KR100981678B1 - Dyes comprising scoria and persimmon juice - Google Patents
Dyes comprising scoria and persimmon juice Download PDFInfo
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- KR100981678B1 KR100981678B1 KR1020080055033A KR20080055033A KR100981678B1 KR 100981678 B1 KR100981678 B1 KR 100981678B1 KR 1020080055033 A KR1020080055033 A KR 1020080055033A KR 20080055033 A KR20080055033 A KR 20080055033A KR 100981678 B1 KR100981678 B1 KR 100981678B1
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0001—Post-treatment of organic pigments or dyes
- C09B67/0003—Drying, e.g. sprax drying; Sublimation of the solvent
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
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Abstract
본 발명은 직물용 염료에 관한 것으로, 감즙 100중량부에 대하여 송이석분말 3~7중량부를 포함하는 것을 특징으로 하며, 상기 염료를 이용하여 직물을 염색할 때에는 염료에 직물을 담가 고르게 흡수시킨 후, 직물을 건져서 펴고 일광이나 자외선을 조사한 다음, 다시 물에 담갔다가 건져 일광이나 자외선을 조사하되, 마지막 단계인 물에 담갔다가 건조하는 단계는 5~10회를 반복하는 방법을 이용한다. The present invention relates to a dye for fabric, characterized in that it comprises 3 to 7 parts by weight of pine stone powder with respect to 100 parts by weight of the juice, when dyeing the fabric by using the dye after absorbing the fabric evenly in the dye , Stretch the fabric and irradiate with sunlight or UV rays, and then immerse it again in water, and then irradiate with sunlight or UV rays. The final step is to dip it in water and dry it 5-10 times.
본 발명에 따른 염료를 이용하여 염색한 직물은 항균력, 탈취력을 지니고, 자외선과 전자파를 차단하는 특징이 있으며, 원적외선을 방사하므로 보온력이 뛰어나고, 천의 마모가 적으므로 경제적인 특징이 있다. 또한, 본 발명에 따른 염료는 안전한 천연성분인 송이석과 감즙을 이용하므로 예민한 피부에도 부작용을 발생시키지 않으며, 송이석과 감즙을 동시에 사용하여 염착성이 우수하므로 세탁 후에도 염색상태가 안정적으로 유지될 뿐 아니라 송이석 특유의 기능성이 장기간 지속되는 특징이 있다. Fabrics dyed using the dye according to the present invention has antibacterial and deodorizing properties, and is characterized by blocking ultraviolet rays and electromagnetic waves, and has excellent thermal insulation power because it emits far-infrared rays, and has less economical wear. In addition, the dye according to the present invention does not cause side effects even on sensitive skin because it uses the safe natural ingredients of pine oyster and succulents, and because it is excellent dyeing by using pine oyster and succulent at the same time, the dyeing state is not only kept stable even after washing The unique functionality of the stone is long-lasting.
염료, 염색, 송이석, 감즙. Dye, Dye, Songseok, Juicy.
Description
본 발명은 직물을 염색하는 염료에 관한 것으로, 구체적으로는 송이석분말과 감즙을 포함하는 염료 및 이를 이용한 염색방법에 관한 것이다.The present invention relates to a dye for dyeing fabrics, and more particularly, to a dye containing pine stalk powder and juice and a dyeing method using the same.
송이석은 화산활동으로 생성된 암석으로, 주성분은 SiO2로 이루어지며, TiO2를 2~8% 함유하여 중금속 흡착 능력이 우수한 특징이 있다. 또한, 송이석은 원적외선을 방사하며, 항균효과 및 탈취효과를 지니는 것으로 알려져 있다. 이러한 다양한 기능으로 인하여 송이석은 다양한 용도의 제품에 적용되어 왔으며, 그 예로써 건축용 내외장재, 화장품 등을 들 수 있다. Song-seok is a rock produced by volcanic activity. Its main component is SiO 2, and it contains 2-8% of TiO 2 . In addition, Song-seok is known to emit far infrared rays, have an antibacterial and deodorant effect. Due to such various functions, Song-seok has been applied to products of various uses, for example, interior and exterior materials for building, cosmetics, and the like.
