KR101308146B1 - Liquid extract from thuja orientalis l. and teas, pills produced therefrom - Google Patents

Abstract

PURPOSE: A production method of oriental arbor vitae berry concentrate is provided to extract medicine components of oriental arbor vitae berries in short time without using a separate extractor or solvent. CONSTITUTION: 100 parts by weight of water, 50-150 parts by weight of oriental arbor vitae berries, and 1-10 parts by weight of Glycyrrhizae radix are mixed, and the mixture is stirred at 80-100°C for 9-35 hours to obtain an extract. The extract is filtered to remove the oriental arbor vitae berries and the Glycyrrhizae radix. The filtrate is mixed with honey, and the mixture is heated and concentrated at 80-100°C for 2 hours. The concentrate is cooled to 70-80°C. The concentration of the concentrate is 10-300 g/L. The viscosity of the concentrate is 2,000-100,000 cp.

Description

(Liquid extract from Thuja orientalis L. and teas, pills produced therefrom)

The present invention relates to a method for producing a fenugreek concentrate having a Fenugreek fruit extract as a main component, and a method for producing a fenugreek concentrate using the fenugreek extract.

Recently, due to the occurrence of various diseases caused by western diet and stress due to rapidly changing environment, interest in health is increasing day by day. Among them, there are increasing numbers of people who want to maintain health by using health food supplemented with fruits or herbs in nature, which is not a side effect of changing people's constitution, especially in nature. In other words, after illness, I do not take medicines by prescription, but I try to keep good health condition by taking good health supplements. Through these trends and effects, health supplements made up of herbs and herbal medicines continue to emerge. However, most of the herbal medicines or medicines are processed in the form of an extract, which is carried or stored in a pack such as a pouch, which is inconvenient for taking, and has a problem of avoiding taking because the taste is not familiar.

On the other hand, Thuja orientalis Linne is an evergreen arboreous tree of Phytoplankton, Phyllostachys, Phyllotaxis, and Phyllostachys. It has hemostatic activity, genomic and anti-viral activity, anti-inflammatory effect, , Hemorrhage and so on, and it was also used to treat insomnia. In addition, while analyzing the ingredients in modern times, the Tunja Orientalis Folium contains thujene, fenchone, caryophyllene, cedrol, aromadendrin, quercetrin, etc. And it has been known that there are hemostatic effect, Jinhae genotyping action, antithrombotic action, antitumor action, brain cell protective action and antibacterial action (Korean Pharm. Korean Society for Herbal Medicine) 2002 pp376, ~ 512). Tunja Orientalis Semen, a seed of the periwinkle tree, contains cedrol, cuparenol, biotol, pinusolide, etc., and sedative, , Depilatory healing action, learning ability improving action, and blood lipid lowering action.

In order to utilize the efficacy of such a tree, the leaves were usually taken as a powdered form, or a fermented liquid was prepared, or the hard shell was removed by drying the fruit and the seed was extracted and dried. Or Korean Patent Laid-Open Publication No. 10-2008-0085358, for example, by reflux cooling using a solvent such as ethanol. However, it takes a lot of time to manufacture the puffing or drying method, and the reflux cooling method must precede the pulverization step. In addition to water, a solvent such as ethanol is required and a separate extractor such as a reflux condenser is required. In addition, when the fermentation broth is produced, it is difficult to immerse the fermentation broth at a time and it is difficult to store it.

Thus, there is a need to develop a food product that effectively extracts the active ingredients inherent to the cabbage, without requiring a separate grinding process or apparatus and taking less time.

Korean Patent Publication No. 10-2008-0085358 (September 24, 2008)

The Korean Pharmacopoeia 9th revision pp1463, The Korean Society of Medicinal Chemistry

It is an object of the present invention to provide a method for producing a semi-concentrate which can effectively extract herbal ingredients of a transitional fruit in a relatively short time without requiring a separate extraction device and a solvent . The present invention also provides a method for preparing a concentrated concentrate which easily produces a concentrate even when a large amount of bamboo fruit is used at the same time and does not cause deterioration even when stored for a long period of time. It is also an object of the present invention to provide a high-pitched high-pitched bread using a pantry concentrate which can easily ingest the pantry concentrate.

