KR100650519B1 - Tabaco Filter - Google Patents
Tabaco Filter Download PDFInfo
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- KR100650519B1 KR100650519B1 KR1020040083026A KR20040083026A KR100650519B1 KR 100650519 B1 KR100650519 B1 KR 100650519B1 KR 1020040083026 A KR1020040083026 A KR 1020040083026A KR 20040083026 A KR20040083026 A KR 20040083026A KR 100650519 B1 KR100650519 B1 KR 100650519B1
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- filter
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- microcapsule
- microcapsules
- tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
- A24D3/10—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/16—Use of materials for tobacco smoke filters of inorganic materials
- A24D3/163—Carbon
Abstract
본 발명은 담배필터에 담배의 독성화합물 및 돌연변이 유발물질을 흡착하기 위해 사용되는 활성탄이 혼입되는 셀룰로오스 아세테이트 섬유 필터에 활성탄과 기능성 물질이 내장된 마이크로캡슐을 일정량 혼합하여 제조하는 기능성 담배필터에 관한 것이다.The present invention relates to a functional tobacco filter prepared by mixing a predetermined amount of activated carbon and a microcapsule containing functional carbon in a cellulose acetate fiber filter in which activated carbon used to adsorb toxic compounds and mutagenic substances of tobacco is adsorbed on the tobacco filter. .
기능성 담배필터. 마이크로캡슐, 향, 필터, 천연추출오일 Functional tobacco filter. Microcapsules, Flavors, Filters, Natural Extraction Oils
Description
도1은 본 발명의 단면도.1 is a cross-sectional view of the present invention.
도2는 본 발명의 다른 실시예도.Figure 2 is another embodiment of the present invention.
<도면의 주요 부분에 대한 부호의 설명><Explanation of symbols for the main parts of the drawings>
마이크로캡슐(1), 활성탄(2), 3중필터(3), 활성탄이 충진되지 않은 필터(4), 엽초(5)Microcapsules (1), activated carbon (2), triple filter (3), filter without activated carbon (4), vinegar (5)
본 발명은 마이크로캡슐을 담배필터에 적용함으로써 흡연자들의 흡연시 발생할 수 있는 입안의 냄새를 제거하고 상쾌함을 줄 수 있는 기능성 담배 필터에 관한 것으로, 구체적으로는 기능성물질이 포접된 수마크로에서 수천마이크로크기의 마이크로캡슐을 셀룰로오스 아세테이트 섬유 필터에 혼입하여 기능성 마이크로캡슐이 들어있는 담배필터를 제조하므로서, 기능성물질의 임의 방출에 의한 손실을 막고 흡연시나 흡연후에만 기능성물질을 방출시킬 수 있도록 개발한 마이크로캡슐을 이용한 기능성 담배필터의 제조방법에 관한 것이다.The present invention relates to a functional cigarette filter that can remove the smell of the mouth that may occur during smoking by the microcapsules to the cigarette filter and gives a refreshing, in particular, thousands of micro size in the water macro containing the functional material Microcapsules were incorporated into the cellulose acetate fiber filter to manufacture tobacco filters containing functional microcapsules, preventing microcapsules from being released by the random release of functional substances and releasing functional substances only during or after smoking. It relates to a method for producing a functional tobacco filter used.
현재 흡연시 향이나는 담배의 경우 엽초에 방향제로 멘톨을 용제에 용해하여 분무하는 방식으로 가향하는 방법을 사용하여 향의 지속 효과를 도모하려 하고 있으나, Currently, in case of smoking cigarettes, the fragrance of tobacco is used as a fragrance by spraying menthol as a fragrance and spraying it with solvent.
예를 들면, 대한민국공개특허공보 공개번호 특2002-0082202호에는 무스콘, 영묘향 또는 그의 혼합물을 함친시킨 기능성 담배필터가 기술되어 있으며, 동 공보 공개번호 제95-005400호에는 박하향 방향성 흡착제를 함유하는 담배필터의 제조방법이 기재되어 있고,For example, Korean Patent Laid-Open Publication No. 2002-0082202 describes a functional cigarette filter incorporating muscon, mausoleum, or mixtures thereof, and Publication No. 95-005400 contains a scented odor adsorbent. The manufacturing method of the tobacco filter is described,
대한민국 등록특허공보 공고번호 10-0193377호에는 담배필터용 입상 복합분자체 조성물의 제조방법이 공개되어 있으나, Korean Patent Publication No. 10-0193377 discloses a method for preparing a particulate composite molecular composition for a cigarette filter.