그 외에도 송이석은 직물의 염색용으로도 사용되며, 송이석을 이용한 염색은 통상적으로 미세한 분말의 송이석을 물에 혼합한 후, 직물을 담그는 방법이 이용되었다. 그러나, 이러한 방법으로는 송이석입자가 직물에 견고하게 염착되지 못하므로, 세탁시 물빠짐이 심한 문제가 있었다. 이러한 문제점을 개선하기 위한 방법으로서, 대한민국 등록특허 제548019호 화산석 천연염료 및 제조방법에서는 알긴산 분해 미생물과 다시마를 화산석과 함께 혼합하여 반응시킴으로써 염착성을 높이는 방법을 제공한 바 있다. 그러나, 이러한 방법은 발효에 적절한 온도, 산소량, pH와 같은 여러가지 조건을 충족시켜야 할 뿐 아니라, 5~10일이라는 장기간의 반응시간이 필요하고 반응이 끝난 후에는 별도의 살균처리과정까지 거쳐야 하므로, 염료의 제조공정이 전반적으로 복잡하고 까다로운 단점이 있었다.In addition, Songseok is also used for dyeing of fabrics, and dyeing using Songseok is typically used to mix fine powder of Songseok with water and then immerse the fabric. However, in this method, since the pine granules are not firmly dyed to the fabric, there was a serious problem of water drainage during washing. As a method for improving such a problem, the Republic of Korea Patent No. 548019 Volcanic Stone natural dyes and manufacturing methods have provided a method of improving the dyeing by mixing the alginate decomposition microorganisms and kelp mixed with the volcanic stone. However, this method not only has to satisfy various conditions such as temperature, oxygen amount and pH suitable for fermentation, but also requires a long reaction time of 5 to 10 days and goes through a separate sterilization process after the reaction. The manufacturing process of the dye has been complicated and difficult overall.
이에 본 발명에서는 송이석의 기능성을 갖추면서도 제조방법이 용이하고 염착성이 우수한 염료를 제공하고자 한다.Therefore, the present invention is to provide a dye having excellent functionality and easy dyeing method while having the functionality of Songseok.
본 발명에서는 안전한 천연성분으로 이루어져 예민한 피부에도 부작용이 없으며, 염색 후 세탁시에도 염색상태가 안정적으로 유지되는 염료를 제공하고자 한다.In the present invention, it is made of a safe natural ingredient has no side effects even on sensitive skin, and to provide a dye that is stably maintained even when washing after dyeing.
또한, 본 발명에서는 중금속 흡착, 자외선 차단, 원적외선 방사, 항균, 탈취효과를 나타내는 염료 및 이를 이용한 염색방법을 제공하고자 한다.In addition, the present invention is to provide a dye and a dyeing method using the heavy metal adsorption, UV protection, far infrared radiation, antibacterial, deodorizing effect.
본 발명에서는 송이석분말과 감즙을 혼합한 염료를 사용하여 직물을 염색한다.In the present invention, the fabric is dyed using a dye mixed with pine stone powder and juice.
송이석은 화산활동시 용암이 공중으로 분출된 후 공기 중에서 냉각되어 생성되는 암석으로, 용암이 지표에서 냉각되어 생성되는 현무암에 비하여 통상적으로 기공률이 높고 밀도가 낮은 경향이 있다. 본 발명에서는 분말형태의 송이석을 사용하므로 송이석의 일부 또는 전체를 현무암으로 대체하는 것도 가능하며, 다만 송이석은 상대적으로 적갈색을 띠고 현무암은 흑회색을 띠는 경향이 있으므로, 송이석을 현무암으로 대체할 때에는 색상을 고려하여 적절한 비율을 선택한다.Songi-seok is a rock that is formed by cooling lava in the air after volcanic activity is ejected into the air, and generally has a higher porosity and a lower density than the basalt generated by cooling the lava in the surface. In the present invention, it is also possible to replace part or all of the pine feldspar with basalt because of the use of powdered pine feldspar, except that the feldspar is relatively reddish brown and the basalt tends to be black grey. When choosing a color, choose an appropriate ratio.
본 발명에서 염료에 포함되는 송이석분말은 미세한 입자의 형태로서, 채취한 암석을 분쇄한 후 백필터를 갖춘 여과집진설비를 통과시키는 방법으로 제조할 수 있으며, 이때 석재가공 부산물로 발생하는 송이석의 석분을 정제하여 사용할 경우 환경파괴를 줄일 뿐 아니라 비용절감의 효과까지 더할 수 있다. 송이석분말은 입자 크기가 작으면 직물에 보다 견고하게 흡착되고 직물의 질감이 부드러운 장점이 있는 반면, 입자를 작게 제조하기 위해서는 보다 많은 비용이 소요되는 단점이 있으므로, 본 발명에서는 입도가 5~10㎛인 크기의 입자를 사용하는 것이 바람직하다. The pine stone powder included in the dye in the present invention is in the form of fine particles, and may be manufactured by pulverizing the collected rock and passing through a filter dust collector equipped with a bag filter, wherein the pine stone generated as a stone processing by-product Purified stone powder can not only reduce the environmental damage but also reduce the cost. Small particle size of the granule powder is adsorbed more firmly to the fabric and the soft texture of the fabric has the advantage, while to produce a smaller particle has the disadvantage of more cost, in the present invention, the particle size is 5 ~ 10 Preference is given to using particles of a size that are μm.
