KR100736352B1 - Color cosmetic composition of powder - Google Patents
Color cosmetic composition of powder Download PDFInfo
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- KR100736352B1 KR100736352B1 KR1020020079672A KR20020079672A KR100736352B1 KR 100736352 B1 KR100736352 B1 KR 100736352B1 KR 1020020079672 A KR1020020079672 A KR 1020020079672A KR 20020079672 A KR20020079672 A KR 20020079672A KR 100736352 B1 KR100736352 B1 KR 100736352B1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/12—Face or body powders for grooming, adorning or absorbing
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Abstract
본 발명은 분백류 색조화장료 조성물에 관한 것으로, 특히 피지굴절율과 유사한 표면처리제로 코팅한 산화철색소를 포함하여 화장 후 분비된 피지에 의해 분체화장막이 젖더라도 실제 발생하는 색상변화를 줄여 최초의 색상 변화가 적을 뿐만 아니라, 동시에 화장효과의 지속성 및 사용감이 우수한 분백류 색조화장료 조성물에 관한 것이다.The present invention relates to a powder powder composition of powdery white powder, in particular, including the iron oxide pigment coated with a surface treatment agent similar to sebum refractive index, the first color change by reducing the color change actually occurs even if the powder cosmetic film is wet by sebum secreted after makeup In addition, the present invention relates to a powdery color cosmetic composition which is not only low but also excellent in durability and usability of the cosmetic effect.
분백류 색조화장료, 표면처리제, 실리콘계 고분자, 아크릴계 고분자, 산화철색소, 색상변화, 화장 지속성Powdery color cosmetics, surface treatment agent, silicone polymer, acrylic polymer, iron oxide, color change, makeup persistence
Description
본 발명은 분백류 색조화장료 조성물에 관한 것으로, 더욱 상세하게는 화장 후 분비된 피지에 의해 분체화장막이 젖더라도 실제 발생하는 색상변화를 줄여 최초의 색상 변화가 적을 뿐만 아니라, 동시에 화장효과의 지속성 및 사용감이 우수한 분백류 색조화장료 조성물에 관한 것이다.The present invention relates to a powdery tonal cosmetic composition, and more particularly, to reduce the color change that actually occurs even if the powder cosmetic film is wetted by sebum secreted after makeup, the first color change is less, and at the same time the persistence of the makeup effect and The present invention relates to powdery color cosmetic composition having excellent usability.
종래 분백류 색조화장료는 분체-오일의 2 성분으로 구성되어 있으며, 그 구성비, 제형, 및 사용목적에 따라 페이스파우더, 콤팩트, 파우더파운데이션, 투웨이케익 등으로 구분할 수 있다.Conventional powder powder colorants are composed of two components of powder-oil, and may be classified into face powder, compact, powder foundation, two-way cake and the like according to the composition ratio, formulation, and purpose of use.
일반적으로 이들 제품은 피부에 도포되어 대략 8∼12 시간 동안 부착되어 있고, 이 시간 중 피부에서 분비되는 땀이나 피지 등의 피부분비물에 의해 화장막의 변화가 발생하게 된다. 이러한 변화를 보면, 들뜸, 뭉침, 색상변화, 번들거림 현상 등 지속성에 관한 것이 대부분이며, 이중 화장 후 경시에 따라 분비된 피지에 의해 분체화장막이 젖었을 때 나타나는 색상변화 현상은 현재 분백류 색조화장료를 사용하는 여성들의 큰 불만사항 중 하나이다.In general, these products are applied to the skin and adhered for about 8 to 12 hours. During this time, a change in the cosmetic film is caused by skin secretions such as sweat or sebum secreted from the skin. These changes are mostly related to sustainability such as lifting, agglomeration, color change, and lumping phenomenon, and the color change phenomenon that occurs when the powdery membrane gets wet due to sebum secreted over time after the double make-up One of the big complaints of women who use it.
