KR100665966B1 - Silicate a ginkgo-leaf extraction of bath type a component and manufacture. - Google Patents

Abstract

A bath composition comprising silicate and ginkgo-leaf extract and a manufacturing method thereof are provided to convert hard water into soft water, restore fatigue, inhibit skin aging, promote blood circulation, and improve skin diseases. The method for manufacturing the bath composition comprising silicate and ginkgo-leaf extract comprises the steps of: mixing 42-58 wt.% of high purity silicate or SiO2, 30-38 wt.% of Na2CO3, 1-3 wt.% of Na2B4O7, 10-15 wt.% of Na4P2O7, and 1-2 wt.% of calcium carbonate, and heating the mixture at 1,400-1,500 deg.C to prepare transparent glass phase containing 40-60% of SiO2; liquefying the transparent glass phase in an autoclave and adding distilled water to prepare the solution A containing 14-24% of SiO2; extracting ginkgo leaf with ethyl alcohol to prepare solution B containing 1-5% flavonoids; and mixing 95-99% of the solution A with 1-5% of the solution B, wherein the bath composition regulates pH of water to 7-11 in a bath.

Description

Silicate a ginkgo-leaf extraction of bath type a component and manufacture. }

1 is a composition chart of the silicate A liquid of the present invention

2 is a manufacturing process diagram of the present invention

The present invention relates to a composition of a bath preparation prepared by silicate and ginkgo biloba extract and a method for preparing the preparation. As a bathing agent using silicate and ginkgo leaf extract containing rare minerals, water quality is reduced to soft water, it has a refreshing bath, and it has a fatigue recovery effect, and it is reduced to elastic skin by anti-aging effect of skin cells. It prevents fat accumulation, and is effective in improving athlete's foot and various skin diseases, and is used regardless of water quality anytime, anywhere, and it is harmless to human body even when drinking the composition as a food additive and high temperature condensation.

In the field of conventional bathing agents, there are many pre-registered patents by simply mixing the composition, etc., a bathing agent which dissolves in water to generate carbon dioxide by combining organic acid and carbonate of the pre-registered patent No. 0184283, natural salt and pine needle of No. 0433380 Bath composition of Hwangsol Pack containing extracted essential oil, ocher powder and charcoal powder, No. 0560775 Eoseongcho and ocher, bathing agent with charcoal ingredients, No.0512148 Although bathing agents are registered, there is a distance between the composition and the manufacturing method of the present technology. The composition for artificial hot spring bath of No. 0463747 is a method for preparing a simple composition in which potassium carbonate, sodium chloride, sodium bicarbonate, sodium sulfate, sodium fluoride, and lithium carbonate are mixed and dissolved in water. And is showing a different aspect.

In the production method of the present invention, the composition is mixed and introduced into a melting furnace to prepare a colorless transparent glass by condensation melting at a temperature of 1,400 ° C. to 1,500 ° C., and liquefy in an auto-clave to obtain a solution of SiO ₂ 14-24%. The solution to which distilled water was added is called A solution. The ginkgo leaves were mixed with A and B solutions using 1 to 5% of flavonoids extracted with ethyl alcohol (CH ₃ CH ₂ OH) as a solvent. And a solid bath is prepared by combining 1: 1 of anhydrous sodium carbonate (Na ₂ CO ₃ ) in the liquid.

The silicate, composed mainly of silicate (SiO ₂ ) with mysterious self-cleaning ability, contains rare minerals, contains abundant far-infrared rays, which are beneficial to the living body, and is beneficial to the skin by the water softening action. It has been used for the treatment of diseases with therapeutic drugs, high blood pressure, blood circulation, and blood circulation promoting action.Recovering healthy skin color and powerful antioxidant action to remove free radicals harmful to our body, preventing skin damage caused by harmful oxygen, blood Improves circulation, improves blood circulation, maintains clear and transparent skin, stabilizes cell membranes, prevents cell damage and prevents blood aging, ginkgo flavone, protects skin aging or dry skin, ginkgetin, and skin Terpenoids to prevent fine lines, flavonoids with excellent skin moisturizing and astringent effects (fl The use of ginkgo biloba extract, such as avonoid, is becoming wider, and this pharmacological action is known to be caused by the flavonoids contained in the ginkgo biloba leaves. Was high. Refreshing bath has fatigue recovery effect, reduces skin cells' elasticity by anti-aging effect of skin cells, prevents fat accumulation by circulating blood in the body, and is excellent in improving skin diseases such as athlete's foot and various make-up poisons. The composition is formulated as a food additive and condensed at high temperature, so it is harmless to the human body even when drinking water or drinking, and is completed by adding various fragrances to give a odor as necessary.

