KR100862646B1 - Composition of hair color and method for preparing thereof - Google Patents

Abstract

The present invention includes an alkaline fermented pomegranate extract in the hair dye to improve the scalp trouble through antibacterial action to harmful scalp bacteria, and also has an excellent astringent effect on the scalp to prevent scalp trouble, protect the scalp and quickly restore damaged hair. In addition, the present invention relates to a hair dye composition and a method of preparing the same, which gives elasticity and nutrition to maintain long-term shine.

The above-mentioned characteristics of this invention are 50.45-55.20 weight% of pomegranate fermentation alkaline agents, 42.54-44.26 weight% of bases, 2.1-5.05 weight% of dyes, 0.08-0.12 weight% of EDTA which is a metal ion blocking agent, and 0.08 to 0.12 weight% of ascorbate sodium as a preservative. It can be achieved by the hair dye composition, characterized in that consisting of ~ 0.12% by weight.

Hair, hair dye, pomegranate

Description

Hair dye composition and preparation method {Composition of hair color and method for preparing}

Figure 1a, 1b is a test report of one embodiment of the present invention

The present invention relates to a hair dye composition and a method for preparing the same, and more specifically, to include a alkaline fermented pomegranate extract in the hair dye to improve scalp troubles through antibacterial action to harmful scalp bacteria, and also has an excellent astringent effect on the scalp. The present invention relates to a hair dye composition and a method for producing the same, which prevents scalp troubles, protects the scalp and recovers damaged hair rapidly, and gives elasticity and nutrition for long-term shine.

Generally, in the case of hair dyes widely used for hair dyeing in homes or beauty salons, the contents of heterogeneous products of different ingredients should be mixed and used. These mixed contents are inevitably mixed immediately before use due to the characteristics of the product. Only then can the effect be fully exerted.

Such hair dyes are typically used by mixing an alkali dye, an alkali dye, and the like with the first agent, and hydrogen peroxide solution with the second agent, and mixing the first agent and the second agent at a predetermined ratio immediately before use. Doing. The alkaline component of the first agent swells the hair so that the dye can be easily diffused and penetrated into the hair, and when mixed with the second agent, it helps to generate oxygen necessary to decompose hydrogen peroxide to oxidize the dye. Let this be done.

However, these hair dyes are susceptible to skin allergies and use strong acidic or alkaline ingredients to dissolve the hair components and damage the hair. In addition, since dyeing is performed by oxidation polymerization inside the hair, the gloss and luster may be lost, and the hair may be severely damaged, resulting in an unnatural color and a deteriorated texture.

On the other hand, dyes that produce color are most important chemicals such as paraphenylamine, diaminotoluene, and diaminoisosol, which cause toxic or allergic reactions on the skin, causing severe irritation to mucous membranes and eyes. May cause hypersensitivity, rashes in the scalp spread from the face to the neck, fever and asthma, and, in severe cases, burns or alopecia.

The present invention has been made in view of the above problems, and its object is to include an alkaline fermented pomegranate extract in the hair dye, thereby improving both pitables through the antibacterial action of harmful scalp bacteria, and also having an excellent astringent effect on the scalp. It is to provide a hair dye composition and a method for preparing the same, which prevents scalp trouble, protects the scalp and recovers damaged hair quickly, and gives elasticity and nutrition for long-term shine.

The characteristics of the present invention for achieving the above object are 50.45 to 55.20 wt% of pomegranate fermentation alkaline agent, 42.54 to 44.26 wt% of base, 2.1 to 5.05 wt% of dye, 0.8 to 1.2 wt%, EDTA 0.08 to metal ion blocking agent. It can be achieved by the hair dye composition characterized by consisting of 0.12% by weight, 0.08 to 0.12% by weight of ascorbate sodium as a preservative.

Another feature of the present invention is the dye 42.54 to 44.26% by weight, the metal ion encapsulant EDTA 0.08 to 0.12% by weight, and the preservative ascorbate sodium 0.08 to 0.12% by weight heated to 80 ℃ in a mixer and mixed with stirring and then dye 2.1 It can be achieved by the method for producing a hair dye composition characterized in that the mixture is cooled to room temperature with stirring to add 5.05% by weight, and then 50.45 to 55.20% by weight of pomegranate fermentation alkaline agent is added to uniformly stir and mix.

Hereinafter, described in detail by the preferred embodiment for achieving the above object is as follows.

