KR100398375B1 - A method of manufacturing as-rolled wire rods for - Google Patents

A method of manufacturing as-rolled wire rods for Download PDF

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Publication number
KR100398375B1
KR100398375B1 KR10-1998-0034966A KR19980034966A KR100398375B1 KR 100398375 B1 KR100398375 B1 KR 100398375B1 KR 19980034966 A KR19980034966 A KR 19980034966A KR 100398375 B1 KR100398375 B1 KR 100398375B1
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South Korea
Prior art keywords
steel
wire
strength
rolling
steel wire
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KR10-1998-0034966A
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Korean (ko)
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KR20000015194A (en
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신병현
이덕락
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주식회사 포스코
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    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/06Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of rods or wires
    • C21D8/065Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of rods or wires of ferrous alloys
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/06Surface hardening
    • C21D1/09Surface hardening by direct application of electrical or wave energy; by particle radiation
    • C21D1/10Surface hardening by direct application of electrical or wave energy; by particle radiation by electric induction
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/18Hardening; Quenching with or without subsequent tempering
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/001Ferrous alloys, e.g. steel alloys containing N
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/02Ferrous alloys, e.g. steel alloys containing silicon
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/04Ferrous alloys, e.g. steel alloys containing manganese
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/06Ferrous alloys, e.g. steel alloys containing aluminium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/24Ferrous alloys, e.g. steel alloys containing chromium with vanadium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/28Ferrous alloys, e.g. steel alloys containing chromium with titanium or zirconium

Abstract

본 발명은 자동차 조향장치부품 등에 사용되는 고주파소입용 선재의 제조방법에 관한 것이며; 그 목적은 강성분을 적절히 조정하고 열간선재압연과 냉각조건을 적절히 제어함으로써 소입-소려열처리를 생략하고도 조질강 선재와 동등한 가공특성 및 기계적성질을 나타내는 고강도 고주파소입용 비조질강 선재의 제조방법을 제공함에 있다.The present invention relates to a method for producing a high frequency quenching wire used in automobile steering device parts and the like; The purpose of this method is to manufacture a high-strength high-strength non-coated steel wire that has the same processing characteristics and mechanical properties as steel wire without omitting hardening-treatment heat treatment by appropriately adjusting steel components and controlling hot wire rolling and cooling conditions. In providing.

본 발명은, 중량%로, C:0.30-0.60%, Si:0.10-0.40%, Mn:0.8-2.0%, Cr:0.03-1.0%, V:0.03-0.15%, Ti:0.010-0.040%, Al:0.01-0.10%, P:0.030%이하, S:0.020-0.10%, N:0.005-0.030%와 나머지 Fe 및 기타 불가피하게 함유되는 불순물로 조성되는 강을 1000-1150℃로 가열하여 열간선재압연하고 코일형태로 권취한다음, 550-750℃ 구간을 0.1-1.0℃/sec의 속도로 냉각한 후, 5.0-30%의 단면감소율로 냉간인발하여 이루어지는 고주파소입용 비조질강선재의 제조방법에 관한 것을 그 기술적요지로 한다.The present invention is, in weight%, C: 0.30-0.60%, Si: 0.10-0.40%, Mn: 0.8-2.0%, Cr: 0.03-1.0%, V: 0.03-0.15%, Ti: 0.010-0.040%, Hot wire material by heating steel with Al: 0.01-0.10%, P: 0.030% or less, S: 0.020-0.10%, N: 0.005-0.030% and the remaining Fe and other unavoidable impurities to 1000-1150 ℃ After rolling and winding in the form of a coil, the 550-750 ° C section is cooled at a rate of 0.1-1.0 ° C / sec, and cold drawn at a cross-sectional reduction rate of 5.0-30%. Make that technical point.

Description

고주파 소입용 비조질강선재의 제조방법{A METHOD OF MANUFACTURING AS-ROLLED WIRE RODS FOR }Manufacturing method of non-coarse steel wire for high frequency quenching {A METHOD OF MANUFACTURING AS-ROLLED WIRE RODS FOR}

본 발명은 자동차 조향장치부품 등에 사용되는 고주파소입용 선재의 제조방법에 관한 것으로, 보다 상세히는 열간선재압연후 행하는 소입-소려열처리를 생략한 비조질강 선재의 제조방법에 속한다.BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for manufacturing high frequency quenched wire rods used in automobile steering device parts and the like, and more particularly, to a method for manufacturing non-coated steel wire rods without the hardening-treatment heat treatment performed after hot wire rolling.

