KR100454574B1 - sulfur eliminated noxious ingredient and producing method thereof - Google Patents

sulfur eliminated noxious ingredient and producing method thereof Download PDF

Info

Publication number
KR100454574B1
KR100454574B1 KR10-2002-0045974A KR20020045974A KR100454574B1 KR 100454574 B1 KR100454574 B1 KR 100454574B1 KR 20020045974 A KR20020045974 A KR 20020045974A KR 100454574 B1 KR100454574 B1 KR 100454574B1
Authority
KR
South Korea
Prior art keywords
sulfur
weight
mixed solution
feed
juice
Prior art date
Application number
KR10-2002-0045974A
Other languages
Korean (ko)
Other versions
KR20020074431A (en
Inventor
양복동
Original Assignee
양복동
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 양복동 filed Critical 양복동
Priority to KR10-2002-0045974A priority Critical patent/KR100454574B1/en
Publication of KR20020074431A publication Critical patent/KR20020074431A/en
Application granted granted Critical
Publication of KR100454574B1 publication Critical patent/KR100454574B1/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/02Preparation of sulfur; Purification
    • C01B17/027Recovery of sulfur from material containing elemental sulfur, e.g. luxmasses or sulfur containing ores; Purification of the recovered sulfur
    • C01B17/033Recovery of sulfur from material containing elemental sulfur, e.g. luxmasses or sulfur containing ores; Purification of the recovered sulfur using a liquid extractant

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Fodder In General (AREA)

Abstract

본 발명은 유해성분이 제거된 유황 및 그의 제조방법에 관한 것으로, 참나무 삶은 물 25∼50중량%, 식초 0.1∼0.5중량%, 보릿가루 용액 5∼10중량%, 순무즙 5∼30중량%, 솔잎즙 5∼15중량%와 나머지 양의 물을 혼합하여 혼합용액을 조성하는 단계, 상기 혼합용액에 혼합용액의 전체 중량을 기준으로 35∼40중량%의 유황을 혼합하는 단계, 상기 혼합물을 40∼50℃ 온도로 2∼3시간 동안 저어주면서 숙성시키는 단계, 상기 숙성된 혼합물을 건조시키는 단계를 통하여 제조된 유해성분이 제거된 유황을 사료와 혼합하여 가축에 공급함으로써 항생제등을 투여하지 않고도 면역성을 높이는 효과는 물론 육질이 향상되는 효과를 얻을 수 있을 뿐 아니라, 인체에 복용이 가능하여 해독작용, 통증·염증 완화작용, 혈관팽창작용, 노화방지 및 양기를 회복시켜주는 효과를 얻을 수 있다.The present invention relates to sulfur without harmful components and a method for producing the same, which includes boiled water of oak 25-50% by weight, vinegar 0.1-0.5% by weight, 5-10% by weight of barley flour solution, 5-30% by weight of turnip juice, pine needles 5-15% by weight of the juice and the remaining amount of water to form a mixed solution, 35 to 40% by weight of sulfur based on the total weight of the mixed solution to the mixed solution, the mixture 40 to Aging while stirring for 2 to 3 hours at a temperature of 50 ℃, and drying the aged mixture to remove the harmful components prepared by feeding the feed to livestock to increase the immunity without administering antibiotics, etc. Not only can the effect improve the quality of the meat, but it can also be taken by the human body to help detoxify, relieve pain and inflammation, dilate blood vessels, prevent aging and nourishment. The can get.

Description

유해성분이 제거된 유황 및 그의 제조방법{sulfur eliminated noxious ingredient and producing method thereof}Sulfur eliminated noxious ingredient and producing method

본 발명은 유해성분이 제거된 유황 및 그의 제조방법에 관한 것으로, 더욱 상세하게는 가축류, 가금류 및 양식 어류의 사육을 위한 사료조성물에 함유시켜 성장률 및 면역성을 증가시키며 육질을 개선시킬 수 있는 유해성분이 제거된 유황 및 그 제조방법에 관한 것이다.The present invention relates to sulfur and a method for manufacturing the same, wherein the harmful components have been removed. More particularly, the present invention relates to a feed composition for raising livestock, poultry, and farmed fish, thereby increasing the growth rate and immunity and removing the harmful ingredients that can improve meat quality. Sulfur and a method for producing the same.

축산업계에서는 가축의 생육을 촉진시키기 위한 방법으로 성장촉진제, 항생제, 호르몬제 등을 사용하여 가축의 발육증진을 도모하여 왔는데 이러한 성장촉진제나 호르몬제는 축산 동물로 하여금 화학약품이나 질병에 대한 면역성을 약하게 하여 쉽게 질병에 걸리게 되는 문제점이 있었다.The livestock industry has been promoting growth of livestock by using growth accelerators, antibiotics, and hormones as a way to promote livestock growth. These growth promoters and hormones make livestock animals immune to chemicals and diseases. There was a problem of weakening and becoming easily diseased.

또, 생활수준의 향상과 더불어 건강에 대한 관심이 높아지면서 비만과 동맥경화 등 성인병 예방과 보다 건강한 생활을 위한 다양한 건강식품이 개발되고 있는데, 최근 건강식품의 일종으로 유황에 대한 관심이 더욱 높아지고 있다.In addition, with the improvement of living standards and increasing interest in health, various health foods for preventing adult diseases such as obesity and arteriosclerosis and healthier living are being developed. Recently, interest in sulfur is increasing as a kind of health food. .