The present invention relates to a method for producing a whitish fruit extract, and to a high-order side and side whitening using the same.

According to an aspect of the present invention,

 a) preparing an extract liquid which is prepared by adding bamboo fruit and licorice to water, stirring and heating the mixture;

b) filtering the extract to remove opium fruit and licorice;

c) a concentrate preparation step of adding honey to the filtrate of step b), heating and concentrating the concentrate; And

d) cooling the concentrate;

Wherein the step a) is carried out by adding 50 to 150 parts by weight of a captive fruit and 1 to 10 parts by weight of licorice to 100 parts by weight of water and stirring at 80 to 100 캜 for 9 to 35 hours And more specifically, to a method for preparing a semi-concentrate which comprises adding 10 to 50 parts by weight of water in the middle of stirring and heating, and repeating the addition three to five times. At this time, the concentration of the extract may be 10 to 300 g / L.

In step c), 5 to 20 parts by weight of honey is added to 100 parts by weight of the filtrate. The honey is heated and concentrated at 80 to 100 ° C for 2 hours, cooled to 70 to 80 ° C and concentrated for 8 to 10 hours. The heating and concentration may be repeated 3 to 5 times. The viscosity of the concentrate prior to filtration may be between 2,000 and 100,000 cp.

Another aspect of the present invention relates to a method for preparing a ginseng root, comprising the steps of: a) preparing a mixture of ginseng, ginger, jujube, jujube, ginseng, ginseng, jujube, ginseng, ginseng, And one or more herbs selected from the group consisting of the herbal composition and the herbal composition.

Another aspect of the present invention relates to a method for producing a half-dried concentrate, wherein the step c) further comprises adding one or a mixture selected from spices, fruit extract, plant extract, gelling agent and antioxidant.

Another aspect of the present invention relates to a faceted high-order, or semi-faced, circle using a faceted concentrate prepared by the method.

The present invention can effectively extract the herbal medicine ingredient of the sominal fruit in a relatively short time without requiring a separate extraction device and a solvent. Also, the concentrated liquid can be easily prepared even when a large amount of the whiteness fruit is used at the same time, and even if it is stored for a long time, no deterioration occurs.

Hereinafter, a method for preparing a leish extract and a leukocyte higher side and a leukocyte using the same will be described in more detail.

In the present invention,

a) preparing an extract liquid which is prepared by adding bamboo fruit and licorice to water, stirring and heating the mixture;

b) filtering the extract to remove opium fruit and licorice;

c) a concentrate preparation step of adding honey to the filtrate of step b), heating and concentrating the concentrate; And

d) cooling the concentrate;

. ≪ / RTI >

First, in step a), the whitish fruit and licorice are added to water, stirred and heated.

The above-mentioned bamboo fruit can be used without restrictions such as those cultivated or marketed, and dried fruits may be used, but it is preferable to use fruits within 7 days of collection.

Licorice ( Glycyrrhiza uralensis Fischer ) is called perennial herb, licorice, mandarin, and kelp, and uses the perennial herb licorice root belonging to legume. Licorice binds and detoxifies with toxic substances in the liver and is effective for drug poisoning, hepatitis, urticaria, dermatitis and eczema. In addition, Jinhae also has a genetic function, antihistamine, anti-catecholin action. It has been shown to be effective in relieving pain caused by sudden tensions in muscles and tissues, increasing body weight, increasing leukocyte counts, diuretic action, and anti-inflammatory effects. In particular, components such as liquiritin and liquiritigenin inhibit the development of peptic ulcers have. Licorice is also used as an antidote for all addicts, and is widely used as a medicinal herb for both new and alternative medicines, as well as herbal medicine such as Jinhae expectorant, martial artifact, and emollient. In the present invention, licorice root also plays a role of sweetening the flavor of the root extract, but also enhances the drug efficacy of the root extract.

The Licorice root can be used regardless of the type of licorice as long as it is commercially available, and it is preferable to cut the Licorice root to a suitable size for easy extraction.

The water may be water commonly used in the art, and it is preferable to use purified water.

