KR101162980B1 - Natural detergent - Google Patents
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- KR101162980B1 KR101162980B1 KR1020100127297A KR20100127297A KR101162980B1 KR 101162980 B1 KR101162980 B1 KR 101162980B1 KR 1020100127297 A KR1020100127297 A KR 1020100127297A KR 20100127297 A KR20100127297 A KR 20100127297A KR 101162980 B1 KR101162980 B1 KR 101162980B1
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/44—Vegetable products
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/02—Inorganic compounds
- C11D7/20—Water-insoluble oxides
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/50—Solvents
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Abstract
본 발명은 천연세제 및 그 제조방법에 관한 것으로, a) 세제성분을 포함하는 천연소재를 물에 침지시키는 단계와, b) 상기 a) 단계의 결과물에 입경이 100nm 이하의 백금 입자를 5 내지 10ppm의 농도로 첨가하는 단계와, c) 상기 b) 단계의 결과물에 피톤치드오일, 용제 및 유화제를 첨가하는 단계와, d) 분쇄 및 분산기에 상기 c) 단계의 결과물과 입경이 3mm인 지르코니아볼을 함께 투입하고, 분쇄하여 상기 천연소재를 100nm 이하의 입경으로 분쇄 및 분산시키는 단계를 포함한다. 본 발명 천연세제 및 그 제조방법은, 무화과, 사과 등의 천연소재를 물에 침지시킨 후, 촉매와 수용성 오일 등의 첨가물을 첨가하여 100nm 이하의 입경으로 분쇄함으로써, 그 천연소재 전체에 포함된 세제성분을 사용하여 천연세제를 제조하여, 대량생산이 가능한 효과가 있다.The present invention relates to a natural detergent and a method for manufacturing the same, comprising: a) immersing a natural material including a detergent component in water, and b) 5 to 10 ppm of platinum particles having a particle size of 100 nm or less in the product of step a). C) adding phytoncide oil, a solvent and an emulsifier to the resultant of step b), and d) a zirconia ball having a particle size of 3 mm and a particle diameter of 3mm in a pulverizer and a disperser. Injecting, pulverizing and pulverizing and dispersing the natural material to a particle size of 100nm or less. The natural detergent of the present invention and the method for producing the same are detergents contained in the whole natural material by immersing natural materials such as figs and apples in water, and then adding an additive such as a catalyst and a water-soluble oil and grinding them to a particle size of 100 nm or less. By using natural ingredients to produce natural detergents, mass production is possible.
Description
본 발명은 천연세제 및 그 제조방법에 관한 것으로, 보다 상세하게는 대량생산이 용이하고, 세정력을 향상시킬 수 있는 천연세제 및 그 제조방법에 관한 것이다.
The present invention relates to a natural detergent and a method for manufacturing the same, and more particularly, to a natural detergent and a method for producing the same, which can be easily mass-produced and improve cleaning power.
일반적으로, 무화과, 사과 등의 과일 또는 기타의 식물로부터 세제성분을 추출하는 방법으로서 일반에 알려진 방법은 알코올에 침지시켜, 세제성분으로 사용할 수 있는 산을 추출하는 방법이 사용되고 있다.In general, a method known in the art as a method for extracting a detergent component from fruits, such as figs, apples, or other plants, is immersed in alcohol, and a method of extracting an acid that can be used as a detergent component is used.
그러나 과일이나 기타 식물에서 추출할 수 있는 세제성분은 극히 적으며 따라서 세제성분을 추출하기 위하여 대량의 재료를 사용해야 하기 때문에 세제의 가격이 증가하게 된다.However, the amount of detergent that can be extracted from fruits and other plants is extremely small, and thus the price of the detergent increases because a large amount of material is used to extract the detergent.
또한 알코올에 침지시켜 추출하는 방법은 시간이 많이 소요되기 때문에 생산성이 매우 낮아 대량생산에는 적합하지 않은 문제점이 있었다.
In addition, the method of extracting by dipping in alcohol takes a lot of time, so the productivity is very low, there was a problem that is not suitable for mass production.
