KR101074176B1 - Method for making extract of Dulcis - Google Patents

Abstract

The present invention relates to a method for preparing a sterile bark extract. More specifically, by extracting the seeds after removing them from the pulp, more efficient and more effective extracts can be obtained, and by performing natural drying for a certain period of time, it removes the toxic contained in the live tree and does not burden the organs of the elderly. , By preparing a reverse phase extraction tea and heating it in a separate extraction tank to completely remove the toxicity of the fruit as well as to a method for producing a sterile hut extract which can obtain a polymer of a gel state which is a crystal of the active ingredient.
To this end, the present invention comprises the steps of (a) removing the seeds of the barn fruit and preparing the slices and leaves of the branches; (b) removing the water after washing the fruit pulp and the branch slices and leaves; (c) sterilizing the fruit pulp and branch slices and leaves from which moisture has been removed by heating with steam; (d) cutting the fruit pulp and branch slices and leaves through the crusher to a certain length through the crusher; (e) inserting the cut fruit pulp and eggplant slices and leaves into an extractor and adding purified water to provide a method for producing sterile barn extract.

Description

Method for making sterile bark extract {Method for making extract of Dulcis}

The present invention relates to a method for preparing a sterile bark extract. More specifically, by extracting the seeds after removing them from the pulp, more efficient and more effective extracts can be obtained, and by performing natural drying for a certain period of time, it removes the toxic contained in the live tree and does not burden the organs of the elderly. , By preparing a reverse phase extraction tea and heating it in a separate extraction tank to completely remove the toxicity of the fruit as well as to a method for producing a sterile hut extract which can obtain a polymer of a gel state which is a crystal of the active ingredient.

Korean huts are known as Hovenia dulcis var. Koreana or Hovenia dulcis var. Koreana Nakai. The barn tree belongs to the sea buckthorn family, grows in the sub-central part of Korea, and is a leaf-like tree. Barn trees generally bloom in early summer from June to July, bearing fruit from October and ripening around November.

The fruit shape looks like a chicken's toes, and the nature is cold, sweet and astringent. The barn tree is shaped like a coral and is sometimes called a coral reef, Hyunpori, Baekseok, or earth.

Recently, the research on the effectiveness of the bark tree is active, and it is good for liver, colon, stomach, and kidney, and it is particularly effective for detoxification after drinking alcohol on 'herbaceous cortex' and 'dangerous herb'. This is because the fruit, leaves, and branches of the larvae contain beneficial ingredients such as glucose, malic acid, calcium, furanguranine, hobenoside, and habenic acid. In addition, the barn tree is effective in relieving liver diseases and thirst such as alcoholic hepatitis, fatty liver, cirrhosis, etc., the active substance of the barn tree shows the effects on hangover removal and bad breath removal and constipation.

Indeed, the fruit of the walnut tree or a healthy medicine is mixed with liquor and the liquor can be seen with the naked eye.

Briefly, the hangover removal mechanism of the bark tree is as follows.

In the body, alcohol is decomposed into acetaldehyde by alcohol dehydrogenase produced by the liver, and acetaldehyde paralyzes the central nerve and causes hangover. 'Hangover' and 'odor' are the unpleasant feelings after drinking alcohol. Odor refers to headaches and vomiting that appear after 4-5 hours after drinking, and hangover refers to discomfort that continues after sleeping. In general, it is reasonable to think that a hangover is a systemic deprivation condition in which electrolyte imbalance and dehydration due to alcohol-induced diuresis, hypoglycemia due to liver function decrease, and gastritis symptoms are combined rather than nausea caused by nerve stimulation of acetaldehyde. .

In order to relieve hangovers, alcohol must be decomposed directly or promoted through absorption in the body. Currently, products for hangover relief are commercially available, and many herbal extracts have been commercialized as drinks. However, the existing products contain a large amount of masking compound for the removal of bad breath rather than relieve hangover, there is a problem that it is not clear whether the hangover effect actually focused on the palatability of the drink.

