JPS6369767A - Cutting tip and machining tool - Google Patents
Cutting tip and machining toolInfo
- Publication number
- JPS6369767A JPS6369767A JP61209581A JP20958186A JPS6369767A JP S6369767 A JPS6369767 A JP S6369767A JP 61209581 A JP61209581 A JP 61209581A JP 20958186 A JP20958186 A JP 20958186A JP S6369767 A JPS6369767 A JP S6369767A
- Authority
- JP
- Japan
- Prior art keywords
- cutting
- toughness
- test
- silicon carbide
- zirconia
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000005520 cutting process Methods 0.000 title claims description 28
- 238000003754 machining Methods 0.000 title claims description 5
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 10
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical class [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims description 8
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 6
- 229910002077 partially stabilized zirconia Inorganic materials 0.000 claims description 5
- 239000002245 particle Substances 0.000 claims description 5
- 229910010271 silicon carbide Inorganic materials 0.000 claims description 5
- 239000002131 composite material Substances 0.000 claims description 4
- 238000012360 testing method Methods 0.000 description 19
- 239000000919 ceramic Substances 0.000 description 12
- 230000000694 effects Effects 0.000 description 6
- 238000005452 bending Methods 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 5
- 230000007423 decrease Effects 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 238000007656 fracture toughness test Methods 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- 229910001018 Cast iron Inorganic materials 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000007542 hardness measurement Methods 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 239000011812 mixed powder Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 230000035939 shock Effects 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- 238000005491 wire drawing Methods 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 229910001141 Ductile iron Inorganic materials 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 229910052581 Si3N4 Inorganic materials 0.000 description 1
- 230000005856 abnormality Effects 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 229910003460 diamond Inorganic materials 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- 238000005553 drilling Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000019441 ethanol Nutrition 0.000 description 1
- 238000005242 forging Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 238000001192 hot extrusion Methods 0.000 description 1
- 238000007731 hot pressing Methods 0.000 description 1
- 238000007373 indentation Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 238000013001 point bending Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 238000007514 turning Methods 0.000 description 1
Landscapes
- Compositions Of Oxide Ceramics (AREA)
- Cutting Tools, Boring Holders, And Turrets (AREA)
Abstract
(57)【要約】本公報は電子出願前の出願データであるた
め要約のデータは記録されません。(57) [Abstract] This bulletin contains application data before electronic filing, so abstract data is not recorded.
Description
【発明の詳細な説明】
産業上の利用分野
本発明は切削用チップおよび加工用工具に係り、更に詳
しくはセラミックス製の衝撃に強い高靭性、高強度、高
硬度を具備した高速切削用チップおよびロール、ダイス
等の耐磨耗性加工用工具に関する。DETAILED DESCRIPTION OF THE INVENTION Field of Industrial Application The present invention relates to a cutting tip and a processing tool, and more particularly to a high-speed cutting tip and a ceramic tip having impact resistance, high toughness, high strength, and high hardness. It relates to wear-resistant machining tools such as rolls and dies.
従来技術と問題点
従来、鋼や鋳鉄の高速切削工具用材料としては高速切削
時における優れた耐摩耗性を示すこと、且つ鉄との摩擦
係数が小さい等の理由で現在A1□03−TiCのセラ
ミックス製工具が実用化され主流となついる。しかしな
がらA]20.− T i Cは靭性に難があり耐衝撃
性が不十分であるため欠損を起こしやすい欠点があり安
定して使用することができない。Conventional technology and problems Conventionally, A1□03-TiC has been used as a material for high-speed cutting tools for steel and cast iron because it exhibits excellent wear resistance during high-speed cutting and has a small coefficient of friction with iron. Ceramic tools were put into practical use and became mainstream. However, A]20. - T i C has poor toughness and insufficient impact resistance, so it has the drawback of being easily damaged and cannot be used stably.
そこで近年切削工具として機械的強度、高硬度、衝撃性
に優れたSi3N4セラミックスが注目されているが、
513N4は耐摩耗性に劣り摩耗が激しく汎用性が低い
こと、機械加工における加工抵抗が大きく生産性が低い
等の問題点を有している。Therefore, in recent years, Si3N4 ceramics, which have excellent mechanical strength, high hardness, and impact resistance, have been attracting attention as cutting tools.
