KR100373986B1 - Method for preparing rice wine(Yakju) adding spiced-alcohol - Google Patents

Method for preparing rice wine(Yakju) adding spiced-alcohol Download PDF

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KR100373986B1
KR100373986B1 KR10-2002-0018914A KR20020018914A KR100373986B1 KR 100373986 B1 KR100373986 B1 KR 100373986B1 KR 20020018914 A KR20020018914 A KR 20020018914A KR 100373986 B1 KR100373986 B1 KR 100373986B1
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alcohol
wine
yakju
alcoholic beverages
fermented
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KR20020034124A (en
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권상일
김형식
박병태
한승수
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대한민국
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/04Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
    • C12G3/06Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with flavouring ingredients
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/02Preparation of other alcoholic beverages by fermentation
    • C12G3/021Preparation of other alcoholic beverages by fermentation of botanical family Poaceae, e.g. wheat, millet, sorghum, barley, rye, or corn
    • C12G3/022Preparation of other alcoholic beverages by fermentation of botanical family Poaceae, e.g. wheat, millet, sorghum, barley, rye, or corn of botanical genus Oryza, e.g. rice
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12HPASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/02Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
    • C12H1/06Precipitation by physical means, e.g. by irradiation, vibrations
    • C12H1/063Separation by filtration
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12HPASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/22Ageing or ripening by storing, e.g. lagering of beer

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Abstract

본 발명은 약주 제조방법을 다양화하고 약주 본래의 맛과 향을 유지하면서 제조비용을 절감할 수 있도록 조미주정을 제조하여 이를 약주 숙성술덧(또는 여과약주)에 첨가하는 제조방법이다. 약주에 주정을 단순히 첨가하면 제조비용은 절감할 수 있으나, 주정을 첨가한 만큼 약주 본래의 맛과 향이 감소함으로 이를 보완하기 위하여 주정 첨가로 인하여 감소되는 약주의 향미성분을 정밀 분석하여 감소한 양만큼 아미노산류, 퓨젤유 등 향미성분을 주정에 혼화하여 조미주정을 제조하고, 쌀 (또는 밀가루)을 원료로 발효가 완료된 약주 숙성술덧에 숙성술덧의 알코올분과 같도록 조정한 조미주정을 첨가하는 증양약주의 제조방법에 관한 것이다.The present invention is a manufacturing method for manufacturing a seasoning alcohol so as to reduce the manufacturing cost while diversifying the production method and maintaining the original taste and aroma of the medicine and add it to the wine wine aged (or filtered wine). Manufacturing costs can be reduced by simply adding alcohol to Yakju, but the original taste and aroma of Yakju decreases as much as alcohol is added. Preparation of seasoned alcoholic beverages by mixing flavors such as liquor and fusel oil into alcoholic beverages, and adding flavored alcoholic beverages adjusted to be the same as alcohol content of aged alcoholic beverages in fermented fermented rice wine with fermented rice (or flour) as raw materials It is about a method.

Description

조미주정을 이용한 증양약주 제조방법{Method for preparing rice wine(Yakju) adding spiced-alcohol}Method for preparing medicinal herb wine using seasoning alcohol {Method for preparing rice wine (Yakju) adding spiced-alcohol}

약주제조에 있어서 종래의 통상적인 제조방법은 쌀이나 밀가루 등을 증자하여 국균을 접종, 입국을 제조하고 입국으로 밑술 제조와 1단담금을 한 후 증미를 넣어 2단담금을 하여 발효시킨 다음 여과하여 제성하고 있으나,Conventional manufacturing method in the production of medicine is inoculated with rice or wheat flour to inoculate the Korean bacterium, prepare the entry, prepare the sake brewing and enter the single-dose after entering the fermentation, and add fermentation with two-stage dipped fermentation and then filter it. I'm holy,

본 발명은 약주 숙성술덧에 가격이 저렴한 조미주정을 첨가하면서도 약주 본래의 맛과 향을 유지할 수 있도록 제조하는 원가 절감형 증양약주 제조방법이다.The present invention is a cost-saving type increase in the production of medicinal herbs to maintain the original taste and aroma of Yakju while adding low-cost seasoning spirits to aged wine sake.

