JPS63230625A - Bath liquid - Google Patents

Bath liquid

Info

Publication number
JPS63230625A
JPS63230625A JP62065369A JP6536987A JPS63230625A JP S63230625 A JPS63230625 A JP S63230625A JP 62065369 A JP62065369 A JP 62065369A JP 6536987 A JP6536987 A JP 6536987A JP S63230625 A JPS63230625 A JP S63230625A
Authority
JP
Japan
Prior art keywords
extract
skin
parts
bath
bathing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP62065369A
Other languages
Japanese (ja)
Inventor
Osamu Ushio
牛尾 理
Takanobu Kashiwabara
柏原 孝信
Junichiro Mesaki
潤一郎 目崎
Akira Nishimura
昭 西村
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Earth Corp
Original Assignee
Earth Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Earth Chemical Co Ltd filed Critical Earth Chemical Co Ltd
Priority to JP62065369A priority Critical patent/JPS63230625A/en
Publication of JPS63230625A publication Critical patent/JPS63230625A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]

Abstract

PURPOSE:To obtain a bath liquid capable of providing smoothness to a skin in bathing and having beauty effect such as keeping the skin after bathing in a moist state as well as excellent effect such as prevention and improvement of skin from chapping and cell activation of the skin, by blending the extract of sponge gourd. CONSTITUTION:An optional part of whole the sponge gourd grass is directly or after dividing into fine pieces immersed in a water-soluble solvent warmed, filtered to afford the extract solution, which is then condensed to provide the extract, which is further subjected to spray drying treatment to give dry extract, which is blended in an amount of 0.01-10wt.%, preferably 0.1-5wt.% in the total amount of bath liquid.

Description

【発明の詳細な説明】 〔産業上の利用分野〕 本発明は、ヘチマの抽出物を配合してなる浴用剤に関す
る。
DETAILED DESCRIPTION OF THE INVENTION [Industrial Field of Application] The present invention relates to a bath agent containing a loofah extract.

〔従来の技術〕[Conventional technology]

一般に、浴用剤は粉末及び顆粒の場合には、保温効果を
目的とするために、硫酸ナトリウム、炭酸ナトリウム、
炭酸水素ナトリウム等を主剤としており、発泡性を付与
するには、上記成分にリンゴ酸、コハク酸、アジピン酸
等の有機酸が加えられる。又、浴用剤が液体の場合には
、皮膚の保護を目的としたり或は皮膚への感触を良くす
るために、例えばラノリン、ラノリン誘導体、イソプロ
ピルアルコール、イソプロピルミリステート、スクワラ
ン、グリセリン、その他の各種動植物油及びそのエステ
ル類等の柔軟剤を主剤としており、これに色素、香料、
殺菌剤などを加えたものが大部分を占めている。
Generally, in the case of powders and granules, bath additives contain sodium sulfate, sodium carbonate, etc. for the purpose of heat retention.
The main ingredient is sodium hydrogen carbonate, and to impart foaming properties, organic acids such as malic acid, succinic acid, and adipic acid are added to the above ingredients. In addition, when the bath agent is a liquid, it may contain lanolin, lanolin derivatives, isopropyl alcohol, isopropyl myristate, squalane, glycerin, and other various substances for the purpose of skin protection or to improve the feel of the skin. The main ingredients are fabric softeners such as animal and vegetable oils and their esters, along with pigments, fragrances, and
Most of the ingredients contain disinfectants and other additives.

〔発明が解決しようとする問題点〕[Problem that the invention seeks to solve]

上記のように従来の粉末浴用剤は、温泉構成成分の一部
を配合したものが多く、主として保温、血行促進効果を
目的としているため、皮膚への感触の点では劣っている
0発泡性を付与したものも、同等の効果しかない、又、
液体浴用剤の場合は、皮膚への感触を良くするために皮
膚柔軟剤が使用されているが、これらもその配合量に問
題があり、使用量は限定されている。しかも、乳化、可
溶化のために多量の界面活性剤を必要とする欠点も有し
ている。
As mentioned above, conventional powder bath preparations often contain some of the hot spring constituents, and are mainly aimed at retaining heat and promoting blood circulation. The ones given have the same effect, and
In the case of liquid bath preparations, emollients are used to improve the feel on the skin, but these also have problems with their blending amount, and the amount used is limited. Moreover, it also has the disadvantage of requiring a large amount of surfactant for emulsification and solubilization.