유황은 주기율표 제6B족에 속하는 산소족 원소의 하나로, 옛 동의보감에 의하면 열이 많고 독성이 강하나 몸 안의 냉기를 몰아내어 양기 보족을 돕는 한편 심장의 적취(積聚)와 사기를 다스리며, 단독(丹毒)을 풀어준다 라고 쓰여 있다. 또 중국의 고전 문헌에 의하면 유황은 만병(萬病)을 물리친다는 천하의 명약으로 알려진 금단(金丹)의 주원료로서 불로장생의 선약(仙藥)이요 늙은 노인도 젊음을 되찾게 된다는 "회춘의 묘약"으로 전해 내려올 만큼 그에 대한 약성(藥性)의 평가는 대단하다. 또한, 유황은 보양작용뿐 아니라 암과 각종 난치병의 원인으로 대두되고 있는 중금속, 농약, 기타 화공독 등의 공해 해독작용이 뛰어난 것으로 알려져 있다.Sulfur is an element of oxygen group belonging to group 6B of the periodic table. According to the old agreement, it has a lot of heat and toxicity, but it helps drive the nourishment by driving cold air in the body, while controlling the capture and fraud of the heart. It says Also, according to the classical Chinese literature, sulfur is the main ingredient of the forbidden tree known as the medicine of the world that defeats all kinds of diseases. "The evaluation of the weakness of it is great. In addition, sulfur is known to have excellent pollution detoxification effects such as heavy metals, pesticides and other chemical poisons, which are emerging as a cause of cancer and various incurable diseases as well as rejuvenation.

그러나, 광물질 유황은 열독성이 매우 강하여 법제과정(法製過程)이 선행되지 않고서는 내복 할 수 없음은 물론 법제하지 않은 유황을 가축류나 가금류에 급여하는 경우 거의 100% 사멸된다.However, mineral sulfur is very thermally toxic and cannot be surrendered without prior legal process, and nearly 100% of the sulfur is killed when livestock or poultry is fed.

따라서, 종래에는 독물의 취급에 사용되는 사기그릇에 유황을 투입하고 밀봉하여 약 48시간 동안 가열하여 구워낸 후, 이를 분말화 하는 공지된 유황의 법제방법에 따라 유황을 법제하여 독성을 감소시켜 이를 사료의 일부로 급여하여 가축류나 가금류를 사육하여 그로부터 유황성분을 함유하는 식용육을 건강식으로 보급하고 있다.Therefore, conventionally, sulfur is put into a porcelain bowl used for handling poisons, sealed, heated and baked for about 48 hours, and then sulfur is regulated according to a known sulfur legal method of powdering it to reduce toxicity and feed it. As part of the diet, livestock and poultry are raised and edible meat containing sulfur is supplied as a healthy food.

그러나, 이렇게 법제하여 독성을 감소시킨 유황을 가축류나 가금류에 급여하는 경우에도 사멸율이 매우 높기 때문에 급여량에 제한을 두어야 하였다. 종래의 법제된 유황의 급여량은 일반적으로 독성물질에 대해 높은 내성을 갖는 것으로 알려진 오리에 대하여도 1일 최대 10g을 넘지 못하는 것으로 알려져 왔다.However, even in the case of feeding livestock or poultry with sulfur, which has been reduced by the law, the killing rate has to be limited because the mortality rate is very high. Conventional dietary sulfur feed is generally known to not exceed 10 g per day, even for ducks known to have high resistance to toxic substances.

또한, 이러한 종래의 유황의 법제방법 및 법제된 유황을 이용한 사육방법에따르면, 법제된 유황을 사용하여도 사멸율이 최소 30%이상으로 높게 나타나 법제된 유황의 급여량에 상당한 제한이 따르고, 급여된 유황도 거의 2시간 이내에 배설물과 함께 배설되어 잔류효과가 적어지는 등의 문제점이 있었다.In addition, according to the conventional legislation method of sulfur and the breeding method using the sulfur, the mortality rate is high at least 30% even when the legal sulfur is used, which imposes a significant limit on the amount of legal sulfur. Sulfur was also excreted with the excreta within almost 2 hours, such that there was a problem of less residual effect.

본 발명은 전술한 바와 같은 종래의 법제된 유황의 문제점을 해결하기 위한 것으로 가축류, 가금류 및 양식어류에 사료와 함께 급여하더라도 이를 섭취한 동물에 전혀 피해가 없이 안전하게 생육되며 성장률 및 면역성이 증가되는 것은 물론 육질이 개선되는 효과를 나타내는 유해물질이 제거된 유황을 제공하는 것을 목적으로 한다.The present invention is to solve the problems of the conventional legislative sulfur as described above, even when fed with feed to livestock, poultry and farmed fish is safely grown without any damage to the animal ingesting it and the growth rate and immunity is increased Of course, it is an object of the present invention to provide sulfur from which no toxic substances have an effect of improving meat quality.

본 발명의 또 다른 목적은 제조방법이 단순하여 저렴한 비용으로 유해성분이 제거된 유황을 제조할 수 있어 경제적으로 축산업에 이용할 수 있도록 하는 것을 그 목적으로 한다.Still another object of the present invention is to provide a simple method of manufacturing sulfur to remove harmful components at low cost, so that it can be economically used for livestock industry.

본 발명에 의한 유해성분이 제거된 유황은 참나무 삶은 물 25∼50중량%, 식초 0.1∼0.5중량%, 보릿가루 용액 5∼10중량%, 순무즙 5∼30중량%, 솔잎즙 5∼15중량%와 나머지 양의 물로 이루어진 혼합용액과 상기 혼합용액의 전체 중량을 기준으로 35∼40중량%의 유황을 혼합하여 40∼50℃ 온도로 2∼3시간 동안 교반하면서 숙성시킨 후 건조시켜서 제조되는 것을 특징으로 한다.Sulfur from which the harmful components are removed according to the present invention is 25-50% by weight of oak boiled water, 0.1-0.5% by weight of vinegar, 5-10% by weight of barley flour solution, 5-30% by weight of turnip juice, 5-15% by weight of pine needle juice And 35 to 40% by weight of sulfur, based on the total weight of the mixed solution and the mixed solution consisting of the remaining amount of water and aged at 40 to 50 ° C. for 2 to 3 hours with stirring, followed by drying. It is done.

