KR100427682B1 - The product composition of a FIR(Far Infrared Ray) energy emitting rubber bed sheet containing mud derived from tourmaline by chemical treatments - Google Patents
The product composition of a FIR(Far Infrared Ray) energy emitting rubber bed sheet containing mud derived from tourmaline by chemical treatments Download PDFInfo
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- KR100427682B1 KR100427682B1 KR10-2001-0026262A KR20010026262A KR100427682B1 KR 100427682 B1 KR100427682 B1 KR 100427682B1 KR 20010026262 A KR20010026262 A KR 20010026262A KR 100427682 B1 KR100427682 B1 KR 100427682B1
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- tourmaline
- mud
- bed sheet
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- chemical treatment
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- 229910052613 tourmaline Inorganic materials 0.000 title claims abstract description 37
- 239000011032 tourmaline Substances 0.000 title claims abstract description 37
- 229940070527 tourmaline Drugs 0.000 title claims abstract description 37
- 238000011282 treatment Methods 0.000 title claims abstract description 16
- 239000000126 substance Substances 0.000 title claims abstract description 14
- 239000000203 mixture Substances 0.000 title claims abstract description 11
- 229920001971 elastomer Polymers 0.000 title claims abstract description 8
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000000843 powder Substances 0.000 claims abstract description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000000853 adhesive Substances 0.000 claims abstract description 8
- 230000001070 adhesive effect Effects 0.000 claims abstract description 8
- 239000012153 distilled water Substances 0.000 claims abstract description 8
- 239000003513 alkali Substances 0.000 claims abstract description 6
- 238000004519 manufacturing process Methods 0.000 claims abstract description 5
- 235000011121 sodium hydroxide Nutrition 0.000 claims abstract description 5
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 claims abstract description 4
- 239000002759 woven fabric Substances 0.000 claims abstract description 4
- 229910021578 Iron(III) chloride Inorganic materials 0.000 claims description 7
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 claims description 7
- 239000002244 precipitate Substances 0.000 claims description 3
- 229920005989 resin Polymers 0.000 claims 2
- 239000011347 resin Substances 0.000 claims 2
- 239000004743 Polypropylene Substances 0.000 claims 1
- 229920000800 acrylic rubber Polymers 0.000 claims 1
- 229920000058 polyacrylate Polymers 0.000 claims 1
- 229920001225 polyester resin Polymers 0.000 claims 1
- 239000004645 polyester resin Substances 0.000 claims 1
- 229920013716 polyethylene resin Polymers 0.000 claims 1
- -1 polypropylene Polymers 0.000 claims 1
- 229920001155 polypropylene Polymers 0.000 claims 1
- 229920005749 polyurethane resin Polymers 0.000 claims 1
- 229920002379 silicone rubber Polymers 0.000 claims 1
- 239000004945 silicone rubber Substances 0.000 claims 1
- 238000001035 drying Methods 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 3
- 238000000227 grinding Methods 0.000 abstract 2
- 238000004898 kneading Methods 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 239000000047 product Substances 0.000 description 13
- 229910052500 inorganic mineral Inorganic materials 0.000 description 8
- 239000011707 mineral Substances 0.000 description 8
- 235000010755 mineral Nutrition 0.000 description 8
- 239000006228 supernatant Substances 0.000 description 7
- 239000011120 plywood Substances 0.000 description 6
- 239000007788 liquid Substances 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- 241000282414 Homo sapiens Species 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 230000032683 aging Effects 0.000 description 3