이러한 방법으로 가향을 하게 되면 기능성 물질이 공기와 노출되어 변형이 일어나거나, 지속력과 시간의 경과에 따라 향취강도가 약해지는 문제가 있다. In this way, there is a problem that the functional material is exposed to the air and the deformation occurs, or the fragrance intensity is weakened over time and over time.
또한, 대한민국등록특허공보 등록번호 10-0301342호(WO1998/15197 ;1998.4.16)에서 담배필터에 캡슐을 이용한 제품으로는 다공성 기재에 피로글루탐산나트륨과 같은 습윤제를 함유시켜 담배연기를 습식여과하여 독성물질을 제거하기위해 사용되어 졌다. In addition, the Korean Registered Patent Publication No. 10-0301342 (WO1998 / 15197; 1998.4.16) as a product using a capsule in the tobacco filter is a toxic by wet filtration of tobacco smoke by containing a wetting agent such as sodium pyroglutamate in the porous substrate It is used to remove material.
그러나 이러한 제품들의 경우 가향제의 휘산량이 증가함에 따라 담배의 사용 수명이 결정된다는 단점을 보유하고 있다.However, these products have a disadvantage in that the service life of the cigarette is determined as the amount of volatilizer is increased.
상기 종래의 기술에 대한 문제점을 해결하고자, 본 출원의 발명은 기능성물질(향, 천연출오일 등)을 화학적 및 물리적인 방법으로 수미크론에서 수천미크론의 크기로 고분자물질 또는 무기물질로 마이크로캡슐화시켜 사용자가 원할 때 마이크로캡슐에 충격을 가하므로서 마이크로캡슐 벽재가 파괴되어 활성성분(향, 천연추출오일 등)이 방출을 일으켜 흡연시나 흡연후에 상쾌감을 제공하기 위한 마이크로캡슐이 혼입된 기능성 담배필터의 제조방법을 제공함에 본 발명의 목적이 있다.
In order to solve the problems of the prior art, the invention of the present application microencapsulates a functional material (fragrance, natural oil, etc.) into a polymer material or an inorganic material in the size of several microns to several thousand microns by chemical and physical methods When the user wants to impact the microcapsules, the microcapsule wall is destroyed and the active ingredient (fragrance, natural extract oil, etc.) is released to produce a functional cigarette filter incorporating microcapsules to provide a refreshing feeling during or after smoking. It is an object of the present invention to provide a method.
상기한 바와 같은 목적을 달성하기 위하여, 본 발명은 폴리비닐알코올(중합도 1700) 10중량부를 증류수 60중량부에 용해시키고, 방향제나 천연추출오일인 내부충전물을 20중량부 가하여 5000~10000rpm에서 3분간 교반한 후, 반응성 우레아수지 10중량부를 가하여 60℃까지 온도를 상승시킨 다음, 2시간 동안 유지하여 마이크로캡슐을 제조하는 과정과;In order to achieve the above object, the present invention dissolves 10 parts by weight of polyvinyl alcohol (polymerization degree 1700) in 60 parts by weight of distilled water, and adds 20 parts by weight of an internal filler, which is a fragrance or natural extraction oil, to 3 minutes at 5000-10000 rpm. After stirring, adding 10 parts by weight of a reactive urea resin to increase the temperature to 60 ℃, and then maintained for 2 hours to prepare a microcapsule;
제조한 마이크로캡슐을 흡입여과 장치를 이용해 분리하여 실온에서 건조하여 마이크로캡슐분말을 분리하는 과정과; 제조한 마이크로캡슐을 셀룰로오스아세테이트 섬유에 활성탄과 함께 분무하여 필터를 제조하거나, 3중 필터의 흡착제층에 활성탄과 마이크로캡슐을 충진하여 마이크로캡슐이 충진된 담배필터를 성형하는 과정으로 이루어지는 기능성 담배필터의 제조방법에 관한 것이다.Separating the prepared microcapsules using a suction filtration apparatus and drying them at room temperature to separate the microcapsule powder; A filter of a functional tobacco filter comprising spraying the prepared microcapsules with cellulose acetate fibers together with activated carbon to form a filter or by filling activated carbon and microcapsules in an adsorbent layer of a triple filter to form a microfilter-filled tobacco filter. It relates to a manufacturing method.
