KR100758252B1 - Preparation method for rice wine being made from japanese cornel and the rice wine - Google Patents
Preparation method for rice wine being made from japanese cornel and the rice wine Download PDFInfo
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Abstract
Description
본 발명은 고항산화능을 가진 산수유를 이용하여 향미와 색조가 로제와인과 유사한 전통약주를 제조하는 방법과 이에 의해 제조되어지는 약주에 관한 것이다. 보다 상세하게는 약주 제조공정에서 산수유의 첨가시기를 조절하여 품질이 안정되고, 부가적으로 산수유의 안토시안 색소의 침출을 통해 와인과 유사한 색상을 냄으로서 기호성이 높은 관능적 특성을 가진 전통약주를 제조하는 방법과 산수유 약주에 관한 것이다.The present invention relates to a method for producing a traditional herbal medicine similar to the rose wine with flavor and color tone using a cornus oil having a high antioxidant capacity, and a herbal medicine produced thereby. More specifically, the quality is stable by adjusting the addition time of cornus milk in the manufacturing process of the liquor, and in addition, the traditional medicines having high taste characteristics are produced by giving a color similar to wine through leaching of anthocyanin pigment of cornus milk. It is about method and cornus medicinal herbs.
종래 대부분의 약주들은 숙취 또는 누룩으로부터 유래되는 잡미향, 갈변 착색 등으로 인한 주질 열화의 문제와 약주 자체가 가지는 오래된 이미지 등으로 소비자들의 선호도가 점점 감소하고 있으며, 현재에는 대개 일부 장년층들에게만 음용되고 있다. 반면 와인시장은 급속히 증가하고 특히 젊은 세대에도 크게 어필하고 있는 실정이다. 따라서 우리나라 전통주인 약주의 문제점들을 개선하여 약주에 대한 선호도를 높이기 위하여, 기존의 전통약주의 틀에서 벗어나 우수한 향미 및 외 관 뿐만 아니라, 건강성, 품질 안정성이 우수한 개량 약주를 제조할 필요성이 절실히 대두되고 있다. In the past, most herbal medicines are declining due to the problem of deterioration due to hangover or malt flavor, browning, etc., and the old image of the medicine itself, and now it is usually only consumed by some elderly people. have. On the other hand, the wine market is rapidly increasing and especially appealing to the young generation. Therefore, in order to improve the problems of Yakju, the traditional liquor of Korea, it is urgently needed to manufacture improved Yakju with excellent health and quality stability as well as excellent flavor and appearance, out of the existing traditional Yakju framework. It is becoming.
산수유는 부교감 신경을 흥분시키는 코르닌(cornin), 약간의 중추신경 흥분작용이 있는 로가닌(loganin), 사포닌(saponin) 등의 배당체와 탄닌 구성성분의 하나로서 수렴작용에 효과가 있는 몰식자산 (gallic acid)과 포도산 (tartaric acid), 사과산 (malic acid) 등의 유기산, 수렴성분인 탄닌(tannin)과 비타민 A가 다량 함유되어 자양강정과 수렴작용에 효과가 있고, 암을 예방할 수 있는 셀레늄 (Se) 등의 기능성분이 있어 복분자(覆盆子), 구기자(枸杞子)와 함께 3대 강정제로 대표되기도 한다.Cornus is one of the glycosides of tannin and saponin, such as cornin, which stimulates parasympathetic nerves, loganin, which has some central nervous excitability, and saponin. Organic acids such as gallic acid, tartaric acid and malic acid, and tannin and vitamin A, which are astringent ingredients, are effective in nourishing and astringent effects, and selenium can prevent cancer. There are functional ingredients such as (Se) and it is also represented as three major tablets together with Bokbunja (覆盆子) and Gojija (枸杞 子).
하지만 종래 전통적인 약주의 제조방법에 따라 단순히 약재의 침출액 등을 발효과정에 투입하는 것으로는 균일한 제품과 약재 자체가 지니는 관능적 특성을 살리기 어려운 문제가 있다. However, simply injecting the leachate of the medicinal herbs into the fermentation process according to the conventional method of manufacturing traditional medicine has a problem that it is difficult to utilize the sensory characteristics of the uniform product and the medicinal herbs themselves.