The present invention is prepared by mixing the pomegranate fermentation alkaline agent into a mixed solution consisting of a base, a dye, a metal ion sequestrant and a preservative to prepare a hair dye composition.

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The present invention mixes the base 42.54 to 44.26% by weight, 0.08 to 0.12% by weight of EDTA as a metal ion blocking agent, 0.08 to 0.12% by weight of ascorbate sodium as a preservative and 2.1 to 5.05% by weight of a pomegranate fermentation alkaline 50.45 to 55.20 weight The hair dye composition which mixes%, and its manufacturing method are provided.

The hair dye composition according to the present invention includes an alkaline fermented pomegranate extract, thereby improving scalp troubles through antibacterial action against harmful scalp bacteria, and also having an excellent astringent effect on the scalp to prevent scalp troubles, protect scalp and damage hair. Not only does it recover quickly, but it also gives elasticity and nutrition for long lasting shine.

The pomegranate is known to be used as dozens of drugs in Dongbobogam to treat diarrhea and dysentery and have insecticidal and antibacterial and hemostatic effects. The main active ingredient is alkaloids, isopelletierine, and other tannins, punicalin ( punicalin), punicalagins and the like are known.

Referring to the manufacturing process of the pomegranate fermented alkaline agent is as follows.

The quantity of pomegranate is checked and washed with water to remove impurities.Then, the washed and finely divided pomegranate from which impurities are removed, the skin is separated, filtered using water pressure, and the pomegranate extract is separated by centrifuge. Pomegranate extract is stored in the stock tank.

The pomegranate extract of the stock solution tank is heated to 75 ° C. in a vacuum to sterilize to make pomegranate purified juice, and then the purified juice is distilled at 105 ° C. for about 1 minute and rapidly frozen at 20 ° C. to obtain a pomegranate extract.

Pomegranate extract is aged for 30 to 35 days in a cold dark at room temperature to obtain a pomegranate fermentation alkaline agent.

The pomegranate extract is preferably extracted from black pomegranate.

The dye of the present invention is p-Phenylenediamine, N-phenyl-p-Phenylenediamine, N-Phenyl-p-Phenylenediamine, Resorcinol, o-Aminophenol ), 4-amino-2-hydrotoluene (4-Amino-2-Hydroxytoluene), m-phenylenediamine, p-aminophenol, m-aminophenol , 1-naphthol (l-Naphthol), 2-methylresorcinol (2-Methylresorcinol) is used in combination of one or two or more and used in 2.1 to 5.05% by weight of the total composition.

The base of the present invention is sodium ascorbate, sodium myristoyl glutamate, sodium cocoyl isethionate, cocamidopropyl betain, polyquaternium- One or two or more of 10 (Polyquaternium-10), 2-Pyrrolidone-5-Carboxylic Acid and Glycylizate Ammonium (Ammonium Glycyrrhizate) It is used at 42.54-44.26 weight% of a composition.

The metal ion sequestrant of the present invention uses EDTA (Ethylenediaminetetraacetic Acid) and is used at 0.08 to 0.12% by weight of the total composition.

Preservative of the present invention uses methyl paraben (Methyl Paraben) is used in 0.08 to 0.12% by weight of the total composition.

The amount of the hair dye composition according to the present invention may be appropriately adjusted according to the condition of the hair, the age of the user, the length of the hair, and the like, and the application time may also be appropriately adjusted according to the individual.

In addition, the hair dye composition is used in a 1: 1 mixture with an oxidizing agent, which is a second agent, immediately before use, and the oxidizing agent is hydrogen peroxide, erythorbic acid as a metal ion blocking agent, and phosphoric acid as a stabilizer. Disodium Phosphate, pH adjuster, Cetanol, Lanolin, Glyceryl Isostearate, Isopropyl Myristate, Sodium Laureth Sulfate ), Glycyrazide ammonium (Ammonium Glycyrrhizate) and purified water.

Preparation of hair dye composition (first agent)

First, 42.54 to 44.26 wt% of the base, 0.08 to 0.12 wt% of the EDTA, which is a metal ion blocking agent, and 0.08 to 0.12 wt% of the ascorbate sodium, which is a preservative, are heated and stirred at 80 ° C. in a mixer, followed by mixing of 2.1 to 5.05 wt% of the dye. After cooling to room temperature with addition and stirring, 50.45 to 55.20% by weight of pomegranate fermentation alkali was added and uniformly stirred and mixed to prepare a hair dye composition having a composition as shown in Tables 1, 2 and 3.