선재는 다양한 기계부품류에 이용되고 있으며 일례로 도 1에 도시된 자동차 조향장치의 기어샤프트인 랙바(10)에도 적용되고 있다. 선재를 랙바로 이용하기 위해서는 치차(齒車)를 형성하기 위해 선재를 절삭가공한 다음, 치차부위에 내마모성을 부여하기 위하여 고주파소입열처리 및 소려열처리를 하여야 한다. 보통 고주파소입열처리하여 제품에 이용되는 선재를 고주파소입용 선재라 하며, 이 선재는 냉간가공성(절삭가공성 및 드릴링 가공성)과 고주파소입성 및 기계적특성이 무엇보다 중요하다.Wire rods are used in various mechanical parts and are also applied to the rack bar 10, which is a gear shaft of the automobile steering apparatus shown in FIG. In order to use the wire rod as a rack bar, the wire rod should be cut to form gears, and then subjected to high frequency quenching heat treatment and sorrow heat treatment to give abrasion resistance to the gear portion. Usually, the wire used for high frequency quenching heat treatment is called high frequency quenching wire, and cold wire workability (cutting workability and drilling workability), high frequency quenchability and mechanical properties are important.

고주파소입용 선재로는 통상 아래 표 1에 나타낸 기계구조용 탄소강인 S45C가 많이 이용되고 있으며, 그 제조방법은 강을 열간선재압연한 다음 적정한 강도와 인성을 확보하기 위해 소입-소려열처리한 후 냉간인발하고 있다. 이와 같이 소입-소려 열처리하여 제조되는 선재를 조질강선재라 한다.S45C, a mechanical structural carbon steel shown in Table 1, is commonly used as a high-frequency hardened wire rod, and the manufacturing method is cold drawn after hot-rolled steel, followed by quenching-treating heat treatment to secure proper strength and toughness. Doing. As such, the wire produced by quenching-seal heat treatment is referred to as a tempered steel wire.

강종Steel grade 화학조성(중량%)Chemical composition (% by weight) CC SiSi MnMn PP SS S45CS45C 0.42-0.480.42-0.48 0.15-0.350.15-0.35 0.60-0.900.60-0.90 0.030이하Less than 0.030 0.035이하Less than 0.035

한편, 70년대 중반부터 유럽 및 일본을 중심으로 상기와 같은 소입-소려 열처리를 생략하여 원가절감을 획기적으로 꾀할 수 있는 비조질강 선재가 개발되어 널리 사용되고 있다.On the other hand, since the mid-70s, non-coarse steel wire rods have been developed and widely used in Europe and Japan, which can significantly reduce cost by eliminating the hardening-seal heat treatment.

비조질강 선재는 합금설계를 적절히 하고, 제어압연 및 제어냉각을 통해 고강도 고인성 소재를 제조함으로써 열간단조 또는 냉간단조후에 뒤따르는 소입-소려 열처리공정을 생략할 수 있도록 개발된 강이다. 비조질강 선재로는 일본 공개특허공보84-136420호 및 일본 공개특허공보 95-54040호에 제안된 기술을 예로 들 수 있다.Non-coated steel wire is a steel that has been developed so that the alloy design is appropriate and high strength tough material is manufactured through controlled rolling and controlled cooling to omit the quenching-thinning heat treatment process following hot forging or cold forging. Examples of the non-coarse steel wire include the techniques proposed in Japanese Patent Application Laid-Open Nos. 84-136420 and 95-54040.