- 239000000376 reactant Substances 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 208000035475 disorder Diseases 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 239000010977 jade Substances 0.000 description 2
- 239000013049 sediment Substances 0.000 description 2
- 238000012795 verification Methods 0.000 description 2
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- 238000005481 NMR spectroscopy Methods 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 208000002193 Pain Diseases 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 239000003610 charcoal Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000009313 farming Methods 0.000 description 1
- 239000011790 ferrous sulphate Substances 0.000 description 1
- 235000003891 ferrous sulphate Nutrition 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 description 1
- 229910000359 iron(II) sulfate Inorganic materials 0.000 description 1
- 208000032839 leukemia Diseases 0.000 description 1
- 230000009245 menopause Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 208000004296 neuralgia Diseases 0.000 description 1
- 239000000565 sealant Substances 0.000 description 1
- 239000013464 silicone adhesive Substances 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
- 238000004065 wastewater treatment Methods 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/16—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/62222—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining ceramic coatings
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/62605—Treating the starting powders individually or as mixtures
- C04B35/6261—Milling
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- A—HUMAN NECESSITIES
- A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
- A47C—CHAIRS; SOFAS; BEDS
- A47C27/00—Spring, stuffed or fluid mattresses or cushions specially adapted for chairs, beds or sofas
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61N—ELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
- A61N5/00—Radiation therapy
- A61N5/06—Radiation therapy using light
- A61N2005/0658—Radiation therapy using light characterised by the wavelength of light used
- A61N2005/0659—Radiation therapy using light characterised by the wavelength of light used infrared
- A61N2005/066—Radiation therapy using light characterised by the wavelength of light used infrared far infrared
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2103/00—Function or property of ingredients for mortars, concrete or artificial stone
- C04B2103/0068—Ingredients with a function or property not provided for elsewhere in C04B2103/00
- C04B2103/0097—Anion- and far-infrared-emitting materials
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J175/00—Adhesives based on polyureas or polyurethanes; Adhesives based on derivatives of such polymers
- C09J175/04—Polyurethanes
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Ceramic Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Radiation-Therapy Devices (AREA)
Abstract
본발명은 토르마린을 화학처리하여 유도된 머드를 이용한 원적외선 에너지 방출 고무침대시트 제조조성물에 관한 것이다.1. 토르마린을 350메쉬 이상으로 분말화 하는 단계.2. 증류수, 가성소다, 토르마린을 강알카리로 조성 하는 단계.3. 염화철을 가하여 반응시키는 단계.4. 염산으로 중화 및 정치, 생성된 머드 분리단계.5. 분리된 머드 건조 및 분말화 단계.6. 생성된 분말과 탄성의 접착제와 배합혼연단계.7.혼연물을 직조물에 도포부착 단계를 특징으로 한다.The present invention relates to a far-infrared energy-releasing rubber bed sheet manufacturing composition using mud derived from chemical treatment of tourmaline. Powdering tourmaline to at least 350 mesh. 2. 3. Distilled water, caustic soda and tourmaline are prepared with strong alkali. React by adding iron chloride. 4. Neutralize and settle with hydrochloric acid, resulting mud separation step. Separated mud drying and powdering step. 6. 7. Mixing kneading step with the resulting powder and elastic adhesive. 7. Characterizing the step of applying the kneaded material to the woven fabric.
