JPS6333897B2 - - Google Patents

Info

Publication number
JPS6333897B2
JPS6333897B2 JP55147366A JP14736680A JPS6333897B2 JP S6333897 B2 JPS6333897 B2 JP S6333897B2 JP 55147366 A JP55147366 A JP 55147366A JP 14736680 A JP14736680 A JP 14736680A JP S6333897 B2 JPS6333897 B2 JP S6333897B2
Authority
JP
Japan
Prior art keywords
liquid
mixing tank
treated
conical bottom
nozzle
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP55147366A
Other languages
Japanese (ja)
Other versions
JPS5771628A (en
Inventor
Megumi Kibe
Kazuo Tanaka
Saburo Moritomo
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Osaka Gas Co Ltd
Original Assignee
Osaka Gas Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Osaka Gas Co Ltd filed Critical Osaka Gas Co Ltd
Priority to JP55147366A priority Critical patent/JPS5771628A/en
Publication of JPS5771628A publication Critical patent/JPS5771628A/en
Publication of JPS6333897B2 publication Critical patent/JPS6333897B2/ja
Granted legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/50Mixing liquids with solids
    • B01F23/56Mixing liquids with solids by introducing solids in liquids, e.g. dispersing or dissolving
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/20Jet mixers, i.e. mixers using high-speed fluid streams
    • B01F25/21Jet mixers, i.e. mixers using high-speed fluid streams with submerged injectors, e.g. nozzles, for injecting high-pressure jets into a large volume or into mixing chambers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F2025/91Direction of flow or arrangement of feed and discharge openings
    • B01F2025/911Axial flow
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F2025/91Direction of flow or arrangement of feed and discharge openings
    • B01F2025/913Vortex flow, i.e. flow spiraling in a tangential direction and moving in an axial direction
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/50Circulation mixers, e.g. wherein at least part of the mixture is discharged from and reintroduced into a receptacle

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)

Description

【発明の詳細な説明】 本発明は、縦向きの円筒状部分と、その下部に
連なる下狭まりの正芯型錐形底部を混合槽に備え
させ、前記円筒状部分に、その内部で被処理液を
縦軸芯周りで旋回流動させるべく、前記混合槽か
ら抜出した被処理液を噴出するための第1ノズル
を付設した混合装置に関する。
DETAILED DESCRIPTION OF THE INVENTION The present invention provides a mixing tank with a vertically oriented cylindrical portion and a right-centered conical bottom portion that is continuous with the lower part of the vertically oriented cylindrical portion, and in which the cylindrical portion is provided with The present invention relates to a mixing device equipped with a first nozzle for spouting the liquid to be treated extracted from the mixing tank in order to cause the liquid to swirl around the vertical axis.

上述のようにノズルからの液噴出による旋回流
を利用して、混合を行うに、例えば混合槽底部が
平板で構成されていると、混合槽内壁面による制
動作用で、殊に底部角部分での旋回流速が大巾に
低下し、底部角部分にコーキング物質やスラリー
粒子が付着堆積するが、上述のように正芯型錐形
底部を設けると、そのような問題を抑制できる。
しかし、従来一般に行われているように、錐形底
部の下端部から被処理液を循環のために抜出す
と、その抜出し流路に旋回流による空芯から気泡
が流入しやすくて、循環用ポンプのトラブルを生
じやすく、その上、混合槽の全高を小にすべく円
筒状部分及び錐形底部の内面どうしの角度を比較
的小さくすると、その角部へのコーキング物質や
スラリー粒子の付着堆積を回避できない。
As mentioned above, when mixing is performed using the swirling flow caused by the liquid ejected from the nozzle, for example, if the bottom of the mixing tank is made of a flat plate, the inner wall of the mixing tank acts as a brake, especially at the bottom corners. The swirling flow velocity of the pipe is greatly reduced, and caulking material and slurry particles are deposited on the bottom corners, but such problems can be suppressed by providing a conical bottom with a straight core as described above.
However, when the liquid to be treated is extracted from the lower end of the conical bottom for circulation, as is commonly done in the past, air bubbles tend to flow into the extraction channel from the air core due to swirling flow, and Pump problems are likely to occur, and in addition, if the angle between the inner surfaces of the cylindrical part and the conical bottom is made relatively small in order to reduce the overall height of the mixing tank, caulking material and slurry particles may adhere to the corners and accumulate. cannot be avoided.