일본 공개특허공보 84-136420호에 개시된 강은 종래의 기계구조용 탄소강 대비 망간(Mn) 함량을 증가시켜 인성의 저하없이 강도증가를 꾀하는 한편, 석출경화 원소인 바나듐(V)을 약 0.1% 내외 첨가하여 열간단조후 냉각과정에서 페라이트 기지조직내에 바나듐탄질화물[V(CN)]을 미세하게 석출시킴으로써 강도증가를 도모함으로써 뒤따르는 소입소려 열처리공정의 생략을 가능케 한 것이다.Steel disclosed in Japanese Unexamined Patent Publication No. 84-136420 increases manganese (Mn) content compared to conventional carbon steel for mechanical structure to increase strength without deterioration of toughness, and adds about 0.1% of vanadium (V), a precipitation hardening element. Therefore, during the hot forging, the vanadium carbonitride [V (CN)] is finely precipitated in the ferrite matrix to increase the strength, thereby eliminating the subsequent hardening and annealing process.

그런데, 이 선재의 경우에는 열간단조 가공을 통하여 특정형상의 부품을 만드는 소재로 사용하기에는 적합하나, 절삭가공성이나 드릴링(drilling) 가공성이 좋지 않으므로 냉간가공용 소재로 사용하기에는 부적합하다.However, this wire rod is suitable to be used as a material for making a specific shape part through hot forging, but it is not suitable for use as a cold work material because of its poor machinability or drilling ability.

또한, 일본 대동특수강 주식회사에서 개발하여 일본 공개특허공보 94-54040호에 제안한 비조질강 선재는, 냉간가공성을 향상시키기 위해 탄소(C)함량을 매우 낮추고 또 조직미세화를 통한 강의 강도와 인성을 개선시키기 위해 니오븀이 소량 첨가된 것이다. 이 비조질강 선재는 냉간신선 및 압조용 소재로 사용하기에는 적합하나 쾌삭성원소가 함유되지 않아 절삭가공용으로 사용하기에 부적합하며 또한 탄소함량이 낮아 고주파소입성도 좋지 않다.In addition, the non-coarse steel wire developed by Daedong Special Steel Co., Ltd. and proposed in Japanese Laid-Open Patent Publication No. 94-54040 improves the strength and toughness of the steel by significantly lowering the carbon content and improving the microstructure in order to improve cold workability. Niobium is added in small amounts. This non-coated steel wire is suitable for use in cold drawing and forging materials, but it does not contain free cutting elements, which makes it unsuitable for cutting. It also has low carbon content and poor high frequency quenchability.

지금까지 제안된 비조질강선재는 소입-소려열처리를 생략하여 원가절감을 꾀할 수는 있으나, 절삭가공성 또는 고주파소입성이 좋지 않아 고주파소입용 선재로 사용할 수 없다는 문제가 있다.So far, the proposed non-coated steel wire can reduce cost by omitting quenching-concern heat treatment, but there is a problem in that it cannot be used as a wire for high frequency quenching due to poor cutting processability or high frequency hardening.

본 발명자들은 상기와 같은 선행기술들이 갖는 문제점들을 해결함으로써 열간압연재를 소입-소려처리하지 않고 바로 냉간인발 및 절삭가공을 한후 고주파소입으로 표면강화처리를 하여 제작하는 자동차 부품용 비조질강 선재를 개발하기 위해 연구와 실험을 행하고 그 결과에 근거하여 본 발명을 제안하게 이르렀다.The present inventors have developed a non-manufactured steel wire rod for automobile parts which is manufactured by performing surface hardening by high frequency quenching after cold drawing and cutting without hot-rolled material by hardening and treating the hot rolled material. In order to do so, studies and experiments have been carried out and the present invention has been proposed based on the results.

본 발명은 강성분을 적절히 조정하고 열간선재압연과 냉각조건을 적절히 제어함으로써 소입-소려열처리를 생략하고도 조질강 선재와 동등한 가공특성 및 기계적성질을 나타내는 고강도 고주파소입용 비조질강 선재의 제조방법을 제공하는데, 그 목적이 있다.The present invention provides a method for producing a high-strength non-coated steel wire for high-frequency quenching that exhibits the same processing characteristics and mechanical properties as those of a crude steel wire without omitting hardening-treatment heat treatment by appropriately adjusting steel components and controlling hot wire rolling and cooling conditions. To provide, the purpose is.

도 1은 자동차 조향장치의 개략도1 is a schematic diagram of a vehicle steering apparatus

도 2는 발명강의 미세조직사진.Figure 2 is a microstructure photograph of the invention steel.