송이석분말을 이용하여 염색한 직물은 중금속을 흡착하고, 항균 및 탈취효과를 나타내며, 자외선을 차단하고 원적외선을 방사하는 특성이 있다. 그러나, 송이석분말만으로 염색할 경우에는 염착성이 떨어져 세탁시 물빠짐이 매우 심하며, 물빠짐과 동시에 송이석 특유의 기능성도 함께 떨어지므로 중금속 흡착, 항균, 탈취 등의 효과가 오래 지속되지 못하는 문제가 있다. 따라서, 본 발명에서는 송이석분말의 염착성을 높이기 위한 방법으로 감즙과 함께 혼합하여 염색하는 방법을 선택한다.Fabrics dyed using Songseok Stone powder adsorb heavy metals, exhibit antibacterial and deodorizing effects, block ultraviolet rays and emit far infrared rays. However, when dying only with pine stone powder, there is a problem that the water absorption is very severe when washing, and the peculiar functionality of pine stone is also dropped along with water dripping. Therefore, the effects of heavy metal adsorption, antibacterial and deodorization do not last long. have. Therefore, the present invention selects a method of mixing and dyeing with the juice as a method for increasing the dyeability of pine stone powder.
통상적으로 염색에 사용되는 감즙은 탄닌성분이 다량 함유된 풋감을 사용하며, 감즙에 포함된 탄닌 성분이 섬유에 염착된 후, 일광이 조사됨에 따라 점차 고분자화되어 색상이 발현되는 원리로 염색이 이루어진다. 본 발명에서도 마찬가지로 풋감으로부터 감즙을 수득하는데, 일반적으로 감 중량의 약 50중량% 정도를 수득할 수 있다. Normally, the juice used for dyeing uses a green persimmon containing a large amount of tannin, and the tannin component contained in the juice is dyed onto the fiber, and then dyes on the principle that the color is gradually polymerized as sunlight is irradiated. . The present invention likewise obtains the juice from the green persimmon, generally about 50% by weight of the persimmon weight can be obtained.
본 발명에서는 감즙과 송이석분말이 혼합된 염료를 이용하여 염색하므로, 감즙의 탄닌성분과 송이석분말이 혼합되어 섬유에 염착된 다음, 일광의 조사에 따라 탄닌성분이 서로 결합하여 고분자화되는 과정에서 송이석분말이 탄닌의 고분자 속에 갇히게 되는 원리로 염색이 진행된다. 따라서, 송이석만으로 염색 후 감즙으로 염색하거나, 감즙만으로 염색 후 송이석으로 염색하는 방법으로는 송이석분말이 섬유에 고착되기 어려우며, 본 발명에서와 같이 송이석분말과 감즙을 균일하게 혼합한 염료를 이용하여 동시에 염색하여야만 염착상태가 안정적으로 유지될 수 있다.In the present invention, since the dye is mixed with a juice and pine stone powder dyeing, the tannin component of the juice and pine stone powder is mixed and dyed to the fiber, and then the tannin components are combined with each other according to the irradiation of daylight Dyeing proceeds on the principle that stone powder is trapped in the polymer of tannin. Therefore, it is difficult to fix the pine mushroom powder to the fiber by dyeing with pineapple after dyeing only with pine stone, or staining with pine stone after dyeing with only pine mushroom, and uniformly mixing the pine mushroom powder and juice as in the present invention. The dyeing state can be stably maintained only by staining at the same time.