본 발명은 상기한 바와 같은 종래기술이 가지는 문제를 해결하기 위해 안출된 것으로,The present invention has been made to solve the problems of the prior art as described above,
본 발명의 목적은 향미와 음용성이 우수하고, 품질 안정성에 있어 우수한 성질을 갖고 고항산화능 뿐만 아니라 코르닌, 로가닌 등 각종 약리성분과 유기산, 몰직자산, 사과산, 포도산 등을 함유하여, 자양강장, 숙취해소 및 피로회복에 효과적인 산수유를 원료로 하는 약주의 제조방법 및 약주를 제공하는 것이다.An object of the present invention is excellent in flavor and drinkability, has excellent properties in quality stability and contains not only high antioxidant activity, but also various pharmacological components such as cornine, loganin, organic acids, woolen assets, malic acid, grape acid, etc. It is to provide a method and method of manufacturing Yakju, which is based on cornus oil, which is effective for nourishing tonic, hangover and fatigue recovery.
상기한 목적을 달성하기 위해서 본 발명은 산수유를 원료로 하는 약주의 제조방법에 있어서, 산수유 침출액을 알콜발효 이후의 숙성과정에서 알콜발효액에 첨가하는 단계를 포함함을 특징으로 하는 산수유를 원료로 하는 약주의 제조방법을 제공한다.In order to achieve the above object, the present invention provides a method for producing medicinal liquor made from cornus oil, wherein the cornus oil leaching solution is added to the alcoholic fermentation solution during the aging process after alcoholic fermentation. It provides a method of manufacturing medicine.
본 발명에 의하면 바람직하게는 자초 침출액을 산수유 침출액과 함께 더 첨가한다.According to the present invention, preferably, the licorice leachate is further added together with the cornus leachate.
본 발명에 의하면 바람직하게는 산수유 침출액 및 자초 침출액의 첨가량은 발효액 1L당 각각 0.1~0.2L 및 0.02~0.03L의 비로 첨가한다.According to the present invention, preferably, the addition amount of the cornus leachate and the licorice leachate are added in a ratio of 0.1 to 0.2L and 0.02 to 0.03L per 1 L of the fermentation broth, respectively.
또한, 본 발명은 알콜발효 이후의 숙성 과정에 첨가되어진 산수유 침출액을 함유하는 것을 특징으로 하는 산수유를 원료로 하는 약주를 제공한다.In addition, the present invention provides a medicinal liquor made from cornus oil, which comprises a cornus leachate added during the aging process after alcoholic fermentation.
본 발명에 의하면 바람직하게는 알콜발효 이후의 숙성 과정에 첨가되어진 자초 침출액을 더 포함하는 것이 좋다.According to the present invention, preferably, the licorice leachate added to the aging process after alcohol fermentation may be further included.
이하, 본 발명의 내용을 보다 상세하게 설명하면 다음과 같다.Hereinafter, the content of the present invention in more detail as follows.
본 발명에서는 전통 약주의 하나로서, 본초 강목, 한약 전문서적 및 한국식품의약품안전청 등에 고시된 식용가능 한약재 중에서 항산화능이 높으면서 와인과 유사한 색상을 낼 수 있는 산수유를 주 약재로 사용한다. In the present invention, as one of the traditional herbal medicine, the medicinal herbs that can produce a color similar to wine while having high antioxidant power among edible herbal medicines published in herbal wood, Chinese herbal medicine books and the Korea Food and Drug Administration, etc. are used as main medicines.
표 1에 산수유를 포함한 다른 약재의 항산화능을 측정하여 분석한 결과를 나타내고 있다 [항산화능의 분석법: DPPH 방법, 암실에서 DPPH시약을 0.012g을 취하여 100㎖ EtoH(LC grade)에 녹인 후 1시간 동안 교반한 후에, 100㎖ 증류수를 넣 고, 흡광도가 1이 되도록 50% 에탄올(LC grade)을 이용하여 조절하고, 스펙트로포토미터(spectrophotometer)를 517nm에 맞추고 20분 반응시켜 측정].Table 1 shows the results of measuring the antioxidant capacity of other medicinal herbs, including cornus oil. [Analytical method of antioxidant activity: DPPH method, take 0.012g of DPPH reagent in the dark and dissolve in 100ml EtoH (LC grade) for 1 hour. After stirring for 100 minutes, distilled water was added, and the absorbance was adjusted using 50% ethanol (LC grade) to 1, the spectrophotometer (spectrophotometer) was adjusted to 517 nm and reacted for 20 minutes.