위와 같은 이유로 종래 천연세제는 천연재료를 알코올에 침지시켜 얻어진 세제성분의 함유량이 낮을 수 밖에 없으며, 세정력이 합성세제에 비하여 저하되어 친환경적이라는 장점에 비하여 소비자들은 가격이 저렴하고 세정력이 우수한 합성세제를 선호하고 있다.
For these reasons, conventional natural detergents have a low content of detergent components obtained by immersing natural materials in alcohol, and the cleaning power is lower than that of synthetic detergents. I prefer.
따라서 현재 천연세제시장에서는 천연세제를 보다 저가격으로 대량생산할 수 있는 방법이 요구되고 있다.
Therefore, in the current natural detergent market, a method for mass production of natural detergent at a lower price is required.
상기와 같은 문제점을 감안한 본 발명이 해결하고자 하는 기술적 과제는, 천연세제를 제조하기 위한 천연재료 전체를 사용하여 저가격으로 대량생산이 가능하며, 천연재료에 함유된 세제성분 전체를 사용함으로써, 세정력을 보다 향상시킬 수 있는 천연세제 및 그 제조방법을 제공함에 있다.
The technical problem to be solved by the present invention in consideration of the above problems, it is possible to mass-produce at a low price by using the entire natural material for manufacturing a natural detergent, by using the entire detergent component contained in the natural material, cleaning power It is to provide a natural detergent and a method of manufacturing the same that can be improved more.
상기와 같은 과제를 해결하기 위한 본 발명 천연세제는, 물과 혼합된 입경이 100nm 이하인 천연소재입자와, 상기 물에 분산된 피톤치드오일과, 용제에 의하여 상기 천연소재입자에 결합된 입경이 100nm 이하의 백금 입자와, 상기 물에 용해된 유화제를 포함한다.The natural detergent of the present invention for solving the above problems is a natural material particles having a particle size of 100 nm or less mixed with water, phytoncide oil dispersed in the water, and a particle size of 100 nm or less bonded to the natural material particles by a solvent Platinum particles and an emulsifier dissolved in the water.
또한 본 발명 천연세제 제조방법은, a) 세제성분을 포함하는 천연소재를 물에 침지시키는 단계와, b) 상기 a) 단계의 결과물에 입경이 100nm 이하의 백금 입자를 5 내지 10ppm의 농도로 첨가하는 단계와, c) 상기 b) 단계의 결과물에 피톤치드오일, 용제 및 유화제를 첨가하는 단계와, d) 분쇄 및 분산기에 상기 c) 단계의 결과물과 입경이 3mm인 지르코니아볼을 함께 투입하고, 분쇄하여 상기 천연소재를 100nm 이하의 입경으로 분쇄 및 분산시키는 단계를 포함한다.
In addition, the natural detergent manufacturing method of the present invention, a) immersing a natural material containing a detergent component in water, and b) adding a platinum particle having a particle size of 100nm or less to the product of step a) at a concentration of 5 to 10ppm And c) adding phytoncide oil, a solvent and an emulsifier to the resultant of step b), and d) adding the zirconia ball having a particle size of 3 mm and the particle size of the step c) together to a grinding and dispersing machine. By pulverizing and dispersing the natural material to a particle size of 100nm or less.
본 발명 천연세제 및 그 제조방법은, 무화과, 사과 등의 천연소재를 물에 침지시킨 후, 촉매와 수용성 오일 등의 첨가물을 첨가하여 100nm 이하의 입경으로 분쇄함으로써, 그 천연소재 전체에 포함된 세제성분을 사용하여 천연세제를 제조하여, 대량생산이 가능한 효과가 있다.The natural detergent of the present invention and the method for producing the same are detergents contained in the whole natural material by immersing natural materials such as figs and apples in water, and then adding an additive such as a catalyst and a water-soluble oil and grinding them to a particle size of 100 nm or less. By using natural ingredients to produce natural detergents, mass production is possible.
또한 세제성분의 효과 발현을 촉진하는 촉매를 이용하여 세정력을 향상시킬 수 있는 효과가 있다.
In addition, there is an effect that can improve the cleaning power by using a catalyst that promotes the effect of the detergent component.