Hereinafter, with reference to the accompanying diagram of the present invention will be described in detail.

1 is a composition chart of the silicate A liquid of the present invention in the preparation of the present invention,

2 is a manufacturing process chart of the present invention.

The composition of the present invention of Figure 1 is 42 to 58 wt% of high purity silica sand or silica (SiO ₂ : 99.9%), 30 to 38 wt% anhydrous sodium carbonate (Na ₂ CO ₃ ), 1 to 1 borax (Na ₂ B ₄ O ₇ ) 3 wt%, sodium pyrophosphate (Na ₄ P ₂ O ₇ ), 10-15 wt%, calcium carbonate 1-2 wt% (CaCO ₃ ) were added to the melting furnace, condensation melted, cooled and solidified, and then placed in an autoclave. put the liquid in which the alkali solution to the solution a, and the Ginkgo biloba is ethyl alcohol (CH ₃ CH ₂ OH) with a solution containing a flavonoid extract with a solvent to 2-4% B liquid a liquid and the B liquid are mixed is prepared It is a bath.

Silica or silica, formed by the solidification of magma, contains rare minerals, contains abundant far-infrared rays, which are beneficial to the living body, and is beneficial to the skin by the water softening action, and anhydrous sodium carbonate (Na ₂ CO ₃ ) In sodium carbonate hot spring water, it is an alkaline source, which has a significant effect on anti-aging, skin care, and fatigue recovery, and is effective for neuralgia, arthritis, hypertension, and liver function improvement. Sodium silicate (Na ₂ SiO ₃ ) is dissolved when dissolved with silica.

Borax (Na ₂ B ₄ O ₇ ) has a weak bactericidal effect on the skin and is used as an antiseptic. Sodium pyrophosphate (Na ₄ P ₂ O ₇ ) is soluble in water, and the aqueous solution is alkaline and strong against thermal hydrolysis. It nourishes and calcium carbonate (CaCO ₃ ) provides calcium nutrition to the skin and gives the silicate melt strength. Ginkgo biloba extract extracted with ethyl alcohol (CH ₃ CH ₂ OH) as a solvent is rich in ginnol, Ginkgolic acid, hydroginkgolinic acid, ginkgetin, iso-ginkgetin, ginkgolide A, methylpyridoxine, ginkgotoxin, and sugars (mainly starch 31.5%). Protein is a lot of high-quality tryptophane. Fat is low and contains some ergosterine. Vitamins A, C and niacin also contain significant amounts. It contains starch, sugar, bentosan, fatty oils, and cytokinin. Ginkgo biloba has been used for various diseases since ancient times, especially as a medicine for improving blood circulation. In particular, it was found that insects do not eat well and bees and fungi do not like ginkgo biloba, and the most important antimicrobial active ingredient was flavonoids. The efficacy of ginkgo biloba leaves consists of a combination of a single active ingredient or multiple active ingredients in the extract, the most important of which are Ginkgo-flavon glycosides and terpenoids (Ginkgolides and bilogalides). Ginkgolides in Ginkgo biloba extract have A, B, and C forms, as well as a small amount of J form. Ginkgolides are not found in other species except ginkgo biloba. They cause platelet aggregation, neutrophil degeneration and free radical production, microvascular permeability and bronchospasm in vivo. In animal studies of cerebral ischemia, Ginkgolides are known to improve brain metabolism and prevent hypoxic brain damage. Heart disease treatment drug, high blood pressure, blood circulation agent, blood circulation promoting action to restore healthy skin color, strong antioxidant action prevents skin damage caused by free radicals, improve blood circulation, improve blood circulation, maintain clear and transparent skin, cell damage by cell membrane stabilization Prevent and prevent aging.

The bathing agents of the present invention are harmless to humans and animals and plants, are nontoxic, odorless, and do not cause pollution problems when they flow into rivers or seas during wastewater, and are environmentally friendly bathing agents in view of the environment.

In the manufacturing process of FIG. 2, the composition is mixed and continuously introduced into an electric furnace or a gas melting furnace, and the melting temperature is 1,400 ° C to 1,500 ° C at 4-5 hours. The solution was dissolved in a pressurized steam of 5 to 6 atm in a high temperature reactor (AUTOCLAVE) to make liquid A. The leaves of Ginkgo biloba were extracted with ethyl alcohol (CH ₃ CH ₂ OH) as a solvent. Mix liquid A and liquid B and add the finished water-soluble liquid bath after checking the content of the product. A mixture of anhydrous sodium carbonate (Na ₂ CO ₃ ) in a liquid bath at a ratio of 1: 1 is poured into a mold, and after 12 hours, it is fixed and dried to become a solid bath. It is packed and put into a solid bath.