상기 제조방법에서 마이크로캡슐(1)내에 충전되는 기능성물질로는 향 등 천연 추출오일과 합성오일 중의 하나나 이들의 혼합물을 사용한다.In the manufacturing method, as the functional material to be filled in the
또한, 마이크로캡슐(1)을 제조하는 방법으로는 In-suit polymerization법(Core 물질로 오일을 선택해 먼저 유화제가 혼입되어 있는 수계에 유화시킨 후 벽재물질인 멜라민-포름알데히드 수지를 첨가하여 온도와 pH의 조건을 맞추어주면 서서히 반응하여 오일 계면에서 벽재가 성장하는 방법으로 형상된 벽재는 열경화성 수지로 열에 안정하며, 압력에 의해서만 내부 물질의 방출을 유도할 수 있는 방법), 계면중합법, coacervation법(고분자 용액이 서로간의 반응을 유도할 수 있는 염, 금속 또는 pH를 조절함으로써 고분자간의 이온 complex를 일으켜 벽재를 형성하는 방법) 등을 이용하여 제조할수 있으며, 마이크로캡슐의 벽재를 구성할 수 있는 물질로는 멜라민수지, 우레아수지, 우레탄수지, 젤라틴, 전분, 셀룰로오스 및 고비점의 유지를 단독 또는 그의 혼합물을 사용한다.In addition, as a method of preparing the microcapsules (1), in-suit polymerization method (selecting oil as the core material, emulsifying it in an aqueous system in which an emulsifier is mixed, and then adding melamine-formaldehyde resin as a wall material, temperature and pH If the conditions are met, the wall material is slowly reacted and grows at the oil interface.The wall material is thermosetting resin, which is stable to heat, and can induce the release of internal materials only by pressure), interfacial polymerization method, and coacervation method ( It can be prepared using a method of forming a wall material by forming an ionic complex between polymers by adjusting a salt, a metal or a pH that a polymer solution can induce a reaction between each other, and a material capable of forming a wall material of a microcapsule. Melamine resin, urea resin, urethane resin, gelatin, starch, cellulose and high boiling point of the sole or mixture thereof The.
마이크로캡슐(1)내에 충전되는 방향용 물질로 레몬, 박하, 라벤더, 오렌지, 포도, 바닐라, 제라늄, 솔 등 천연 추출오일과 합성오일 중에서 선택된 하나의 화합물이거나, 추출오일에 대해 합성오일을 1-95중량부 로 혼합한 혼합물을 사용하는 것이다.As a fragrance substance filled in the microcapsules (1), it is a compound selected from natural and synthetic oils such as lemon, peppermint, lavender, orange, grape, vanilla, geranium, sol, or synthetic oil. It is to use a mixture of 95 parts by weight.
한편, 도 2의 도시와 같이 마이크로캡슐(1)을 활성탄과 혼합하여 필터를 제조하였을 경우 기능성이 부여된 담배용 필터를 손쉽게 제조할 수 있으며, 기능성을 발휘할 수 있는 시기를 조절할 수 있다는 장점이 있다.On the other hand, as shown in Figure 2, when the filter is manufactured by mixing the microcapsules (1) with activated carbon, it is easy to manufacture a filter for a cigarette given the functionality, there is an advantage that can adjust the time to exhibit the functionality .
이하, 상기와 같은 본 발명 제조방법에 의해 아래와 같이 마이크로캡슐제조에 관한 방법은 멜라민을 이용한 방법을 일예로 들어 설명하였으며, 상기의 마이크로캡슐을 이용해 기능성 담배필터를 제조하였다.Hereinafter, the method for preparing microcapsules according to the present invention as described above has been described by using a method using melamine as an example, to prepare a functional tobacco filter using the microcapsules.
이하 본 발명을 실시예를 통해 상세히 설명하면 다음과 같다.Hereinafter, the present invention will be described in detail with reference to the following Examples.
실시예 1Example 1
제1공정(마이크로캡슐 제조)First step (microcapsule manufacturing)
삼구플라스크에 폴리비닐알코올(중합도 1700) 100g을 증류수 600g에 용해시키고, 내부충전물로 라벤더에서 추출한 오일 200g 을 가하여 5000rpm에서 3분간 교 반한 후 반응성 우레아수지 100g을 가하여 60℃까지 온도를 상승시킨 후 2시간 동안 유지한 다음, 흡인 여과하여 상온에서 건조하여, 다양한 크기(수마이크로에서 수천마이크로)를 갖는 마이크로캡슐을 제조하여 준비한 다음,Dissolve 100 g of polyvinyl alcohol (polymerization degree 1700) in 600 g of a three-necked flask, add 200 g of oil extracted from lavender as an internal filling, stir at 5000 rpm for 3 minutes, and add 100 g of reactive urea resin to raise the temperature to 60 ° C. After maintaining for a period of time, the resultant was filtered by suction, dried at room temperature, and prepared by preparing microcapsules having various sizes (several to several thousand micros),
제2공정(담배필터 제조) 2nd process (tobacco filter manufacture)
상기의 마이크로캡슐을 3중필터 제조시 독성물질을 여과하고 담배의 맛을 좋게하기 위해 사용되는 셀룰로오스 아세테이트 필터와 필터사이에 활성탄을 투입하는 부분에 마이크로캡슐을 일정량 투입하여 마이크로캡슐이 함유된 기능성 담배용 3중필터를 제조하였다.Functional capsule containing microcapsules by inserting a certain amount of microcapsules into a portion in which activated carbon is injected between the cellulose acetate filter and the filter used to filter the toxic substances and improve the taste of cigarettes when the microcapsules are manufactured in the triple filter. A triple filter was prepared.