도 1은 본 발명의 바람직한 실시예에 따른 천연세제 제조공정의 순서도이다.1 is a flow chart of a natural detergent manufacturing process according to a preferred embodiment of the present invention.
이하, 본 발명 천연세제 및 그 제조방법의 실시예를 첨부한 도면을 참조하여 상세히 설명한다.
Hereinafter, with reference to the accompanying drawings, an embodiment of the present invention natural detergent and its manufacturing method will be described in detail.
도 1은 본 발명의 바람직한 실시예에 따른 천연세제 제조공정 순서도이다.1 is a flow chart of a natural detergent manufacturing process according to a preferred embodiment of the present invention.
도 1을 참조하면 본 발명의 바람직한 실시예에 따른 천연세제 제조방법은, 무화과, 사과 등의 천연재료를 물에 침지시키는 단계(S11)와, 상기 물에 침지된 천연재료에 100nm 입경 이하의 백금을 미량 첨가하는 단계(S12)와, 상기 S12단계의 결과물에 피톤치드오일과 글리세린을 첨가하는 단계(S13)와, 상기 S13단계의 결과물에 유화제를 첨가하는 단계(S14)와, 상기 S14단계의 결과물을 지르코니아 볼을 사용하는 분쇄 및 분산기에 투입하여 상기 천연재료를 100nm 이하의 입경으로 분쇄하는 단계(S15)를 포함한다.
Referring to Figure 1 is a natural detergent manufacturing method according to a preferred embodiment of the present invention, the step of immersing a natural material, such as figs, apples in water (S11), and the platinum material of less than 100nm particle diameter in the natural material immersed in water Adding a trace amount (S12), adding phytoncide oil and glycerin to the resultant product of step S12 (S13), adding an emulsifier to the resultant product of step S13 (S14), and the resultant product of step S14. Injecting the zirconia ball into a pulverizing and dispersing step comprising the step of pulverizing the natural material to a particle size of 100nm or less (S15).
이하, 상기와 같이 구성되는 본 발명의 바람직한 실시예에 따른 천연세제 및 그 제조방법을 보다 상세히 설명한다.
Hereinafter, a natural detergent and a manufacturing method according to a preferred embodiment of the present invention configured as described above will be described in more detail.
먼저, S11단계에서는 무화과나 사과 등의 천연재료를 물에 침지시킨다. 상기 물의 양은 천연재료 10 내지 50wt%에 50 내지 90wt%로 혼합한다.First, in step S11, natural materials such as figs and apples are immersed in water. The amount of water is mixed in 50 to 90wt% with 10 to 50wt% of natural materials.
이때 물에 침지된 천연재료는 종래 알코올에 침지된 상태와는 다르게 세제성분이 추출되지 않으며, 첨가된 물의 역할은 이후에 분쇄 및 분산이 이루어지며, 제조된 천연세제를 희석하는 역할을 한다.At this time, the natural material immersed in water does not extract detergent components differently from the state immersed in alcohol, the role of the added water is subsequently pulverized and dispersed, and serves to dilute the manufactured natural detergent.
따라서 천연재료를 물에 침지한 상태에서 즉시 이후의 공정을 진행할 수 있으며, 따라서 종래와는 다르게 제조공정시간이 매우 짧아 대량생산에 적합하다.
Therefore, it is possible to proceed to the subsequent process immediately in the state of immersing the natural material in water, and therefore unlike the conventional manufacturing process time is very short, it is suitable for mass production.
그 다음, S12단계에서는 상기 S11단계의 결과물에 미량의 백금 입자를 혼합한다.Then, in step S12 is mixed with a small amount of platinum particles to the product of step S11.
상기 백금입자는 100nm 이하의 입경을 가지는 것이 바람직하며, 하한은 10nm 이상임이 바람직하나, 그 입경이 작을 수록 표면적이 증가하여 촉매로서의 효과가 향상되기 때문에 입경이 작을 수록 바람직하다.The platinum particles preferably have a particle size of 100 nm or less, and the lower limit is preferably 10 nm or more, but the smaller the particle size, the smaller the particle size is, because the surface area is increased and the effect as a catalyst is improved.
상기 백금 입자의 첨가량은 그 농도가 5 내지 10ppm이 되도록 첨가한다.