本発明は、上記実情に鑑みて、液抜出し流路へ
の気泡流入防止、並びに、混合槽内面へのコーキ
ング物質がスラリー粒子の付着堆積防止を、いず
れも効果的に行えるようにする事を目的とする。
In view of the above-mentioned circumstances, the present invention aims to effectively prevent air bubbles from flowing into the liquid extraction channel and prevent slurry particles from adhering to the inner surface of the mixing tank due to coking material. purpose.

次に、例示図により本発明の実施態様を説明す
る。
Next, embodiments of the present invention will be described with reference to illustrative figures.

縦向きの円筒状部分1a、その下部に連なる下
狭まりの正芯型錐形底部1b、及び、天井部1c
によつて混合槽1を形成し、コーキング性向の強
い液やスラリー等の被処理液を定量的に連続供給
する供給管2を混合槽1の上部に接続し、円筒状
部分1aに、その内部に被処理液を縦軸芯周りで
旋回流動させるべく、第1ポンプ付管路3により
混合槽1から抜出した被処理液を噴出するための
第1ノズル4を付設し、錐形底部1bの下端部
に、第1ポンプ付管路3からの被処理液を吹上げ
る第2ノズル5を付設し、錐形底部1bの下端寄
りに、錐形底部1b内でその中心軸芯周りで旋回
しながら上昇流動させるべく、各別の第2ポンプ
付管路6a,6bにより混合槽1から抜出した被
処理液を噴出する2個の第3ノズル7a,7bを
設け、処理済の液を定量的に連続排出する排出管
路8を混合槽1に接続し、もつて、連続的に混合
処理し、必要に応じて反応処理するための装置を
構成してある。
A vertically oriented cylindrical portion 1a, a right-centered conical bottom portion 1b that narrows downward, and a ceiling portion 1c.
A mixing tank 1 is formed by forming a mixing tank 1, and a supply pipe 2 that continuously supplies a liquid to be treated such as a liquid with a strong coking tendency or slurry in a quantitative manner is connected to the upper part of the mixing tank 1. In order to make the liquid to be treated swirl around the vertical axis, a first nozzle 4 for spouting out the liquid to be treated drawn out from the mixing tank 1 through a pipe line 3 with a first pump is attached, and a first nozzle 4 is attached to the conical bottom part 1b. A second nozzle 5 for blowing up the liquid to be treated from the first pump-equipped pipe line 3 is attached to the lower end, and the second nozzle 5 rotates around the central axis within the conical bottom 1b near the lower end of the conical bottom 1b. Two third nozzles 7a and 7b are provided to eject the liquid to be treated extracted from the mixing tank 1 through separate conduits 6a and 6b with second pumps in order to cause the liquid to flow upward while the liquid is being treated quantitatively. A discharge pipe 8 for continuous discharge is connected to the mixing tank 1, thereby forming an apparatus for continuous mixing treatment and reaction treatment as required.

前記第1及び第3ノズル4,7a,7bのいず
れも、その先端を混合槽1内に突出させない状態
で、かつ、混合槽1内周面に対してほぼ接線方向
に向く状態で設けて、ノズル4,7a,7bに起
因してコーキング物質やスラリー粒子が付着堆積
する事を防止すると共に、混合槽1内での被処理
液旋回を効率良く行えるようにしてある。
Each of the first and third nozzles 4, 7a, 7b is provided such that its tip does not protrude into the mixing tank 1 and is oriented substantially tangentially to the inner peripheral surface of the mixing tank 1, This prevents coking substances and slurry particles from adhering and accumulating due to the nozzles 4, 7a, and 7b, and enables efficient swirling of the liquid to be treated within the mixing tank 1.