통상적인 송이석분말을 이용한 염색은 염착성이 떨어져 세탁시 물빠짐이 심하고 시간이 경과함에 따라 송이석 특유의 기능성도 점차 떨어지게 되는 반면, 본 발명에 따른 송이석 감즙 염료를 이용하여 염색할 경우에는 송이석분말이 탄닌의 고분자 속에 단단히 고정되므로 반복적인 세탁시에도 염색상태가 안정적으로 유지되고 송이석 특유의 기능성 또한 장기간 유지되는 특징이 있다. 또한, 본 발명에 따른 송이석 감즙 염료는 까다롭고 복잡한 공정을 거칠 필요가 없으므로 염료의 제조과정도 용이한 장점이 있다.Dyeing using conventional pine stone powder is poor in dyeing, the water is difficult to wash off, and as the time passes, the peculiar functionality of Songseok stone gradually decreases, whereas when dyed using the pine mushroom sucrose dye according to the present invention Since the stone powder is firmly fixed in the polymer of tannin, the dyeing state is stably maintained even after repeated washing, and the characteristic of Song-seok is also maintained for a long time. In addition, the pine oyster succulent dye according to the present invention does not need to go through a complicated and complicated process, there is an advantage that the manufacturing process of the dye is also easy.
본 발명에서는 감즙 100중량부에 대하여 송이석분말 3~7중량부를 혼합하여 염료를 제조한다. 본 발명에 있어서 상기 혼합비가 절대적인 것은 아니나, 송이석분말의 혼합량이 너무 적으면 항균력, 탈취력, 자외선차단, 원적외선방사 등의 효과가 떨어지게 되고, 반대로 송이석분말의 혼합량이 너무 많으면 송이석입자가 직물에 견고하게 흡착되지 못하는 문제가 발생할 수 있으므로 상기 범위를 벗어나지 않는 것이 바람직하다.In the present invention, a dye is prepared by mixing 3-7 parts by weight of pine needle powder with respect to 100 parts by weight of juice. In the present invention, the mixing ratio is not absolute, but if the mixing amount of pine stone powder is too small, the effects of antimicrobial activity, deodorizing power, UV protection, far infrared radiation, etc. are reduced, on the contrary, if the mixing amount of pine stone powder is too large, the pine stone particles are fabric It is preferable not to go out of the above range because it may cause a problem that can not be adsorbed firmly.
본 발명에 따른 염료를 이용하여 직물을 염색할 때에는 염료에 직물을 담가 고르게 흡수시킨 후, 직물을 건져서 펴고 일광이나 자외선을 조사한 다음, 다시 물에 담갔다가 건져 일광이나 자외선을 조사하되, 마지막 단계인 물에 담갔다가 건조하는 단계는 5~10회를 반복하는 방법을 이용한다. When dyeing the fabric using the dye according to the present invention, soaking the fabric in the dye evenly absorbed, and then stretched and stretched the fabric and irradiated with sunlight or ultraviolet rays, and then immersed again in water to irradiate the sunlight or ultraviolet rays, the last step Soaking in water and drying is a method of repeating 5 to 10 times.
이때, 염색시 소요되는 염료의 양은 두께를 비롯한 직물의 특성에 따라 달라지나, 본 발명에 따른 염료 20kg을 이용하여 통상적인 의류용 면직물을 염색할 경우 약 50㎡면적의 직물을 염색할 수 있다. 또한, 염료 또는 물에 직물을 담글 때에는 충분히 주무름으로써 직물에 염료 또는 물이 균일하게 흡수되도록 하며, 각 단계에서 일광을 조사할 때에는 직사광선에서 5 내지 7시간 동안 일광을 쪼임으로써 충분히 발색이 이루어지도록 한다. 본 발명에 따른 염료를 이용하여 염색함에 있어서, 상기 제시된 시간이나 횟수가 절대적인 것은 아니나, 상기 범위를 크게 벗어날 경우 염색이 제대로 이루어지지 못할 수 있으므로 상기 범위를 벗어나지 않는 것이 바람직하다.At this time, the amount of dye required for dyeing depends on the characteristics of the fabric, including the thickness, when using a 20kg dye according to the present invention when dyeing a conventional garment cotton fabric can be dyed fabric of about 50㎡ area. In addition, when the fabric is soaked in dye or water, the dye or water is uniformly absorbed by the fabric so that it is uniformly absorbed, and when irradiated with sunlight at each step, the color is sufficiently developed by directing sunlight for 5 to 7 hours in direct sunlight. . In the dyeing using the dye according to the present invention, the time or the number of times presented is not absolute, it is preferable not to go out of the range because the dyeing may not be made properly if greatly out of the range.
본 발명에 따른 염료는 천연성분인 송이석과 감즙으로 이루어져 예민한 피부에도 부작용없이 안전하며 천의 마모가 적어 경제성이 우수하다. 또한, 본 발명에 따른 염료를 이용하여 염색한 직물은 항균력, 탈취력을 지니고, 자외선과 전자파를 차단하는 특징이 있으며, 적외선을 방사하므로 보온력이 뛰어나고, 염착성이 우수하므로 상기 효과들이 장기간 지속되는 특징이 있다.Dye according to the present invention is composed of natural ingredients Song-seok and succulent is safe without side effects even on sensitive skin and less wear of cloth is excellent economical. In addition, the fabric dyed using the dye according to the present invention has the characteristics of antibacterial, deodorizing, blocking ultraviolet rays and electromagnetic waves, and excellent heat retention by radiating infrared rays, excellent dyeing properties, so that the effects are long-lasting have.