The amount of the platinum particles added is added so that the concentration is 5 to 10 ppm.
상기 백금 나노 입자는 천연재료의 세제성분의 세정력의 발현을 촉진시키는 촉매의 역할을 하며, 염산에 용해시켜 이온화한 후 가열 환원시켜 그 입경이 100nm 이하가 되도록 형성한다.
The platinum nanoparticles serve as a catalyst for promoting the expression of the cleaning power of the detergent component of the natural material, dissolved in hydrochloric acid and ionized, and then reduced by heating to form a particle size of 100 nm or less.
그 다음, S13단계에서는 상기 S12단계의 결과물에 피톤치드오일과 글리세린을 첨가한다.Next, in step S13, phytoncide oil and glycerin are added to the resultant of step S12.
상기 피톤치드오일은 항균성과 보습성을 가지는 것으로, 수용성이기 때문에 혼합이 용이하다. 또한 피톤치드오일 또한 인체에 이로운 천연성분이다.
The phytoncide oil has antimicrobial properties and moisturizing properties, and is easily mixed because it is water-soluble. Phytoncide oil is also a natural ingredient that is beneficial to the human body.
또한 용제로서 글리세린을 첨가한다. 이때 글리세린은 상기 피톤치드오일과 동일량을 첨가하며, 상기 피톤치드오일과 글리세린의 혼합량이 상기 물과 천연재료의 혼합중량 96 내지 98wt%에 대하여 2 내지 4wt%의 중량으로 첨가한다.In addition, glycerin is added as a solvent. In this case, glycerin is added in the same amount as the phytoncide oil, and the mixed amount of the phytoncide oil and glycerin is added in a weight of 2 to 4 wt% based on the mixed weight of 96 to 98 wt% of the water and the natural material.
상기 글리세린은 용제로 끈기가 있는 액체이며, 이는 이후 천연소재의 분쇄물에 상기 첨가된 백금 나노 입자가 점착되어 촉매로서의 작용 효과를 높일 수 있다.
The glycerin is a liquid having a tenacity as a solvent, which is then adhered to the added platinum nanoparticles to the pulverized product of natural materials to enhance the effect as a catalyst.
그 다음, S14단계에서는 상기 S13단계의 결과물에 유화제를 첨가한다.Next, in step S14, an emulsifier is added to the resultant of step S13.
상기 유화제로는 산탄검을 사용할 수 있으며, 상기 혼합된 피톤치드오일 98wt%에 2wt%를 혼합한다.
Xanthan gum may be used as the emulsifier, and 2wt% is mixed with 98wt% of the mixed phytoncide oil.
그 다음, S15단계에서는 S14단계의 결과물을 분쇄 및 분산기에 투입하고, 분쇄 및 분산시켜 상기 천연소재를 100nm 이하의 입경으로 분쇄한다.Then, in step S15, the resultant of step S14 is put into a pulverizer and a disperser, pulverized and dispersed to pulverize the natural material to a particle size of 100nm or less.
이때 천연소재 역시 그 입경이 작으면 작을 수록 표면적이 증가하여 세정효과를 높일 수 있으며, 천연소재는 섬유질을 포함하기 때문에 3mm 입경의 지르코니아볼을 분쇄 및 분산기에 함께 투입하여 분쇄가 보다 용이하게 한다.
In this case, the smaller the particle size of the natural material is, the more the surface area is increased to increase the cleaning effect. Since the natural material includes fiber, zirconia balls having a 3 mm particle diameter are added together in the pulverizer and the disperser to make the pulverization easier.
이와 같이 100nm 이하로 천연소재 전체를 분쇄하여 천연세제를 제조하며, 따라서 천연소재의 전체 및 천연소재에 함유된 세제성분을 모두 사용할 수 있게 되어, 세정효과를 높일 수 있다. 또한 백금 나노 입자를 촉매로 사용하여 세정효과를 더욱 높일 수 있다.
In this way, the entire natural material is pulverized to 100 nm or less to prepare a natural detergent. Therefore, all of the natural ingredients and the detergent ingredients contained in the natural material can be used, thereby increasing the cleaning effect. In addition, the cleaning effect can be further enhanced by using platinum nanoparticles as a catalyst.