상기 목적을 달성하기 위한 본 발명의 비조질강 선재의 제조방법은, 중량%로, C:0.30-0.60%, Si:0.10-0.40%, Mn:0.8-2.0%, Cr:0.03-1.0%, V;0.03-0.15%, Ti:0.010-0.040%, Al:0.01-0.10%, P:0.030%이하, S:0.020-0.10%, N:0.005-0.030%와 나머지 Fe 및 기타 불가피하게 함유되는 불순물로 조성되는 강을 1000-1150℃로 가열하여 열간선재압연하고 코일형태로 권취한다음, 550-750℃ 구간을 0.1-1.0℃/sec의 속도로 냉각한 후, 5.0-30%의 단면감소율로 냉간인발하여 구성된다.In order to achieve the above object, the manufacturing method of the non-coated steel wire of the present invention, in weight%, C: 0.30-0.60%, Si: 0.10-0.40%, Mn: 0.8-2.0%, Cr: 0.03-1.0%, V ; 0.03-0.15%, Ti: 0.010-0.040%, Al: 0.01-0.10%, P: 0.030% or less, S: 0.020-0.10%, N: 0.005-0.030% and the remaining Fe and other unavoidable impurities The resulting steel is heated to 1000-1150 ℃, hot rolled and coiled, then cooled to 550-750 ℃ at a rate of 0.1-1.0 ℃ / sec. It is constructed by drawing.

상기와 같이 냉간인발한 선재는 절삭가공을 하고 마지막으로 고주파 소입 및 소려처리를 실시하여 표면을 경화시킨다.As described above, the cold drawn wire is subjected to cutting and finally subjected to high frequency quenching and thinning to harden the surface.

이하, 본 발명을 상세히 설명한다.Hereinafter, the present invention will be described in detail.

본 발명은 선재의 절삭성을 확보하기 위해 [S]을 적정수준으로 관리하는 한편, 기계적성질을 확보하기 위해 기타 성분을 적절히 제어하는 데 그 특징이 있는 것으로, 이를 각 성분별로 설명하면 다음과 같다.The present invention is characterized in that [S] is managed at an appropriate level to secure the cutting property of the wire rod, while appropriately controlling other components to secure mechanical properties, which will be described for each component as follows.

상기 탄소(C)는 소재의 강도를 결정짓는 주요원소이다. 탄소함량이 너무 낮은 경우에는 필요강도의 확보가 불가능하고 너무 높은 경우에는 필요한 인성 및 연성의 확보가 불가능하므로 탄소의 함량은 0.30-0.60%로 제한하는 것이 바람직하다.The carbon (C) is a major element that determines the strength of the material. If the carbon content is too low, it is impossible to secure the required strength. If the carbon content is too high, the required toughness and ductility cannot be secured. Therefore, the carbon content is preferably limited to 0.30-0.60%.

규소(Si)는 고용강화에 의한 강도증가 효과를 얻기 위해 0.40% 까지 첨가하나 그 이상 첨가되면 소재의 표면탈탄이 발생하게 된다. 그리고 필요강도를 확보하고 또 탈산을 충분히 해주기 위해서 0.10%이상 첨가하는 것이 바람직하다.Silicon (Si) is added up to 0.40% in order to increase the strength by solid solution strengthening, but if it is added more than that, surface decarburization of the material occurs. In order to ensure the required strength and to sufficiently deoxidize, it is preferable to add 0.10% or more.

망간(Mn)은 소입성증가 및 고용강화 효과에 의하여 강의 강도를 증가시키기 위해0.8%이상 첨가하나 2.0%이상 첨가될 경우 인성을 감소시킨다. 따라서, 인성을 크게 저하시키지 않고 필요강도를 얻기 위해서는 상기 망간의 함량은 0.8-2.0%로 한정하는 것이 바람직하다.Manganese (Mn) is added more than 0.8% to increase the strength of steel due to the increase in hardenability and solid solution, but decreases the toughness when added more than 2.0%. Therefore, in order to obtain the required strength without significantly reducing the toughness, the content of the manganese is preferably limited to 0.8-2.0%.