前記第1及び第2ポンプ付管路3,6a,6
b、並びに、排出管路8入口を、混合槽1内に突
出させない状態で、かつ、混合槽1内周面に対し
てほぼ接線方向に向く状態で、円筒状部分1aと
錐形底部1bの境界部A付近に配置して、それら
管路3,6a,6b,8の入口側部分に起因して
コーキング物質やスラリー粒子が付着堆積する事
を防止すると共に、混合槽1内での被処理液旋回
を助長し、かつ、円筒状部分1aと錐形底部1b
の内面どうしの角度θを比較的小さくして、混合
槽の全高lを小に構成しても、上記境界部A付近
でのコーキング物質がスラリー粒子の付着堆積を
防止できるようにしてある。
Said first and second pumped pipe lines 3, 6a, 6
b, and the cylindrical portion 1a and the conical bottom portion 1b in a state in which the inlet of the discharge pipe 8 does not protrude into the mixing tank 1 and is oriented substantially tangentially to the inner peripheral surface of the mixing tank 1. It is arranged near the boundary part A to prevent coking substances and slurry particles from adhering and accumulating due to the inlet side parts of these pipes 3, 6a, 6b, and 8, and to prevent The cylindrical portion 1a and the conical bottom portion 1b
Even if the angle θ between the inner surfaces of the mixing tank is made relatively small and the total height l of the mixing tank is made small, the coking substance can prevent slurry particles from adhering and accumulating near the boundary A.

尚、前述のように、第1ポンプ付管路3からの
被処理液を第1及び第2ノズル4,5に分配供給
すると、高濃度の被処理液を混合槽1の上下に分
配できて、均一混合の面から有利であるが、例え
ば、第1ポンプ付管路3を第1及び第2ノズル
4,5の一方にのみ接続して、他方には別の循環
用ポンプ付管路を接続したり、あるいは、第2ポ
ンプ付管路6a,6bを省略して、第1ポンプ付
管路3を第1ないし第3ノズル4,5,6a,6
bの全てに接続したり、その他各種の流路構成変
更が可能であり、要するに、混合槽1内の被処理
液をその循環のために取出す管路3あるいは6
a,6bを、円筒状部分1aと錐形底部1bの境
界部Aあるいはその近くに接続してあればよい。
As mentioned above, when the liquid to be treated from the first pump conduit 3 is distributed and supplied to the first and second nozzles 4 and 5, the liquid to be treated with high concentration can be distributed to the upper and lower parts of the mixing tank 1. This is advantageous in terms of uniform mixing, but for example, it is possible to connect the first pump-equipped pipe 3 to only one of the first and second nozzles 4 and 5, and connect the other pump-equipped pipe to the other. Alternatively, by omitting the second pump-equipped pipelines 6a and 6b, the first pump-equipped pipeline 3 is connected to the first to third nozzles 4, 5, 6a, 6.
b. It is possible to connect to all of the pipes 3 or 6, or to change the flow path configuration in various ways. In short, it is possible to connect to all of
a, 6b may be connected at or near the boundary A between the cylindrical portion 1a and the conical bottom portion 1b.

前記第1ノズル4を複数個設けてもよく、ま
た、一個の第3ノズル7を設けてよく、さらに、
複数個設ける場合、同種のノズルを、互に混合槽
1の周方向や上下方向に位置が異る状態で配置し
てもよい。
A plurality of the first nozzles 4 may be provided, or one third nozzle 7 may be provided, and further,
When a plurality of nozzles are provided, the same type of nozzles may be arranged at different positions in the circumferential direction or the vertical direction of the mixing tank 1.

前記円筒状部分1a及び錐形底部1bの形状
は、幾何学的観念に厳密に拘束されるものでは無
く、本発明の技術思想を損わない範囲で変更が可
能である。
The shapes of the cylindrical portion 1a and the conical bottom portion 1b are not strictly limited to geometrical concepts, and can be changed without impairing the technical idea of the present invention.

以上要するに、本発明は、冒記混合装置におい
て、前記錐形底部1bの下端部から前記混合槽1
内にそこから抜出した被処理液を吹上げる第2ノ
ズル5を設け、前記錐形底部1b内でその中心軸
芯周りで旋回しながら上昇流動させるべく、前記
混合槽1から抜出した被処理液を前記錐形底部1
b内に噴出する第3ノズル7を設け、前記円筒状
部分1aと錐形底部1bの境界部分Aあるいはそ
の近くに、前記混合槽1内の被処理液をその循環
のために取出す管路3あるいは6a,6bを接続
してある事を特徴とする。
In summary, the present invention provides the above-mentioned mixing device, in which the mixing tank 1 is
A second nozzle 5 is provided in the interior of the mixing tank 1 to blow up the liquid to be treated, which is drawn out from the mixing tank 1, so that the liquid to be treated flows upwardly while rotating around its central axis within the conical bottom 1b. The conical bottom 1
A third nozzle 7 ejecting into the mixing tank 1 is provided at or near the boundary A between the cylindrical portion 1a and the conical bottom portion 1b, and a conduit 3 for taking out the liquid to be treated in the mixing tank 1 for circulation. Alternatively, it is characterized in that 6a and 6b are connected.