본 발명의 유해성분이 제거된 유황은 참나무 삶은 물 25∼50중량%, 식초 0.1∼0.5중량%, 보릿가루 용액 5∼10중량%, 순무즙 5∼30중량%, 솔잎즙 5∼15중량%와 나머지 양의 물을 혼합하여 혼합용액을 조성하는 단계, 상기 혼합용액에 혼합용액의 전체 중량을 기준으로 35∼40중량%의 유황을 혼합하는 단계, 상기 혼합물을 40∼50℃ 온도로 2∼3시간 동안 교반하면서 숙성시키는 단계, 상기 숙성된 혼합물을 건조시키는 단계를 통하여 제조된다.Sulfur from which the harmful components of the present invention are removed is 25 to 50% by weight of oak boiled water, 0.1 to 0.5% by weight of vinegar, 5 to 10% by weight of barley flour solution, 5 to 30% by weight of turnip juice, 5 to 15% by weight of pine needle juice and Mixing the remaining amount of water to form a mixed solution, and mixing 35-40% by weight of sulfur based on the total weight of the mixed solution with the mixed solution; Aging with stirring for a time, it is prepared through the step of drying the aged mixture.

상기 혼합용액을 조성하는 참나무 삶은 물, 보릿가루 용액, 순무즙, 솔잎즙의 한정된 혼합 법위는 수회의 반복 실험을 통하여 유황으로부터 만족할 정도의 독을 제거할 수 있게 설정된 양으로서, 상기 한정된 양을 초과하거나 그 이하로 하여 혼합용액을 조성할 경우 제독시간이 전체적으로 오래 걸리고 만족할만한 상태로 유해물질이 제거되지 않는다.The limited mixing method of oak boiled water, barley flour solution, turnip juice, and pine needle juice that forms the mixed solution is an amount set to remove satisfactory poison from sulfur through several repeated experiments, and exceeds the limited amount. When the mixed solution is prepared at or below the detoxification time, the detoxification time is long and the harmful substances are not removed in a satisfactory state.

상기 참나무 삶은 물, 식초, 보릿가루 용액, 순무즙, 솔잎즙 및 물로 이루어진 혼합용액에 유황을 혼합시키는 단계에서 40중량%까지는 효과적으로 유해물질이 제거되나, 유황 제독의 경제적인 면과 효율적인 면을 감안하여 35중량% 이상의 유황을 첨가시킨다. 그러나, 40중량% 이상의 유황을 첨가시킬 경우 완성된 유황에서 심하게 역겨운 맛이 나고 유해물질이 만족할 만큼 제거되지 않으므로 복용이 불가능하다. 따라서, 상기 유황 혼합단계에서는 혼합용액 전체의 중량을 기준으로 35∼40중량%의 유황을 첨가시키는 것이 가장 바람직하다.The oak boiled water, vinegar, barley flour solution, turnip juice, pine needle juice and the mixture of sulfur in the step of mixing the sulfur up to 40% by weight effectively removes harmful substances, considering the economic and efficient aspects of sulfur poisoning To add 35% by weight or more of sulfur. However, when 40% by weight or more of sulfur is added, it is impossible to take since the finished sulfur has a bad disgusting taste and harmful substances are not removed to the satisfaction. Therefore, in the sulfur mixing step, it is most preferable to add 35 to 40% by weight of sulfur based on the total weight of the mixed solution.

상기 혼합물을 숙성시키는 단계에서는 40℃이하의 온도로 설정할 경우 숙성이 제대로 되지 않으며 50℃ 이상의 온도로 설정할 경우 식초 성분이 증발하는 등의 용액의 구성성분에 변화가 생기므로 40∼50℃ 온도를 유지시키는 것이 중요하다.In the step of aging the mixture is not properly aged when set to a temperature of 40 ℃ or less, if set to a temperature of 50 ℃ or more because the constituents of the solution, such as evaporation of the constituents evaporate to maintain a temperature of 40 ~ 50 ℃ It is important to let them.

또, 숙성시간은 2시간 이하로 하면 소정의 효과를 얻을 만큼 유황의 독이 제거되지 않으며 3시간 이상부터는 제독 효과가 크게 차이가 나지 않아 3시간 이상 숙성시키는 것은 의미가 없다. 따라서, 숙성시간은 2∼3시간이 가장 바람직하다. 이때, 신속하고 균일한 숙성을 위해 반드시 교반하면서 숙성시킨다.In addition, when the aging time is 2 hours or less, sulfur poisoning is not removed so as to obtain a predetermined effect, and from 3 hours or more, the detoxification effect does not vary significantly, so it is meaningless to ripen for 3 hours or more. Therefore, the aging time is most preferably 2-3 hours. At this time, it is aged with stirring to ensure rapid and uniform aging.