Next will be described with an example according to the embodiment of the present invention.

(Example 1)

In the manufacturing process of FIG. 2, the composition is mixed and continuously introduced into an electric furnace or a gas melting furnace, and the melting temperature is 1,400 ° C to 1,500 ° C at 4-5 hours. The solution was dissolved in a pressurized steam of 5 to 6 atm in a high temperature reactor (AUTOCLAVE) to make liquid A. The leaves of Ginkgo biloba were extracted with ethyl alcohol (CH ₃ CH ₂ OH) as a solvent. Mix liquid A and liquid B and add the finished water-soluble liquid bath after checking the content of the product. A mixture of anhydrous sodium carbonate (Na ₂ CO ₃ ) in a liquid bath at a ratio of 1: 1 is poured into a mold, and after 12 hours, it is fixed and dried to become a solid bath. It is packed and put into a solid bath.

Example 2

High purity silica sand or silica powder (SiO ₂ : 99.9%) 45wt%, anhydrous sodium carbonate (Na ₂ CO ₃ ) 40wt%, borax (Na ₂ B ₄ O ₇ ) 2wt%, sodium pyrophosphate (Na ₄ P ₂ O ₇ ) 12 wt% and calcium carbonate 1wt% (CaCO ₃ ) were added to the electric melting furnace to prepare condensation melting at 1,400 ℃ ~ 1,500 ℃ to make colorless transparent glass (SiO ₂ 50.8%), and then to auto-cleave liquefied by SiO ₂ as a solution the addition of distilled water to a 20% solution a solution, and Ginkgo biloba extract in ethyl alcohol (CH ₃ CH ₂ OH) 1 from: a flavonoid 2% solution is extracted with a first solvent to the solution B A liquid and a liquid B were mixed to prepare a liquid bath.

Example 3

High purity silica sand or silica powder (SiO ₂ : 99.9%) 48wt%, anhydrous sodium carbonate (Na ₂ CO ₃ ) 36wt%, borax (Na ₂ B ₄ O ₇ ) 2wt%, sodium pyrophosphate (Na ₄ P ₂ O ₇ ) 13 wt% and calcium carbonate 1wt% (CaCO ₃ ) were added to an electric melting furnace to prepare condensation melting at a temperature of 1,400 ° C to 1,500 ° C to give a colorless and transparent glassy phase (51.9% of SiO ₂ ), followed by auto-cleave. liquefied by SiO ₂ as a solution the addition of distilled water to a 20% solution a solution, and Ginkgo biloba extract in ethyl alcohol (CH ₃ CH ₂ OH) 1 from: a flavonoid 1% solution is extracted with a first solvent to the solution B A and B liquids were mixed to prepare a liquid bath. Anhydrous sodium carbonate (Na ₂ CO ₃ ) was poured into the mold in a 1: 1 combination, and then fixed and dried after 12 hours to prepare a solid bath. .

Example 4

High purity silica sand or silica powder (SiO ₂ : 99.9%) 50wt%, anhydrous sodium carbonate (Na ₂ CO ₃ ) 35wt%, borax (Na ₂ B ₄ O ₇ ) 2wt%, sodium pyrophosphate (Na ₄ P ₂ O ₇ ) 12 wt% and calcium carbonate 1wt% (CaCO ₃ ) were added to the electric melting furnace to prepare condensation melting at 1,400 ℃ ~ 1,500 ℃ to make colorless transparent glass (SiO ₂ 53.5%), and then to auto-cleave liquefied by SiO ₂ as a solution the addition of distilled water to a 20% solution a solution, and Ginkgo biloba extract in ethyl alcohol (CH ₃ CH ₂ OH) 1 from: a flavonoid 1% solution is extracted with a first solvent to the solution B A liquid and a liquid B were mixed to prepare a liquid bath.

Example 5

High purity silica sand or silica powder (SiO ₂ : 99.9%) 53wt%, anhydrous sodium carbonate (Na ₂ CO ₃ ) 33wt%, borax (Na ₂ B ₄ O ₇ ) 2wt%, sodium pyrophosphate (Na ₄ P ₂ O ₇ ) 11 wt% and calcium carbonate 1wt% (CaCO ₃ ) were added to the electric melting furnace to prepare condensation melting at a temperature of 1,400 ° C to 1500 ° C to produce a colorless, transparent glass ((SiO ₂ 55.0%), and then to auto-cleave Solution was added to distilled water to make a solution of SiO ₂ 20%, called solution A. Ginkgo biloba extract was extracted with ethyl alcohol (CH ₃ CH ₂ OH) as a 1: 1 solvent. A and B liquids were mixed to prepare a liquid bath. Anhydrous sodium carbonate (Na ₂ CO ₃ ) was poured into the mold in a combination of 1: 1, and after 12 hours, it was fixed and dried to prepare a solid bath. It was.