(Example 1, blackish brown)

division Purpose of Mixing ingredient Content (% by weight) One dyes   p-phenylenediamine     2.50 2 dyes   N-phenyl-p-phenylenediamine     0.90 3 dyes   Resorcinol     0.20 4 dyes   o-aminophenol     0.75 5 dyes   4-amino-2-hydrotoluene     0.28 6 dyes   m-phenylenediamine     0.32 7 Metal Ion Blocker   EDTA     0.10 8 antiseptic   Methyl paraben     0.10 9 Mechanism   Ascorbate Sodium     0.30 10 Mechanism   Myristoyl Glutamate Sodium    15.00 11 Mechanism   Cocoyl Isocionate Sodium    20.00 12 Mechanism   Cocamidophoropil Betamin     5.00 13 Mechanism   Polyquaternium-10     1.00 14 timber   Pomegranate Fermented Alkaline    51.45 15 Mechanism   2-pyrrolidone-5-carboxylic acid     2.00 16 Mechanism   Glycylizate Ammonium     0.10

(Example 2, natural brown)

division Purpose of Mixing ingredient Content (% by weight) One dyes   p-phenylenediamine     0.56 2 dyes   N-phenyl-p-phenylenediamine     0.56 3 dyes   Resorcinol     0.78 4 dyes   m-aminophenol     0.42 5 dyes   p-aminophenol     0.14 6 dyes   l-naphthol     0.07 7 Metal Ion Blocker   EDTA     0.10 8 antiseptic   Methyl paraben     0.10 9 Mechanism   Ascorbate Sodium     0.30 10 Mechanism   Myristoyl Glutamate Sodium    15.00 11 Mechanism   Cocoyl Isocionate Sodium    20.00 12 Mechanism   Cocamidophoropil Betamin     5.00 13 Mechanism   Polyquaternium-10     1.00 14 timber   Pomegranate Fermented Alkaline    53.87 15 Mechanism   2-pyrrolidone-5-carboxylic acid     2.00 16 Mechanism   Glycylizate Ammonium     0.10

(Example 3, light brown)

division Purpose of Mixing ingredient Content (% by weight) One dyes   p-phenylenediamine     0.35 2 dyes   N-phenyl-p-phenylenediamine     0.35 3 dyes   Resorcinol     0.90 4 dyes   m-aminophenol     0.20 5 dyes   p-aminophenol     0.20 6 dyes   2-methylresorcinol     0.20 7 Metal Ion Blocker   EDTA     0.10 8 antiseptic   Methyl paraben     0.10 9 Mechanism   Ascorbate Sodium     0.30 10 Mechanism   Myristoyl Glutamate Sodium    15.00 11 Mechanism   Cocoyl Isocionate Sodium    20.00 12 Mechanism   Cocamidophoropil Betamin     5.00 13 Mechanism   Polyquaternium-10     1.00 14 timber   Pomegranate Fermented Alkaline    54.20 15 Mechanism   2-pyrrolidone-5-carboxylic acid     2.00 16 Mechanism   Glycylizate Ammonium     0.10

Preparation of oxidant (second agent)

An oxidant of the composition as shown in Table 4 was prepared.

division Purpose of Mixing ingredient Content (% by weight) One chief ingredient   Hydrogen peroxide     9.00 2 Metal Ion Blocker   Erythorbic acid     0.20 3 stabilizator   Phosphoric Acid     0.01 4 Mechanism   Cetanol     3.20 5 Mechanism   lanolin     1.00 6 Mechanism   Glycerine Isostearate     1.40 7 Mechanism   Isopropyl myristate     0.10 8 Mechanism   Laureate sulfate     2.40 9 pH adjuster   Disodium and Phosphate     0.24 10 Mechanism   Glycylizate Ammonium     0.05 11 timber   Purified water    82.40

(Comparative Example)

Commercially available dyes were used as comparative examples.

Experimental Example 1 Measurement of Heavy Metal Content

Applicant of the present invention, Gapbu Representative Jung Hak requested the heavy metal content of Example 2 to the environmental resource analysis center to obtain the same results as the test report of Figure 1a, 1b.

According to the test report, no heavy metals such as lead, cadmium, mercury and arsenic were detected in the present invention.