513N4 has problems such as poor wear resistance, severe wear, and low versatility, and high machining resistance and low productivity.
問題点を解決するための手段
本発明は、上述の従来の切削用チップおよび加工用工具
の問題点に鑑みてなされたもので、高靭性、高硬度を有
し特に高級鎚鉄やダクタイル鋳鉄等の切削工具として適
した材料を開発すべく、各種の材料を用いて鋭意研究と
試験を重ねた結果、衝撃に強い高強度、高靭性のアルミ
ナ−ジルコニア−炭化珪素複合焼結体がこの目的に適う
ことを見出した。Means for Solving the Problems The present invention was made in view of the problems of the conventional cutting tips and machining tools mentioned above, and they have high toughness and high hardness, and are particularly suitable for cutting tools such as high-grade hammer iron and ductile cast iron. As a result of extensive research and testing using a variety of materials in order to develop materials suitable for cutting tools, alumina-zirconia-silicon carbide composite sintered bodies with high impact resistance, high strength, and high toughness were found to be suitable for this purpose. I found something suitable.
本発明の衝撃に強い高強度、高靭性のアルミナ−ジルコ
ニア−炭化珪素複合焼結体からなる切削用チップおよび
加工用工具は、平均粒径0.1〜1.0μmの部分安定
化ジルコニア5〜50容積%;直径1μm以下、アスペ
クト比3〜200の炭化珪素ウィスカー3〜40容積%
(但し、この炭化珪素ウィスカーと前記ジルコニアの合
計は55容積%以下);残部が実質的にアルミナからな
ることを特徴としている。The cutting tip and processing tool made of the impact-resistant, high-strength, high-toughness alumina-zirconia-silicon carbide composite sintered body of the present invention are made of partially stabilized zirconia with an average grain size of 0.1 to 1.0 μm. 50% by volume; 3-40% by volume of silicon carbide whiskers with a diameter of 1 μm or less and an aspect ratio of 3-200
(However, the total amount of the silicon carbide whiskers and the zirconia is 55% by volume or less); the remainder is substantially composed of alumina.
次に、衝撃に強い高強度、高靭性アルミナ−ジルコニア
−炭化珪素複合焼結体の成分範囲の限定理由について述
べる。Next, the reason for limiting the range of components of the impact-resistant, high-strength, high-toughness alumina-zirconia-silicon carbide composite sintered body will be described.
部分安定化ジルコニア粉末は、粒径が0.1μm未満で
あると安定し過ぎ又1.0μmを超えると不安定化にな
り過ぎて、いずれも強度改善に寄与しなくなるため粒径
の範囲を0.1〜1.0μmとした。その量は5%未満
では高靭化の効果が顕著でなく、50%を超えると硬度
の低下をきたすため5〜50%の範囲とする。Partially stabilized zirconia powder is too stable if the particle size is less than 0.1 μm, and becomes too unstable if it exceeds 1.0 μm, neither of which contributes to strength improvement, so the particle size range is reduced to 0. .1 to 1.0 μm. If the amount is less than 5%, the effect of increasing toughness will not be significant, and if it exceeds 50%, the hardness will decrease, so the amount is set in the range of 5 to 50%.
炭化珪素ウィスカーは、アスペクト比が3未満では高靭
化の効果が充分でなく、200を超えると高靭化の効果
が減退するのでその範囲を3〜200とする。その直径
は1+n+nを超えると強度を低下させるので1mm以
下とした。その量は炭化珪素ウィスカーの効果を奏させ
るためには少なくとも3%以上を必要とし、40%を超
えると却って強度を低下するため3〜40%の範囲とす
る。When the aspect ratio of silicon carbide whiskers is less than 3, the effect of increasing toughness is insufficient, and when the aspect ratio exceeds 200, the effect of increasing toughness decreases, so the range is set to 3 to 200. If the diameter exceeds 1+n+n, the strength decreases, so the diameter was set to 1 mm or less. The amount of silicon carbide whiskers needs to be at least 3% or more in order to exhibit its effects, and if it exceeds 40%, the strength will decrease, so it should be in the range of 3 to 40%.
前記ジルコニアと炭化ウィスカーとの合計量は55%を
超えるとウィスカー又はジルコニアの添加過多となり靭
性又は硬度が低下するのでその合計は55%以下とした
。If the total amount of the zirconia and carbonized whiskers exceeds 55%, too much whisker or zirconia will be added, resulting in a decrease in toughness or hardness, so the total amount is set to 55% or less.