<표 1> 산수유를 포함한 한약재의 항산화능<Table 1> Antioxidant Activity of Herbal Medicines including Cornus
본 발명에서는 또한 산수유와 함께 보조 약재로서 자초가 더 첨가될 수 있다. 자초는 산수유의 향미와 색상에 부정적 영향을 미치지 않고 와인과 유사한 고항산화능 전통약주를 제공할 수 있다는 점에서 바람직하다.In the present invention, it is also possible to further add the vinegar as auxiliary medicine with cornus. Licorice is preferable in that it can provide a wine-like high antioxidant traditional medicine without adversely affecting the flavor and color of cornus.
상기한 바와 같은 산수유 및 자초는 침출액의 형태로 이용되어질 수 있으며, 이들은 알콜 발효의 후속단계인 숙성 단계에서 첨가되어지는 것이 바람직하다. 이 에 의하면, 발효액에 따른 품질의 차이가 없어 최종 제품에서의 품질 안정성을 기할 수 있다.Cornus and licorice as described above may be used in the form of leaching liquors, which are preferably added in the ripening step, which is a subsequent step of alcoholic fermentation. According to this, there is no difference in quality according to the fermentation broth can ensure the quality stability in the final product.
본 발명에 따른 산수유 침출액과 자초 침출액의 제조방법은 특별히 한정되어지는 것은 아니며, 예를 들어 알콜 또는 주정에 산수유와 자초를 각각 소정량 첨가하여 침출시키는 과정에 의해 달성될 수 있다. 보다 구체적인 예를 들면, 45% 에탄올 18L에 산수유 5Kg을 48시간 침출시켜 얻을 수 있다. 유사하게 자초 침출액은 45% 에탄올 5L에 자초 5Kg을 48시간 침출시켜 얻을 수 있다.The manufacturing method of the cornus leachate and the leachate liquor according to the present invention is not particularly limited, and may be achieved by, for example, leaching by adding a predetermined amount of cornus and licorice to alcohol or alcohol. For example, it can be obtained by leaching 5 kg of cornus oil in 18 L of 45% ethanol for 48 hours. Similarly, the leaching licorice can be obtained by leaching 5Kg of licorice in 5L of 45% ethanol for 48 hours.
산수유 침출액과 자초 침출액의 첨가량은 특별히 한정되는 것은 아니며, 예를 들어 산수유 침출액은 발효액 1L를 기준으로 하여 0.1~0.2L의 비율로 첨가될 수 있으며, 자초 침출액은 발효액 1L를 기준으로 하여 0.02~0.03L의 비율로 첨가될 수 있다.The addition amount of the cornus leachate and the licorice leachate are not particularly limited. For example, the cornus leachate may be added at a ratio of 0.1 to 0.2L based on 1L of the fermentation broth, and the licorice leachate is 0.02 to 0.03 based on 1L of the fermentation broth. It can be added at a ratio of L.
본 발명에 의한 산수유를 원료로 하는 약주의 제조과정은 지금까지 알려진 전통 약주의 일반적인 제조과정을 따를 수 있다. 다만, 본 발명에서는 종래 알려진 일반적인 약주의 제조공정 중 알콜 발효 이후의 숙성단계에서 당해 알콜 발효액내에 상기 산수유 침출액과 자초 침출액이 첨가되어진다는 점에서 차이가 있다. The manufacturing process of Yakju using raw cornus according to the present invention may follow the general manufacturing process of traditional Yakju known to date. However, the present invention is different in that the oxalic acid leachate and licorice leachate are added to the alcoholic fermentation broth in the aging step after alcoholic fermentation during the manufacturing process of a conventionally known chemical liquor.