Description
원적외선 에너지 방출물질은 다양하다. 옥(玉)을 소재로한 제품, 참나무숯을 소재로한 제품, 맥반석등 다양하다. 토르마린을 물에 희석 사용하였고, 접착제외 혼합 시트등으로 만드는 정도였다. 그러나 이들 제품의 원적외선 에너지 방출량은 40내지 100㎛정도였다. 가장순도가 높은 옥(玉)을 시험한 결과 약100㎛였다. 적어도 원적외선 에너지 방출량은 100내지 1000㎛ 되어야 한다는 전문의 들의 견해였다. 토르마린 광물이 원적외선 에너지 방출량이 가장 크다는 것을 문헌을 찾아 알수 가 있었다. 토르마린의 순도가 가장 높다는 부라질산으로 연구에 임하였다. 그러나 부라질산 토르마린은 원적외선 에너지 방출량은 높았으나 반면 구입가격이 매우 높아 사용하기에 주저하지 않을수 없었다. 어떻게하면 원료가격을 떨어뜨릴수 있는가에 대하여 연구를 거듭하였다. 토르마린의 그중요 성분을 유지시키면서 액화할 수가 없는가 연구를 거듭한결과 액화에 성공하였다. 액화된 맑은 액의 원적외선 에너지 방출량은 액화전 토르마린 광석의 원적외선 에너지 방출량과 거의 동일 하였다. 매우만족 하였다. 그러나 화학처리에서 발생한 침전물 처리에 매우 고심하였다. 수십번의 실험결과 그침전된 머드에서도 원적외선 에너지 방출량을 높게 할 수가 있었다. 이머드를 시험한 결과 원적외선 에너지 방출량을 높이는 기준을 정하여 처리한후 시험결과 매우 만족하였다. 이 소모되는 머드를 건조 분말로 하여 재사용시 건조비를 감안하더라도 원래 토르마린의 구입가격의 20％ 수준으로 낮출수가 있으며 이머드를 사용하더라도 기존 제품들의 원적외선 에너지 방출량보다 2내지 5배의 우수한 원적외선 에너지 방출 제품을 제조할 수가 있는 획기적인 제조법이라고 할 수가 있는 것이다. 이점이 본발명의 특징인 것이다.Far infrared energy emitters vary. There are various kinds of products, such as jade, oak charcoal and elvan. Tourmaline was diluted with water and used to make a mixed sheet besides adhesive. However, the far-infrared energy emissions of these products ranged from 40 to 100 µm. The highest purity jade was tested and found to be about 100 μm. At least it was the opinion of the practitioners that far-infrared energy emissions should be between 100 and 1000 µm. The literature found that tourmaline minerals have the highest far-infrared energy emissions. The study was conducted with brazilic acid, which is said to have the highest purity of tourmaline. However, tourmaline tourmaline has a high far-infrared energy emission, but the purchase price is very high, so hesitate to use it. Research has been conducted on how to lower raw material prices. Research on whether it is not possible to liquefy while maintaining the important components of tourmaline has succeeded in liquefaction. The far-infrared energy emission of the liquefied clear liquid was almost the same as that of the tourmaline ore before liquefaction. Very satisfied. However, it was very hard to treat sediment from chemical treatment. Dozens of experiments have resulted in higher far-infrared energy emissions in the mud. As a result of testing immud, it was satisfied with the test result after setting the standard to increase far-infrared energy emission. Even if the dry mud is used as a dry powder, the cost can be lowered to 20% of the original purchase price of tourmaline even if the drying cost is considered. It can be said to be a breakthrough manufacturing method that can produce. This is a feature of the present invention.
토르마린의 구조식은 XㆍY9B3Si6O27(OㆍOHㆍF)4로 표시되며 여기서 X는 Ca, Na, K, Mn등의 물질로서 1개 또는 2이상이다. Y는 Mg, Fe, Al, Cr, Mn, Ti, Li 등의 물질로서 1개 또는 2이상이다. 토르마린은 흑, 청, 적, 녹, 자, 백색등의 색상을 가지며 외형으로는 6면을 갖는 결정체이다. 그특성은 부스러지기 쉬우며 수분을 빨아드림을 돕는 붕소를 포함하는 광물이며 전기석이라고도 불리어지고 있다. 또한 미약한 0.O6mA의 전류가 흐르는 광물이다.The tourmaline structural formula is represented by X.Y 9 B 3 Si 6 O 27 (O.OH.F) 4 , wherein X is one, two or more substances such as Ca, Na, K, and Mn. Y is Mg, Fe, Al, Cr, Mn, Ti, Li and the like, one or two or more. Tourmaline is black, blue, red, green, purple, white and other colors. Its properties are brittle, minerals containing boron that help to soak up moisture, and are also called tourmaline. It is also a mineral with a weak current of 0.6 mA.
