KR101610834B1 - Apparatus for Generating Hypochlorous Acid - Google Patents
Apparatus for Generating Hypochlorous Acid Download PDFInfo
- Publication number
- KR101610834B1 KR101610834B1 KR1020150086094A KR20150086094A KR101610834B1 KR 101610834 B1 KR101610834 B1 KR 101610834B1 KR 1020150086094 A KR1020150086094 A KR 1020150086094A KR 20150086094 A KR20150086094 A KR 20150086094A KR 101610834 B1 KR101610834 B1 KR 101610834B1
- Authority
- KR
- South Korea
- Prior art keywords
- main body
- raw water
- reaction liquid
- stirring
- hypochlorous acid
- Prior art date
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Classifications
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/46—Treatment of water, waste water, or sewage by electrochemical methods
- C02F1/461—Treatment of water, waste water, or sewage by electrochemical methods by electrolysis
- C02F1/467—Treatment of water, waste water, or sewage by electrochemical methods by electrolysis by electrochemical disinfection; by electrooxydation or by electroreduction
- C02F1/4672—Treatment of water, waste water, or sewage by electrochemical methods by electrolysis by electrochemical disinfection; by electrooxydation or by electroreduction by electrooxydation
- C02F1/4674—Treatment of water, waste water, or sewage by electrochemical methods by electrolysis by electrochemical disinfection; by electrooxydation or by electroreduction by electrooxydation with halogen or compound of halogens, e.g. chlorine, bromine
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- B01F13/00—
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
- C25B1/24—Halogens or compounds thereof
- C25B1/26—Chlorine; Compounds thereof
- C25B1/265—Chlorates
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B9/00—Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
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- B01F2215/0052—
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2201/00—Apparatus for treatment of water, waste water or sewage
- C02F2201/46—Apparatus for electrochemical processes
- C02F2201/461—Electrolysis apparatus
- C02F2201/46105—Details relating to the electrolytic devices
- C02F2201/4612—Controlling or monitoring
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2209/00—Controlling or monitoring parameters in water treatment
- C02F2209/06—Controlling or monitoring parameters in water treatment pH
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2209/00—Controlling or monitoring parameters in water treatment
- C02F2209/40—Liquid flow rate
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Metallurgy (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Water Treatment By Electricity Or Magnetism (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Abstract
Description
The present invention relates to a hypochlorous acid water producing apparatus, and more particularly, to a hypochlorous acid water producing apparatus which improves stirring efficiency by directly mixing a reaction liquid of an electrolyzer with raw water and cooling an electrolytic cell to improve electrolysis reaction efficiency .
In general, hypochlorous acid water has wide and strong sterilization power of colorless, tasteless, and odorless, and its use is gradually increasing as safe and environmentally friendly sterilization and disinfection water.
The hypochlorous acid water is approved as food sterilization or general disinfection disinfectant in Korea KFDA, European EPA, USA PDA, Japan Ministry of Health, FDA-FSIS, USDA through test results of sterilization of food poisoning bacteria, harmful microorganisms, viruses and fungi by more than 99.9% And has been authorized.
The hypochlorous acid part is prepared by electrolyzing diluted hydrochloric acid with an electrolytic bath and diluting it with water.
However, in the apparatus for producing hypochlorous acid water, the electrode is fixed in the electrolytic cell and the reaction area can not be controlled in the electrolytic cell.
Therefore, there is a limitation in current control only when the HOCl flow rate is changed, so that it is virtually impossible to cope with various changes in the HOCl flow rate, and the reaction control is not possible depending on the raw water pH and hardness.
In addition, in the conventional hypochlorous acid water producing apparatus, a stirrer for diluting a reaction solution electrolyzed by an electrolytic bath and an electrolytic bath with water is separately provided, requiring a large space for installation, and the problem of heat generation during electrolysis in the electrolytic bath can not be solved, There is a problem in that the reactivity is lowered due to the heat generated at the time of the reaction and the reaction efficiency is low.
An object of the present invention is to provide a device for producing hypochlorous acid which improves stirring efficiency by directly mixing a reaction liquid of an electrolytic bath with raw water and cooling the electrolytic bath to improve electrolysis reaction efficiency.
Another object of the present invention is to provide a hypochlorous acid water producing device capable of controlling the reaction area by moving an electrode in an electrolytic bath.