쌀을 원료로 발효한 약주 숙성술덧에 주정첨가로 인하여 감소되는 향미성분을 정밀 분석한 후 정제한 주정에 감소된 양만큼의 향미성분인 아미노산, 포도당, 물엿, 젖산을 인위적으로 첨가하여 조미주정을 제조하고 이를 숙성술덧의 알코올분으로조정하여 혼화하는 방법이다.After thoroughly analyzing the flavor components reduced by the addition of alcohol to fermented Yakju fermented with rice as a raw material, seasoning alcohol was artificially added to the refined alcohol by adding amino acids, glucose, syrup, and lactic acid, which are reduced amounts. It is a method of mixing and adjusting it to alcohol content of aging wine.

주정을 첨가하면서도 약주 본래의 맛과 향을 유지하기 위해서는 조미주정의 제조가 중요하다. 먼저 주정 특유의 주정취를 제거하기 위하여 활성탄을 첨가하여 무미·무취가 되도록 하고 주정 첨가로 인하여 감소되는 약주 고유의 향미성분을 정밀 분석하여 감소되는 양만큼의 향미성분 중 주류에 이로운 향미성분만을 선택하여 주정에 첨가하여 조미주정을 제조한다.In order to maintain the original taste and aroma of Yakju while adding alcohol, it is important to prepare seasoned alcohol. First of all, in order to remove alcoholic odors, activated carbon is added to make it tasteless and odorless, and by analyzing the flavors inherent in Yakju reduced by the addition of alcoholic beverages, only the flavors that are beneficial to alcoholic beverages are selected. Seasoning alcohol is prepared by adding to alcohol.

이 조미주정을 숙성술덧의 알코올분과 같도록 조정하여 숙성술덧에 혼화하고 여과, 제성하면 약주 본래의 맛과 향을 느끼면서도 원가절감과 제조공정을 단축하는 약주를 개발할 수 있다.By adjusting the seasoning alcohol to be the same as the alcohol content of aging wine, blending, filtering, and forming it, it is possible to develop a medicine that reduces the cost and manufacturing process while feeling the original taste and aroma of the wine.

도1은 쌀 입국으로 밑술 및 1차 발효시킨 술덧에 증미(덧밥)를 넣고 2차 발효시킨 숙성술덧에 조미주정을 첨가하는 제조방법을 나타낸 공정도이며,1 is a process diagram showing a manufacturing method of adding seasoning alcohol to the fermented rice wine after adding fermented rice (sadded rice) to the rice wine which has been fermented and first fermented with rice.

도2는 주정을 활성탄으로 정제한 후 아미노산류와 퓨젤유 등을 첨가하는 조미주정의 공정도이다.2 is a process diagram of seasoning alcohol in which the alcohol is purified with activated carbon and then amino acids and fusel oil are added.

원료미 중 25%를 수세, 침지, 증자하여 36∼38℃로 식힌 후 종국(種麴)을 파종하여 입국(粒麴)을 제조하고, 제조된 입국의 5.4%에 고체효모, 젖산, 물을 가하여 밑술을 제조, 1일간 발효한 후 나머지 입국과 물을 가하여 1단담금하고 25℃에서 2∼3일간 발효시킨다. 1단담금한 술덧에 나머지 원료미를 수세, 침지, 증자하고 물과 함께 2단담금하여 25℃에서 4∼5일간 발효시킨 숙성술덧을 가스크로마토그래피, 아미노산 분석기 등으로 알코올분, 산도, 아미노산도, 총당분, 퓨젤유 등의 성분을 1차 분석하였다. 이와는 별도로 숙성술덧에 주정을 알코올분 총량으로 환산하여 숙성술덧과 주정의 비율을 1:1 및 1:2로 혼화한 후 같은 방법으로 가스크로마토그래피, 아미노산 분석기 등을 이용하여 알코올분, 산도, 아미노산도, 총당분, 퓨젤유등의 성분을 2차로 분석하고 1차 분석 데이터와 2차 분석 데이터를 비교하여 주정을 첨가함으로서 감소된 숙성술덧의 향미성분 양을 주정에 첨가하여 만든 조미주정을 숙성술덧에 첨가하는 방법에 대하여 연구한 결과 본래의 약주 특유의 맛을 가질 뿐만 아니라 소비자가 원하는 맛을 낼 수 있으면서도 제조원가를 절감할 수 있는 약주를 발명하게 되었다.25% of the raw rice is washed, immersed and increased in water, cooled to 36 ~ 38 ℃, and then seeded (국) to make an entry. 5.4% of the prepared entry contains solid yeast, lactic acid, and water. After the addition of fermented liquor, fermented for 1 day, the rest of the immigration and water were added, and then quenched in 1 stage and fermented at 25 ℃ for 2-3 days. 1-dip dipped with the remaining raw rice washed, immersed, increased with water and immersed two-stage with water and fermented at 25 ℃ for 4-5 days alcohol gas, acidity, amino acid degree by gas chromatography, amino acid analyzer, etc. , Primary sugars, fusel oil and other components were analyzed first. Separately, the alcohol content is converted to the total alcohol content in the fermentation broth, and the ratio between the fermentation broth and the alcohol is mixed at 1: 1 and 1: 2. The seasoning alcohol made by adding the flavor component of the aged fermentation powder to the alcohol by reducing the amount of flavor, total sugar, fusel oil, etc. by secondary analysis and comparing the primary analysis data with the secondary analysis data. As a result of the research on the method of addition, the inventors have invented a medicine that can not only have a taste unique to the original medicine, but can also produce a desired taste while reducing the manufacturing cost.