발명인은 일본에서 발행된 "원적외선과 물"이란 문헌에서 큰 흥미를 가진바 있다. 한골짜기에 있는 농작물은 매우 풍성한 수학을 걷을 수 있었는데 다른골짜기에 있는 농산물은 그러하지 않았다. 인간의 눈으로 보아서는 동일한 곳인데 왜 전자의 골짜기 농사는 풍성한가에 대하여 연구한 결과 풍성한 골짜기에 물은 원적외선 에너지 방출 함량이 높은 물이였다고 하였다. 발명인은 이점에 착안하여 토르마린을 물로 전환 할 수가 있다는 확신을 갖게 되었다. 3개년의 연구를 거듭한 결과 토르마린 광물에서 물을 빼낼수가 있었다. 처음에는 토르마린 분자식에 무었을 첨가하여 액화시킬수 있을까. 강산을 처리하여 보았으나 실패하였다. 강알카리로 처리하였을 때 용해된 처리액을 맑은물로 유도 하는데도 매우 어려웠다. 폐수처리제인 수산화알마늄을 처리하였으나 실패하였다. 수산화칼슘처리에도 실패를 하였다. 황산제일철로 처리 하였을 때 가능성이 보였으나 실패하였다. 염화제일철로 처리하였을 때 가능성이 보였으나 실패하였다. 염화제이철로 처리하였을 때 그 가능성이 있었다. 염화제이철로 다시 연구를 거듭하여 처리하였을 때 원 적외선 에너지 방출량을 확인할 수가 있었다. 토르마린을 시험하였을 때 방사율은 0.906 정도였다. 어떻게 하면 방사율을 높일수 있을가 시험을하였다. 200여회 시험 끝에 방사율 0.913(5-20㎛), 방사에너지(W/㎡ ㎛. 37℃) 3.52x102(습윤상태,37℃) 결과에 이르게 되었다. 매우 만족하였다. 부산물로 취득한 상등액 맑고 투명한 용액에서도 방사율 0.906 및 에지 방출량이 3.65x102(40℃) 매우 만족 하였다. 이유도 한 머드를 건조 분말로 하여 탄성의 접착제와 혼연하여 직조물에 부착 시킨결과 매우 흡족한 제품을 제조할 수가 있어 특허 출원에 이른 것 이다.The inventors are of great interest in the literature entitled "Far Infrared and Water" issued in Japan. Crops in one valley were able to learn abundant mathematics, while crops in another valley were not. The human eye sees the same place, but the study of why the former valley farming is abundant showed that water in the rich valley was water with high far-infrared energy emission. The inventors have been convinced that this can convert the tourmaline to water. After three years of research, it was possible to extract water from tourmaline minerals. At first, what can be added to the tourmaline formula to liquefy it? I tried to process strong acid but failed. When treated with strong alkali, it was also very difficult to induce dissolved treatment solution into clear water. The treatment with wastewater treatment aluminum hydroxide failed. Calcium hydroxide treatment also failed. When treated with ferrous sulfate, the likelihood was seen but failed. When treated with ferric chloride a possibility was seen but failed. This was possible when treated with ferric chloride. When irradiated with ferric chloride again, far infrared energy emission could be confirmed. The emissivity was about 0.906 when the tourmaline was tested. How to increase emissivity was tested. 200 yeohoe test end Emissivity 0.913 (5-20㎛), the radiant energy (W / ㎡ ㎛. 37 ℃ ) 3.52x10 2 led to the (wet state, 37 ℃) results. Very satisfied. The supernatant obtained as a by-product was also very satisfied with emissivity of 0.906 and edge emission of 3.65x10 2 (40 ℃) in a clear and clear solution. The reason is that a mud is mixed with an elastic adhesive and attached to a woven fabric with a dry powder, and thus, a very satisfactory product can be manufactured and the patent application is applied.