기존의 분백류 색조화장료에서는 얼굴에 도포된 화장막이 경시에 따라 분비 된 피지에 젖게 되면 명도가 저하되거나 색조가 변하는 등의 색상변화현상이 발생한다. 이러한 색상변화현상의 원인을 살펴보면 분체가 피지에 젖었을 때 나타나는 반사량 차이나 백색분체내에 함유된 철 등의 불순물 등에 의한 명도저하 등이 원인이며, 특히 피지에 의한 산화철색소의 웨팅 색상차에 의한 영향이 가장 크다.In conventional powdery whitening cosmetics, when the makeup coat applied to the face gets wet with secreted sebum over time, color change occurs such as brightness decreases or color tone changes. The cause of the color change is caused by the difference in reflectance when the powder is wet with sebum or the decrease in brightness due to impurities such as iron contained in the white powder, especially the effect of wet color difference of iron oxide by sebum. This is the biggest.
상기와 같은 문제점을 해결하기 위하여, 일본공개특허공보 평7-119168호는 불소계 표면처리제로 코팅된 산화철색소를 사용하여 불소 특유의 발유성으로 분체가 피지에 젖지 않게 하여 피지 웨팅시 발생하는 색상차를 줄이는 방법에 대하여 개시하고 있다. 그러나, 상기 방법은 사용감이나 제형상의 문제점, 즉 강한 발유특성으로 분체는 젖지 않으나 화장막 자체가 들 따 뭉치는 현상 때문에 적용이 어렵다는 문제점이 있었다. 이외에도 흡유성이 우수한 분체를 배합하여 분비되는 과잉의 피지를 흡유함으로써 분체 웨팅을 최소화하는 방법이 있었어나, 이 방법 또한 얼굴에 도포되는 분체량과 분비되는 피지의 양을 고려할 때 피지를 완전히 흡유하여 분체가 젖지 않게 하는 것이 불가능하다는 문제점이 있다.In order to solve the above problems, Japanese Patent Application Laid-Open No. 7-119168 uses iron oxide pigments coated with a fluorine-based surface treatment agent so that the powder does not get wet with sebum due to the fluorine-specific oil repellency, so that the color difference occurs during sebum wetting. Discloses a method for reducing However, the method has a problem in that the powder is not wet due to the feeling of use or formulation, that is, a strong oil repellent property, but is difficult to apply due to the phenomenon that the makeup film itself is swollen. In addition, there has been a method of minimizing powder wetting by formulating powders having excellent oil absorption properties to absorb excess sebum secreted. However, this method also completely absorbs sebum when considering the amount of powder applied to the face and the amount of sebum secreted. There is a problem that it is impossible to prevent the powder from getting wet.
따라서, 피지 웨팅시 색상변화를 줄여 밝고 깨끗한 화장효과를 나타낼 수 있는 분백류 색조화장료에 대한 연구가 더욱 필요한 실정이다.Therefore, there is a need for further research on powdery tincture cosmetics that can reduce the color change during sebum wetting and have a bright and clean makeup effect.
상기와 같은 종래기술의 문제점을 해결하고자, 본 발명은 화장 후 분비된 피지에 의해 분체화장막이 젖더라도 실제 발생하는 색상변화를 줄여 최초의 색상 변화가 적을 뿐만 아니라, 동시에 화장효과의 지속성 및 사용감이 우수한 분백류 색조화장료 조성물을 제공하는 것을 목적으로 한다.In order to solve the problems of the prior art as described above, the present invention reduces the color change that actually occurs even if the powder cosmetic film is wetted by sebum secreted after make-up, the first color change is less, and at the same time the persistence and feeling of use An object of the present invention is to provide an excellent powder color cosmetic composition.
상기 목적을 달성하기 위하여, 본 발명은 분백류 색조화장료 조성물에 있어서, 표면처리제 10 내지 60 중량부로 코팅한 산화철색소를 포함하는 분백류 색조화장료 조성물을 제공한다.In order to achieve the above object, the present invention provides a powder tin colorant composition comprising iron oxide pigment coated with 10 to 60 parts by weight of the surface treatment agent.