Preferably, 50 to 150 parts by weight of the backbone fruit and 1 to 10 parts by weight of licorice are added to 100 parts by weight of water. If less than 50 parts by weight of bamboo fruit is added, the added amount is too small to sufficiently manifest the efficacy of the bamboo fruit, and there is a fear of deterioration in long-term storage due to increased amount of water added. When it is added in an amount exceeding 150 parts by weight, stirring and extraction are difficult. When the amount of the licorice is less than 1 part by weight, the added amount thereof is small and the sweetness unique to the licorice is hardly exhibited. When the amount exceeds 10 parts by weight, the sweetness becomes strong,

The extract preparation step may be carried out by heating and stirring at 80 to 100 ° C for 9 to 35 hours. At this time, water may be further added in the middle of the production step to compensate for water loss due to heating. The amount of water to be added is preferably 10 to 50 parts by weight, preferably 3 to 5 times. When the heating time is less than 9 hours, the backbone component does not come out properly, and when heated for more than 35 hours, the backbone is lost in shape and is difficult to be filtered, and the concentration of the backbone component becomes too strong.

The stirring and heating apparatus used in the production step is not particularly limited, and the stirring speed is also preferably adjusted appropriately according to the content and temperature of water. It is preferable to maintain the speed of 10 to 60 rpm at the stirring speed. The concentration of the extract obtained through step a) is preferably 10 to 300 g / L.

Next, in step b), the extract solution having been subjected to the step of preparing the extract is filtered to remove the whitish fruit and licorice. The filtration can be performed by an apparatus or a method commonly used in the art. It is also possible to use a sieve to remove the cabbage fruit and licorice, and to separate the cabbage fruit and licorice through a conventional filtration device.

The filtrate after the filtration step is collected to prepare a concentrated liquid. In the concentrate preparation step, honey is added to the filtrate, followed by heating and concentration.

The honey (Apis cerana Fabricius) is a honey bee that converts the seeds and pollen collected from the flowers of various plants into their foodstuffs and stores them. Two monosaccharides, namely glucose and fructose, carbohydrates, minerals, Refers to a viscous liquid of sweet taste containing vegetable coloring matter, enzymes and pollen. It is effective in asthma, constipation, rubella, ulcer, trauma, sores, and so on. It is effective in antibacterial, molding, topography, detoxification, Dermatitis, anemia, nervous breakdown, hypertension, heart disease and chronic diseases. The honey used in the present invention enhances the efficacy of the extract and acts as a preservative for killing bacteria and germs that may be present in the extract.

The above honey can be used in all kinds of flowers such as acacia honey, sour honey, bramble honey, sour honey, honey honey, honey, cherry honey, It is not limited to the place and method of collection such as Mukyeong, Seokcheong, etc.

It is preferable that 5 to 20 parts by weight of the honey is added to 100 parts by weight of the filtrate. When the amount of the extract is less than 5 parts by weight, the effect of the honey is not sufficiently exhibited. When the amount of the extract exceeds 20 parts by weight, the flavor of the extract is increased.

The filtrate to which honey has been added can be heated and concentrated (hot water) to prepare a concentrate. The concentrate preparation step is firstly heated and concentrated at 80 to 100 ° C for 2 hours (primary bath) and then cooled to 70 to 80 ° C. After cooling, the mixture is concentrated for about 8 to 10 hours while maintaining the cooling temperature (secondary bath). This process may be repeated one to three times to five times. That is, the temperature is maintained at the cooling temperature and the temperature is raised to 80 to 100 ° C. when the concentration process is finished for 8 to 10 hours, and the process is heated and concentrated for 2 hours. When the temperature is lower than the above temperature, the active ingredient of the panicle extract is not properly concentrated. If the temperature is higher than the above temperature, the active ingredient is destroyed.

The concentrated solution after the filtration process preferably has a viscosity of 2,000 to 100,000 cp. When the viscosity is less than 2,000 cp, it is too light to produce a high-order side chain or a messy circle. When the viscosity exceeds 100,000 cp, the viscosity is too high, and the addition of additives to the extract is not uniform.

After the concentrate preparation step is completed, the concentrate is cooled. The cooling may be carried out by a conventional method used in the art, and preferably by using tap water at 5 to 20 DEG C for 12 to 36 hours.