1) A용기에 증류수 1500내지 3000중량부를 취하고 여기에 98％ 가성소다 100내지 210중량부를 용해시킨후 토르마린 350메쉬이상의 분말 100내지 300중량부를 투입 1700rpm 교반기로 30분이상 교반 강알카리로 한다. 여기에 염화철 100내지 300중량부를 가하고 교반기로 60분 이상 교반한다. 반응액이 청색에서 갈색으로 완전히 변활 때 반응 종말점으로 하고 12시간이상 정치 숙성시킨다. 여기에 염산을 가하여 ph7내지 10으로 중화시킨다. 여기에 증류수 1500내지 3000중량부를 가하고 교반후 정치 숙성시킨다. 24시간후 반응물의 상등액과 침전액 머드를 분리한다. 이것이 토르마린을 화학처리하여 유도된 머드인 것이다. 이유도 분리된 머드를 농축 건조기에서 건조 분말로 하여 분말머드 80내지 250중량부를 취득한다. 상등액 투명액체 2000내지 6000중량부를 부산물로 취득한다.1) Take 1500 to 3000 parts by weight of distilled water in container A, dissolve 100 to 210 parts by weight of 98% caustic soda, and add 100 to 300 parts by weight of tourmaline 350 mesh or more. Use 1700rpm stirrer for 30 minutes or more with strong alkali. 100 to 300 parts by weight of iron chloride were added thereto and stirred for 60 minutes or more with a stirrer. When the reaction solution completely changes from blue to brown, the reaction end point is allowed to stand for at least 12 hours. Hydrochloric acid is added to neutralize it to ph7-10. 1500 to 3000 parts by weight of distilled water are added thereto, followed by stirring and still aging. After 24 hours, the supernatant of the reactants and the precipitate mud are separated. This is the mud derived from the chemical treatment of tourmaline. The mud separated from the reason is used as a dry powder in a concentrated dryer to obtain 80 to 250 parts by weight of the powder mud. Acquisition of 2000 to 6000 parts by weight of the supernatant clear liquid as a by-product.
2) B용기에 위 취득물 50내지 100중량부를 취하고 여기에 우레탄 접착제 50내지 100중량부를 취하고 잘 혼연시킨다.2) Take 50 to 100 parts by weight of the above material in container B, and add 50 to 100 parts by weight of the urethane adhesive and knead well.
3) 합판을 평평하게 놓은후 직조물 50x50cm를 압핀으로 고정시킨 후 이위에 상기 B혼연물을 고루 편후 로라로 0.5mm 내지 10mm 두께로 편후 로라질하여 24시간 건조 시킨다. 완전히 굳은후 합판과 고무 침대시트를 분리하여 제품으로 한다. 용도에 따라 건조머드 접착제 비율을 20:80, 30:70, 40:60, 50:50 로 다양하게 조정하여 생산한다.3) After placing the plywood flat, the woven fabric 50x50cm fixed with a pushpin, and then the B mixture is evenly unevenly rolled into a 0.5mm to 10mm thick roll and then rolled to dry for 24 hours. After completely hardening, separate the plywood and rubber bed sheet to make the product. Depending on the application, it is produced by adjusting the dry mud adhesive ratio to 20:80, 30:70, 40:60, 50:50.
[실시예 1]Example 1
1) A용기에 증류수 1000g을 취하고 여기에 98％가성소다 50g을 가하여 용해시킨후 부라질산 토르마린 350메쉬 이상의 분말 50g을 가하고 1700 rpm 교반기로 30분이상 교반하여 강알카리로 한후 37보메 염화제2철 80g을 투입 교반시킨다. 30분이상 교반하면 청색반응물이 갈색으로 완전히 변할 때 반응종말점으로 한다. 12시간이상 정치 숙성시킨후 염산 으로 ph 8로 조정후 증류수 1000g을 가하고 30분이상 교반후 정치 숙성시킨다. 정치 24시간후 상등액과 침전물 머드를 분리시킨다. 토르마린을 화학처리하여 유도된 이머드를 농축 건조분말로 취득한다.1) Take 1000g of distilled water in A container, add 50g of 98% caustic soda, dissolve it, add 50g of powder of 350M or more of tourmaline toruccinate, and stir for 30 minutes with 1700rpm stirrer to make strong alkali. 80 g is added and stirred. After stirring for 30 minutes or more, the reaction product becomes an end point when the blue reactant turns completely brown. After aging for more than 12 hours, adjust to ph 8 with hydrochloric acid, add 1000 g of distilled water, and stir for more than 30 minutes. After 24 hours of standing, the supernatant and the sediment mud are separated. The tourmaline is chemically treated to obtain an emulsified extract as a concentrated dry powder.
