KR100330080B1 - Manufacturing process of increasing egg of poultry supplied calcium-silicate systems mixing sericile with infrared ray - Google Patents

Manufacturing process of increasing egg of poultry supplied calcium-silicate systems mixing sericile with infrared ray Download PDF

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KR100330080B1
KR100330080B1 KR1019990037774A KR19990037774A KR100330080B1 KR 100330080 B1 KR100330080 B1 KR 100330080B1 KR 1019990037774 A KR1019990037774 A KR 1019990037774A KR 19990037774 A KR19990037774 A KR 19990037774A KR 100330080 B1 KR100330080 B1 KR 100330080B1
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mixing
egg
poultry
sericile
infrared ray
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KR20010026451A (en
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신현택
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신현택
하재관
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B14/00Use of inorganic materials as fillers, e.g. pigments, for mortars, concrete or artificial stone; Treatment of inorganic materials specially adapted to enhance their filling properties in mortars, concrete or artificial stone
    • C04B14/02Granular materials, e.g. microballoons
    • C04B14/04Silica-rich materials; Silicates
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K40/00Shaping or working-up of animal feeding-stuffs
    • A23K40/10Shaping or working-up of animal feeding-stuffs by agglomeration; by granulation, e.g. making powders
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B14/00Use of inorganic materials as fillers, e.g. pigments, for mortars, concrete or artificial stone; Treatment of inorganic materials specially adapted to enhance their filling properties in mortars, concrete or artificial stone
    • C04B14/02Granular materials, e.g. microballoons
    • C04B14/26Carbonates
    • C04B14/28Carbonates of calcium
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/06Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by burning-out added substances by burning natural expanding materials or by sublimating or melting out added substances
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2103/00Function or property of ingredients for mortars, concrete or artificial stone
    • C04B2103/0068Ingredients with a function or property not provided for elsewhere in C04B2103/00
    • C04B2103/0097Anion- and far-infrared-emitting materials

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Civil Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Zoology (AREA)
  • Food Science & Technology (AREA)
  • Fodder In General (AREA)

Abstract

본원 발명은 양계산란계의 증란을 위한 방안으로 소석을 제조하여 증란효과를 가져오는 증란소석 제조방법에 관한 것으로 원적외선광을 방사하는 견운모에 석회재로서 소석회, 탄산칼슘 또는 규회계합성재를, 실리카로서 규사분을 결합재로 하고, 발포제로 알루미늄분을 조합하여 발포시킨후 수증기로 경화시키는 규회수계 경화체의 단미를 양계용 난각보강제로 제조하는 산란계 증란소석을 제조하는 방법이다.The present invention relates to a method for producing a spawning stone that produces a sapphire as a method for the production of hens laying hens, which results in a spawning effect. The present invention relates to a calcined mica that emits far-infrared light. It is a method for producing a laying hen sapphiresite which is prepared by using the egg shell reinforcing agent for poultry farming, in which the silica sand powder is used as a binder and the aluminum powder is foamed in combination with the foaming agent, followed by foaming.

Description

원적외선광을 방사하는 견운모를 이용한 규회수계의 산란계증란소석의 제조방법{Manufacturing process of increasing egg of poultry supplied calcium-silicate systems mixing sericile with infrared ray}Manufacturing process of increasing egg of poultry supplied calcium-silicate systems mixing sericile with infrared ray}

본 발명은 양계시에 알을 낳는 횟수를 증가시키는 산란계 증란소석의 제조방법이다.The present invention is a method for producing laying hen laying stones to increase the number of eggs laid in poultry.

양계시에 노지에서 방사하는 닭은 때때로 토양에 있는 소석 즉 모래를 소화조제로서 주어 먹고, 사료를 소화흡수하여 성장생존하고 있었다. 그러나 대량 사육 산란시켜야하는 현대에는 양계사에서 산란하는 닭은 인공소석을 첨가하여야 하는 바 그 방법으로 현재 방해석 또는 패각분등을 미분쇄하여 모래알크기로 하여 약 8%내외를 사료에 혼합하여 급여하여 사육하고 있다.Chickens radiating from open fields at poultry farms sometimes lived by feeding on calcined sand in the soil as a digestive aid and digesting and absorbing feed. In modern times, however, chickens spawned in poultry houses have to be added artificial calculus. In this way, pulverized calcite or shells are pulverized. Breeding.