마지막 단계로, 상기 숙성된 혼합물을 건조시켜서 본 발명의 유해성분이 제거된 유황이 완성되는데, 상기 건조단계에서는 상기 숙성된 혼합물을 30분∼1시간가량 방치시켜 하부에는 침전물이 가라앉고 상부에는 맑은 액체가 떠서 상·하부가 분리되도록 하여, 상부에 뜬 맑은 액체는 따라버리고 가라앉은 침전물은 응달에서 수분이 완전하게 증발하도록 건조시키는 것이 좋다. 상기 건조 공정에서는 다양한 방법이 사용될 수 있으나 진공건조기 등의 기기를 사용하여도 무난하다.In the final step, the aged mixture is dried to complete sulfur from which the harmful components of the present invention are removed. In the drying step, the aged mixture is left for about 30 minutes to 1 hour so that a precipitate sinks in the lower part and a clear liquid in the upper part. The upper and lower parts are separated and the clear liquid floating on the top is poured out and the settled precipitate is dried to completely evaporate water in the shade. Various methods may be used in the drying process, but a device such as a vacuum dryer may be used.

상기와 같은 방법으로 제조된 본 발명의 유해성분이 제거된 유황은 기존의 가축용 배합사료와 함께 가축류, 가금류 및 양식어류에 직접 급여할 수 있을 뿐 아니라 인체에 복용도 가능하다.Sulfur from which the harmful components of the present invention prepared by the above method is removed can be directly fed to livestock, poultry, and farmed fish together with conventional feed for livestock, and can also be taken to the human body.

상기 유해성분이 제거된 유황을 섭취한 가축류, 가금류 및 양식어류는 통상 30일 후에는 장기능에 약성이 차고 2개월 후에는 살과 피에 약성이 고루 퍼지며 2개월 이상이 되면 뼈까지 유황성분이 작용하여 강골의 형태가 되는 것을 확인할 수 있다.Sulfur-ingested livestock, poultry, and farmed fish that have had the harmful components removed are usually weak in intestinal function after 30 days, and evenly spread in flesh and blood after 2 months, and the sulfur component acts on bones after 2 months or more. It can be confirmed that the shape of the steel frame.

즉, 본원의 유황을 처리한 가축류, 가금류 및 양식어류는 일반 사료만을 처리한 것 보다 성장속도가 15∼20% 증가하며 면역력이 향상되어 질병 및 전염병 발생률이 거의 없고 특히 양식어류의 경우 피부병 발생이 억제되었으며, 육질이 향상되고 지방질이 감소하는 효과가 있다.In other words, the sulfur-treated livestock, poultry, and farmed fish increased the growth rate by 15-20% and improved immunity compared to the general feed alone, resulting in little disease and infectious disease, especially in the case of farmed fish. It has been suppressed and has the effect of improving meat quality and reducing fat.

이하, 본 발명에 따르는 유해물질이 제거된 유황의 제조방법 및 유해물질이 제거된 유황을 가축에 적용한 실시예를 설명하면 다음과 같다.Hereinafter, a description will be given of an embodiment of applying the sulfur to the method for producing sulfur and the removal of harmful substances according to the present invention to livestock.

<실시예 1><Example 1>

유해물질이 제거된 유황의 제조방법Sulfur production method without harmful substances

(1) 혼합용액 조성단계(1) Mixed solution composition step

물 1ℓ에 참나무 15g을 넣고 1시간 동안 삶아서 식힌 참나무 삶은 물을 준비하였다. 보릿가루 10g을 물 1ℓ에 넣어 혼합한 다음 30분간 방치시켜 침전물을 가라앉히고 상부에 뜬 맑은 액체만을 분리한 보릿가루 용액을 준비하였다. 순무즙은 순무를 갈아서 액체만을 취하였고 솔잎즙은 물 1ℓ에 솔잎 8g을 넣고 1시간 동안 삶아서 준비하였다.15 g of oak was added to 1 l of water, and boiled for 1 hour to prepare boiled oak. 10 g of barley flour was added to 1 L of water, mixed, and allowed to stand for 30 minutes to settle the precipitate and prepare a solution of barley powder separated only from the clear liquid floated on the top. Turnip juice was prepared by grinding turnip and taking only liquid. Pine needle juice was prepared by adding 8g of pine needles to 1ℓ of water and boiling for 1 hour.

상기와 같이 준비된 참나무 삶은 물 40중량%, 식초 0.3중량%, 보릿가루 용액 10중량%, 순무즙 30중량%, 솔잎즙 10중량%와 나머지 양의 물을 혼합하여 혼합용액을 조성하였다.The oak boiled water prepared as described above was mixed with 40% by weight of water, 0.3% by weight of vinegar, 10% by weight of barley flour solution, 30% by weight of turnip juice, 10% by weight of pine needle juice and the remaining amount of water.

(2) 유황 첨가단계(2) sulfur addition step

상기 혼합용액에 혼합용액의 전체 중량을 기준으로 35중량%의 유황을 혼합하였다.35 wt% of sulfur was mixed with the mixed solution based on the total weight of the mixed solution.

(3) 숙성단계(3) aging stage

상기 혼합물을 40℃ 온도로 3시간 동안 교반하며 숙성시켰다.The mixture was aged with stirring at 40 ° C. for 3 hours.

(4) 건조단계(4) drying step

상기 숙성된 혼합물을 30분 동안 방치시켜 하부에는 침전물이 생기고 상부에는 맑은 액체가 떠서 분리되도록 하였다. 상부에 뜬 맑은 액체는 따라버리고 가라앉은 침전물은 응달에서 건조시켰다.The aged mixture was left to stand for 30 minutes to form a precipitate on the bottom and a clear liquid floating on the top to separate. The clear liquid on top was poured out and the settled precipitate was dried in the shade.

상기와 같은 방법으로 제조된 본원의 유해성분이 제거된 처리 유황과 일반 유황은 요업기술원에 의뢰하여 x-ray 촬영 및 비중 측정을 하여 다음과 같이 분석하였다.Sulfur and general sulfur treated with harmful components of the present application prepared by the above method were analyzed by X-ray imaging and specific gravity measurement as requested by the Institute of Ceramics and Technology as follows.