실시예 2Example 2
상기 실시예1의 제1공정에서 제조한 마이크로캡슐을 담배용 필터의 원료인 셀룰로오스아세테이트 섬유에 마이크로캡슐을 분무투입하여 셀룰로오스아세테이트 섬유에 마이크로캡슐이 골고루 함유된 기능성 담배용 2중필터를 제조하였다.The microcapsules prepared in the first step of Example 1 were spray-injected into the cellulose acetate fibers, the raw material for the tobacco filter, to prepare a dual-use tobacco filter containing microcapsules evenly in the cellulose acetate fibers.
실시예3Example 3
상기 실시예1의 제1공정에서 제조한 마이크로캡슐 10g을 활성탄90g으로 혼합하여, 3중 필터의 활성탄 투입부에 일정량 혼입하여 마이크로캡슐이 함유된 기능성 담배용 3중필터를 제조하였다.10 g of the microcapsules manufactured in the first step of Example 1 were mixed with 90 g of activated carbon, and a predetermined amount was mixed into the activated carbon inlet of the triple filter to prepare a triple filter for functional tobacco containing microcapsules.
실시예4Example 4
삼구플라스크에 스티렌-말렉익 안히드라이드 폴리머(Poly(styrene-maleicanhydride)) 10g를 증류수 700g에 용해시키고, 레몬 오일을 200g 가하여 10000rpm에서 3분간 교반한 후 멜라민 수지 190g을 가하여 60℃까지 온도를 상승시킨 후 2시간 동안 유지하여 마이크로캡슐을 제조하고, 흡인 여과하여 상온에서 건조하여 기능성물질이 함유된 마이크로캡슐을 제조 하는 과정과;10 g of styrene-maleic anhydride (Poly (styrene-maleicanhydride)) was dissolved in 700 g of distilled water in a three-necked flask, 200 g of lemon oil was added, stirred at 10000 rpm for 3 minutes, and 190 g of melamine resin was added to raise the temperature to 60 ° C. Preparing the microcapsules by holding the mixture for 2 hours, and performing suction suction filtration to dry at room temperature to prepare microcapsules containing a functional material;
제조한 마이크로캡슐을 담배용 필터의 원료인 셀룰로오스아세테이트 섬유에 마이크로캡슐을 분무투입하여 셀룰로오스아세테이트 섬유에 마이크로캡슐이 골고루 함유시켜 기능성 담배필터를 제조하였다.The prepared microcapsules were spray-injected into the cellulose acetate fibers which are raw materials for the tobacco filter, and microcapsules were evenly contained in the cellulose acetate fibers to prepare functional tobacco filters.
상기와 같이 본 발명은 흡연시 연기와 같이 흡입되는 독성물질을 여과하는 필터 부분에 기능성물질(향, 추출오일 등)을 함유하고 있는 마이크로캡슐을 수마이크로에서 수천마이크로의 크기로 제조하여 흡연시 발생하는 독성물질을 여과시키거나, 입안의 냄새와 이로인한 거부감을 감소시킬 수 있는 효과를 유도할 수 있는 것이다.As described above, the present invention is produced when smoking microcapsules containing a functional substance (fragrance, extracting oil, etc.) in the filter portion for filtering toxic substances inhaled, such as smoke during smoking, in the size of several micro to several thousand microns. It can induce an effect that can filter out toxic substances or reduce the smell and rejection of the mouth.
이하, 본 발명의 바람직한 실시예를 첨부된 도면을 참조하여 상세히 설명한다.Hereinafter, exemplary embodiments of the present invention will be described in detail with reference to the accompanying drawings.