그러나 산란계의 경우는, 방사하는 계분에는 미소화 단백질이 다량 함유되어 있어 완전소화를 위한 대책이 요구되고 있다. 산란시에 파란률이 평균 10%에 이르고 유통단계까지는 연란과 파란으로 인하여 극단적으로 15%까지 상승하여 파란률 손실에 의한 국가 경제적으로 큰 손실을 가져오고 있다.However, in the case of laying hens, the spinning egg meal contains a large amount of micronized protein, and measures for complete digestion are required. In spawning, the blue rate reaches an average of 10%, and until the distribution stage, up to an extreme 15% due to egg and blue, bringing the national economic loss caused by the loss of the blue rate.

국내 사료의 약 90%이상을 수입하고 있는 현실정으로서는 심각한 우려의 문제가 아닐 수 없고, 낭비자원절약이나 외화절약을 위해서나 시급히 해결하여야 할 중대한 과제이다.The reality of importing more than 90% of domestic feed is a matter of serious concern, and is an important task that needs to be addressed urgently for the purpose of saving waste resources and foreign currency.

양계시의 소석의 공급은 사료의 효율적인 분쇄조제로서 반드시 필요하며, 양계시에 효율적인 소석의 공급대책이 요구되고 있었으나 소석의 중요성이 경시되고 있었다고 사료된다는 것이 현실정이며, 또한 종래와 같이 분쇄된 방해석을 광물질사료에 첨가하는 방식은 보다 과학적이고 합리적인 방법이 요구되는 실정이다.The supply of hydrated stone at poultry farming is essential as an effective grinding aid for feed, and it is believed that the calcite has been neglected, but the importance of hydrated stone is being neglected. The method of adding to the mineral feed requires a more scientific and rational method.

상기와 같은 실정을 감안하여 산란계의 사료에 방해석을 첨가함 있어 획기적인 방안을 강구하여 소석의 기능을 강화하고 난각의 강도를 강화할 수 있는 방안을 구축하고 대책이 수립될 필요가 있다.In view of the above situation, calcite is added to the feed of laying hens, so it is necessary to find a ground-breaking way to establish the function to strengthen the function of the calcination and the strength of the egg shell and establish the countermeasure.

본 발명은 상기와 같이 사육, 산란계에서 나타나는 제반 사항을 감안한 것으로 산란계 사료에 첨가되는 방해석은 분쇄조제의 역활만을 하지 않고, 소석의 기능으로서 산란계가 석회의 흡수능을 극대화하고 소화과정에서 각종 미생물이 소화기관을 통과하면서 다공성의 소석이 흡수한 영양분을 보다 효율적으로 소화 흡수를 도울 수 있도록 하고, 소화과정에서 미 소화 단백질의 완전 소화를 돕고 양계시에 각종 미생물에 의한 질병을 효과적으로 예방하고져 다공질의 소석경화체를 공급하여 질병없고 파란감소제로서의 역활을 하는 소석을 공급하는데 있으며, 현재의 양계사료에 첨가되는 방해석이나 패각의 기능을 유지하면서 소량의 본 증란소석을 첨가하여 그의 소화 흡수기능을 증가시킬 수 있도록 하는데 목적을 두고 발명한 것이다.The present invention has been made in view of the general conditions appearing in breeding and laying hens, calcite added to laying hens feed does not only serve as grinding aid, but as a function of calcining, the laying hens maximize the absorption of lime and various microorganisms are digested in the digestion process. Porous calcined hardened body through the trachea to help digestion of nutrients absorbed by porous calciner more efficiently, and to help complete digestion of undigested protein during digestion process and to effectively prevent diseases caused by various microorganisms in poultry farming. It is to supply calcite that plays a role as a blue reducing agent without disease and to increase its digestive absorption function by adding a small amount of this dilute calcite while maintaining the function of calcite or shell added to the current poultry feed. It was invented for the purpose.

본 발명은 상기와 같은 목적을 추구하고자 하는 수단으로서The present invention as a means for pursuing the above object

규산질원료로서는 규사분을, 석회질재료로서는 소석회, 또는 패각이나 굴껍질을, 발포 및 강도보강재로서는 시멘트분말(이하 규회계합성재라 칭한다)을 사용하고 소석에 CaO 함량을 증량시키고 그 흡수가 잘되는 합성 탄산칼슘을 첨가하고, 고효율로 원적외선광을 방사하는 견운모를 이용하여 계란의 신선도를 높이고, 장기보관에 유효토록 하였다. 첨가된 탄산칼슘은 닭체내에서 흡수가 용이한 상태로서 두꺼운 난각의 형성에 크게 기여할 수 있도록 하였으며, 본 발명에 사용한 규사, 견운모 및 규회계합성재의 화학 성분은 다음과 같다.Synthetic carbonic acid with silica sand powder, slaked lime or shell or oyster shell as lime material, and cement powder (hereinafter referred to as whey composite material) as foaming and strength reinforcing material. Calcium was added to the eggs to improve the freshness of the eggs by using the villus that emits far infrared light with high efficiency, and was effective for long-term storage. The added calcium carbonate was easy to absorb in the chicken body, and contributed greatly to the formation of a thick egg shell, and the chemical components of the silica sand, biotite, and whey composite material used in the present invention are as follows.