일반적인 전통 약주의 제조과정은 밑술제조, 1단 담금, 2단 담금, 1차 여과, 저온 숙성, 여과 및 블렌딩, 여과, 살균 및 병입 등의 일련의 과정을 포함할 수 있으나, 본 발명에서는 반드시 이에 한정되는 것은 아니다. 즉, 상기 과정에서 일부는 필요에 따라 변형되어지거나, 생략되어질 수도 있다.General manufacturing process of traditional Yakju may include a series of processes, such as manufacturing base wine, single stage immersion, two stage immersion, primary filtration, low temperature aging, filtration and blending, filtration, sterilization and bottling, but in the present invention, It is not limited. In other words, in the above process, some may be modified or omitted as necessary.
이하 본 발명의 내용을 실시예를 통해 상세히 설명하기로 한다. 다만 하기 실시예는 본 발명의 내용을 설명하기 위한 것으로서 본 발명의 권리범위가 이에 한정되지는 아니한다.Hereinafter, the contents of the present invention will be described in detail through examples. However, the following examples are provided to explain the contents of the present invention, but the scope of the present invention is not limited thereto.
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<실시예 1> 산수유주의 제조
증자미 10kg, 젖산(90%) 120ml, 효모 100g, 정제효소 30g, 물20L를 투입한 후 실내온도 20℃ 유지하에 5일간 발효시켜 밑술을 제조하였다.
상기의 밑술에 증자미 180kg, 액화효소(α-amylase) 3L, 정제효소 400g, 물300L를 투입한 후 실내온도 20℃ 유지하에 5일간 발효시켜 1단 담금을 실시하였다.
상기 1단 담금물에 증자미 510kg, 액화효소(α-amylase) 3L, 정제효소 400g, 물900L를 투입한 후 실내온도 20℃ 유지하에 15일간 발효 및 숙성시켜 2단 단금을 실시하였다.
상기 2단 담금 후 필터프레스를 이용하여 여과하여 발효액 1400L(알콜분 13.5%), 술지게미(주박) 245kg로 분리하였다.
45% 에탄올 18L에 산수유 5kg을 48시간 침출시킨 후 침출액 17L와 45% 에탄올 5L에 자초 3kg을 함께 48시간 침출시킨 후 침출액 3.5L를 상기에서 얻은 발효액 중 발효액 140L에 투입한 후 실내온도 4℃에서 20일 이상 숙성시켰다.Example 1 Preparation of Cornus
10 kg of cooked rice, lactic acid (90%) 120ml, yeast 100g, purified enzyme 30g, water 20L was added to ferment for 5 days at 20 ℃ to prepare a base liquor.
180 kg of cooked rice and liquefied enzyme (α-amylase) After 3L, 400g of purified enzyme and 300L of water were added, fermentation was carried out for 5 days at 20 ° C at room temperature, followed by one-stage immersion.
After adding 510 kg of steamed rice, liquefied enzyme (α-amylase) 3L, purified enzyme 400g, and 900L of water to the first stage immersion, fermentation and aging for 15 days at room temperature 20 ℃ was carried out to perform two stages of annealing.
After two stages of immersion, the resultant was filtered using a filter press to separate the fermentation broth 1400L (alcohol content 13.5%) and sake lees (sour sake) 245 kg.
After leaching 5kg of cornus oil for 48 hours in 18L of 45% ethanol, leaching 3L of 17L of leachate with 5L of 45% ethanol for 48 hours, 3.5L of leachate was added to 140L of fermentation broth from fermentation broth obtained above, and then at room temperature 4 ℃. Aged more than 20 days.
상기 발효액에 산수유 침출액 및 자초 침출액규을 첨가한 후 숙성시킨 숙성액에 규조토 여과기를 이용하여 2차 여과한 후 자체 블렌딩 방식으로 13% 산수유주로 보정한 다음 0.2㎛ 한외 카트리지 여과기로 여과한 후 85℃, 20분 동안 살균한 후 병입하여 산수유주를 제조하였다.After adding the cornus leachate and the vinegar leaching solution to the fermentation broth, the fermentation broth was filtered through a diatomaceous earth filter using a diatomaceous earth filter, and then calibrated with 13% cornus in a self-blending manner, followed by filtration with a 0.2㎛ ultra-cartridge filter, followed by 85 ℃ After sterilization for 20 minutes, bottling was prepared.