크롬(Cr)은 양호한 소입성을 확보하기 위해 필요한 원소로서 특히 기지조직을 강화하여 강도를 증가시키고 또한 내마모성과 내부식성을 개선시킨다. 이러한 효과를 얻기 위해서는 0.03%이상 첨가할 필요가 있지만 1.0%이상 첨가되면 인성이 저하되고 소재의 가격이 비싸지므로 첨가범위를 0.03-1.0%로 제한하는 것이 바람직하다.Chromium (Cr) is an element necessary to ensure good quenching properties, in particular, to strengthen the matrix structure to increase the strength and also improve the wear resistance and corrosion resistance. In order to obtain such an effect, it is necessary to add 0.03% or more, but when it is added more than 1.0%, toughness is lowered and the price of the material is expensive, so it is preferable to limit the addition range to 0.03-1.0%.

바나듐(V)은 강중에서 탄소 및 질소와 결합하여 바나듐탄질화물을 형성한다. 냉각과정에서 생성되는 미세한 바나듐탄질화물은 강도향상에 매우 효과적이다. 필요한 효과를 얻기 위해서는 최소한 0.03%이상 첨가할 필요가 있지만 0.15%이상 첨가되면 강도가 필요이상 증가하고 인성 및 연성이 저하되기 때문에 첨가범위를 0.03-0.15%로 제한하는 것이 바람직하다.Vanadium (V) combines with carbon and nitrogen in steel to form vanadium carbonitrides. The fine vanadium carbonitride produced during the cooling process is very effective in improving the strength. In order to obtain the required effect, it is necessary to add at least 0.03% or more, but if it is added more than 0.15%, the strength is increased more than necessary and the toughness and ductility are lowered. Therefore, it is preferable to limit the addition range to 0.03-0.15%.

티타늄(Ti)은 강중에서 질소와 결합하여 티타늄질화물을 형성한다. 티타늄질화물은 재가열과정에서 오스테나이트 입성장을 억제시켜 강의 충격인성을 개선시킨다. 티타늄첨가량이 너무 적으면 티타늄질화물의 절대량이 적어 효과적으로 입성장을 억제시키기 곤란하고 첨가량이 일정량을 넘으면 효과가 포화되거나 오히려 감소하게 된다. 따라서 적정 첨가량은 0.010-0.040% 범위가 바람직하다.Titanium (Ti) combines with nitrogen in steel to form titanium nitride. Titanium nitride improves the impact toughness of the steel by inhibiting austenite grain growth during reheating. If the amount of titanium added is too small, the absolute amount of titanium nitride is difficult to effectively inhibit grain growth, and if the amount exceeds a certain amount, the effect is saturated or rather reduced. Therefore, the appropriate addition amount is preferably in the range of 0.010-0.040%.

알루미늄(Al)은 탈산을 위하여 첨가하며 또한 알루미늄질화물을 형성시켜 오스테나이트를 미세화하여 강의 충격인성을 개선시키기 위해 첨가한다. 첨가량이 적으면 필요로 하는 효과를 얻지 못하고, 첨가량이 많으면 효과가 포화되므로 첨가량은 0.01-0.10%범위로 제한하는 것이 바람직하다.Aluminum (Al) is added for deoxidation and also to form aluminum nitride to refine the austenite to improve the impact toughness of the steel. If the added amount is small, the required effect is not obtained. If the added amount is large, the effect is saturated. Therefore, the added amount is preferably limited to the range of 0.01-0.10%.

인(P)은 오스테나이트 결정입계에 편석되어 인성을 저하시키므로 그 상한을 0.030%로 제한하는 것이 바람직하다.Phosphorus (P) is segregated at the austenite grain boundary and degrades toughness, so the upper limit is preferably limited to 0.030%.

황(S)은 강중에서 망간과 결합하여 망간황화물을 형성한다. 망간황화물은 강의 쾌삭성을 향상시킨다. 이러한 효과를 얻기 위해서는 0.020%이상 첨가하는 것이 바람직하다. 그러나, 황은 충격인성을 저하시키므로 그 상한을 0.10%로 제한하는 것이 바람직하다.Sulfur (S) combines with manganese in the steel to form manganese sulfide. Manganese sulfide improves the free machinability of steel. In order to acquire such an effect, it is preferable to add 0.020% or more. However, since sulfur reduces impact toughness, it is preferable to limit the upper limit to 0.10%.