이하 본 발명을 상세하게 설명한다. Hereinafter, the present invention will be described in detail.
본 발명자들은 피지 웨팅시 색상변화를 줄여 밝고 깨끗한 화장효과를 나타낼 수 있는 분백류 색조화장료에 대하여 연구하던 중, 피지에 젖었을 때 발생하는 산화철색소의 색상차를 줄이면 분백류 색조화장료에서 나타나는 색상변화가 현저히 저하됨을 확인하고, 이를 토대로 본 발명을 완성하게 되었다.The inventors of the present invention while studying the powdery tint cosmetics that can reduce the color change during sebum wetting, which can give a bright and clean makeup effect, by reducing the color difference of iron oxide pigment generated when wet with sebum It was confirmed that the remarkably lowered, and based on this, the present invention was completed.
본 발명의 분백류 색조화장료 조성물은 표면처리제 10 내지 60 중량부로 표면 코팅한 산화철색소를 포함하는 것을 특징으로 한다.Powder powder composition of the present invention is characterized in that it comprises iron oxide pigment surface-coated with 10 to 60 parts by weight of the surface treatment agent.
본 발명에 사용되는 상기 표면처리제는 산화철색소 100 중량부에 대하여 10 내지 60 중량부로 포함되는 것이 바람직하며, 더욱 바람직하게는 10 내지 40 중량부로 포함되는 것이다. 그 함량이 10 중량부 미만일 경우에는 피지 웨팅시 색상변화현상이 커지는 문제점이 있으며, 60 중량부를 초과할 경우에는 사용감과 제형상에 저하된다는 문제점이 있다.The surface treatment agent used in the present invention is preferably included in 10 to 60 parts by weight, more preferably 10 to 40 parts by weight based on 100 parts by weight of iron pigment. If the content is less than 10 parts by weight, there is a problem that the color change phenomenon is increased during sebum wetting, and if it exceeds 60 parts by weight, there is a problem that the feeling and the formulation is lowered.
상기 표면처리제는 특별히 제한되는 것은 아니나, 바람직하게는 실리콘계 고분자 또는 아크릴계 고분자를 사용하는 것이다.The surface treating agent is not particularly limited, but is preferably a silicone polymer or an acrylic polymer.
상기 실리콘계 고분자는 메틸하이드로겐 폴리실록산(methylhydrogen polysiloxane), 메틸폴리실록산(methylpolysiloxane), 트리에톡시실릴에틸 폴리메 틸실록시에틸 디메티콘(triethoxysilylethyl polymethysiloxyethyl dimethicone), 트리에톡시실릴에틸 폴리디메틸실록시에틸 헥실 디메티콘(triethoxysilylethyl polydimethysiloxyethyl hexyl dimethicone), 또는 n-옥틸 트리에톡시 실란(n-octyl triethoxy silane) 등을 사용할 수 있다.The silicone-based polymer may be methylhydrogen polysiloxane, methylpolysiloxane, triethoxysilylethyl polymethylsiloxyethyl dimethicone, triethoxysilylethyl polydimethylsiloxyethyl hexyl dimethicone Triethoxysilylethyl polydimethysiloxyethyl hexyl dimethicone, or n-octyl triethoxy silane can be used.
상기 아크릴계 고분자는 아크릴레이트/디메티콘 공중합체(acrylates/dimethicone copolymer), 아크릴레이트/트리데실 아크릴레이트/트리에톡시실릴프로필 메타크릴레이트 디메티콘 메타크릴레이트 공중합체(acrylates/tridecyl acrylate/triethoxysilylpropyl methacrylate dimethicone methacrylate copolymer), 또는 알킬 아크릴레이트 공중합체(alkyl acrylate copolymer) 등을 사용할 수 있다.The acrylic polymer is an acrylates / dimethicone copolymer, an acrylate / tridecyl acrylate / triethoxysilylpropyl methacrylate dimethicone methacrylate copolymer (acrylates / tridecyl acrylate / triethoxysilylpropyl methacrylate dimethicone methacrylate copolymer, alkyl acrylate copolymer, etc. may be used.