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본 발명에 따라 3회에 걸쳐 자체 시험한 결과 모두 다 관능상 동일한 산수유주를 제조할 수 있었다. 실 예로 시험실에서 적은 양으로 발효 시험한 산수유주 보다 상쾌함은 더하며 관능상 로즈와인에 가까운 제품을 생산 할 수 있었다. 또한 이러한 방법은 약주와 저온 조건에서 안정한 다른 기능성 물질을 첨가해도 균일 제품 을 생산 할 수 있음을 시사해 준다.As a result of three times of self-testing according to the present invention it was possible to produce all functionally the same corn seed. For example, it was more refreshing than the wild corn wine fermented in the laboratory and produced functionally close to rose wine. In addition, this method suggests that even the addition of chemicals and other functional substances that are stable under low temperature conditions can produce homogeneous products.
<비교예>Comparative Example
시중에서 구입 가능한 전통약주로서, 한약재를 첨가한 6종의 전통약주(진매, 수국, 구기자, 사삼주, 소곡주, 천국)를 구입하여 새롭게 개발된 산수유주와 비교 분석하였다.As a traditional herbal medicine that can be purchased on the market, six traditional herbal medicines (jinmae, hydrangea, gojija, sasamju, Sogokju, heaven) added with Chinese herbal medicines were purchased and analyzed.
본 발명자들은 본 발명의 우수성을 입증하기 위하여, 상기 실시예1 과 비교 예에 따라 제조된 약주들을 가지고, 제품의 항산화능과 소비자 기호도에 대해 하기와 같이 비교분석하였다.In order to demonstrate the superiority of the present invention, the present inventors have the medicines prepared according to Example 1 and Comparative Example, and compared and analyzed the antioxidant capacity and consumer preference of the product as follows.
<실험예 2> 항산화능 테스트Experimental Example 2 Antioxidant Activity Test
실시예 1에서 제조한 약주와 비교예를 위해 수거한 약주의 항산화능을 분석하였다. 항산화능을 분석하기 위하여 DPPH방법을 이용하였다. 암실에서 DPPH시약을 0.012g을 취하여 100ml 에탄올 (LC grade)에 녹인 후 1시간 교반하였다. 후에, 100ml 증류수를 넣고, 흡광도가 1이 되도록 50% 에탄올(LC grade)을 이용하여 조절하였다. 스펙트로포토미터를 517nm에 맞추고 20분 반응시키고 측정하였다. 분석 결과는 표 2과 같다.
<표 2> 산수유주와 시중에 구입 가능한 전통약주의 항산화능 비Antioxidant activity of the medicines prepared in Example 1 and the medicines collected for the comparative example was analyzed. DPPH method was used to analyze antioxidant activity. 0.012 g of DPPH reagent was taken in the dark, dissolved in 100 ml ethanol (LC grade), and stirred for 1 hour. After that, 100 ml of distilled water was added, and the absorbance was adjusted to 50% using ethanol (LC grade). The spectrophotometer was set at 517 nm, reacted for 20 minutes, and measured. The analysis results are shown in Table 2.
<Table 2> Antioxidant Activity Ratio of Cornus Liquor and Traditional Herbal Wine Available Commercially
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상기 표 2에서 나타난 바와 같이 실시예 1(산수유주)은 비교예들에 비해 높거나 최고치와 비슷한 항산화능을 보여 주었다.As shown in Table 2, Example 1 (acid water liquor) showed a high or similar antioxidant capacity compared to the comparative examples.