(Wt.%)(Wt.%)

SiO₂ Al2O3Fe2O3CaO MgO TiO₂ K2O Na2O SO3Ig.loss 기타SiO₂ Al 2 O 3 Fe 2 O 3 CaO MgO TiO₂ K 2 O Na 2 O SO 3 Ig.loss Other

규사 94.42 5.01 0.53 0.04Silica 94.42 5.01 0.53 0.04

견운모 68.10 17.87 1.05 0.87 2.00 0.21 5.90 0.13 3.57Cicada 68.10 17.87 1.05 0.87 2.00 0.21 5.90 0.13 3.57

규회계합성재 21.58 5.21 3.20 64.16 1.74 1.02 1.90 0.60 0.59Weighing Composite 21.58 5.21 3.20 64.16 1.74 1.02 1.90 0.60 0.59

소석회와 탄산칼슘, 패각이나 굴껍질의 산화칼슘의 함량은 순도 90%이상의 것을 사용한다. 견운모의 원적외선 측정치(방사파장 5-20㎛)는 93%이었다(FT-IR Spetrometer를 이용한 Black body대비 측정결과이다).The content of calcium oxide in hydrated lime, calcium carbonate, shells and oyster shells is more than 90% pure. The far infrared ray measurement (radiation wavelength 5-20㎛) of Cicada was 93% (measured by Black body using FT-IR Spetrometer).

석회 대 규사의 비는 경화할 수 있는 CaO가 가능하면 SiO₂함량보다 많은 것이 바람직하며 CaO가 최고가 되는 합성재 CaO/SiO2=2.0∼3.0의 몰비가 되도록 하는 것이 가장 바람직하며, 견운모량과의 혼합비는 적당조절할 수도 있으나 견운모량은 약 70% 정도가 바람직하였다. 또는 여기에 합성 탄산칼슘을 약 30% 정도를 혼합하여 제조할 수도 있다. 합성 탄산칼슘을 혼합하므로서 유효하게 난각 형성시에 쉽게 흡수되어 난각의 두께 및 강도를 향상시킬 수 있는 것이다.The ratio of lime to silica sand is preferably higher than the SiO2 content if the hardenable CaO is possible, and it is most preferable to make the molar ratio of CaO / SiO 2 = 2.0 to 3.0, which is the highest CaO, and the mixing ratio with the amount of mica. May be appropriately adjusted, but about 70% of chorionic hair was preferred. Alternatively, the synthetic calcium carbonate may be prepared by mixing about 30%. By mixing synthetic calcium carbonate, it is effectively absorbed at the time of eggshell formation, thereby improving the thickness and strength of the eggshell.

이 원료 조합무게의 50%의 온수(60℃)를 가하고, 혼합기에서 3분간 교반하면서 적당량의 알루미늄금속분말을 가하여 슬러리로한 후 발포시킨다. 응결시킨후 상압양생(90℃-6시간)하여 경화제를 얻은 다음, 상기 경화체를 10mm이하의 입자 크기로 분쇄하게 되면 모세관 세공이 많은 경량골재를 제조하여 증란소석을 제조한다.50% of the weight of the raw material combination is added to hot water (60 ° C), and an appropriate amount of aluminum metal powder is added to the slurry while stirring for 3 minutes in a mixer to form a slurry, followed by foaming. After condensation, atmospheric curing (90 ° C.-6 hours) to obtain a curing agent, and when the cured product is pulverized to a particle size of 10mm or less to prepare a lightweight aggregate with a lot of capillary pores to produce a sintering stone.

본 발명의 증란소석을 제조하기 위하여 견운모, 석회분 및 규사분을 소정의 입도로 미분하고 알루미늄금속분말을 가하여 슬러리 상태에서 발포시킨후 상온 또는 고온수열 분위기에서 규회수계을 합성하여 경화체를 만들고 알맞는 크기의 입도로 미분쇄하여 증란소석을 제조한다. 이러한 소석에 탄산칼슘(분말)을 약 30% 혼합한 후 기존의 양계사료에 적당량 혼합하여 양계사료에 혼합사용할 수도 있다.In order to prepare the dilute calcite of the present invention, the fine mica, lime powder and silica sand are finely divided to a predetermined particle size, and aluminum metal powder is added to foam in a slurry state, and then, the synthetic water system is synthesized in a room temperature or high temperature hydrothermal atmosphere to make a hardened body and a suitable size. The fine powder is prepared by pulverizing to a particle size of. About 30% of calcium carbonate (powder) may be mixed with the calcined mixture, and then mixed with an existing poultry feed, and may be used in a poultry feed.