시 료 명Sample Name XRDXRD 비 중importance 일반 유황Common sulfur α-S가 주광물α-S is the main mineral 2.182.18 처리 유황Treated sulfur α-S가 주광물α-S is the main mineral 2.132.13

참고) 1. 상기 XRD 시험에 사용된 기기는 MAC Science제임.Reference) 1. The device used for the XRD test is manufactured by MAC Science.

2. 상기 비중 시험에 사용된 기기는 Micromeritics(U.S.A.) AccupycTM1330임.2. The instrument used for the specific gravity test is Micromeritics (USA) Accupyc 1330.

x-ray 촬영 결과, 본원의 유해성분이 제거된 처리 유황과 일반 유황 모두 α-S가 주광물로 나타나 성분상의 변화는 없는 것으로 보였으나, 일반 유황(1)의 비중은 2.18인 반면 본원의 유해성분이 제거된 유황(2)은 2.13로 처리된 유황의 비중이 감소된 결과가 나타났다. 상기 유황(2)의 감소된 비중은 본 발명에 따른 처리방법에 의하여 유해성분이 제거되었음을 의미한다고 판단되었다.As a result of x-ray imaging, α-S was found to be the main mineral in both treated sulfur and ordinary sulfur from which the harmful component was removed, but the specific sulfur (1) had a specific gravity of 2.18, The removed sulfur (2) resulted in a decrease in the specific gravity of sulfur treated with 2.13. The reduced specific gravity of the sulfur (2) was determined to mean that the harmful component was removed by the treatment method according to the present invention.

<실시예 2><Example 2>

유해물질이 제거된 유황의 적용Application of sulfur without harmful substances

① 실시예1과 같이 하여 제조된 유해물질이 제거된 유황을 밀가루와 1:1 비율로 섞어서 3개월 동안 금붕어에게 먹였다.① Sulfur from which harmful substances prepared in Example 1 were removed was mixed with flour at a 1: 1 ratio and fed to goldfish for 3 months.

일반 유황을 금붕어에게 먹일 경우 바로 죽게 되나 본 발명에 따라 제조된 유황을 먹은 금붕어는 오히려 면역력이 높아졌다.When the general sulfur is fed to goldfish, they die immediately, but the sulfur-fed goldfish prepared according to the present invention has increased immunity.

② 실시예 1에 따른 유해물질이 제거된 유황을 사료 중량의 15% 혼합한 사료와 일반사료 및 유해물질이 제거되지 않은 유황을 사료 중량의 15% 혼합한 기존의 유황사료를 각각 오리가 부화한 후부터 급여하기 시작하여 오리를 사육하였다.(2) Ducks hatched each of the feeds in which noxious substances were removed from sulfur according to Example 1 with 15% of the feed weight, and the conventional feeds containing 15% of the feed weight with non-hazardous feed. Later, he started feeding and kept ducks.

이와 같이 사육된 세 종류의 오리를 비교하여 다음과 같은 결과를 얻었다.Comparison of the three types of ducks raised in this way to obtain the following results.

일반사료를 급여한 오리는 면역성이 약하여 질병 발생률이 잦았으며 폐사율이 10∼15%나 되었고, 오리 특유의 비린내와 누린내가 나고 육질이 질겼으며, 기존의 유황사료를 급여한 오리는 유황의 독으로 인한 치사율이 10∼15%로 일반오리와 비슷하였으나 오리 특유의 비린내가 없어지고 육질이 다소 개선되었으나 탄력이 없었다.Ducks fed general feed had a low immunity and had a high incidence of disease, mortality rate of 10-15%, ducky fishy and stingy, meaty, and conventional sulfur feed ducks with sulfur poison. The mortality rate was 10-15%, which was similar to that of ordinary duck, but the fishy characteristic of duck was disappeared and the meat quality was slightly improved.

반면, 본원의 유해물질이 제거된 유황을 급여한 오리는 유황 자체의 독이 완전히 제거되었기 때문에 이로 인한 치사율이 전혀 나타나지 않았을 뿐 아니라 면역력이 높아져 질병 발생률 및 이로 인한 폐사율이 0%로 놀랄만한 결과를 나타냈다. 또한 오리의 체중이 감소되는 현상이 나타나지 않았고 특유의 누린내가 없었으며 지방질이 감소된 부드럽고 담백한 맛의 고품질 식용육을 얻을 수 있었다.On the other hand, the ducks fed sulfur with no harmful substances of the present application did not show any mortality due to the complete removal of the poison of sulfur itself, and the immunity was increased, resulting in a 0% disease incidence and death rate. . In addition, the weight loss of the duck did not appear, there was no peculiar smell, and a high-quality edible meat with a soft and light taste with reduced fat was obtained.

③ 상기 실시예1과 같이 하여 제조된 유해물질이 제거된 유황을 사료에 10중량% 혼합하여 병아리 때부터 먹이기 시작하여 닭으로 성장할 때까지 공급하였다.③ The sulfur produced by removing the harmful substances prepared in the same manner as in Example 1 was mixed with 10% by weight of the feed and fed from the time of chick feeding until feeding into chicken.

본 발명에 따라 제조된 유황을 먹고 자란 닭은 별도의 성장촉진제 및 항생제를 투여하지 않아도 일반 닭 보다 성장속도가 15∼20% 증가했으며, 면역력이 높아져 질병이 거의 발생하지 않았다. 또, 닭들 또한 유해물질이 제거된 본 발명의 유황을 섞은 사료에 별다른 거부반응을 보이지 않아 유황을 더 많이 먹일 수 있었다.Chickens fed with sulfur produced according to the present invention increased the growth rate by 15 to 20% than normal chickens without the use of separate growth promoters and antibiotics, and the immune system was high, almost no disease occurred. In addition, the chickens could also feed more sulfur because it did not show a rejection reaction to the sulfur-containing feed of the present invention from which harmful substances were removed.