질소(N)는 강중에서 티타늄, 바나듐, 알루미늄과 결합하여 티타늄질화물 바나듐질화물 및 알루미늄 질화물을 형성하여 강도와 인성을 개신시킨다. 첨가량이 적으면 이러한 효과를 얻을 수 없고 첨가량이 지나치게 많으면 효과가 포화되므로 첨가범위는 0.005-0.030%가 바람직하다.Nitrogen (N) combines with titanium, vanadium and aluminum in steel to form titanium nitride vanadium nitride and aluminum nitride, thereby improving strength and toughness. If the addition amount is small, such an effect cannot be obtained. If the addition amount is too large, the effect is saturated, so the addition range is preferably 0.005-0.030%.

상기와 같은 조성되는 강을 재가열하여 열간선재압연 하는데, 이때의 재가열온도는 1000-1150℃가 바람직하다. 그 이유는 재가열온도가 1000℃이상이 되어야 조대하게석출된 바나듐질화물을 재고용시킬 수 있으며, 1150℃를 넘으면 오스테나이트가 조대해지고 탈탄이 심해지기 때문이다.Reheating the steel composition as described above is hot wire re-rolling, the reheating temperature is preferably 1000-1150 ℃. The reason for this is that the reheating temperature of 1000 ° C or higher can re-introduce the coarse precipitated vanadium nitride, and if it exceeds 1150 ° C, the austenite becomes coarse and the decarburization becomes severe.

상기와 같이 재가열한 후 열간선재압연하고 코일형태로 권취한 다음 냉각하는데, 이때의 냉각은 상변태 구간인 550-750℃을 0.1-1.0℃/sec의 냉각속도로 냉각시키는 것이 바람직하다. 냉각속도가 0.1℃/sec 보다 느리면 페라이트와 펄라이트 조직이 너무 조대하여져서 강도와 인성을 떨어뜨릴 뿐만 아니라 냉각과정에서 석출되는 바나듐탄질화물도 너무 성장하여 강도증가에 효과적으로 기여하지 못하게 된다. 그리고 냉각속도가 1.0℃/sec 이상으로 빨라지게 되면 저온변태조직이 생성되어 강을 취약하게 만든다.After reheating as described above, the hot wire is re-rolled and wound in a coil form, and then cooled. In this case, it is preferable to cool the phase transformation section at 550-750 ° C. at a cooling rate of 0.1-1.0 ° C./sec. If the cooling rate is slower than 0.1 DEG C / sec, the ferrite and pearlite structures become too coarse to reduce the strength and toughness, and the vanadium carbonitride precipitated during the cooling process is too grown to effectively contribute to the strength increase. And when the cooling rate is faster than 1.0 ℃ / sec is generated low temperature transformation tissue makes the steel vulnerable.

이와 같은 방법으로 제조한 선재는 선재표면에 압축잔류응력을 발생시켜 주기 위하여 최종제품의 치수에 맞도록 냉간인발을 실시하는데 이때의 단면감소율은 5.0-30%로 하는 것이 바람직하다.Wire rods manufactured in this way are cold drawn to fit the final product dimensions in order to generate compressive residual stresses on the wire surface.

냉간인발을 마친 선재는 적당한 길이로 절단한 후 필요한 절삭가공을 거친 뒤 표면을 고주파소입 및 소려처리로 경화시켜 준다.After the cold drawing, the wire is cut to the appropriate length, and after the necessary cutting process, the surface is hardened by high frequency quenching and thinning treatment.

이하, 본 발명을 실시예를 통하여 보다 구체적으로 설명한다.Hereinafter, the present invention will be described in more detail with reference to Examples.

[실시예 1]Example 1

본 발명의 실시예에 적용된 발명강 및 종래강의 화학성분은 아래 표 2와 같다.Chemical compositions of the inventive steel and conventional steel applied to the embodiment of the present invention are shown in Table 2 below.

