JPS6435259A - Measuring apparatus for average number of oxidation in copper of compound containing copper - Google Patents
Measuring apparatus for average number of oxidation in copper of compound containing copperInfo
- Publication number
- JPS6435259A JPS6435259A JP62190020A JP19002087A JPS6435259A JP S6435259 A JPS6435259 A JP S6435259A JP 62190020 A JP62190020 A JP 62190020A JP 19002087 A JP19002087 A JP 19002087A JP S6435259 A JPS6435259 A JP S6435259A
- Authority
- JP
- Japan
- Prior art keywords
- titration
- reducing agent
- electrode
- sample
- copper
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Superconductor Devices And Manufacturing Methods Thereof (AREA)
- Superconductors And Manufacturing Methods Therefor (AREA)
Abstract
PURPOSE:To obtain a higher measuring accuracy, by arranging a means of dissolving an analysis sample and a means of determining the amount of a reducing agent by a coulometric titration method in a closed container which is filled with an electrolytic solution containing a reducing agent to cut oxygen in the air. CONSTITUTION:About 30mg of an analysis sample is placed into a preliminary chamber and a liquid drain cock 21 is opened to inject a specified amount of a reducing agent solution in a burette into a main cell chamber 1. A partition 7 is opened with a push bar 9 to put a sample into the main chamber. After the sample is dissolved stirring up the solution with a rotator 22, a DC power supply with a coulometer is connected between an electrode 2 for titration and an opposed pole 18 to run the DC. Here, with a reaction in the titration electrode, Cu<+> as reducing agent is oxidized to be Cu<2+>. Therefore, when a potential of an indication electrode is measured with respect to a reference electrode simultaneously with the titration, the potential rises with the reaction and then, as the Cu<+> is almost consumed, the potential rises steeply. Thus, at this point, the end of the titration can be judged.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP62190020A JPS6435259A (en) | 1987-07-31 | 1987-07-31 | Measuring apparatus for average number of oxidation in copper of compound containing copper |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP62190020A JPS6435259A (en) | 1987-07-31 | 1987-07-31 | Measuring apparatus for average number of oxidation in copper of compound containing copper |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS6435259A true JPS6435259A (en) | 1989-02-06 |
Family
ID=16251033
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP62190020A Pending JPS6435259A (en) | 1987-07-31 | 1987-07-31 | Measuring apparatus for average number of oxidation in copper of compound containing copper |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6435259A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102680470A (en) * | 2011-12-10 | 2012-09-19 | 河南科技大学 | Method for determining content of arsenic and antimony in copper electrolyte |
-
1987
- 1987-07-31 JP JP62190020A patent/JPS6435259A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102680470A (en) * | 2011-12-10 | 2012-09-19 | 河南科技大学 | Method for determining content of arsenic and antimony in copper electrolyte |
| CN102680470B (en) * | 2011-12-10 | 2014-04-02 | 河南科技大学 | Method for determining content of arsenic and antimony in copper electrolyte |
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