이렇게 키운 닭과 일반 닭의 육질 및 지방질을 비교하였더니, 일반 닭은 비린내가 나며 기름기가 많고 가슴살이 뻑뻑한 질감을 나타낸 반면 본 발명에 따라 제조된 유황을 먹고 자란 닭은 비린내가 전혀 나지 않고 육질이 쫄깃쫄깃하고 연하며 특히 가슴살의 육질은 탄력이 있어 맛이 좋았고 전체적으로 담백한 맛을 냈다.Compared to the meat and fat of the chickens raised in this way and the general chicken, the general chicken has a fishy, greasy, breast-stiff texture, while the chickens produced by eating sulfur according to the present invention does not smell fishy at all It is chewy and tender, especially the flesh of the breast is elastic, so it tastes good and has a light taste overall.

④ 상기 실시예 1의 유해물질이 제거된 유황을 사료에 20중량% 혼합하여 산란계(産卵鷄)에 공급하여 계란을 생산하였다.④ 20% by weight of sulfur removed from the harmful substances of Example 1 was mixed in the feed and fed to the laying hens to produce eggs.

본원의 유황사료를 급여한 산란계와 일반 산란계로부터 생산된 계란을 농촌진흥청 축산기술연구소에 의뢰하여 비교한 결과를 다음과 같이 나타낸다.The results of comparing the egg produced from the sulfur feed and the eggs produced from the normal laying hens to the Rural Livestock Research Institute are as follows.

일반 계란Plain egg 유황사료 급여 계란Sulfur Feed Eggs 성분ingredient 메티오닌(%)Methionine (%) 0.3740.374 0.4250.425 시 스 틴(%)Cysteine (%) 0.3020.302 0.3330.333 황(ppm)Sulfur (ppm) 12.0912.09 26.9126.91 호우 유니트(HU)Heavy rain unit (HU) 44.1344.13 78.6378.63 난각두께(㎜)Eggshell thickness (mm) 0.3810.381 0.3650.365 난황계수Egg yolk coefficient 0.3380.338 0.4490.449

표에서 알 수 있듯이 본원의 유황 사료를 급여하여 생산된 계란은 일반 계란에 비하여 황을 함유한 아미노산인 메티오닌 (methionine)과 시스틴(cystine) 및 황(S)의 함유량이 월등히 높은 결과를 나타내었다.As can be seen from the table, the eggs produced by feeding the sulfur feed of the present application showed a significantly higher content of sulfur-containing amino acids methionine (methionine) and cystine (cystine) and sulfur (S) than normal eggs.

또, 계란은 신선도를 측정하는 호우 유니트(Haugh Unit) 값에 있어서도 본원의 유황 사료 급여 계란은 78.63인 반면 일반 계란은 44.13으로 측정되어 본원의유황 사료 급여 계란의 신선도가 월등함을 알 수 있었다.In addition, in the Haugh Unit value for measuring the freshness of the eggs, the sulfur-feeding eggs of the present application was 78.63, whereas the normal eggs were measured at 44.13, indicating that the sulfur-feeding eggs of the present application were superior in freshness.

또한, 달걀의 신선도를 판정하는 검사방법으로서 달걀을 터트려서 평평한 판 위에 놓고 난황의 최고부의 높이를 난황의 최대직경으로 나눈 값인 난황계수를 이용하는데, 일반적으로 신선한 알의 난황계수는 0.361∼0.442의 범위이며 0.3 이하는 신선하지 않은 것으로 본다.In addition, as an inspection method for determining the freshness of eggs, the egg yolk coefficient is obtained by popping the egg on a flat plate and dividing the height of the highest part of the yolk by the maximum diameter of the yolk. Generally, the egg yolk coefficient of fresh eggs is 0.361 to 0.442. Range and below 0.3 are considered not fresh.

본원의 유황사료를 급여하여 생산된 계란의 난황 계수는 0.449로 측정되었으며 일반 계란은 0.338로 측정되어 본원의 유황사료를 급여하여 생산된 계란의 신선도가 상당히 높음을 알 수 있었다.Egg yolk coefficient of eggs produced by feeding the sulfur feed of the present application was measured to 0.449 and the average egg was measured to 0.338, indicating that the freshness of the eggs produced by feeding the sulfur feed of the present application is quite high.

난각 두께는 본원의 유황사료를 급여하여 생산된 계란은 0.365㎜, 일반 계란은 0.381㎜로 측정되어 일반 계란이 약간 두껍게 나타났으나, 같은 높이에서 낙하실험을 하여 본 결과 난각 강도는 유황사료를 급여하여 생산된 계란이 오히려 더 강한 것으로 나타났다.Egg thickness was 0.365mm for eggs produced by feeding the sulfur feed of our company and 0.381mm for normal eggs, and the average egg was slightly thick. However, dropping strength at the same height resulted in the feeding of sulfur feed. The eggs produced were rather stronger.

또, 본원의 유황사료를 급여하여 생산된 계란은 난황 색이 진하고 탄력이 좋을 뿐 아니라 계란 특유의 비린내도 없었으며 맛도 매우 좋았다.In addition, the egg produced by feeding the sulfur feed of the present application was not only the egg yolk color and good elasticity, but also the unique fishy smell and taste was very good.

⑤ 상기 실시예1의 유해물질이 제거된 유황을 사료에 10중량% 혼합하여 장어에 공급하였다.⑤ 10% by weight of sulfur removed from the harmful substances of Example 1 was mixed with the feed and supplied to the eel.