(실시예)(Example)

비교예 1 :[표1]은 담금배합표로서 백미(또는 소맥분)을 증자한 증미에 백국균(Aspergillus Kawachii)을 접종하여 제조한 입국 100g에 물 140㎖, 고체효모 2.5g 젖산 0.75㎖를 첨가하여 1일간 발효시켜 밑술을 제조하고, 이 밑술에 입국 1,150g과 물 1,750㎖을 넣어 1단담금하여 2∼3일간 발효시킨 후, 여기에다 원료처리·증자한 백미(또는 소맥분) 3,750g과 누룩 100g, 물 6,110㎖를 가하여 2단담금하여 4일간 발효시켜 알코올분 15.2%의 숙성술덧 13,500㎖를 얻었다. 이 숙성술덧에 물 2,050㎖를 가하여 알코올분을 13%로 조정한 후 가스크로마토그래피 및 아미노산분석기 등을 이용하여 퓨젤유[표2]와 각종 아미노산 등[표3]을 정량분석하였다. Comparative Example 1: [Table 1] As a immersion table, 140 ml of water and 0.7 g of lactic acid 2.55 lactic acid were added to 100 g of inoculation prepared by inoculating Bacillus agar (Aspergillus Kawachii) into the rice cooked with white rice (or flour) It is fermented for 1 day to make a base liquor, 1,150 g of entry into the base liquor and 1,750 ml of water are added to it and fermented for 1 to 2 days, followed by 3,750 g of white rice (or wheat flour) and 100 g of malt, 6,110 ml of water was added thereto, and the resultant was immersed in two stages and fermented for 4 days to obtain 13,500 ml of alcohol content of 15.2%. 2,050 ml of water was added to the ethanol to adjust the alcohol content to 13%, followed by quantitative analysis of fusel oil [Table 2] and various amino acids [Table 3] using gas chromatography and amino acid analyzers.

비교예 2 :주정을 정제하기 위하여 95%주정 10,000㎖에 활성탄소 15g을 첨가하여 1일간 방치 후 물 63,076㎖를 가하고 여과하여 알코올분 13% 73,000㎖를 얻었다. Comparative Example 2 In order to purify the alcohol, 15 g of activated carbon was added to 10,000 ml of 95% alcohol, and after standing for 1 day, 63,076 ml of water was added and filtered to obtain 73,000 ml of alcohol content 13%.

실시예 1 :비교예1(원료 :쌀)로 제조한 알코올분 13% 숙성술덧 5,000㎖에 비교예2로 제조한 알코올분 13% 정제주정을 각각 5,000㎖ 및 10,000㎖를 혼화하여 이를 비교예 1의 방법과 동일하게 가스크로마토그래피 및 아미노산분석기 등을 이용하여 분석하여 퓨젤유와 각종 아미노산 등 을 정량분석하고 비교분석 결과를 [표2], [표3]에 나타내었다. Example 1: 13 ml of alcohol content prepared in Comparative Example 1 (raw material: rice) was mixed with 5,000 ml of alcohol content 13% purified alcohol prepared in Comparative Example 2 by mixing 5,000 ml and 10,000 ml of Comparative Example 1, respectively. In the same manner as in the method of gas chromatography and amino acid analyzer and the like analyzed by the quantitative analysis of fusel oil and various amino acids and the results are shown in [Table 2], [Table 3].