In addition, the fecal concentrate according to the present invention may further comprise at least one selected from the group consisting of pseudomonads, ginseng, ginger, jujube, ginseng, ginger, ginseng, ginseng, ginseng, , Boiling, and the specification may be further added. The medicinal herbs all complement well with the taste and flavor of the cabbage concentrate prepared by mixing them well with honey. In particular, it is preferable to use herbaceous moth, ginseng, ginseng, ginger, cinnamon and the like as the herb, If the added honey is pseudomonas, it can play a role of preventing the diarrhea by watching the cold nature of the pseudomonads.

The herb may be added in the form of herb medicine or in the form of an extract, and the size and shape of the herb may be freely adjusted according to the convenience of the production step and the filtration step. Extract or extract, first, the total weight of the herb is mixed with purified water at a weight ratio of 3 to 10, and the bath and cooling are repeated. After mixing the herb and purified water, the herb is cooked at a temperature of 80 to 100 ° C for 60 to 120 minutes, and then the mixture is mixed (first bath). Thereafter, the mixture is further stirred at the same temperature for 60 to 150 minutes, and then the solids are filtered to leave only the extract. Since it is desirable to minimize the content of solids in the filtration process, the mesh of the filter net is not limited to a specific value. In the process of preparing the herb extract, the extracting rate of the herb is lowered when it is boiled to less than 80 ° C, and when the temperature is higher than 100 ° C, the herb ingredient may be destroyed.

The herbal mixture or herbal extract mixture is preferably added in an amount of 1 to 10 parts by weight based on 100 parts by weight of the water.

In the present invention, any one selected from spices, fruit extract, plant extract, gelling agent and antioxidant or a mixture thereof may be further added as an additive in step c).

As a spice, natural spices such as Thaumatin and Stevia extract (for example, Rebaudioside A and Glycyrrhizin) and synthetic spices such as saccharin and aspartame can be used, But is not limited to.

The fruit extract and the plant extract are not limited to the kinds as long as they are conventionally added in the art, and they can be freely selected and added according to the taste and the use of the product.

As the gelling agent, preferably used are proteins such as gelatin, agar, pectin, collagen and casein, or thickening polysaccharides such as guar gum and arabic gum. , But is not limited thereto.

Examples of the antioxidant include natural antioxidants such as vitamin C, tocopherol and lecithin, butylated hydroxytoluene (BHT), ascorbyl palmitate, ethylenediaminetetraacetic acid acid, EDTA), but the present invention is not limited thereto.

The additive may be used alone or in combination, and the additive may be added alone or in admixture in an amount of 1 to 5 parts by weight based on 100 parts by weight of the concentrate.

The cooled filtrate thus obtained is in the form of a concentrate such as Kyeongokgyo (red ginseng) and can be stored in a bottle or a plastic case or the like. Alternatively, the concentrate may be formed into a high-order form by being poured into water, or a ring may be formed by adding an excipient and then using a conventional ring-forming apparatus. The excipient and the ring-forming apparatus may be those conventionally used in the art.

Hereinafter, the present invention will be described in more detail with reference to the following Examples and Comparative Examples. However, the following examples are only illustrative of the present invention in more detail, but the present invention is not limited thereto.

(Production Example 1)

The prepared water was put into a stirrer, and then 100 parts by weight of cinnabar and 100 parts by weight of water and 5 parts by weight of licorice were added to the extractor. After the addition, the mixture was heated at 100 ° C. for 35 hours, and stirred at a speed of 30 rpm to prepare an extract. When the amount of water was reduced to 60% by volume or less, 40 parts by weight of water was added, and the total amount of addition was 3 times.

After the extract was prepared, it was filtered to filter out the moss, and the filtrate was collected and added to the concentrator. At the same time, 10 parts by weight of chalk was added to 100 parts by weight of the filtrate, and the mixture was heated and concentrated at 90 DEG C for 2 hours to be firstly boiled, cooled again to 70 DEG C and concentrated for 8 hours I passed the tea bath. The primary and secondary baths were repeated three times with the same procedure. After the concentration process was completed, the concentrate was sealed to prevent water from entering, and then immersed in running water for 24 hours and cooled to prepare a semi-concentrate.

(Production Example 2)

In the same manner as in Preparation Example 1 except that 5 parts by weight of a mixture of herbal medicine mixed with herbal medicine, cinnamon, ginseng, passerine, and marshmallow was further added in the step of preparing the extract, a semi-concentrate was prepared.