구분division 화학조성(중량%)Chemical composition (% by weight) 비고Remarks CC SiSi MnMn PP SS CrCr MoMo AlAl VV NbNb TiTi NN 발명강Invention steel 0.450.45 0.240.24 0.190.19 0.0160.016 0.0440.044 0.080.08 -- 0.0320.032 0.100.10 -- 0.0160.016 0.0150.015 종래강1Conventional Steel 1 0.430.43 0.250.25 0.850.85 -- 0.0250.025 0.130.13 -- -- 0.100.10 -- -- 0.010.01 일본 특개84-136420Japanese Patent Laid-Open 종래강2Conventional Steel 2 0.150.15 0.250.25 1.151.15 -- -- 0.120.12 0.020.02 -- 0.110.11 0.0150.015 -- -- 일본 특개95-54040Japanese Patent Laid-Open

표 2와 같이 조성되는 강을 가열로에 장입하여 1시간 30분 동안 가열한 후 추출하였으며, 이때의 추출온도는 1050℃였다. 추출된 강을 열간선재압연기를 이용하여 직경 25, 27, 30mm로 압연한 후 코일형태로 권취하였다. 권취한 선재는 냉각설비를 이용하여 550-750℃ 구간을 냉각속도 0.25-0.30℃/sec로 냉각시켰다.The steel, as shown in Table 2, was charged into a heating furnace, heated for 1 hour and 30 minutes, and extracted. At this time, the extraction temperature was 1050 ° C. The extracted steel was rolled to a diameter of 25, 27, 30mm using a hot wire rolling mill, and then wound in a coil form. The wound wire rod was cooled in a 550-750 ° C. section at a cooling rate of 0.25-0.30 ° C./sec using a cooling system.

상기와 같이 열간선재압연 및 조정냉각을 완료한 본 발명강의 미세조직을 도 2에 나타내었다.2 shows a microstructure of the inventive steel that has completed hot wire rolling and adjusted cooling as described above.

도 2에 나타난 본 발명강은, 베이나이트와 같이 재질에 유해한 저온변태조직은 존재하지 않고 미세한 페라이트와 펄라이트로 구성된 양호한 미세조직을 보이고 있다.The steel of the present invention shown in FIG. 2 shows a good microstructure composed of fine ferrite and pearlite without the presence of low temperature transformation tissue harmful to the material such as bainite.

또한, 상기와 같이 열간선재압연을 마친 상태에서 발명강 및 종래강의 선경별 인장강도 및 경도실적을 아래 표 3에 나타내었다.In addition, the tensile strength and hardness performance of the invention steel and conventional steel by wire diameter in the state of finishing hot wire rolling as described above are shown in Table 3 below.

구분division 인장강도(kg/mm2)Tensile Strength (kg / mm 2 ) 연신율(%)Elongation (%) 경도(HRc)Hardness (HRc) 충격치(kg.m/cm2)Impact value (kg.m / cm 2 ) 발명강Invention steel 86-9686-96 12-1812-18 21.4-24.321.4-24.3 5.5-7.05.5-7.0 종래강 1Conventional Steel 1 85-9085-90 12-1412-14 15.7-22.215.7-22.2 5.0-6.05.0-6.0 종래강 2Conventional Steel 2 69-7869-78 17-2217-22 15.2-20.515.2-20.5 7.0-9.07.0-9.0

상기 표 3에 나타난 바와 같이, 본 발명에 따라 제조된 발명강이 종래강에 비해 기계적성질이 향상되는 것을 알 수 있다.As shown in Table 3, it can be seen that the mechanical properties of the inventive steel produced according to the present invention are improved compared to the conventional steel.

상기와 같이 본 발명에 따라 코일상태로 권취한 선재를 냉간상태에서 5-15% 정도의 감면율로 냉간신선한 다음, 일정길이로 절단하였다. 이후 선재의 한쪽면에 치차가공을 하고 선재중심부를 길이 방향으로 드릴 가공을 하여 자동차 조향장치 부품인 랙바를 제조하였다. 축부와 치차부의 표면은 내마모성을 개선시키기 위해 고주파 소입소려 열처리를 실시하였다. 본 발명에 따라 제조된 랙바의 물성치를 기존 소입소려 열처리한 선재(조질강선재)의 물성치를 규격치로 하여 아래 표 4에 함께 나타내었다.As described above, the wire wound in the coil state was cold drawn in a cold state at a reduction rate of about 5-15%, and then cut to a predetermined length. After that, gear processing was performed on one side of the wire rod and the wire rod center was drilled in the longitudinal direction to manufacture a rack bar which is a vehicle steering device part. The surface of the shaft and the gear was subjected to high frequency quenching and heat treatment to improve wear resistance. The physical properties of the rack bar manufactured according to the present invention are shown together in Table 4 below as standard values of the properties of the wire rod (tempered steel wire) subjected to heat treatment.