On the other hand, the bark tree is toxic, children, pregnant women, the elderly, when taking the raw wood extract has a problem in that the burden on the organs, including the stomach and in severe cases cause side effects. In addition, there is a report that toxic substances are concentrated in the fruit of the bark, and research on a method of removing the toxic substances and extracting only active ingredients has not been made yet. Moreover, the fungus and fruit can grow in a variety of bacteria, including mold in the process of harvesting, storage, distribution, especially in the summer and high temperature and humidity increase the amount of bacteria. These molds and bacteria have a problem that is not completely removed only by heating in the extraction process.

The present invention has been devised to solve the above problems, in particular, to obtain an extract more efficient and high content of active ingredients, eliminating the toxicity contained in the live tree does not burden the organs, such as the elderly, fruit of It is an object of the present invention to provide a method for preparing a sterile bark extract which can not only completely remove the toxicity but also obtain a polymer material which is a crystal of the active ingredient.

Method for producing a sterile hut extract according to the present invention devised to achieve the above object comprises the steps of (a) removing the seed of hut fruit and preparing a slice and leaves of the branch; (b) removing the water after washing the fruit pulp and the branch slices and leaves; (c) sterilizing the fruit pulp and branch slices and leaves from which moisture has been removed by heating with steam; (d) cutting the fruit pulp and branch slices and leaves through the crusher to a certain length through the crusher; (e) putting the cut fruit pulp and eggplant slices and leaves into an extractor and adding purified water to extract the extract.

In addition, the step (c) is preferably heated for 5 to 10 minutes with a steam of 140 ~ 180 degrees.

In addition, the manufacturing method may further comprise the step of drying the fruit pulp and eggplant slices and leaves through the step (c) between the steps (c) and (d) using hot air.

Moreover, it is preferable that the temperature of the said hot air is 40-70 degreeC.

In addition, in the step (d), it is preferable to cut the fruit flesh and the branch slices and the leaves to a length of 0.5 ~ 10mm.

In addition, the step (e) is preferably extracted by heating for 60 to 90 minutes at 90 ~ 100 ° C.

In addition, the manufacturing method may further comprise the step of slowly drying the fruit pulp and eggplant slices and leaves from which water is removed between steps (b) and (c) for 30 days or more.

In addition, the step (e) may be carried out at a temperature below the boiling point in the pressure tank to produce a reverse phase extraction difference.

In addition, the manufacturing method may further include the step of preparing a concentrated substance in a gel state by heating the reverse phase extraction difference of step (e) in a separate extraction tank and heating.

According to the present invention, less effective ingredients, not easy to extract active ingredients, take a long time to dry, and remove the seeds that are not easy to handle during the extraction process from the fruit pulp to perform the extraction process, more efficient and more effective extract content There is an effect that can be obtained.

In addition, according to the present invention is carried out by the natural drying to remove the toxicity contained in the live tree has the effect of not burdening the organs, such as the elderly.

In addition, according to the present invention, if the fruit pulp occupies a large portion of the extraction object, by preparing a reverse phase extraction tea and heating it in a separate extraction tank, it is not only completely removes the toxicity of the fruit, but also a polymer of a gel state that is a crystal of the active ingredient. There is an effect that can be obtained.

1 is a flow chart of a method for producing sterile hut extract according to a preferred embodiment of the present invention.

Hereinafter, exemplary embodiments of the present invention will be described in detail with reference to the accompanying drawings. First, in adding reference numerals to the components of each drawing, it should be noted that the same reference numerals are assigned to the same components as much as possible, even if shown on different drawings. In the following description of the present invention, a detailed description of known functions and configurations incorporated herein will be omitted when it may make the subject matter of the present invention rather unclear. In addition, the following will describe a preferred embodiment of the present invention, but the technical idea of the present invention is not limited thereto and may be variously modified and modified by those skilled in the art.

1 is a flow chart of a method for producing sterile hut extract according to a preferred embodiment of the present invention.

Sterile bark tree extract manufacturing method according to a preferred embodiment of the present invention, referring to Figure 1, washing step (S10), natural drying step (S20), steaming step (S30), hot air drying step (S40), shredding step (S50), extraction step (S60), and GEL concentration step (S70) is made. Here, the natural drying step (S20), steaming step (S30), GEL concentration step (S70) is a process for removing the toxicity of fruit pulp and branches and leaves of the bark tree and to remove mold and bacteria, in some cases Note that it can be omitted.