本発明品は、優れた靭性、高硬度および耐摩耗性を有し
且つ耐熱性、耐食性にも優れているので、これらの特性
が要求される鋳物および鋼の低速切削から高速切削まで
の幅広い範囲にわたって、切削用チップとして使用する
のに適するばかりでなく、更に耐熱衝撃性および耐酸化
性にも優れているので、比較的長時間高温に曝される熱
間加工用工具として使用した場合も、使用時の温度上昇
に具体例をあげれば、高速切削用、重切削用および断続
切削用を中心として、旋削加工、フライス加工、穴あけ
加工に用いるスローアウェイチップ、カッター、ドリル
、エンドミル等に、又比較的長時間高温に曝される耐摩
耗性熱間加工用工具として、熱間圧縮ダイス、熱間押出
パンチ、熱間線引ロール、熱間鍛造ダイス等のに広く適
用できる。The product of the present invention has excellent toughness, high hardness, and wear resistance, as well as excellent heat resistance and corrosion resistance, so it can be used in a wide range of applications from low-speed to high-speed cutting of castings and steel that require these properties. Not only is it suitable for use as a cutting tip, but it also has excellent thermal shock resistance and oxidation resistance, so it can be used as a hot working tool that is exposed to high temperatures for a relatively long time. Specific examples of temperature rise during use include indexable inserts, cutters, drills, end mills, etc. used for turning, milling, and drilling, mainly for high-speed cutting, heavy cutting, and interrupted cutting. As a wear-resistant hot working tool that is exposed to high temperatures for a relatively long period of time, it can be widely applied to hot compression dies, hot extrusion punches, hot wire drawing rolls, hot forging dies, etc.
実施例 以下本発明の実施例について具体的に説明する。Example Examples of the present invention will be specifically described below.
容積比でアルミナ粉末70%、炭化珪素ライスカー15
%、部分安定化ジルコニア15%を配合した。Alumina powder 70% by volume, silicon carbide rice car 15
% and 15% partially stabilized zirconia.
アルミナ粉末は純度99%以上、平均粒径0゜7μm、
γ型結晶形のものである。炭化珪素ウィスカーはβ型結
晶形のもので直径0.8μm、長さ20〜200μm、
アスペクト比20〜200である。ジルコニア粉末は2
モル%(3,5重量%)イツトリアで安定化した平均粒
径0.2μmの部分安定化ジルコニアである。Alumina powder has a purity of 99% or more, an average particle size of 0°7 μm,
It is in the γ type crystal form. Silicon carbide whiskers are β-type crystals, with a diameter of 0.8 μm and a length of 20 to 200 μm.
The aspect ratio is 20-200. Zirconia powder is 2
Partially stabilized zirconia with an average particle size of 0.2 μm stabilized with mol% (3.5% by weight) ittria.
この原材料をアルミナ容器とアルミナボールを使用する
ボールミル中でエチルアルコールを混合液に使用して2
4時時間式混合し、次ぎにこれらの混合粉を乾燥した。This raw material was mixed with ethyl alcohol in a ball mill using an alumina container and an alumina ball.
After 4 hours of mixing, these mixed powders were dried.
この混合粉を黒鉛型中に充填し、アルゴンガス雰囲気中
で直径50mmX厚さ5.5mmの円板にホットプレス
した。ホットプレスの条件は温度1500℃、成形圧力
300Kg/cm”、時間は1時間である。This mixed powder was filled into a graphite mold and hot-pressed into a disk having a diameter of 50 mm and a thickness of 5.5 mm in an argon gas atmosphere. The hot pressing conditions were a temperature of 1500° C., a molding pressure of 300 kg/cm”, and a time of 1 hour.
これらの焼結体から、ダイヤモンド砥石を用いて切断し
研削加工によって12.7mmX4.76mmのGIS
規格5NGN430型に則したスローアウェイチップを
作成した。このチップにより旋盤を用いて次の切削条件
によって切削テストを行った。From these sintered bodies, a 12.7mm x 4.76mm GIS was cut and ground using a diamond grindstone.
An indexable tip conforming to the standard 5NGN430 type was created. A cutting test was conducted using this chip using a lathe under the following cutting conditions.