도 1 은 본 발명의 3중필터에 캡슐을 적용한 단면도이며,
담배의 후면에 위치되는 필터에 있어서, 통상 담배필터인 셀룰로오스아세테이트 섬유에 마이크로캡슐(1)을 분무 투입하여 설치된 마이크로캡슐필터와, 상기 마이크로캡슐필터의 전면에 형성된 활성탄(2)으로 구성된 활성탄필터와,
상기 마이크로캡슐필터의 후면에 설치되며 활성탄이 충전되지 않은 필터(4)로 구성된 3중필터를 도시한 것이다.1 is a cross-sectional view of the capsule applied to the triple filter of the present invention,
A filter located at the rear of a cigarette, comprising: a microcapsule filter installed by spraying a microcapsule (1) into cellulose acetate fibers, which is a tobacco filter, and an activated carbon filter composed of activated carbon (2) formed on the front surface of the microcapsule filter; ,
It shows a triple filter is installed on the rear of the microcapsule filter and composed of a filter (4) is not filled with activated carbon.
도 2 는 본 발명의 이중필터에 마이크로캡슐을 적용한 단면도이다. 도 2의 도시와 같이 필터 내부에 방향제나 기능성물질이 충전된 다수의 마이크로캡슐(1)을 활성탄(2)과 혼합하여 셀룰로오스아세테이트 섬유에 분무하여 섬유 내부에 고르게 분산되도록 분무성형하여 형성한 기능성 담배필터이다.2 is a cross-sectional view of applying a microcapsule to a double filter of the present invention. Functional cigarette formed by spray molding the microcapsules (1) filled with the fragrance or functional material in the filter and activated carbon (2) and sprayed onto the cellulose acetate fibers to be evenly dispersed in the fiber as shown in Figure 2 Filter.
실험예 1 Experimental Example 1
상기 실시예에 따라 제조된 담배필터에서 유해 중금속 검출여부를 실험한 결과 하기 표와 같이 유해 중금속이 전혀 검출되지 않았음을 알 수 있었다.As a result of experiments on the detection of harmful heavy metals in the tobacco filter manufactured according to the above example, it was found that no harmful heavy metals were detected.
표1 유해중금속검출 여부Table 1 Detection of Hazardous Heavy Metals
관능검사Sensory evaluation
상기 실시예에 의해 제조된 기능성 담배필터를 사용한 담배를 30~40대 남녀 각 10명씩을 패널요원으로 무작위 추출하여 기능성 담배필터를 이용하여 흡끽연후의 입맛(텃텃한 맛의 잔상)(A), 끽연시의 향(B), 연기의 향(C)에 관한 관능검사 결 과는 표2과 같다.The tobacco using the functional tobacco filter prepared according to the above example was randomly extracted by a panel agent for each 10 men and women in their 30s and 40s, using a functional tobacco filter, and after taste squeeze (afterimages of savory taste) (A), Table 2 shows the results of the sensory test on smoking (B) and smoke (C).
표2 관능테스트 결과Table 2 Sensory Test Results
아주 좋다 10점, 좋다8~9점, 보통6~7점, 나쁘다 4~5, Very good 10 points, good 8-9 points, usually 6-7 points, bad 4-5,
아주 나쁘다 3점이하.Very bad below 3 points.
이상의 본 발명의 다양한 실시예를 통하여 알 수 있는 바와 같이 본 발명의 실시예 3의 기능성 담배필터에 의해 제조된 담배가 일반 담배와 달리 끽연후의 맛과 향이 특이하여, 일반 끽연자에게 보급하고 소비자의 기호에 맞게 개발한 것으로서 그 맛, 색상 및 향이 일반 담배필터보다 현저하게 개량되어 스트레스 해소에 많은 도움이 줄 것으로 예상된다. As can be seen through various embodiments of the present invention, the cigarette manufactured by the functional tobacco filter of the third embodiment of the present invention has a unique taste and aroma after smoking, unlike general tobacco, so that it can be distributed to general smokers and As it was developed according to taste, its taste, color, and aroma are significantly improved than general cigarette filter, and it is expected to help much in relieving stress.
상기와 같이 본 발명은 기능성물질(향 및 추출오일 등)을 화학적 및 물리적인 방법으로 수미크론에서 수천미크론의 크기로 고분자물질 또는 무기물질로 캡슐화시켜 사용자가 원할 때 외부에 충격을 가하므로서 캡슐이 파괴되어 벽재를 통해 기능성물질(향, 추출오일 등)이 투과되어 흡연시 발생하는 독성물질을 여과시키거 나, 입안의 냄새와 이로인한 거부감을 감소시킬 수 있는 효과를 유도할 수 있는 것이다.
As described above, the present invention encapsulates the functional material (scent and extract oil, etc.) by encapsulating the polymer or inorganic material in the size of several microns to several thousand microns by chemical and physical methods, thereby exposing the capsule to the outside when the user wants. Destroyed and penetrates the functional material (fragrance, extracting oil, etc.) through the wall to filter the toxic substances generated during smoking, or to induce an effect that can reduce the smell and rejection in the mouth.
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