According to an aspect of the present invention, there is provided an apparatus for producing hypochlorous acid according to an embodiment of the present invention, wherein at least a portion of the outer wall is formed of an electrode member, a reaction chamber into which a hydrochloric acid solution flows, An electrolytic bath main body having a hydrochloric acid inlet for introducing a hydrochloric acid solution and a reaction liquid outlet port for discharging the reacted reacted solution to the outside on the outer peripheral surface of the upper side; A plurality of raw water inlets into which the electrolytic bath main body is inserted and the stirring chamber formed therein encloses the outer periphery of the electrolytic bath main body including the reaction liquid discharge port and the raw water flows into the upper side, A stirring tank body for stirring and discharging the reaction liquid and the raw water, It characterized in that it comprises a body and a plurality of screw members for stirring, which is installed between stands of the electrolytic cell main body.
In the present invention, the stirring tank body is provided with a plurality of raw water inflow ports for introducing raw water into an internal stirring chamber, and the plurality of raw water inflow ports are opposed to the reaction liquid outlet port of the electrolytic bath at the upper part of the stirring tank main body And the stirring screw member can be disposed between the reaction liquid outlet and the raw water inlet.
In the present invention, the electrolytic bath main body may be formed with a cooling jacket portion in which a part is formed of the electrode member and the remaining portion is a cooling jacket in which cooling water is stored.
In the present invention, the outer wall of the agitating bath main body may have a cooling jacket portion in which cooling water is stored.
The apparatus for producing hypochlorous acid water according to an embodiment of the present invention may further include a cooling water circulating device for circulating cooling water through the cooling jacket section.
In the present invention, the positive electrode assembly is movably coupled to the upper portion of the electrolytic cell body, and the hypochlorous acid solution production device according to an embodiment of the present invention may further include an electrode movement device for moving the positive electrode assembly.
The apparatus for producing hypochlorous acid water according to an embodiment of the present invention includes a first PH sensor installed at a raw water inflow line portion for introducing raw water into the stirring tank main body and sensing PH of raw water, A second PH sensor installed in the raw water inlet line for measuring the flow rate of the raw water, a second PH sensor for sensing the pH of the reaction solution reacted in the electrolytic bath main body, and a second PH sensor for detecting the electrode moving device, the first PH sensor, the flow meter, And a control unit for controlling the amounts of electric currents of the electrode mobile device and the DC power supply unit according to the concentration of hypochlorous acid connected to the cathode electrode and a DC power supply unit for supplying power to the anode electrode body.
In the present invention, the electrode moving device includes: an operating screw portion having a gear portion formed on an outer circumferential surface of the electrode member and being screwed with the positive electrode member; a power transmission gear portion rotating with the operating screw portion; And an electric motor for rotating the power transmitting gear portion.
In the present invention, the control unit may further include a raw water supply control valve provided in the raw water supply line unit, a hydrochloric acid supply pump and a hydrochloric acid supply control valve installed in the hydrochloric acid supply line unit for supplying the hydrochloric acid solution into the electrolytic bath, And may be connected to a discharge control valve installed in a main discharge line portion for discharging the stirred raw water.
INDUSTRIAL APPLICABILITY The present invention has the effect of improving the cooling effect of an electrolytic cell, improving the reactivity in electrolysis, and improving the mixing efficiency of the reaction liquid of the electrolytic cell and the raw water, thereby efficiently producing hypochlorous acid.
The present invention provides a method for producing hypochlorous acid by rapidly mixing the reaction liquid of an electrolytic bath with raw water to shorten the time for producing hypochlorous acid, thereby greatly improving the satisfaction of use, and particularly, when hypochlorous acid is used in a large amount, hypochlorous acid There is an effect that can be done.
The present invention has the effect of broadening the range of HOCl flow rate correspondence and broadly controlling the effective chlorine concentration, thereby providing convenient and accurate hypochlorous acid having a suitable effective chlorine concentration according to various use conditions.
1 is a perspective view illustrating a hypochlorous acid water producing apparatus to which an electrolytic cell for producing hypochlorous acid water according to an embodiment of the present invention is applied;
2 is a longitudinal sectional view showing an electrolytic bath for producing hypochlorous acid according to an embodiment of the present invention
3 is an enlarged sectional view showing an electrolytic bath for producing hypochlorous acid according to an embodiment of the present invention
4 is a plan view showing an electrolytic bath for producing hypochlorous acid according to an embodiment of the present invention.