2) B용기에 우레탄 접착제 50g을 취하고 상기 A용기의 건조머드 50g을 취하고 잘 혼연시킨다.2) Take 50g of urethane adhesive in container B, take 50g of dry mud in container A and mix well.
3) 합판을 평평하게 놓은후 가로세로 50cm 청바지천을 올려놓고 압핀으로 고정시킨후 이위에 2)항 혼연물을 5㎜ 두께로 깐후 로라로 평평하게 로라질한후 건조시킨다. 24시간후 합판과 직조물 고무침대시트를 분리시킨다. 이렇게 제조된 시트를 선반에서 5cm 원형으로 가공하여 제품으로 한다. 이렇게 가공한 원형제품은 견고도가 매우 우수하다. 매트리트 침데시트에 부착하여 상품화 한다.3) Lay the plywood flat and put the 50cm long jeans cloth and fix it with a push pin. Then, place the mixture of 2) above on 5mm thickness and roll it flat with roller and dry it. After 24 hours, the plywood and woven rubber bedsheets are separated. The sheet thus prepared is processed into a 5 cm circle on a shelf to obtain a product. The prototype product processed in this way is very strong. Commercialize it by attaching it to a matrimate needle sheet.
[실시예 2]1) A용기에 증류수 1000g을 취하고 여기에 98％ 가성소다 50g을 취하고 용해시킨다. 여기에 부라질산 토르마린 분말 350메쉬이상 분말 50g을 가하고 1700rpm 이상의 교반기로 강알카리에서 30분이상 용해시킨다. 여기에 염화제일철 10g 과 37보메 염화제이철 60g을 가하여 교반 시킨다. 반응물이 청색에서 갈색으로 완전히 변활 때 반응종말점으로 한다. 12시간 정치 숙성시킨후 염산으로 ph 8.5로 중회시킨후 증류수 1000g을 가하고 잠시 교반후 24시간 정치 숙성시킨다. 정치24시간후 상등액과 침천된 머드를 분리시킨다. 이머드가 토르마린을 화학 처리하여 유도된 머드인 것이다. 이머드를 농축하고 건조하여 분말로 하여 취한다.2) B용기에 실리콘 접착제(실란트) 50g을 취하고 1)항에서 건조분말머드 50g을 취하고 잘 혼연시킨다.3)합판을 평평하게 놓은후 가로세로 50cm 청바지 천을 펴고 압핀으로 고정시킨다. 이위에 2)항의 혼연물을 1mm두께로 편후 로라로 고르게 한후 24시간 건조 시킨다. 24시간후 합판과 고무침대시트를 분리하고 생산품으로 한다. 매우 유연하고 두루마리로 둘둘말아도 구겨지지 않고 보관하가에 좋은 생산품 인 것이다.＜표 1. 실시예 제품 시험＞ [Example 2] 1) 1000 g of distilled water was taken into the A container, and 50 g of 98% caustic soda was dissolved therein. To this, 50 g of tourmaline tormarin powder and 350 g or more of powder were dissolved and dissolved in strong alkali for at least 30 minutes with a stirrer of 1700 rpm or more. 10 g of ferric chloride and 60 g of 37 bome ferric chloride are added thereto and stirred. The reaction endpoint is when the reactant completely changes from blue to brown. After aging for 12 hours, the mixture was repeated with ph 8.5 with hydrochloric acid, and 1000 g of distilled water was added thereto, followed by stirring for 24 hours. After 24 hours, the supernatant and the rested mud are separated. Emud is a mud derived from chemical treatment of tourmaline. 2) Take 50g of silicone adhesive (sealant) in B container and mix 50g of dry powder mud in 1) and mix well.3) Plywood is laid flat Stretch the 50cm jeans cloth and secure it with thumbtacks. The kneaded product of 2) above is rolled up to 1mm thickness and evenly dried by Laura and dried for 24 hours. After 24 hours, plywood and rubber bed sheets are separated and made into products. It is very flexible and is product which is good for storing without being wrinkled even if rolled up. <Table 1. Example Product Test>