상기와 같은 성분을 포함하는 본 발명의 분백류 색조화장료 조성물은 색조화장료에 사용되는 색소를 미리 색상변화시켜 사용함으로써 화장 후 분비된 피지에 의해 화장막이 젖더라도 실제 발생하는 색상차를 줄여 최초의 색상 및 화장효과가 유지되는 효과가 있다.The powder powder composition of the present invention comprising the above components is used by changing the color of the pigment used in the color cosmetics in advance to reduce the color difference that is actually generated even if the cosmetic film is wet by sebum secreted after makeup. And the makeup effect is maintained.
이하, 본 발명의 이해를 돕기 위하여 바람직한 실시예를 제시하나, 하기 실시예는 본 발명을 예시하는 것일 뿐 본 발명의 범위가 하기 실시예에 한정되는 것은 아니다.Hereinafter, preferred examples are provided to help understanding of the present invention, but the following examples are merely to illustrate the present invention, and the scope of the present invention is not limited to the following examples.
[실시예]EXAMPLE
실시예 1Example 1
SI-3 마이카 10 중량부, SI-3 세리사이트 20 중량부, SI-3 탈크 35.6 중량 부, SI-3 실리카 5 중량부, SI-3 나이론 가루 10 중량부, SI-3 이산화티탄 5 중량부, 산화철색소 100 중량부에 대하여 n-옥틸 트리에톡시 실란(Daito Kasei사, 일본) 20 중량부로 코팅한 적색산화철(OTS-20 적색산화철) 0.8 중량부, 산화철색소 100 중량부에 대하여 n-옥틸 트리에톡시 실란 20 중량부로 코팅한 황색산화철(OTS-20 황색산화철) 2.7 중량부, 산화철색소 100 중량부에 대하여 n-옥틸 트리에톡시 실란 20 중량부로 코팅한 흑색산화철(OTS-20 흑색산화철) 0.4 중량부, 및 방부제 5 중량부를 균일하게 혼합한 후, 분쇄하였다. 여기에 유동파라핀 4 중량부, 실리콘 오일 0.2 중량부, 및 향 0.3 중량부를 분무한 후, 혼합 분쇄하여 투웨이케익을 제조하였다.10 parts by weight of SI-3 mica, 20 parts by weight of SI-3 sericite, 35.6 parts by weight of SI-3 talc, 5 parts by weight of SI-3 silica, 10 parts by weight of SI-3 nylon powder, 5 parts by weight of SI-3 titanium dioxide , 0.8 parts by weight of red iron oxide (OTS-20 iron oxide) coated with 20 parts by weight of n-octyl triethoxy silane (Daito Kasei, Japan) and 100 parts by weight of iron oxide, n-octyl 2.7 parts by weight of yellow iron oxide (OTS-20 iron oxide) coated with 20 parts by weight of triethoxy silane and black iron oxide (OTS-20 iron oxide) coated with 20 parts by weight of n-octyl triethoxy silane based on 100 parts by weight of iron oxide 0.4 parts by weight and 5 parts by weight of preservative were mixed uniformly and then ground. After spraying 4 parts by weight of liquid paraffin, 0.2 parts by weight of silicone oil, and 0.3 parts by weight of fragrance, the mixture was milled to prepare a two-way cake.