<실험예 3> 기호도 테스트Experimental Example 3 Symbol Test
기호성을 파악하는데 일반적 분석결과는 참고의 수치 이상은 될 수 없다. 이는 단순히 풍미의 좋고 나쁜 정도를 수치화 하기에는 우리의 과학기술의 한계가 있기 때문이다. 따라서 최종적으로는 기호도 조사에 의존할 수 밖에 없는 실정이다. 관능검사는 외국산 주류에 쉽게 동화되어 있으나, 앞으로 새로운 주류문화를 만들어나갈 20대와 30대를 대상으로 실시하였다. 기호도 조사는 고도로 훈련된 요원을 대상으로 실시하는 것이 아니기 때문에 단순히 비교하여 선호시료를 선택하는 것으로 하였으며, 따라서 관능 대상인원을 60명으로 하였다. 비교예는 시장 점유율이 가장 높은 약주로 하였다. 그 결과 실시예의 선호도가 월등히 높게 나왔다. 이는 향, 맛, 색상의 요인 복합적으로 작용한 결과로 파악된다.In analyzing palatability, general analysis results cannot be more than the reference value. This is because our science and technology is limited to simply quantify the good and bad degree of flavor. Therefore, in the end, it is inevitable to rely on the preference investigation. The sensory test was easily assimilated with foreign alcoholic beverages, but was conducted for those in their twenties and thirties who will create a new mainstream culture. Since palatability surveys are not conducted for highly trained personnel, they were selected by simply comparing them. In the comparative example, the stocks with the highest market share were used. As a result, the preference of the example was much higher. This can be seen as the result of a combination of aroma, taste and color factors.
기호도 조사에 대한 결과는 하기 표 3에 나타내었다.
<표 3>The results for the palatability survey are shown in Table 3 below.
TABLE 3
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상기한 바와 같이 본 발명에 의하면 코르닌, 로가닌 등 각종 약리성분과 특유의 맛 성분을 함유한 산수유를 이용하여 약주발효 공정 중, 적절한 효모의 생육을 유도함으로서 향과 맛이 우수하고, 부가적으로 산수유와 자초의 안토시안 색소를 약주에 효율적으로 전이시키는 방법을 통해 천편일률적인 황색의 약주 색상을 적색과 황색이 잘 조화된 약주를 제조하고 제공함으로써 산수유의 경제적 소비를 촉진하여 농가의 소득 증대에 기여할 것이다.As described above, according to the present invention, it is excellent in flavor and taste by inducing the growth of appropriate yeast during the fermentation process of Yakju by using cornus oil containing various pharmacological ingredients such as cornine and loganine and unique flavor components. By efficiently transferring the anthocyanin pigments of cornus and licorice to the liquor, the red and yellow blends of yellow liquor are produced and provided to promote the economic consumption of cornus milk to increase the income of farmers. Will contribute.
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Cited By (4)
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CN103396909A (en) * | 2013-08-07 | 2013-11-20 | 上海燕瘦生物科技有限公司 | Preparation method of female wine |
KR20160080303A (en) | 2014-12-26 | 2016-07-08 | 대한민국(농촌진흥청장) | Manufacturing method of yak-ju with excellent sensory quality by adding citric acid and heating and yak-ju manufactured thereby |
CN111592957A (en) * | 2020-05-13 | 2020-08-28 | 四川康佰思科技有限公司 | Cornus officinalis fruit wine |
CN111778129A (en) * | 2020-06-17 | 2020-10-16 | 方国胜 | Nucleic acid and amino acid health oral liquid and preparation method thereof |
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KR870006180A (en) * | 1985-12-26 | 1987-07-09 | 나종현 | Method of manufacturing nutrition using herbal medicine |
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KR870006180A (en) * | 1985-12-26 | 1987-07-09 | 나종현 | Method of manufacturing nutrition using herbal medicine |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103396909A (en) * | 2013-08-07 | 2013-11-20 | 上海燕瘦生物科技有限公司 | Preparation method of female wine |
KR20160080303A (en) | 2014-12-26 | 2016-07-08 | 대한민국(농촌진흥청장) | Manufacturing method of yak-ju with excellent sensory quality by adding citric acid and heating and yak-ju manufactured thereby |
CN111592957A (en) * | 2020-05-13 | 2020-08-28 | 四川康佰思科技有限公司 | Cornus officinalis fruit wine |
CN111778129A (en) * | 2020-06-17 | 2020-10-16 | 方国胜 | Nucleic acid and amino acid health oral liquid and preparation method thereof |
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