본 발명은 상기 실시예에 한정되지 않고 본 발명의 기술적 요지를 벗어나지 아니하는 범위 내에서 다양하게 수정?변형되어 실시될 수 있음은 본 발명이 속하는 기술분야에서 통상의 지식을 가진 자에 있어서 자명한 것이다.
It will be apparent to those skilled in the art that the present invention is not limited to the above embodiments and can be practiced in various ways without departing from the technical scope of the present invention. will be.
Claims (7)
b) 상기 a) 단계의 결과물에 입경이 100nm 이하의 백금 입자를 5 내지 10ppm의 농도로 첨가하는 단계;
c) 상기 b) 단계의 결과물에 피톤치드오일, 용제 및 유화제를 첨가하는 단계; 및
d) 분쇄 및 분산기에 상기 c) 단계의 결과물과 입경이 3mm인 지르코니아볼을 함께 투입하고, 분쇄하여 상기 천연소재를 100nm 이하의 입경으로 분쇄 및 분산시키는 단계를 포함하는 천연세제 제조방법.
a) immersing a natural material including a detergent component in water;
b) adding platinum particles having a particle size of 100 nm or less to a resultant of step a) at a concentration of 5 to 10 ppm;
c) adding phytoncide oil, a solvent and an emulsifier to the resultant of step b); And
d) pulverizing and dispersing the product of step c) and the zirconia ball having a particle size of 3mm together, and pulverized, the natural detergent manufacturing method comprising the step of pulverizing and dispersing the natural material to a particle diameter of 100nm or less.
상기 a) 단계는 무화과 또는 사과 10 내지 50wt%에, 물 50 내지 90wt%를 혼합하는 것을 특징으로 하는 천연세제 제조방법.
The method of claim 1,
The step a) is a natural detergent manufacturing method, characterized in that 50 to 90wt% of water, figs or apples 10 to 50wt%.
상기 c) 단계는 상기 피톤치드오일과 용제는 각각 1 내지 2wt%의 중량으로 상기 b) 단계의 결과물 96 내지 98wt%의 중량에 첨가되며,
상기 유화제는, 상기 피톤치드오일 98wt%에 2wt%의 중량비로 첨가되는 것을 특징으로 하는 천연세제 제조방법.
The method of claim 1,
In step c), the phytoncide oil and the solvent are added in a weight of 1 to 2wt%, respectively, to the weight of 96-98wt% of the resultant of step b).
The emulsifier is a natural detergent manufacturing method, characterized in that the weight ratio of 2wt% to 98wt% of the phytoncide oil.
상기 물에 분산된 피톤치드오일;
용제에 의하여 상기 천연소재입자에 결합된 입경이 100nm 이하의 백금 입자;
상기 물에 용해된 유화제를 포함하는 천연세제.
Natural material particles having a particle diameter of 100 nm or less mixed with water;
Phytoncide oil dispersed in the water;
Platinum particles having a particle size of 100 nm or less bonded to the natural material particles by a solvent;
Natural detergent comprising an emulsifier dissolved in the water.
상기 천연소재입자는,
무화과 또는 사과인 것을 특징으로 하는 천연세제.
The method of claim 4, wherein
The natural material particles,
Natural detergents, characterized in that they are figs or apples.
상기 천연소재입자와 물의 혼합비는 천연소재입자 10 내지 50wt%에 물 50 내지 90wt%가 혼합된 것을 특징으로 하는 천연세제.
The method of claim 4, wherein
The mixing ratio of the natural material particles and water is a natural detergent, characterized in that 50 to 90wt% of water mixed with 10 to 50wt% of the natural material particles.
상기 피톤치드와 용제는 동일 중량비로 혼합되며, 상기 천연소재입자와 물의 혼합중량 96 내지 98wt%에 각각 1 내지 2wt%의 중량비로 혼합되는 것을 특징으로 하는 천연세제.
The method of claim 4, wherein
The phytoncide and the solvent are mixed in the same weight ratio, the natural detergent, characterized in that the mixed weight of the natural material particles and water 96 to 98wt% mixed in a weight ratio of 1 to 2wt%.
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