본 발명에 증란소석의 제조방법을 실시예로 상세히 설명하면 다음과 같다.Referring to the present invention in detail the production method of evaporated calcined as follows.

<실시예 1><Example 1>

원적외선광을 방사하는 견운모 500g과 규회계합성재 190g을 실리카분말 10g과 함께 혼합기에 넣고 60℃의 온수 350㎖를 첨가 교반하면서 원료체 무게의 0.1%의 알루미늄분말을 가하여 혼합한 후, 항온항습기(60℃)에서 30분간 발포시킨다. 응 결후 90℃-6시간 상압 양생하여 미세한 다공성의 건조 경화체를 770g을 얻고 이를 10mm이하의 입자크기로 미분쇄하고 합성 탄산칼슘 230g을 혼합하여 증란소석 1000g을 제조하였다. 경화체의 부피비중은 0.5, 압축강도는 10Kg/㎠이었다.500 g of mica that emits far-infrared light and 190 g of whey composite material together with 10 g of silica powder were added to a mixer, and 350 ml of hot water at 60 ° C. was added and stirred with 0.1% aluminum powder of the raw material, followed by mixing. 60 minutes). After curing, the mixture was cured at 90 ° C. for 6 hours at atmospheric pressure to obtain 770 g of a fine porous dry cured product, which was ground to a particle size of 10 mm or less, and 230 g of synthetic calcium carbonate was mixed to prepare 1000 g of distilled stone. The volume specific weight of the cured product was 0.5 and the compressive strength was 10 Kg / cm 2.

<실시예 2><Example 2>

원적외선을 방사하는 견운모 600g에 소석회 140g 및 실리카분말을 60g를 혼합기에 넣고 혼합한다. 여기에 원료무게의 50%의 온수를 가하여 교반하면서 원료 무게의 0.1% 무게량의 알루미늄 분말을 가하여 혼합한후 60℃의 항온항습기에서 30분간 발포시킨다. 응결한 후 90℃에서 6시간 상압양생하여 다공성 건조 경화체 840g를 만들고 이를 10㎜이하의 입자크기로 분쇄하여 합성 탄산칼슘 250g을 혼합하여 증란소석 1090g을 제조하였다.To 600 g of farther-ray mica, 140 g of hydrated lime and 60 g of silica powder are put into a mixer and mixed. 50% of the weight of the raw material is added thereto and stirred while adding 0.1% by weight of aluminum powder to the mixture while stirring and foaming for 30 minutes in a thermo-hygrostat at 60 ° C. After condensation, the mixture was cured at 90 ° C. for 6 hours at atmospheric pressure to make 840 g of porous dry cured product, which was ground to a particle size of 10 mm or less, and 250 g of synthetic calcium carbonate was mixed to prepare 1090 g of dilute calcite.

<사용실험><Use Experiment>

실시예 1에서 제조한 본 발명의 증란소석을 40주령인 산란계의 시판사료중에 3%를 첨가하여서 투여 실험한 결과는 표 1과 같다.The results of the experiment of the administration of the elutriation of the present invention prepared in Example 1 with the addition of 3% in the commercial feed of 40-week-old laying hens are shown in Table 1.

계란의 비교 시험표(40주령 산란계)Comparative test table (40 weeks old laying hens) of egg 사용전Before use 사용후after use 비 고Remarks 산란률Spawn rate 70%70% 90%90% 620수620 count 파란률(%)Blue factor (%) 6%6% 2%2% 200수 1주일 평균치200 number a week average 난각두께Eggshell thickness 0.34mm0.34mm 0.40mm0.40mm 30개 평균치30 averages 난각강도Eggshell strength 4250gr4250gr 5300gr5300gr 30개 평균치30 averages 원적외선 측정치Far Infrared Measurement 88%88% 92%92% 30개 평균치30 averages 신선도Freshness 보통usually 우수Great 10℃, 습도 80%, 30일간 보관후10 ℃, humidity 80%, after 30 days storage 비린내Fishy 있음has exist 없음none