BRIEF DESCRIPTION OF THE DRAWINGS The invention will be described in detail with reference to the accompanying drawings. Hereinafter, a repeated description, a known function that may obscure the gist of the present invention, and a detailed description of the configuration will be omitted. Embodiments of the present invention are provided to more fully describe the present invention to those skilled in the art. Accordingly, the shapes and sizes of the elements in the drawings and the like can be exaggerated for clarity.
1, the apparatus for producing hypochlorous acid water according to an embodiment of the present invention includes a
The
The electrolytic bath
The raw water
The
The hydrochloric acid
FIG. 2 is a longitudinal sectional view illustrating an electrolyzer for hypochlorous acid water according to an embodiment of the present invention, and FIG. 3 is an enlarged sectional view illustrating an electrolyzer for hypochlorous acid water according to an embodiment of the present invention.
2 and 3, the electrolytic bath
A plurality of reaction
A
The
In the electrolytic bath
[Reaction Scheme 1]
2HCl + H 2 O → HCl + HClO + H 2
In the electrolytic bath
The electrolytic bath
The
The upper surface of the electrolytic bath
On the top surface of the electrolytic bath
The electrode moving device (110) includes an operating screw part (111) screwed to the positive electrode body (100) and having a gear part on the outer peripheral surface thereof;
A power transmitting
And an
The upper portion of the
The
The electrolytic bath
A plurality of reaction
The electrolytic bath
The
The cooling
The cooling
The cooling
The cooling
In addition, the water temperature of the hypochlorous acid water formed by stirring the raw water and the reaction liquid in the stirring tank
The raw water
In the electrolytic bath
The
The
The
The
The stirring tank
The
In addition, an outlet for discharging hypochlorous acid water mixed with the raw water and the reaction liquid may be formed at the center of the lower surface of the stirring tank
It is preferable that a plurality of stirring
The stirring
4, the reaction
Further, the stirring
The reaction
The raw water
Also, the reactive liquid discharged from the raw water and the
In addition, a discharge port is provided at the center of the lower surface of the stirring tank
The present invention has the effect of broadening the range of HOCl flow rate correspondence and broadly controlling the effective chlorine concentration, thereby providing convenient and accurate hypochlorous acid having a suitable effective chlorine concentration according to various use conditions.
INDUSTRIAL APPLICABILITY The present invention has the effect of improving the cooling effect of an electrolytic cell, improving the reactivity in electrolysis, and improving the mixing efficiency of the reaction liquid of the electrolytic cell and the raw water, thereby efficiently producing hypochlorous acid.
The present invention has the effect of shortening the time for producing hypochlorous acid, thereby greatly improving the satisfaction of use, and particularly, when hypochlorous acid is used in a large amount, hypochlorous acid having the effective chlorine can be quickly and accurately prepared and provided.
While the present invention has been particularly shown and described with reference to exemplary embodiments thereof, it is evident that many alternatives, modifications, and variations will be apparent to those skilled in the art in light of the above teachings. will be.