본 발명에 따른 염료를 이용하여 염색한 직물은 항균력, 탈취력을 지니고, 자외선과 전자파를 차단하는 특징이 있으며, 원적외선을 방사하므로 보온력이 뛰어나고, 천의 마모가 적으므로 경제적인 특징이 있다. 또한, 본 발명에 따른 염료는 안전한 천연성분인 송이석과 감즙을 이용하므로 예민한 피부에도 부작용을 발생시키지 않으며, 송이석과 감즙을 동시에 사용하여 염착성이 우수하므로 세탁 후에도 염색상태가 안정적으로 유지될 뿐 아니라 송이석 특유의 기능성이 장기간 지속되는 특징이 있다. Fabrics dyed using the dye according to the present invention has antibacterial and deodorizing properties, and is characterized by blocking ultraviolet rays and electromagnetic waves, and has excellent thermal insulation power because it emits far-infrared rays, and has less economical wear. In addition, the dye according to the present invention does not cause side effects even on sensitive skin because it uses the safe natural ingredients of pine oyster and succulents, and because it is excellent dyeing by using pine oyster and succulent at the same time, the dyeing state is not only kept stable even after washing The unique functionality of the stone is long-lasting.
[실시예][Example]
7~8월에 수확한 풋감을 착즙기를 이용하여 압착하여 즙을 내어 준비하고, 송이석을 5~10㎛ 입도로 분쇄한 송이석분말을 준비하였다.The greens harvested in July-August were squeezed using a juicer to prepare juice, and the pine crushed pine crushed granules were prepared in a particle size of 5-10 μm.
상기 준비된 감즙 20kg과 송이석분말 1kg을 혼합하여 염료를 준비하고, 폭 1m의 면직물 50m를 염료에 담근 후, 직물에 염료가 고루 스며들도록 충분히 주무른 다음, 직물을 건져서 편 후 직사광선 아래에서 5 내지 7시간 동안 건조하였다.20 kg of the prepared juice and 1 kg of pine stone powder are mixed to prepare a dye. After dipping 50 m of 1 m of cotton fabric in the dye, the mixture is soaked sufficiently to infiltrate the dye, and then the fabric is dried and straightened and then 5 to 7 under direct sunlight. Dried for hours.
건조를 마친 직물을 물에 담그고 물이 고루 스며들도록 충분히 주무른 후, 직물을 건져서 편 후 직사광선 아래에서 5 내지 7시간 동안 건조하는 과정을 7회 반복하였다.After immersing the dried fabric in water and soaking well with water, the process of drying the fabric for 5 to 7 hours under direct sunlight was repeated seven times.
상기 실시예에 따라 염색한 직물은 반복적인 세탁시에도 염색상태가 안정적으로 유지되어 물빠짐이 적은 것으로 나타났다.The fabric dyed according to the above embodiment was found to be stably maintained even after repeated washing, so that the water was less dripped.
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20040011239A (en) * | 2002-07-29 | 2004-02-05 | 박은원 | Ocher dyeing method |
| KR20050035971A (en) * | 2003-10-14 | 2005-04-20 | 강병욱 | Ability paper and the paper manufacture method that use nature dye |
| KR100548019B1 (en) | 2005-11-30 | 2006-01-31 | (주)세노코 | Manufacturing method of natural dye useing scoria |
| KR20080029709A (en) * | 2006-09-28 | 2008-04-03 | 최명부 | Natural mineral quality powder and natural coloring matter resin anger it will do and the coating which will load the method which it does |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20040011239A (en) * | 2002-07-29 | 2004-02-05 | 박은원 | Ocher dyeing method |
| KR20050035971A (en) * | 2003-10-14 | 2005-04-20 | 강병욱 | Ability paper and the paper manufacture method that use nature dye |
| KR100548019B1 (en) | 2005-11-30 | 2006-01-31 | (주)세노코 | Manufacturing method of natural dye useing scoria |
| KR20080029709A (en) * | 2006-09-28 | 2008-04-03 | 최명부 | Natural mineral quality powder and natural coloring matter resin anger it will do and the coating which will load the method which it does |
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