토르마린 광물은 최근 연구가 활발하게 진행되고 있는 희귀광물이다. 또한 원적외선 에너지 방출량이 매우 높은 광물인 것이다. 그러나 희귀광물로서 구입 가격이 매우 높은 것이다. 이렇게 고가의 원료를 사용시 제조제품의 원가가 높을 수밖에 없는 것이다. 본발명에서는 토르마린을 화학처리하여 유도된 머드(침전물), 액체(상등액)등을 제조하여 부가가치를 높임으로서 고가의 원료가격 부담을 내리는데 있다. 이렇게 토르마린을 화학처리하여 유도된 물질을 다용도로 사용할수 있도록 하는데 그목적이 있는 것이다. 토르마린의 원래 구입가격을 kg당 100이라할 때 토르마린을 화학처리하여 유도된 액과 머드를 비교할 때 이머드의 가격을 건조비 포함하여 약 20정도로 내릴수 있는 것이다. 토르마린을 화학처리하여 유도된 그액을 음료용으로 국립연구소에서 NMR 분석을 하였을 때 47Hz였다. 보통 수돗물은 약 120 Hz임을 비교할 때 너무나 좋은 물이라고 하였다. 이것은 원적외선 에너지 방출 액이기 때문이 였다. 다음 부가가치의 비교표에서 금액으로는 약 15배, 중량비로는 약 21배의 부가가치가 있음을 알수가 있다. 이결과는 구임 토르마린 원료의 구입 단가를 크게 내릴수 있다는 것이다. 반면 제품의 판매단가를 그만큼 내릴 수 있고 판매경쟁에서 소비자에게 저렴한 제품을 공급 할수가 있는 것이다.＜표 2＞ 부가가치의 비교상기 부가가치의 비교표에서 토로마린 1kg을 화학처리 하여 유도된 생산량은 머드 1kg +상등액 20kg =21kg 의 부가가치(중량)를 올리고 금액으로 환산할시 약 15배에 이른다.Tourmaline mineral is a rare mineral that is being actively researched recently. It is also a mineral with a very high far infrared energy emission. However, as a rare mineral, the purchase price is very high. When expensive raw materials are used, the cost of manufactured products is high. In the present invention, mud (precipitate), liquid (supernatant), etc., derived from chemical treatment of tourmaline are manufactured to increase the added value, thereby reducing the burden of expensive raw material prices. The purpose of this is to make the derived material chemically treated with tourmaline for versatile use. When the original purchase price of tourmaline is 100 per kg, the price of the imumed can be reduced to about 20 including the drying cost when comparing the mud and the mud derived from the tourmaline chemical treatment. The liquid derived from the tourmaline chemical treatment was 47 Hz when subjected to NMR analysis by the National Institute for Beverage. Normally, tap water is too good when compared to about 120 Hz. This is because it is far infrared energy releasing liquid. The following table of added values shows that the value added is about 15 times the amount and about 21 times the weight ratio. The result is a significant reduction in the purchase price of boiled tourmaline raw materials. On the other hand, it is possible to lower the selling price of the product and to supply cheaper products to consumers in the sales competition. In the above added value comparison table, 1 kg of toromarin was produced by chemical treatment, and the amount of the added value (weight) of 1 kg of mud + 20 kg = 21 kg of supernatant is about 15 times.