일반 사료를 급여하여 양식하는 장어는 면역력이 약해 피부병이나 전염병에 쉽게 감염되는 반면 본원의 유황사료를 급여하여 양식한 장어는 성장촉진제나 호르몬제 없이도 성장률이 증가했으며, 별도의 항생제를 투여하지 않았음에도 불구하고 면역성이 증가되어 폐사율이 현저히 줄어들었고 특히 피부병이나 항진균증에 우수한 효과를 나타냈다.The eel farmed by feeding a general feed is weakly immune, and easily infected with skin diseases and infectious diseases, while the eel farmed by feeding the sulfur feed of our company increased the growth rate without growth promoters or hormones, even though no antibiotics were administered. Nevertheless, mortality was significantly reduced due to increased immunity, which was particularly effective in skin disease and antifungal disease.

이와 같은 결과를 토대로 하여 닭은 물론 오리, 돼지, 소, 양어장에 이르기까지 사료첨가제로써 적용한다면 그 효능이 뛰어날 것으로 사료된다.Based on these results, it would be excellent if applied as feed additives to chickens, ducks, pigs, cattle, fish farms.

⑥ 상기 실시예1과 같이 제조된 본원의 유해물질이 제거된 유황을 본원인이 직접 6개월째 복용하고 있다.(6) The applicant directly takes sulfur for 6 months after removing harmful substances of the present application prepared as in Example 1.

본원인은 상기 유황의 복용으로 혈액의 콜레스테롤 수치가 격감되었고 혈압이 떨어지고 장이 편안하며 숙변 제거효과를 볼 수 있었을 뿐 아니라 머리가 빠지지 않고 잠을 잘 잘 수 있다.The present inventors have seen that the cholesterol level of the blood is reduced by taking the sulfur, blood pressure is lowered, the intestine is comfortable, the bowel removal effect can be seen as well as the head can not fall out and can sleep well.

상술한 바와 같은 공정을 거쳐서 제조되는 본 발명의 유해물질이 제거된 유황은 적당량의 사료와 혼합하여 가축에 공급함으로써 항생제등을 투여하지 않고도 면역성을 높이는 효과는 물론 육질이 향상되는 효과를 얻을 수 있을 뿐 아니라, 직·간접적으로 인체에 복용이 가능하여 해독작용, 통증·염증 완화작용, 혈관팽창작용, 노화방지 및 양기를 회복시켜주는 효과를 얻을 수 있다.Sulfur from which the harmful substances of the present invention prepared by the above-described process is removed is mixed with an appropriate amount of feed and supplied to the livestock to increase the immunity without administering antibiotics, as well as improve the meat quality. In addition, it can be taken directly or indirectly to the human body to obtain an effect of detoxification, pain and inflammation relief, vasodilation, anti-aging and restoring yang.

특히 본 발명의 유해물질이 제거된 유황은 그 제조방법이 간단하여 저렴한 가격으로 제조할 수 있어 경제성이 있으며 축산업 분야에 효율적으로 적용이 가능하다.In particular, the sulfur removed the harmful substances of the present invention can be manufactured at a low price due to the simple manufacturing method is economical and can be efficiently applied to the livestock industry.

Claims (2)

참나무 삶은 물 25∼50중량%, 식초 0.1∼0.5중량%, 보릿가루 용액 5∼10중량%, 순무즙 5∼30중량%, 솔잎즙 5∼15중량%와 나머지 양의 물로 이루어진 혼합용액과 상기 혼합용액의 전체 중량을 기준으로 35∼40중량%의 유황을 혼합하여 40∼50℃ 온도로 2∼3시간 동안 저어주면서 숙성시킨 후 건조시켜서 제조되는 것을 특징으로 하는 유해성분이 제거된 유황.Oak boiled water 25-50% by weight, vinegar 0.1-0.5% by weight, 5-10% by weight of barley flour solution, 5-30% by weight of turnip juice, 5-15% by weight of pine needle juice and the remaining amount of water Sulfur from which harmful components are removed, characterized in that it is prepared by mixing 35-40% by weight of sulfur based on the total weight of the mixed solution, aging while stirring at 40-50 ° C. for 2 to 3 hours, and drying. 참나무 삶은 물 25∼50중량%, 식초 0.1∼0.5중량%, 보릿가루 용액 5∼10중량%, 순무즙 5∼30중량%, 솔잎즙 5∼15중량%와 나머지 양의 물을 혼합하여 혼합용액을 조성하는 단계;25-50% by weight of oak boiled water, 0.1-0.5% by weight of vinegar, 5-10% by weight of barley flour solution, 5-30% by weight of turnip juice, 5-15% by weight of pine needle juice and the remaining amount of water Formulating; 상기 혼합용액에 혼합용액의 전체 중량을 기준으로 35∼40중량%의 유황을 혼합하는 단계;Mixing 35-40% by weight of sulfur based on the total weight of the mixed solution with the mixed solution; 상기 혼합물을 40∼50℃ 온도로 2∼3시간 동안 저어주면서 숙성시키는 단계;Aging the mixture while stirring at 40-50 ° C. for 2-3 hours; 상기 숙성된 혼합물을 건조시키는 단계를 특징으로 하는 유해성분이 제거된 유황의 제조방법.Sulfur-free method for producing a sulfur, characterized in that for drying the aged mixture.
KR10-2002-0045974A 2002-08-03 2002-08-03 sulfur eliminated noxious ingredient and producing method thereof KR100454574B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
KR10-2002-0045974A KR100454574B1 (en) 2002-08-03 2002-08-03 sulfur eliminated noxious ingredient and producing method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR10-2002-0045974A KR100454574B1 (en) 2002-08-03 2002-08-03 sulfur eliminated noxious ingredient and producing method thereof