比較量として市販のA1□03−TiCセラミックス製
チップについて同一の条件で切削テストを行った・
切削条件
被剛材 強靭鋳鉄(FC30材相当材)製シリンダラ
イす
内径95mmX長さ150mm
切削速度 142 m/min
送り 0 、35 mm/rpm切込み 0
.25mm
切削本数 250本
上記の切削条件でシリンダライナの内周面の仕上げ切削
加工を行い、チップの欠損の発生情況と仕上り寸法の変
化を測定してチップの摩耗程度を推定してチップの寿命
の良否を判定した。For comparison, a cutting test was conducted using a commercially available A1□03-TiC ceramic tip under the same conditions. Cutting conditions: Rigid material: Tough cast iron (equivalent to FC30 material) Cylinder inner diameter: 95 mm x Length: 150 mm Cutting speed: 142 m /min feed 0, 35 mm/rpm depth of cut 0
.. 25mm Number of cuts: 250 Finish cutting of the inner circumferential surface of the cylinder liner is performed under the above cutting conditions, and the occurrence of chip breakage and changes in finished dimensions are measured to estimate the degree of chip wear and determine the life of the chip. It was judged whether it was good or bad.
切削テストの結果を第1図に示す。The results of the cutting test are shown in Figure 1.
更にこれら焼結体から厚さ3mmX幅4 mm X長さ
40mmの曲げ試験片と、4X10X10mmの硬度測
定用試験片と破壊靭性試験片を採取して表面を鏡面仕上
げし、下記の試験を行なった
(1)曲げ試験
(2)硬度試験
(3)破壊靭性試験
試験結果は第1表に示す。Furthermore, a bending test piece with a thickness of 3 mm x width of 4 mm x length of 40 mm, a hardness measurement test piece of 4 x 10 x 10 mm, and a fracture toughness test piece were taken from these sintered bodies, the surfaces were mirror-finished, and the following tests were conducted. (1) Bending test (2) Hardness test (3) Fracture toughness test The test results are shown in Table 1.
尚、比較量として、従来品の切削用チップに用いられて
いるAl2O3−TiCセラミックスを用いて同一の条
件で試験を行なった。As a comparative example, a test was conducted under the same conditions using Al2O3-TiC ceramics used in conventional cutting tips.
第1表
(1)曲げ試験
JIS R1601(ファインセラミックスの曲げ強
さ試験方法)に規定される3点曲げ試験方法によって行
なった。試験片を30mmの距離に配置された2支点間
中央の1点にクロスヘッド速度0.5mm/minの荷
重を加え試験片が破壊するまでの最大荷重を測定した。Table 1 (1) Bending test The three-point bending test method specified in JIS R1601 (bending strength test method for fine ceramics) was used. A load was applied at a crosshead speed of 0.5 mm/min to one point in the center between two supporting points arranged at a distance of 30 mm to the test piece, and the maximum load until the test piece broke was measured.
(2)硬度試験 硬度測定は、ビッカース硬度計によって行った。(2) Hardness test Hardness measurement was performed using a Vickers hardness meter.
(3)破壊靭性試験
本試験はビッカース硬度計を用いたインデンテーション
法によって靭性の評価を行った。靭性の評価は破壊靭性
Kcを求めてその大小によって行った。破壊靭性Kcは
新涼の式によって算出した。(3) Fracture toughness test In this test, toughness was evaluated by the indentation method using a Vickers hardness meter. The toughness was evaluated by determining the fracture toughness Kc. Fracture toughness Kc was calculated by Shinryo's formula.
切削テストの結果、本発明のセラミックスチップは4本
共欠損等の異常の発生は認められず、寸法の変化はQ、
1mm以内にあり問題なく且つ仕上り面も良好であった
のに対して、比較量の市販のA1□01−’[7jCセ
ラミツクスのチップは4本の内3本は加工本数138本
、196本、248本目でチップの欠損が発生した。欠
損の発生しなかったのは1本だけであり、寸法変化は0
.13+n+++と本発明品よりやや大きかったことか
ら、本発明品のセラミックス製チップは良好な耐衝撃性
と耐摩耗性を示すのに対して、比較量は相対的に靭性が
低いために耐衝撃性、耐摩耗性が劣っており、本発明の
セラミックス製チップの寿命が著しく改善されているこ
とが認められる。As a result of the cutting test, no abnormality such as chipping of the four ceramic chips of the present invention was observed, and the dimensional changes were Q.