상기와 같이 생산된 증란소석 사료는 미분쇄하여 10mm이하로 한 후 양계용 배합사료와 배합하여 산란사료로 사육하는 바 산란용은 일주일후부터 산란률이 증가하기 시작하여 원래 배합 사료에 비하여 월평균 30%의 증란 효과를 가져오고, 달걀껍질의 불량률은 평균 7%로 알려져 있으나 1%이하로 그 생산성이 우수하였고, 본 증란소석을 가한 경우에는 난각의 두께는 0.34mm에서 0.40mm로 11%의 두께의 증가를 보여 주었다. 또한 본 발명의 증란소석을 첨가한 계란의 노란자는 젓가락으로 집어올릴 수가 있고, 흰자는 엄지 손가락과 둘째 손가락으로 들어올릴 수 있는 탄력성이 있고, 삶은후에 비린내가 나지않고 노란자가 짙은 계란을 생산하였다.The spawned feed produced as described above is finely pulverized to 10mm or less and then mixed with the poultry feed to breed as a laying feed. The spawning rate starts to increase from one week later to 30% more than the original feed. The eggshell defect rate is known to be 7% on average, but the productivity is less than 1%. The eggshell thickness is 0.34mm to 0.40mm and 11% thick. Showed an increase. In addition, the egg yolk of the present invention is added to the egg yolk can be picked up with chopsticks, the egg white can be lifted by the thumb and the second finger, and after boiling boiled fishy yellow egg produced a dark egg.

기존의 산란계에 비하여 연란 및 파란이 적고, 비린내가 나지 않는 우수한 품질과 증란률이 증란사료를 첨가하지 않은 것보다 월평균 30%의 증란을 보여 주었다.Compared to the existing laying hens, the egg quality and egg color are less fishy, and the excellent quality and the rate of egg breeding show an average of 30% increase per month than the addition of egg feed.

양계시의 산란계의 증란을 위한 방안으로 원적외선광을 방사하는 견운모에석회와 규사를 수증기속에서 합성하여 증란소석을 제조하여 양계사료에 첨가하여 증란효과를 가져오는 소석을 생산하여 품질이 우수한 계란을 생산하고 외화절감에 기여하며 국민건강에 기여할수 있는 증란으로 그 효과는 현격하게 주효하였다.As a method for the spawning of laying hens in poultry farming, it is synthesized by the formation of steamed calcined limestone and silica sand which emit far infrared rays in water vapor. The effect was remarkable as a result of production, contribution to foreign currency reduction and contribution to national health.

Claims (1)

원적외선을 방사하는 견운모 70∼75%와, 소석회 또는 규회계합성재중 어느 한 물질을 선택하여 10∼28% 및 실리카분말 1∼10%의 무게비로 하되 CaO/SiO2=2.0∼3.0의 몰비가 되도록 혼합기에 넣고 혼합한후 여기에 원료무게의 50%의 온수를 가하여 교반하면서 원료무게의 0.1%무게량의 알루미늄분말을 가하여 혼합한 후 60℃의 항온항습기에서 30분간 발포시켜서 응결한 후 90℃에서 6시간 상압양생하여 다공성 경화체를 만들고 이를 10㎜이하의 입자크기로 미분쇄하고 이 경화체에 20∼35% 무게량의 탄산칼슘을 혼합하여서 제조함을 특징으로 하는 견운모를 이용한 규회계의 산란계증란소석의 제조방법.70-75% of the hard mica that emits far infrared rays and either slaked lime or whey-based material are selected to have a molar ratio of 10-28% and silica powder 1-10%, with a molar ratio of CaO / SiO 2 = 2.0-3.0. After mixing and mixing 50% hot water of raw material weight and adding 0.1% weight of aluminum powder of raw material weight to the mixer, mixing it, foaming by condensation at 60 ℃ constant temperature and humidity room for 30 minutes, and condensing at 90 ℃ 6 hours of atmospheric curing to make a porous cured product, which is prepared by pulverizing it to a particle size of 10 mm or less and mixing 20 to 35% by weight of calcium carbonate. Manufacturing method.
KR1019990037774A 1999-09-07 1999-09-07 Manufacturing process of increasing egg of poultry supplied calcium-silicate systems mixing sericile with infrared ray KR100330080B1 (en)

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Publication number Priority date Publication date Assignee Title
KR100639294B1 (en) 2005-05-13 2006-10-27 하종훈 Natural mineral composition for poultry farming and health functional assistance feed for poultry farming thereby and its manufacturing method

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100639294B1 (en) 2005-05-13 2006-10-27 하종훈 Natural mineral composition for poultry farming and health functional assistance feed for poultry farming thereby and its manufacturing method

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