(Production Example 3)

In the concentration step, 20% by weight of rebaudioside A (Levatine 60%, Yongseong International), 75% by weight of blueberry concentrate (blueberry essence 100, Chunho Food) and 5% by weight of lecithin (Centrophase, Of the filtrate was further added in an amount of 3 parts by weight based on 100 parts by weight of the filtrate.

(Production Example 4)

In the same manner as in Production Example 1 except that licorice and honey were not added in the production step, a shalpa concentrate was prepared.

(Production Example 5)

A semi-concentrate was prepared in the same manner as in Preparation Example 1, except that the extract was heated for 5 hours in the step of preparing the extract.

(Production Example 6)

A shale concentrate was prepared in the same manner as in Preparation Example 1, except that 40 parts by weight of chalk was added in the concentration step.

(Production Example 7)

A semi-concentrate was prepared in the same manner as in Preparation Example 1, except that 30 parts by weight of cinnabar fruit was added to 100 parts by weight of water in the step of preparing the extract.

(Examples 1 to 3 and Comparative Examples 1 to 4)

The shale concentrate prepared in Preparation Examples 1 to 7 was prepared in high order and in a ring. First, 200 ml of water at 70 캜 was prepared for each production example for high-order production, and 10 g of each of the waxy concentrate was added thereto. In addition, for the manufacture of pellets, excipients (STARLAC, Hwawon chemical) were added in proper amounts and mixed to prepare pellets having an average weight of 3 g.

(Test Example 1)

The sensory evaluation was carried out on 30 male and female 20 to 45 year-old male and female female high-order and white-tailed men, prepared by the methods of Examples 1 to 3 and Comparative Examples 1 to 4, and the results are shown in Table 1 below.

[Table 1]

(Very good?, Good:?, Fair:?, Poor: X)

(Test Example 2)

In order to investigate the deterioration of the semi-concentrate prepared in Preparation Examples 1 to 7, 50 g of each of the semi-concentrate was put into a glass container and stored at 25 캜 for 3 months in a sealed space without light. After that, the glass container was taken out and its deterioration was measured and it is shown in Table 2 below.

[Table 2]

As shown in the results of Table 1 above, the high-order side and back side rings according to the present invention improve the flavor, taste and the higher-order flavor and taste produced by adding the herbal mixture to the comparative example, I was able to confirm. In addition, as shown in Table 2, it was confirmed that by controlling the water content in the manufacturing process or by adding honey, it is possible to prevent deterioration such as separation of a high-volume liquid or generation of fungi even after storage for a long time.

Claims (11)

(a) 50 to 150 parts by weight of a prolapse fruit and 1 to 10 parts by weight of licorice are added to 100 parts by weight of water, stirred and heated at 80 to 100 DEG C for 9 to 35 hours, and 10 to 50 parts by weight 3 to 5 times more;
b) filtering the extract to remove opium fruit and licorice;
c) a concentrate preparation step of adding honey to the filtrate of step b), heating and concentrating the concentrate; And
d) cooling the concentrate;
≪ / RTI > delete delete The method according to claim 1,
Wherein the concentration of the extract in step (a) is 10 to 300 g / L. The method according to claim 1,
Wherein the honey is added in an amount of 5 to 20 parts by weight per 100 parts by weight of the filtrate. The method according to claim 1,
Wherein the step c) comprises heating and concentrating at 80 to 100 캜 for 2 hours, cooling to 70 to 80 캜 and concentration for 8 to 10 hours for 3 to 5 times. The method according to claim 1,
Wherein the viscosity of the c) step concentrate is 2,000 to 100,000 cp. The method according to claim 1,
In step (a), any one selected from the group consisting of papaya leaf, papaya leaf, mackerel, passerine, mungum-dong, windbreak, pine bark, white pine, Baekbokryeong, ≪ / RTI > wherein one or more herbs are added. The method according to claim 1,
Wherein the method further comprises adding at least one selected from the group consisting of spices, fruit extracts, plant extracts, gelling agents and antioxidants or a mixture thereof to step c). 9. A method for producing a high-pitched high-paddy tea product using a paddy fruit concentrate prepared by the method of any one of claims 1 to 9. 9. The method of claim 1, wherein the scabbard is produced by the method of any one of claims 4 to 9.