Before performing the washing step (S10), first remove the seeds of the fruit of the barn tree to prepare the fruit pulp, and prepare the sections and leaves of the branches. The active ingredient of the barberry fruit is contained in the flesh most than the seed, the seed is not easy to extract the active ingredient, takes a long time to dry, and is not easy to handle during the extract manufacturing process. Therefore, by removing the seeds from the fruit, it is preferable to use only fruit pulp for extract preparation.

The washing step (S10) is a step of removing the water remaining on the surface after washing the prepared fruit pulp and eggplant slices and leaves. The washing step (S10) is to remove the dirt and foreign matter on the surface of the fruit pulp and eggplant slices and leaves and to activate the surface of them to increase the extraction efficiency.

The natural drying step (S20) is a step of slowly drying the fruit pulp and branch slices and leaves from which water is removed through the washing step (S10). At this time, the natural drying step (S20) is preferably performed at least 30 days in a well-ventilated place.

Since the bark tree (fresh branch) and the fruit of the fruit contains toxicity, it is preferable to dry them before use to remove the toxicity. At this time, if the drying is made rapidly, the toxicity is not sufficiently removed, if too dry, the extraction of the effective substance is not easy.

In particular, in the summer and rainy season, mold may grow in the natural drying process, so it is necessary to be careful, and it is preferable to proceed with drying by artificially lowering the humidity while avoiding the rainy season as much as possible.

The steaming step (S30) is a step of sterilizing by heating the fruit pulp and eggplant slices and leaves from which moisture is removed through steam. Fruit pulp, eggplant slices, and leaf surfaces are capable of breeding bacteria through harvesting, storage, transport, and drying, so that bacteria and fungi are removed by steaming.

At this time, the temperature of the steam is preferably about 140 ~ 180 degrees, and the heating time is preferably about 5 ~ 10 minutes. If the temperature of the steam is less than 140 degrees Celsius, the sterilization effect is insignificant, and if it exceeds 180 degrees Celsius, the surface of fruit flesh and leaves may be denatured or the active ingredients may be denatured. If the heating time is less than 5 minutes, the sterilization is not made sufficiently, and if it exceeds 10 minutes, the fruit pulp and leaves are excessively receded, so that the process is difficult to proceed smoothly.

Hot air drying step (S40) is a step of drying the fruit pulp and eggplant slices and leaves sterilized through the heating using hot air. Since steam is absorbed on the surface of the fruit pulp and the branch slices and the leaves during the heating, the hot air drying step (S40) is performed to completely dry the moisture remaining on the surface.

At this time, it is preferable that the temperature of hot air is about 40-70 degreeC. If the temperature of the hot air is less than 40 degrees Celsius takes a long time to dry and difficult to dry completely, if the temperature exceeds 70 degrees is a problem that the fruit pulp and leaves are mushy.

Shredding step (S50) is a step of cutting the fruit pulp and branch slices and leaves of the hot air drying to a certain length using a shredder. If the fruit pulp and the like has an irregular specification, not only does it occupy a large volume, but the concentration of the extract becomes uneven. By cutting fruit pulp, etc. to a certain length, it is possible to increase the surface area to improve the extraction efficiency and to reduce the volume of the fruit pulp. In addition, even if the manufacturing process repeatedly performed it is possible to maintain a uniform extract concentration every time.

At this time, the cut length of the fruit pulp and branch slices and leaves is preferably about 0.5 ~ 10mm. If the cutting length is less than 0.5mm it takes a long time for cutting and becomes almost powdery, so handling is not easy, and there is a problem that a large amount of fruit pulp and the like remain in the crusher. If the cutting length exceeds 10mm, the specific surface area becomes small, resulting in low extraction efficiency.

Extraction step (S60) is a step of extracting the cut fruit pulp and eggplant slices and leaves into the extractor and adding purified water. In the extraction step (S60) it is also possible to manufacture a reverse phase extraction difference by heating to a temperature below the boiling point using an extractor equipped with a pressurized tank.

In the extraction process, the heating temperature and heating time have a significant effect on the quality of the extract.