구분division 규격standard 발명강Invention steel 소재직진도Material straightness 0.40/1000mm이하0.40 / 1000mm or less 0.26/1000-0.30/1000mm0.26 / 1000-0.30 / 1000mm 브로치(Broach)가공 후 휨방향Bending direction after broach processing 정방향Forward direction 정방향Forward direction 치부경도(HRc)Dental Hardness (HRc) 58-6258-62 58.5-59.058.5-59.0 축부경도Shaft hardness 55-6455-64 60-6160-61

상기 표 4에 나타난 바와 같이, 본 발명강이 기존 조질강 선재에 비해 랙바의 물성치가 동등이상임을 알 수 있었다.As shown in Table 4, it can be seen that the inventive steel has an equivalent physical property or higher than that of the existing tempered steel wire.

상술한 바와 같이, 본 발명은 원가절감 및 제조공정이 단순화되는 고주파소입용 비조질강선재의 제조방법을 제공할 수 있으며, 제공된 비조질강선재는 자동차 랙바 등에 적용될 수 있는 유용한 효과가 있는 것이다.As described above, the present invention can provide a method for manufacturing high-frequency annealed nonferrous steel wire that is cost-saving and simplifies the manufacturing process, and the provided non-ferrous steel wire has a useful effect that can be applied to automobile rack bars and the like.

Claims (1)

중량%로, C:0.30-0.60%, Si:0.10-0.40%, Mn:0.8-2.0%, Cr:0.03-1.0%, V:0.03-0.15%, Ti:0.010-0.040%, Al:0.01-0.10%, P:0.030%이하, S:0.020-0.10%, N:0.005-0.030%와 나머지 Fe 및 기타 불가피하게 함유되는 불순물로 조성되는 강을 1000-1150℃로 가열하여 열간선재압연하고 코일형태로 권취한다음, 550-750℃ 구간을 0.1-1.0℃/sec의 속도로 냉각한 후, 5.0-30%의 단면감소율로 냉간인발하여 이루어지는 고주파소입용 비조질강선재의 제조방법.By weight%, C: 0.30-0.60%, Si: 0.10-0.40%, Mn: 0.8-2.0%, Cr: 0.03-1.0%, V: 0.03-0.15%, Ti: 0.010-0.040%, Al: 0.01- Steel wire composed of 0.10%, P: 0.030% or less, S: 0.020-0.10%, N: 0.005-0.030% and the remaining Fe and other unavoidable impurities are heated to 1000-1150 ° C for hot wire re-rolling and coil shape. After winding in the 550-750 ℃ section at a rate of 0.1-1.0 ℃ / sec, and then cold drawn at a cross-sectional reduction rate of 5.0-30% of the high-frequency quenching amorphous steel wire manufacturing method.
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Publication number Priority date Publication date Assignee Title
JPH0432514A (en) * 1990-05-30 1992-02-04 Nippon Steel Corp Production of soft wire rod free from surface abnormal phase in as-rolled state
KR20000041269A (en) * 1998-12-22 2000-07-15 이구택 Method for producing wire rod for shaft having excellent shock property
KR20010060772A (en) * 1999-12-28 2001-07-07 이구택 A non qt steel having superior strength and toughness and a method for manufacturing wire rod by using it

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0432514A (en) * 1990-05-30 1992-02-04 Nippon Steel Corp Production of soft wire rod free from surface abnormal phase in as-rolled state
KR20000041269A (en) * 1998-12-22 2000-07-15 이구택 Method for producing wire rod for shaft having excellent shock property
KR20010060772A (en) * 1999-12-28 2001-07-07 이구택 A non qt steel having superior strength and toughness and a method for manufacturing wire rod by using it

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