실시예 2, 및 비교예 1Example 2, and Comparative Example 1
상기 실시예 1에서 하기 표 1에 나타낸 성분과 조성비로 사용한 것을 제외하고는 상기 실시예 1과 동일한 방법으로 실시하여 투웨이케익을 제조하였다. 이때 표 1의 단위는 중량부이다.A two-way cake was manufactured in the same manner as in Example 1, except that Example 1 was used as a component and a composition ratio shown in Table 1 below. At this time, the unit of Table 1 is a weight part.
실험예 1Experimental Example 1
상기 실시예 1 또는 2, 및 비교예 1에서 제조한 투웨이케익의 화장시 나타나는 색상변화를 측정하기 위하여, 실제 피지와 유사한 조성으로 인조피지를 제조한 후, 상기 실시예 1 또는 2, 및 비교예 1의 투웨이케익에 20 중량%로 피지 웨팅(wetting)시켜 명도, 및 색상변화를 Chroma Meter CR-300 색차계(일본 미놀타 주식회사)를 이용하여 5 회 반복 측정하였으며, 그 평균값을 하기 표 2에 나타내었다. In order to measure the color change appearing on the makeup of the two-way cake prepared in Example 1 or 2, and Comparative Example 1, after manufacturing artificial sebum with a composition similar to the actual sebum, Example 1 or 2, and Comparative Example Sebum wetting at 20% by weight in two-way cake of 1 was measured five times with brightness and color change using Chroma Meter CR-300 colorimeter (Minolta Japan Co., Ltd.), the average value is shown in Table 2 below It was.
상기 표 2를 통하여, 본 발명에 따라 피지굴절율과 유사한 표면처리제 10 내 지 60 중량부로 코팅한 산화철색소를 포함하는 실시예 1 또는 2의 투웨이케익이 비교예 1과 비교하여 화장막이 피지에 의해 젖어서 발생하는 색상변화 억제 효과가 우수함을 확인할 수 있었다.Through Table 2, the two-way cake of Example 1 or 2 containing iron oxide pigment coated with a surface treatment agent 10 to 60 parts by weight in accordance with the present invention is sebum wet by sebum in comparison with Comparative Example 1 It was confirmed that the color change suppression effect is excellent.
실험예 2Experimental Example 2
상기 실시예 1 또는 2, 및 비교예 1에서 제조된 투웨이케익의 사용감을 측정하기 위하여, 20∼50 세의 여성 30 명을 대상으로 브라인드 테스트를 실시하고 화장시 지속성, 사용감, 및 화장효과를 하기 표 3의 평가기준에 따라 관능평가하고, 그 평균값을 하기 표 4에 나타내었다.In order to measure the feeling of use of the two-way cake prepared in Examples 1 or 2, and Comparative Example 1, a blind test was conducted on 30 women aged 20 to 50 years and the persistence, feeling, and makeup effects during makeup Sensory evaluation according to the evaluation criteria of Table 3, the average value is shown in Table 4 below.
상기 표 4를 통하여, 본 발명에 따라 피지굴절율과 유사한 표면처리제 10 내지 60 중량부로 코팅한 산화철색소를 포함하는 실시예 1 또는 2의 투웨이케익이 비교예 1과 비교하여 화장시 화장 지속성, 사용감, 및 사용효과가 우수함을 확인할 수 있었다. Through Table 4, the two-way cake of Example 1 or 2 comprising iron oxide coated with 10 to 60 parts by weight of a surface treatment agent similar to sebum refractive index according to the present invention compared to Comparative Example 1, makeup persistence, feeling, And it was confirmed that the use effect is excellent.
본 발명에 따른 분백류 색조화장료 조성물은 화장 후 분비된 피지에 의해 분 체화장막이 젖더라도 실제 발생하는 색상변화를 줄여 최초의 색상 변화가 적을 뿐만 아니라, 동시에 화장효과의 지속성 및 사용감이 우수한 효과가 있다.Powder powder composition according to the present invention reduces the color change actually occurs even if the powder cosmetic film is wetted by sebum secreted after make-up, not only the first color change is small, but at the same time excellent effect of the makeup effect and durability have.
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