すなわち、第2ノズル5の作用により錐形底部
1bの下端部における流速を大に維持すると共
に、第3ノズル7の作用により錐形底部1b内面
付近の流速を大に維持する事によつて、錐形底部
1bへのコーキング物質やスラリー粒子の付着堆
積を効果的に防止できるようになり、さらに、第
2及び第3ノズル5,7の協働作用により錐形底
部1b内の被処理液を円筒状部分1a側に流動さ
せると共に、円筒状部分1aと錐形底部1bとの
境界部分Aあるいはその近くから被処理液を排出
する事によつて、たとえ円筒状部分1a及び錐形
底部1bの内面どうしの角度θを比較的小さくし
て、混合槽の全高lを小に構成しても、境界部分
A及びその近くにおける流速をも大に維持でき、
そこでのコーキング物質やスラリー粒子の付着堆
積も効果的に防止でき、全体として、コーキング
物質やスラリー粒子の付着堆積に起因する装置的
トラブルや混合不均一を防止して、良好な混合を
確実に行えるようになつた。
That is, by maintaining a high flow velocity at the lower end of the conical bottom part 1b by the action of the second nozzle 5, and by maintaining a high flow velocity near the inner surface of the conical bottom part 1b by the action of the third nozzle 7, It is now possible to effectively prevent the adhesion and accumulation of caulking substances and slurry particles on the conical bottom part 1b, and furthermore, the cooperative action of the second and third nozzles 5 and 7 allows the liquid to be treated in the conical bottom part 1b to be removed. By causing the liquid to flow toward the cylindrical portion 1a side and discharging the liquid from the boundary portion A between the cylindrical portion 1a and the conical bottom portion 1b or its vicinity, even if the liquid is Even if the angle θ between the inner surfaces is made relatively small and the total height l of the mixing tank is made small, the flow velocity at and near the boundary portion A can also be maintained high;
The adhesion and accumulation of coking substances and slurry particles can also be effectively prevented, and as a whole, equipment troubles and uneven mixing caused by adhesion and accumulation of caulking substances and slurry particles can be prevented, and good mixing can be ensured. It became like that.

その上、均一混合のために混合槽1に対して循
環すべく被処理液を取出す管路3あるいは6a,
6bが、混合槽1に液旋回中心から横方向に離れ
た位置で接続されているから、液旋回で生じる空
芯から管路3あるいは6a,6bに気泡が流入せ
ず、循環用ポンプのトラブルも効果的に抑制で
き、より一層装置の安定作動を確実に行えるよう
になつた。
In addition, a pipe line 3 or 6a for taking out the liquid to be treated to be circulated to the mixing tank 1 for uniform mixing;
6b is connected to the mixing tank 1 at a position laterally away from the liquid swirling center, so air bubbles do not flow into the pipes 3 or 6a and 6b from the air core caused by liquid swirling, which prevents problems with the circulation pump. This also effectively suppresses the amount of heat generated, making it possible to ensure even more stable operation of the device.

【図面の簡単な説明】[Brief explanation of the drawing]

図面は本発明に係る混合装置の実施の態様を例
示し、第1図は概略縦断面図、第2図は第1図の
−線断面図である。 1……混合槽、1a……円筒状部分、1b……
錐形底部、3あるいは6a,6b……取出管路、
4……第1ノズル、5……第2ノズル、7……第
3ノズル、A……境界部分。
The drawings illustrate an embodiment of the mixing device according to the present invention, and FIG. 1 is a schematic longitudinal sectional view, and FIG. 2 is a sectional view taken along the line -- in FIG. 1. 1... Mixing tank, 1a... Cylindrical part, 1b...
Conical bottom, 3 or 6a, 6b...take-out pipe,
4...First nozzle, 5...Second nozzle, 7...Third nozzle, A...Boundary portion.

