours,
Wherein the process loss rate by the step of vacuum drying and producing the powder is 3% or less.
Wherein the red ginseng extract or the ginseng extract is extracted using water, ethanol, or a mixed solvent thereof, or a red ginseng or a ginseng extract.
Wherein the concentrated red ginseng or ginseng concentrate has a solid content of 40 wt% or more.
Wherein the vacuum drying is performed until the water content of the mixed concentrate becomes 10 wt% or less.
Wherein the vacuum drying is performed at a temperature of 85 캜 or less.
Wherein the raw material loss rate in the step of preparing the powder is 3% or less.
Wherein the ginsenoside content loss ratio of the mixed ginseng to the red ginseng or ginseng extract is 10% or less.
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| KR20210115747A (en) * | 2020-03-16 | 2021-09-27 | 주식회사 한국인삼공사 | Hydrated Herb Seed Composite Containing Gingsenoside And Food Composition Comprising Thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JP2003040791A (en) * | 2002-07-05 | 2003-02-13 | Itbs:Kk | Dried powder of extract from fruit of panax ginseng |
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| JP2003040791A (en) * | 2002-07-05 | 2003-02-13 | Itbs:Kk | Dried powder of extract from fruit of panax ginseng |
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| KR20210115747A (en) * | 2020-03-16 | 2021-09-27 | 주식회사 한국인삼공사 | Hydrated Herb Seed Composite Containing Gingsenoside And Food Composition Comprising Thereof |
| KR102403393B1 (en) * | 2020-03-16 | 2022-05-30 | 주식회사 한국인삼공사 | Hydrated Herb Seed Composite Containing Ginsenoside And Food Composition Comprising Thereof |
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