Experimental Example 2 Dyeing Characteristics

The first and second preparations of the compositions of Examples 1, 2, 3 and Comparative Examples were mixed 1: 1 and evenly applied to the test hair, and after about 20 minutes, shampooed, rinsed with lukewarm water and dried I was. Table 5 shows the results obtained by measuring the dyeing and dyeing fastness to the hair after drying.

Example 1 Example 2 Example 3 Comparative example Dyeing 67 65 64 59 Dyeing fastness Very good Very good Very good Good

The color difference between the dyed hair and the untreated hair was measured using a spectrophotometer. The larger the color difference, the better the dyeing property of the hair dye.

The fastness of the dye was immersed in the acid solution similar to the sweat component of the dyed hair and observed the degree of discoloration after a certain time.

Experimental Example 3 Scalp Stimulus Characteristics

Allergy incidence and hair damage prevention effects of Examples 1, 2, 3 and Comparative Examples were tested.

40 males of 25 to 40 years and 40 females of 25 to 40 years of age were selected and dyed in each of the above Examples 1, 2, 3 and Comparative Examples, and then allergic reactions on the scalp and hair damage occurred. Investigations are shown in Table 6.

Example 1 Example 2 Example 3 Comparative example Allergy occurrence number 0 2 One 7 Hair damage 0 One 0 11

As can be seen in Table 6, allergy or hair damage hardly occurred in the hair dye composition of the present invention.

Although the preferred embodiments of the present invention have been illustrated and described above, the present invention is not limited to the above-described embodiments, and the present invention is not limited to the above-described embodiments without departing from the spirit of the present invention as claimed in the claims. Various modifications can be made by those skilled in the art, and such modifications are intended to fall within the scope of the appended claims.

As described above, the present invention includes a pomegranate fermentation alkaline agent to improve scalp trouble through antibacterial action to harmful scalp bacteria, and also has an excellent astringent effect on the scalp to prevent scalp trouble, scalp protection and damaged hair quickly. In addition to restoring the elasticity and nutrition to give a long lasting shine effect.

Claims (6)

50.45 to 55.20% by weight of pomegranate fermented alkali, 42.54 to 44.26% by weight, 2.1 to 5.05% by weight of dye, 0.08 to 0.12% by weight of EDTA, a metal ion blocking agent, and 0.08 to 0.12% by weight of ascorbate sodium Hair dye composition. The method of claim 1, The pomegranate fermentation alkaline agent hair dye composition, characterized in that the fermentation of the pomegranate extract in a dark place for 30 to 35 days at room temperature. The method of claim 1, The dye is p-phenylenediamine, N-phenyl-p-phenylenediamine, resorcinol, o-aminophenol, 4-amino-2-hydrotoluene, m-phenylenediamine, p-aminophenol, m- A hair dye composition comprising one or two or more of aminophenol, l-naphthol and 2-methylresorcinol. The method of claim 1, The base is selected from among ascorbate sodium, myristoyl glutamate sodium, cocoyl isocionate sodium, cocamidopropyl betamin, polyquaternium-10, 2-pyrrolidone-5-carboxylic acid, glycyrazate ammonium A hair dye composition comprising a species or two or more kinds thereof. Base 42.54 to 44.26% by weight, 0.08 to 0.12% by weight of a metal ion sequestrant, 0.08 to 0.12% by weight of sodium ascorbate as a preservative, were heated and stirred at 80 ° C. in a mixer, followed by addition of 2.1 to 5.05% by weight of dye. After cooling to room temperature with stirring, 50.45-55.20 weight% of pomegranate fermentation alkaline agents are added, and it stirred and mixed, The manufacturing method of the hair dye composition characterized by the above-mentioned. The method of claim 5, The pomegranate fermentation alkaline agent is a process for removing impurities by checking the quantity of pomegranate and washing with water; Rinsing and slicing the pomegranate from which impurities are removed and separating the shell; Filtering the chopped pomegranate using water pressure; Separating the pomegranate extract using the filtered pomegranate using a centrifuge; Storing the separated pomegranate extract in a stock tank; Making pomegranate purified juice by sterilizing the pomegranate extract of the stock solution tank at 75 ° C. under vacuum; Heating the pomegranate refined juice to 105 ° C. and distilling it to rapidly freeze it at 20 ° C. to obtain a pomegranate extract; A method for producing a hair dye composition, characterized in that the pomegranate extract is obtained by the process of fermentation at room temperature in a cold dark place for 30 to 35 days.

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