The chip size was within 1mm, there were no problems, and the finished surface was good, whereas the comparative amount of commercially available A1□01-'[7jC Ceramics chips had three out of four chips with processed numbers of 138, 196, A chip breakage occurred on the 248th chip. Only one piece had no damage, and the dimensional change was 0.
.. 13+n+++, which was slightly larger than the inventive product, indicating that the inventive ceramic chip exhibits good impact resistance and abrasion resistance, whereas the comparative product has relatively low toughness and thus has poor impact resistance. , the wear resistance is poor, and it is recognized that the life of the ceramic chip of the present invention is significantly improved.
又試験片による試験結果を示す第1表から明らかなよう
に、曲げ強度は比較量のAl2O3−TiCの74 k
g / mm2に較べて115.3kg/mm2と改善
された強度を示しており、特に破壊靭性は比較量のKc
が4.2MPav″′iに対して7.2MPa1と著し
く上回っており靭性、耐衝撃性に優れていることが認め
られる。硬度は耐摩耗性に優れているA1□Q3−Ti
Cセラミックスと略同等の高硬度を示しており耐摩耗性
に優れていることが認められる。Also, as is clear from Table 1 showing the test results using test pieces, the bending strength is 74 k for the comparative amount of Al2O3-TiC.
It shows an improved strength of 115.3 kg/mm2 compared to Kc of the comparative amount.
It is recognized that the hardness is 7.2 MPa1, which is significantly higher than 4.2 MPav'''i, and it has excellent toughness and impact resistance.
It is recognized that it exhibits high hardness almost equivalent to that of C ceramics and has excellent wear resistance.
効果
本発明のセラミックス環の切削用チップおよび加工用工
具は衝撃に強く高靭性、耐摩耗性に優れた切削用チップ
に適するばかりでなく、更に耐熱衝撃性、耐酸化性にも
優れているので、熱間線引きロールのような熱間用加工
工具にも適用でき、長期にわたって安定した使用が可能
となった実用上の効果は顕著である。Effect The ceramic ring cutting tip and processing tool of the present invention are not only suitable for cutting tips that are strong against impact, have high toughness, and excellent wear resistance, but also have excellent thermal shock resistance and oxidation resistance. It can also be applied to hot processing tools such as hot wire drawing rolls, and has a remarkable practical effect in that it can be used stably over a long period of time.
Claims (1)
5〜50容積%;直径1μm以下、アスペクト比3〜2
00の炭化珪素ウィスカー3〜40容積%(但し、この
炭化珪素ウィスカーと前記ジルコニアの合計は55容積
%以下);残部が実質的にアルミナからなるアルミナ−
ジルコニア−炭化珪素複合焼結体で構成したことを特徴
とする切削用チップおよび加工用工具。5-50% by volume of partially stabilized zirconia with an average particle size of 0.1-1.0 μm; diameter of 1 μm or less, aspect ratio 3-2
00 silicon carbide whiskers 3 to 40% by volume (however, the total of the silicon carbide whiskers and the zirconia is 55% by volume or less); the remainder is essentially alumina.
A cutting tip and a machining tool comprising a zirconia-silicon carbide composite sintered body.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP61209581A JPS6369767A (en) | 1986-09-08 | 1986-09-08 | Cutting tip and machining tool |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP61209581A JPS6369767A (en) | 1986-09-08 | 1986-09-08 | Cutting tip and machining tool |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS6369767A true JPS6369767A (en) | 1988-03-29 |
Family
ID=16575200
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP61209581A Pending JPS6369767A (en) | 1986-09-08 | 1986-09-08 | Cutting tip and machining tool |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS6369767A (en) |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS61270266A (en) * | 1985-05-25 | 1986-11-29 | 株式会社リケン | High strength high hardness alumina-zirconia-silicon carbidecomposite sintered body and manufacture |
-
1986
- 1986-09-08 JP JP61209581A patent/JPS6369767A/en active Pending
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS61270266A (en) * | 1985-05-25 | 1986-11-29 | 株式会社リケン | High strength high hardness alumina-zirconia-silicon carbidecomposite sintered body and manufacture |
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