10: main body casing 20: hydrochloric acid tank
21: hydrochloric acid supply line unit 30: electrolytic bath main body
30a: reaction chamber 31: negative electrode body
32: reaction liquid outlet port 40: stirring tank body
40a: stirring chamber 41: raw water inlet
50: raw water
50b: branch supply pipe 51: raw water control valve
60: Flow meter 70: Main discharge line section
71: discharge control valve 80: hydrochloric acid supply pump
90: hydrochloric acid supply control valve 100: positive electrode body
101: moving threaded portion 110: electrode moving device
111: operating thread portion 112: power transmission gear portion
113: Electric motor 120: Cooling jacket part
130: Cooling water circulation device 131: Cooling water inflow pipe
132: cooling water discharge pipe 133: cooling water tank
134: Cooling water circulation control valve 135: Cooling water circulation pump
136: heat exchanger 140: screw member for stirring
150: first PH sensor 160: second PH sensor
170: controller 180: DC power supply
Claims (9)
A positive electrode assembly disposed movably in a part of the reaction chamber of the electrolytic bath body;
Wherein the electrolytic bath main body is inserted into an internal stirring chamber, and the reaction liquid and raw water reacted in the electrolytic bath main body are introduced into the stirring bath main body to stir and discharge the reaction liquid and the raw water in the stirring chamber. And
And a plurality of agitating screw members installed in a state of being set up and fixed between the stirring tank main body and the electrolytic bath main body in the stirring chamber,
A plurality of reaction liquid outlets through which the reaction liquid electrolyzed in the reaction chamber is discharged are formed on the outer circumferential surface of the electrolytic bath body,
The electrolytic bath main body is disposed on the upper side of the stirring bath main body so as to be inserted into the stirring bath main body and the outer peripheral surface including the reaction liquid outlet port is surrounded by the stirring chamber in the stirring bath main body,
A plurality of raw water inflow ports for introducing raw water into an internal stirring chamber are provided on an upper side of the stirring tank main body,
A main discharge line portion for discharging the stirred hypochlorous acid water is connected to the lower surface of the stirring tank main body,
Wherein the reaction liquid outlet is arranged on the upper side of the electrolytic bath main body so as to correspond to the raw water inlet,
And a reaction liquid discharge port which is disposed opposite to the raw water inlet and the reaction liquid discharge port so as to face each other,
Wherein the stirring screw member is disposed between the reaction liquid outlet and the raw water inlet so as to guide the reactive liquid discharged from the reaction liquid outlet and the raw water introduced from the raw water inlet to flow spirally,
Wherein the electrolytic bath main body is formed with a cooling jacket portion in which a part is formed of the electrode member and the remaining portion is a cooling jacket in which cooling water is stored,
Wherein the outer wall of the stirring tank body is formed with a cooling jacket portion for storing cooling water therein.
Priority Applications (1)
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KR1020150086094A KR101610834B1 (en) | 2015-06-17 | 2015-06-17 | Apparatus for Generating Hypochlorous Acid |
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KR1020150086094A KR101610834B1 (en) | 2015-06-17 | 2015-06-17 | Apparatus for Generating Hypochlorous Acid |
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KR101610834B1 true KR101610834B1 (en) | 2016-04-08 |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20190040351A (en) * | 2016-09-02 | 2019-04-17 | 비투비 코스메틱스 | Mixer systems and dispensing bottles to produce cosmetics |
KR102544953B1 (en) * | 2022-10-31 | 2023-06-16 | 윤용성 | the apparatus and method for generating hypochlorous acid |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100794106B1 (en) * | 2007-02-01 | 2008-01-10 | 남궁정 | Electrolyzor for generating hypochlorous acid, apparatus and method for generating hypochlorous acid by use the same |
KR100970708B1 (en) * | 2009-09-01 | 2010-07-16 | 한국코스믹라운드(주) | Method and apparatus for producing slight acidic hypochlorous acid water |
KR101391193B1 (en) * | 2012-07-25 | 2014-05-02 | 동인메디텍 주식회사 | Apparatus for manufacturing of weak-acidic hypochlorous acid water |
-
2015
- 2015-06-17 KR KR1020150086094A patent/KR101610834B1/en active IP Right Grant
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100794106B1 (en) * | 2007-02-01 | 2008-01-10 | 남궁정 | Electrolyzor for generating hypochlorous acid, apparatus and method for generating hypochlorous acid by use the same |
KR100970708B1 (en) * | 2009-09-01 | 2010-07-16 | 한국코스믹라운드(주) | Method and apparatus for producing slight acidic hypochlorous acid water |
KR101391193B1 (en) * | 2012-07-25 | 2014-05-02 | 동인메디텍 주식회사 | Apparatus for manufacturing of weak-acidic hypochlorous acid water |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20190040351A (en) * | 2016-09-02 | 2019-04-17 | 비투비 코스메틱스 | Mixer systems and dispensing bottles to produce cosmetics |
US11433363B2 (en) | 2016-09-02 | 2022-09-06 | B2B Cosmetics | Mixer system for producing a cosmetic product and dispensing bottle |
KR102511895B1 (en) * | 2016-09-02 | 2023-03-20 | 비투비 코스메틱스 | Mixer systems and dispensing bottles for producing cosmetics |
KR102544953B1 (en) * | 2022-10-31 | 2023-06-16 | 윤용성 | the apparatus and method for generating hypochlorous acid |
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