실시예 2 :비교예2로 제조한 정제주정에 포도당, 물엿, 젖산, 아미노산류, 퓨젤유 등을 비교예1과 실시예1의 성분분석 결과 향미성분 중 주류 품질에 좋지 않은 성분을 제외하고 감소된 양만큼 첨가하여 [표4]와 같이 100% 증양할 수 있는 조미주정A와 200% 증양할 수 있는 조미주정B를 제조하였다. Example 2 glucose, starch syrup, lactic acid, amino acids, fusel oil, etc. in the tablet alcohol prepared in Comparative Example 2 as a result of the component analysis of Comparative Example 1 and Example 1 was reduced except for the components that are not good for the mainstream quality of flavor By adding the amount as shown in Table 4 to prepare 100% increase in seasoning alcohol A and 200% increase in seasoning alcohol B was prepared.

실시예 3 :비교예1(원료 :쌀)로 제조한 알코올분 13% 숙성술덧 5,000㎖와 알코올분 13%조미주정A 5,000㎖(약주 숙성술덧 : 조미주정=1:1)를 혼화한 후 여과하여 술지게미 1,000㎖를 제외하고 9,000㎖의 100% 증양약주를 제조하였다. Example 3 After mixing 13 ml of alcohol content 13% aged alcohol supplement 5,000 ml of alcohol powder 13% seasoned alcohol A (medicine wine aged seasoning: seasoning alcohol = 1: 1) prepared by Comparative Example 1 (raw material: rice) 9,000 ml of 100% boost was prepared except for 1,000 ml of sake lees.

실시예 4 :비교예1(원료 :쌀)로 제조한 알코올분 13% 숙성술덧 5,000㎖와 알코올분 13%조미주정B 10,000㎖(약주 술성술덧 : 조미주정=1:2)를 혼화한 후 여과하여 술지게미 1,000㎖를 제외하고 14,000㎖의 200%증양약주를 제조하였다. Example 4 After mixing 13 ml of alcohol content 13% aged alcohol supplement 5,000 ml of alcohol content 13% seasoned alcohol B prepared by Comparative Example 1 (raw material: rice) 14,000ml of 200% by weight except for 1,000ml of sake lees was prepared.

주) 실험1 ; 숙성술덧과 정제주정=1:1, 실험2 ; 숙성술덧과 정제주정=1:2NOTE 1 Experiment 1; Aging and refined alcohol = 1: 1, experiment 2; Aging and refined drink = 1: 2

- 분석방법 : 국세청기술연구소 주류분석규정-Method of Analysis: Regulations for liquor analysis

- 분석조건-Analysis conditions

· G.C : M 600DG.C: M 600D

· Detector : FIDDetector: FID

· Injection temp : 170℃Injection temp: 170 ℃

· Detector temp : 220℃Detector temp: 220 ℃

· Oven 온도 Program: 50℃(2min) -10℃/min승온 -100℃(0min) -30℃/min 승온 -200℃(1min)Oven temperature program: 50 ℃ (2min) -10 ℃ / min Temperature rise -100 ℃ (0min) -30 ℃ / min Temperature rise -200 ℃ (1min)

주) 실험1, 숙성술덧과 정제주정=1:1, 실험2, 숙성술덧과 정제주정=1:2Note 1) Experiment 1, Aging and refined alcohol = 1: 1, Experiment 2, Aging refined and purified alcohol = 1: 2

- 분석조건-Analysis conditions

· 칼럼온도 : 57℃Column temperature: 57 ℃

· 반응온도 : 130℃Reaction temperature: 130 ℃

· Pump 1(완충용액) 유량 : 0.40㎖/minPump 1 (buffer solution) flow rate: 0.40ml / min

· Pump 2(닌히드린용액) 유량 : 0.35㎖/minPump 2 (ninhydrin solution) flow rate: 0.35ml / min