In the extraction process, the heating temperature is preferably about 90 to 100 degrees Celsius, and the heating time is preferably about 60 to 90 minutes. If the heating temperature is less than 90 degrees Celsius, extraction takes a long time and the concentration of the extract is lowered. When the heating temperature exceeds 100 degrees Celsius, a large amount of bubbles are generated during the extraction process and the amount of vaporization is high, so that the yield is lowered. If the heating time is less than 60 minutes, the extraction is not sufficient, the quality of the extract is lowered, if it exceeds 90 minutes, the extract is excessively concentrated, the amount of the extract is less, there is a side of energy waste required for heating.

GEL concentration step (S70) is a step of preparing a concentrated substance in the gel state by heating the reverse phase extraction difference into the separation extraction tank when the reverse phase extraction difference is manufactured using a pressure tank extractor in the extraction step (S60). If you want to use sterile hut extract as a liquid, it is noted that the GEL concentration step (S70) may not be performed.

In particular, the GEL concentration step (S70) is a method that can be useful when the specific gravity of the fruit pulp among the components of the bark tree to be extracted. Recent studies have reported that toxic concentrations are concentrated in the fruit part of the barn tree. Therefore, if the fruit pulp occupies the majority in the extraction object, after preparing the reverse phase extraction tea in the extraction step (S70), the toxic component contained in the fruit is completely removed by heating in a separate extraction tank.

In the GEL concentration step (S70), not only completely remove the toxicity of the fruit, but also obtain a sticky gel concentrate. Through this process, the highly concentrated gel-like material is removed from the low molecular weight material without the active ingredient, leaving only the polymer material, which is a crystal of the active ingredient.

The above description is merely illustrative of the technical idea of the present invention, and various modifications, changes, and substitutions may be made by those skilled in the art without departing from the essential characteristics of the present invention. will be. Accordingly, the embodiments disclosed in the present invention and the accompanying drawings are not intended to limit the technical spirit of the present invention but to describe the present invention, and the scope of the technical idea of the present invention is not limited by the embodiments and the accompanying drawings. . The protection scope of the present invention should be interpreted by the following claims, and all technical ideas within the equivalent scope should be interpreted as being included in the scope of the present invention.

The present invention can be widely applied in the field of preparation of extracts, in particular, sterile bark extracts, which are helpful for liver detoxification and liver function improvement.

S10-washing step S20-natural drying step
S30-Steaming Stage S40-Hot Air Drying Stage
S50-shredding step S60-extraction step
S70-GEL concentration stage

Claims (9)

(a) removing the seeds of the barberry and preparing the slices and leaves of the branches;
(b) removing the water after washing the fruit pulp and the branch slices and leaves;
(c) sterilizing the fruit pulp and branch slices and leaves from which moisture has been removed by heating with steam;
(d) cutting the fruit pulp and branch slices and leaves through the crusher to a certain length through the crusher;
(e) putting the cut fruit pulp and eggplant slices and leaves into an extractor and adding purified water to extract
Sterile biloba extract manufacturing method comprising a. The method of claim 1,
The step (c) is a method for producing sterile barn extract, characterized in that the heating for 5 to 10 minutes with a steam of 140 ~ 180 degrees. The method according to claim 1 or 2,
The method of claim 1, further comprising the step of drying the fruit pulp and eggplant slices and leaves passed through the step (c) using hot air between the steps (c) and (d). The method of claim 3,
The temperature of the hot air is a sterilized hawthorn extract manufacturing method, characterized in that 40 to 70 degrees. The method of claim 1,
The step (d) is a method of producing a sterile hut tree extract, characterized in that the fruit flesh and branch slices and leaves are cut to a length of 0.5 ~ 10mm. The method of claim 1,
The step (e) is a method for producing sterile barn extract, characterized in that the extraction by heating for 60 to 90 minutes at 90 ~ 100 degrees. The method of claim 1,
The method of claim 1, further comprising the step of slowly drying the fruit pulp and eggplant slices and leaves from which the water is removed between the steps (b) and (c) for more than 30 days. The method of claim 1,
The step (e) is carried out at a temperature below the boiling point in the pressurized tank to produce a sterilized bilberry extract, characterized in that for producing a reverse phase extraction tea. The method of claim 8,
A method of producing a sterile hut extract, characterized in that it further comprises the step of preparing a concentrated substance in a gel state by heating the reverse phase extraction difference of step (e) in a separate extraction tank.

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