문헌상의 원적외선 효과는 다음과 같다.The far infrared effect in the literature is as follows.
1) 원적외선이 인체에 접하였을 때 인간이 가지거 있는 제기능을 증진시킨다.1) When far infrared rays come into contact with the human body, it enhances the function of human beings.
2) 암이나 백혈병 세포를 약화시킨다.2) To weaken cancer or leukemia cells.
3) 각기, 신경통등의 통증을 저하시킨다.3) respectively, reduce pain such as neuralgia.
4) 혈액순환 장해, 냉증, 뇌, 심장등 갱년기의 모든 장해를 순화시키는 역할을 한다.4) Blood circulation disorders, cold, brain, heart, etc. It serves to purify all disorders of menopause.
일본국에서는 1996년 토르마린을 식품, 화장품의 첨가물로서 규정하고 있다. 따라서 본 발명품 역시 학계의 인체에 유용한 검증이 요구되며 앞으로 검증에 최선을 다할 것이다.In 1996, tourmaline was defined as an additive in food and cosmetics. Therefore, the present invention also requires useful verification in the human body of academia and will do its best in the future verification.
Claims (8)
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| KR101452973B1 (en) | 2014-06-24 | 2014-10-21 | (주) 케이 앤 지 스틸 | Antimicrobial ceramic and oxide-containing epoxy resin coating having a steel pipe |
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|---|---|---|---|---|
| JPH07149956A (en) * | 1993-11-26 | 1995-06-13 | Kubo Gijutsu Jimusho:Kk | Tourmaline-carrying rubber composition and its production |
| JPH09121996A (en) * | 1995-10-30 | 1997-05-13 | Beam Kogyo Kk | Bedclothes |
| KR970027134U (en) * | 1995-12-01 | 1997-07-24 | 김성줄 | Health Promotion Poultry Mat |
| KR980008254A (en) * | 1995-01-31 | 1998-04-30 | 토시오 스기하라 | Layered fabric mattress |
| JPH11279445A (en) * | 1998-03-31 | 1999-10-12 | Nippon Hanekku:Kk | Paint |
| JPH11335485A (en) * | 1998-05-25 | 1999-12-07 | Tm Techno:Kk | Resin containing tourmaline powder |
| KR20000031317A (en) * | 1998-11-05 | 2000-06-05 | 박주민 | Nonwoven fabric having radiation of far infrared ray and process for producing thereof |
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2001
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Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH07149956A (en) * | 1993-11-26 | 1995-06-13 | Kubo Gijutsu Jimusho:Kk | Tourmaline-carrying rubber composition and its production |
| KR980008254A (en) * | 1995-01-31 | 1998-04-30 | 토시오 스기하라 | Layered fabric mattress |
| JPH09121996A (en) * | 1995-10-30 | 1997-05-13 | Beam Kogyo Kk | Bedclothes |
| KR970027134U (en) * | 1995-12-01 | 1997-07-24 | 김성줄 | Health Promotion Poultry Mat |
| JPH11279445A (en) * | 1998-03-31 | 1999-10-12 | Nippon Hanekku:Kk | Paint |
| JPH11335485A (en) * | 1998-05-25 | 1999-12-07 | Tm Techno:Kk | Resin containing tourmaline powder |
| KR20000031317A (en) * | 1998-11-05 | 2000-06-05 | 박주민 | Nonwoven fabric having radiation of far infrared ray and process for producing thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101452973B1 (en) | 2014-06-24 | 2014-10-21 | (주) 케이 앤 지 스틸 | Antimicrobial ceramic and oxide-containing epoxy resin coating having a steel pipe |
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