Publications (2)

Publication Number Publication Date
KR20020074431A KR20020074431A (en) 2002-09-30
KR100454574B1 true KR100454574B1 (en) 2004-11-03

Family

ID=27727622

Family Applications (1)

Application Number Title Priority Date Filing Date
KR10-2002-0045974A KR100454574B1 (en) 2002-08-03 2002-08-03 sulfur eliminated noxious ingredient and producing method thereof

Country Status (1)

Country Link
KR (1) KR100454574B1 (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100589714B1 (en) * 2004-12-03 2006-06-19 신일선 Method for neutralinzing poison of sulfur and feed for chicken thereof
KR100665474B1 (en) * 2005-04-14 2007-01-04 박도명 An exclusion method of the virulence of sulfar and the nonpoisonous sulfar
KR20070023315A (en) * 2005-08-24 2007-02-28 이강준 Additive feed of sulfur and method thereof
KR100980707B1 (en) * 2008-02-18 2010-09-07 박운순 The liquefied sulfuric fertilizer with radish juice and the manufacturing method thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR970025419A (en) * 1997-03-28 1997-06-24 김상춘 Sulfur Feed for Ducks
KR19980082030A (en) * 1998-08-17 1998-11-25 김상춘 Chinese herbal medicine including sulfur, manufacturing method of feed containing mineral
KR19980082031A (en) * 1998-08-17 1998-11-25 김상춘 Process for producing sulfur fermented feed
KR20000024651A (en) * 2000-02-25 2000-05-06 신범선 A method of counteracting sulfur's poisonous effects and counteracted sulfur thereof
KR20020016729A (en) * 2000-08-26 2002-03-06 박한동 Manufacturing method and composite of duck feed that materials are the sulfur and mineral matter
KR20030061045A (en) * 2002-01-07 2003-07-18 이상철 Sulfuric water composition detoxified by loess and method of preparing the same

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR970025419A (en) * 1997-03-28 1997-06-24 김상춘 Sulfur Feed for Ducks
KR19980082030A (en) * 1998-08-17 1998-11-25 김상춘 Chinese herbal medicine including sulfur, manufacturing method of feed containing mineral
KR19980082031A (en) * 1998-08-17 1998-11-25 김상춘 Process for producing sulfur fermented feed
KR20000024651A (en) * 2000-02-25 2000-05-06 신범선 A method of counteracting sulfur's poisonous effects and counteracted sulfur thereof
KR20020016729A (en) * 2000-08-26 2002-03-06 박한동 Manufacturing method and composite of duck feed that materials are the sulfur and mineral matter
KR20030061045A (en) * 2002-01-07 2003-07-18 이상철 Sulfuric water composition detoxified by loess and method of preparing the same

Also Published As

Publication number Publication date
KR20020074431A (en) 2002-09-30

Similar Documents

Publication Publication Date Title
Suchý et al. Chemical composition of muscles of hybrid broiler chickens during prolonged feeding
KR100843625B1 (en) Method for safely pork yielding without antibiotic by dietary methyl sulfonyl methane
KR100454574B1 (en) sulfur eliminated noxious ingredient and producing method thereof
SI22407A (en) Application of coenzyme q10 for more effective breeding of animals and obtaining animal tissues with increased content of this coenzyme
Ajiboye et al. Effect of garlic-supplemented diets on growth response, survival, nutrient utilization and body composition of monosex Tilapia zillii
KR100911279B1 (en) Feed mixture for replacing antibiotics
KR100655504B1 (en) Sulfur eliminated method
Saatci et al. Effects of fattening length, feather colour and sex on some traits in native Turkish geese. II. Carcass traits
KR100585970B1 (en) Method for rearing duck and meat therefor
Samanthi et al. Dietary garlic (Allium sativum L.) supplementation on performance, meat quality and lipid profile in broilers
RU2311793C1 (en) Canine fodder and method for its obtaining
JP2561619B2 (en) Egg production method
JP2003339346A (en) Health food preparation and method for producing the same
CN105360688A (en) Chromium containing meat duck feed
CN101248840B (en) Livestock and poultry feed stuff added with equisetum
KR20060011053A (en) Composition of natural selenium fodder for feeding rabbit
JP3285630B2 (en) Chicken feed
RU2806136C1 (en) Method for increasing physiological maturity of meat when fattening broilers
RU2798343C1 (en) Method for improving the quality of meat of broiler chickens
RU2534279C1 (en) Method of feeding meat goslings
PETROV et al. Effect of herbal and immunomodulatory supplements on growth performance and meat quality in broilers
Ayanwale et al. Evaluation of Dietary Garlic (Allium sativum) extract on Growth, Survival and Stress Biomarkers on Heteroclarias fingerlings under Laboratory conditions in Minna, Nigeria
Swickard et al. Palatability of turkeys fed experimental diets containing aureomycin and fish products
Papunidi ORGANOLEPTIC INDICATORS AND TASTE EVALUATION OF BROILER CHICKEN MEAT USING COMPLEXLY ZEOLITE AND MICROWAVE TREATED-FEED, INFECTED WITH MICROTOXINS
Williams The effect of Nutrifen® and Nutrifen Plus® in the diet of Hy-Line layers on production, egg quality and egg shelf life

Legal Events

Date Code Title Description
A201 Request for examination
G15R Request for early opening
A302 Request for accelerated examination
E701 Decision to grant or registration of patent right
GRNT Written decision to grant
FPAY Annual fee payment

Payment date: 20110418

Year of fee payment: 7

LAPS Lapse due to unpaid annual fee