· N2Gas압력 : 0.35∼ 0.4㎏/㎠N 2 Gas pressure: 0.35∼ 0.4㎏ / ㎠

본 발명의 방법으로 제조된 약주는 무미, 무취의 정제주정을 첨가하여 감소된 약주 고유의 향미성분 중 주류 품질에 바람직하지 않는 성분은 제외하고, 감소된 향미성분 양만큼 정제주정에 첨가하여 제조한 조미주정을 약주 숙성술덧(또는 여과약주)에 첨가함으로써 약주 본래의 향미를 그대로 유지하면서 원료비 절감 및 제조공정 단축 등의 제조원가 절감 효과가 있다.Medicinal herbs prepared by the method of the present invention are prepared by adding to the refined alcohol by the amount of reduced flavor components, except for the undesirable flavor of alcoholic beverages inherent in the reduced flavor of indigenous flavors by adding tasteless and odorless refined alcohol By adding seasoning alcohol to medicinal liquor aging wine (or filtered medicinal liquor), the original flavor of the medicinal liquor can be maintained while reducing the production cost such as reducing raw material cost and manufacturing process.

Claims (2)

「쌀을 원료로 제조한 약주(13v/v% 10ℓ기준)」와, 정제주정에 포도당 900g, 물엿 200g, 젖산 18g, 아르기닌 3g, 티로신 2g을 포함한 아미노산 11g, 이소아밀알코올 0.8㎖, 이소부틸알코올 0.5㎖, 노르말프로필알코올 0.2㎖ 및 물을 첨가하여 13v/v%로 조정한 조미주정 10ℓ을 혼화하는 증양약주 제조방법`` Yellow liquor made from rice (13v / v% 10l) '', 900g of glucose, 200g of starch syrup, 18g of lactic acid, 3g of arginine, 2g of tyrosine, 0.8g of isoamyl alcohol, 0.8ml of isobutyl alcohol, isobutyl alcohol A process for preparing an enhanced liquor which mixes 10 liter of seasoned alcohol adjusted to 13v / v% by adding 0.5ml, 0.2ml of normal propyl alcohol and water 「밀가루를 원료로 제조한 약주(13v/v% 10ℓ기준)」와, 정제주정에 포도당 900g, 물엿 200g, 젖산 18g, 프롤린 2.5g, 스로오닌 2g을 포함한 아미노산 12g, 이소아밀알코올 1㎖, 이소부틸알코올 0.5㎖, 노르말프로필알코올 0.2㎖ 및 물을 첨가하여 13v/v%로 조정한 조미주정 10ℓ을 혼화하는 증양약주 제조방법`` Wheat liquor made from wheat flour (13v / v% 10ℓ standard) '', refined alcohol, 900g of glucose, 200g of starch syrup, 18g of lactic acid, 2.5g of proline, 2.5g of chloroonin, 2g of isoamyl alcohol, 1ml of isoamyl alcohol, iso A method for preparing an enhanced liquor which mixes 10 l of seasoned alcohol adjusted to 13v / v% by adding 0.5 ml of butyl alcohol, 0.2 ml of normal propyl alcohol and water.
KR10-2002-0018914A 2002-04-08 2002-04-08 Method for preparing rice wine(Yakju) adding spiced-alcohol KR100373986B1 (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6261575A (en) * 1985-09-12 1987-03-18 Setsujiyaku Syuzo Kk Production of novel brewed liquor
KR890004015A (en) * 1987-08-25 1989-04-19 도요다 요시도시 Weft Treatment Apparatus for Jet Looms
KR100201215B1 (en) * 1997-02-21 1999-06-15 박광희 Liquors based on chestnut and method for the preparation thereof
KR19990070818A (en) * 1998-02-25 1999-09-15 김길용 How to make pumpkin wine
KR20010044713A (en) * 2001-03-19 2001-06-05 권상일 Method For Preparing Kiwii Wine.
JP2001149057A (en) * 1999-11-29 2001-06-05 Mitsukan Group Honsha:Kk Method for producing mirin

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6261575A (en) * 1985-09-12 1987-03-18 Setsujiyaku Syuzo Kk Production of novel brewed liquor
KR890004015A (en) * 1987-08-25 1989-04-19 도요다 요시도시 Weft Treatment Apparatus for Jet Looms
KR100201215B1 (en) * 1997-02-21 1999-06-15 박광희 Liquors based on chestnut and method for the preparation thereof
KR19990070818A (en) * 1998-02-25 1999-09-15 김길용 How to make pumpkin wine
JP2001149057A (en) * 1999-11-29 2001-06-05 Mitsukan Group Honsha:Kk Method for producing mirin
KR20010044713A (en) * 2001-03-19 2001-06-05 권상일 Method For Preparing Kiwii Wine.

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