Claims (1)

【特許請求の範囲】[Claims] 1 縦向きの円筒状部分1aと、その下部に連な
る下狭まりの正芯型錐形底部1bを混合槽1に備
えさせ、前記円筒状部分1aに、その内部で被処
理液を縦軸芯周りで旋回流動させるべく、前記混
合槽1から抜出した被処理液を噴出するための第
1ノズル4を付設した混合装置であつて、前記錐
形底部1bの下端部から前記混合槽1内にそこか
ら抜出した被処理液を吹上げる第2ノズル5を設
け、前記錐形底部1b内でその中心軸芯周りで旋
回しながら上昇流動させるべく、前記混合槽1か
ら抜出した被処理液を前記錐形底部1b内に噴出
する第3ノズル7を設け、前記円筒状部分1aと
錐形底部1bの境界部分Aあるいはその近くに、
前記混合槽1内の被処理液をその循環のために取
出す管路3あるいは6a,6bを接続してある事
を特徴とする混合装置。
1. The mixing tank 1 is equipped with a vertically oriented cylindrical portion 1a and a right-centered conical bottom portion 1b that is continuous at the bottom and narrows downward, and the liquid to be treated is distributed inside the cylindrical portion 1a around the vertical axis. The mixing device is equipped with a first nozzle 4 for spouting out the liquid to be treated extracted from the mixing tank 1 in order to swirl and flow the liquid into the mixing tank 1 from the lower end of the conical bottom 1b. A second nozzle 5 is provided to blow up the liquid to be treated extracted from the mixing tank 1, and the liquid to be treated drawn from the mixing tank 1 is directed upwardly in the conical bottom part 1b while rotating around its central axis. A third nozzle 7 ejecting into the shaped bottom part 1b is provided at or near the boundary part A between the cylindrical part 1a and the conical bottom part 1b,
A mixing device characterized in that a pipe line 3 or 6a, 6b is connected to take out the liquid to be treated in the mixing tank 1 for circulation.
JP55147366A 1980-10-20 1980-10-20 Mixer Granted JPS5771628A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP55147366A JPS5771628A (en) 1980-10-20 1980-10-20 Mixer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP55147366A JPS5771628A (en) 1980-10-20 1980-10-20 Mixer

Publications (2)

Publication Number Publication Date
JPS5771628A JPS5771628A (en) 1982-05-04
JPS6333897B2 true JPS6333897B2 (en) 1988-07-07

Family

ID=15428584

Family Applications (1)

Application Number Title Priority Date Filing Date
JP55147366A Granted JPS5771628A (en) 1980-10-20 1980-10-20 Mixer

Country Status (1)

Country Link
JP (1) JPS5771628A (en)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3342016C2 (en) * 1983-11-22 1986-11-13 VLT Gesellschaft für verfahrenstechnische Entwicklung mbH, 7000 Stuttgart Device for mixing and settling liquids containing particles
JP4889452B2 (en) * 2006-11-13 2012-03-07 水道機工株式会社 Powder mixing method and powder mixer
JP5771099B2 (en) * 2011-01-26 2015-08-26 株式会社タクマ Fermentation processing apparatus and method for generating combustible gas in fermentation processing
JP5466732B2 (en) * 2012-06-21 2014-04-09 月島機械株式会社 Method for producing reactive aggregated particles, method for producing positive electrode active material for lithium ion battery, method for producing lithium ion battery, and apparatus for producing reactive aggregated particles
JP5619837B2 (en) * 2012-08-28 2014-11-05 月島機械株式会社 Continuous reaction equipment for inorganic particles
JP6255649B2 (en) * 2013-12-25 2018-01-10 月島機械株式会社 Continuous reaction crystallization apparatus and inorganic particle continuous reaction crystallization method
JP6660609B2 (en) * 2018-03-15 2020-03-11 日立金属株式会社 Slurry storage stirring device and slurry stirring method
CN112225571A (en) * 2020-09-30 2021-01-15 曹芬 Refractory material processing device

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Publication number Publication date
JPS5771628A (en) 1982-05-04

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