Example 6

High purity silica sand or silica powder (SiO ₂ : 99.9%) 55wt%, anhydrous sodium carbonate (Na ₂ CO ₃ ) 30%, borax (Na ₂ B ₄ O ₇ ) 1wt%, sodium pyrophosphate (Na ₄ P ₂ O ₇ ) 13 wt% of calcium carbonate and 1 wt% of calcium carbonate (CaCO ₃ ) were added to an electric melting furnace to prepare a colorless and transparent glassy phase (SiO ₂ 57.7%) by condensation melting at a temperature of 1,400 ° C to 1,500 ° C, followed by an auto-claave. liquefied by SiO ₂ as a solution the addition of distilled water to a 20% solution a solution, and Ginkgo biloba extract in ethyl alcohol (CH ₃ CH ₂ OH) 1 from: a flavonoid 2% solution is extracted with a first solvent to the solution B A liquid and a liquid B were mixed to prepare a liquid bath.

Example 7

High purity silica sand or silica powder (SiO ₂ : 99.9%) 58wt%, anhydrous sodium carbonate (Na ₂ CO ₃ ) 30wt%, borax (Na ₂ B ₄ O ₇ ) 1wt%, sodium pyrophosphate (Na ₄ P ₂ O ₇ ) 10 wt% and calcium carbonate 1wt% (CaCO ₃ ) were added to the electric melting furnace to prepare condensation melting at 1,400 ℃ ~ 1,500 ℃ to make a colorless transparent glass ((SiO ₂ 59.0%), and then auto-claave Solution was added to distilled water to make a solution of SiO ₂ 20%, called solution A. Ginkgo biloba extract was extracted with ethyl alcohol (CH ₃ CH ₂ OH) as a 1: 1 solvent. A and B liquids were mixed to prepare a liquid bath. Anhydrous sodium carbonate (Na ₂ CO ₃ ) was poured into the mold in a combination of 1: 1, and after 12 hours, it was fixed and dried to prepare a solid bath. It was.

In order to evaluate the moisture of the skin, the smoothness of the water, the state of washing the skin, etc., the bath preparation prepared in Example 3 was used as a bathing agent (25cc per 180l bath water, pH 8.3 to 8.9) for 30 female users. After the sample was used five times or more for two weeks, testimonials were collected and the results are shown in Table 1 below.

The results of the safety sensory test were 'very satisfied 5 points', 'satisfaction 4 points', 'normal 3 points', 'slightly dissatisfied 2 points' and 'very dissatisfied 1 point'.

Table 1

As shown in (Table 1), 'water softness and smoothness' and 'hair softness' obtained overall satisfaction, and 'moisture after bathing' and 'freshness after bathing' , 'Eating after bathing' and 'elasticity of skin' items showed high satisfaction with the bathing agent of the present invention.

The bathing agent prepared from the silicate and ginkgo leaf extract of the present invention has a refreshing bath, has a fatigue recovery effect, reduces skin elasticity by preventing skin aging and maintains elastic skin, and prevents fat accumulation by circulating blood in the body. It is excellent in improving skin diseases such as athlete's foot and various crematory poisons.The composition is formulated as a food additive and condensed at high temperature. It is a bathing agent that can have a hot spring effect.

Claims (3)

High purity silica sand or silica powder (SiO ₂ : 99.9%) 42-58 wt%, anhydrous sodium carbonate (Na ₂ CO ₃ ) 30-38 wt%, borax (Na ₂ B ₄ O ₇ ) 1-3 wt%, sodium pyrophosphate (Na ₄ P ₂ O ₇ ) 10-15 wt% and calcium carbonate 1-2 wt% (CaCO ₃ ) were added to the electric melting furnace to prepare a colorless and transparent glass by condensation melting at a temperature of 1,400 ° C. to 1,500 ° C. (SiO ₂ content 40 to 60%) are, again the autoclave (by liquefaction in Auto-cleave) SiO ₂ content as the solution was added to distilled water such that the solution a 14-24% solution, and Ginkgo biloba extract in ethyl alcohol (CH ₃ CH ₂ OH) A liquid bath composition and a method for producing a flavonoid 1% to 5% containing solution extracted as a 1: 1 solvent by mixing B solution, 95% to 99% of A solution and 1% to 5% of B solution. A solid bath composition and a method for preparing a liquid bath composition according to claim 1 and an anhydrous sodium carbonate (Na ₂ CO ₃ ) in a combination of 1: 1. The bath composition according to claim 1, wherein the pH of the bath is adjusted to an alkaline water of 7 to 11.

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