さらに、入浴時の気分を楽しくしたり、疲労回復等の効
果に加え、肌にしっとり、なめらかな感じを与える効果
を有する浴用剤が望まれているにもかかわらず、従来の
浴用剤には美容的効果を有 。
Furthermore, although there is a desire for bath additives that have the effect of making the skin feel moisturized and smooth, in addition to making people feel more comfortable while bathing and relieving fatigue, conventional bath additives are It has a certain effect.

するものがみられない。I can't see anything to do.

、そこで、本発明者は、従来の浴用剤の欠点である皮膚
への感触を改善すべく研究した結果、ウリ科植物のヘチ
マの抽出物が極めて有用であることを見出した。
Therefore, the present inventor conducted research to improve the skin feel, which is a drawback of conventional bath preparations, and found that an extract of loofah, a plant of the Cucurbitaceae family, is extremely useful.

〔問題点を解決するための手段〕[Means for solving problems]

すなわち、本発明の浴用剤は、ヘチマの抽出物を配合し
てなるものである。
That is, the bath agent of the present invention contains a loofah extract.

本発明で使用するヘチマは、ウリ科(Cucurbi−
taceae)ルフ7”シンドリカ・ロエム(Luff
a Cy−indrica M、Roe+5en)であ
り、その抽出物は、ヘチマ全草の任意の部分、すなわち
ヘチマの葉、茎、根、望ましくは果実から得ることがで
きる。
The loofah used in the present invention is from the Cucurbitaceae family (Cucurbitaceae).
taceae) Luff 7” Cindrika Roem (Luff
a Cy-indrica M, Roe+5en), the extract of which can be obtained from any part of the whole loofah plant, namely the leaves, stems, roots, and preferably fruits of the loofah.

前記、抽出物は、以下の抽出操作によって調整すること
ができる。
The above-mentioned extract can be prepared by the following extraction operation.

まず、第1段階の抽出操作としてヘチマ原料をそのまま
の形で又は細片化してから、水溶性溶媒、例えば水、又
はメチルアルコール、エチルアルコール、n−プロピル
アルコール、イソプロピルアルコール、n−ブチルアル
コール等のアルコール、及びこれらの含水アルコールに
温浸し、濾過して得られる抽出液を濃縮する。このよう
にして得られた赤褐色の抽出エキスをさらに濃縮した後
、n−ブタノールと水に分配し、ブタノール層を濃縮し
て、ヘチマ粗サポニンを得、それをシリカゲルクロマト
グラフィーなどの吸着系クロマトグラフィーを用いて分
画してルシオシドを得る。本発明で使用するヘチマの抽
出物は、この第1段階の抽出操作により得られる抽出液
、あるいはその抽出液を濃縮したもの、さらにはスプレ
ードライ処理により得られる乾燥エキス等が好ましい。
First, in the first stage extraction operation, the loofah raw material is used as it is or after being cut into pieces, using a water-soluble solvent such as water, methyl alcohol, ethyl alcohol, n-propyl alcohol, isopropyl alcohol, n-butyl alcohol, etc. alcohol and these hydrous alcohols, and the extract obtained by filtration is concentrated. After further concentrating the reddish-brown extract obtained in this way, it is partitioned between n-butanol and water, and the butanol layer is concentrated to obtain loofah crude saponin, which is then subjected to adsorption chromatography such as silica gel chromatography. to obtain lucioside. The loofah extract used in the present invention is preferably an extract obtained by the first stage extraction operation, a concentrated extract thereof, or a dried extract obtained by spray drying.

本発明のヘチマの抽出物の配合量は、浴用剤の重量中、
乾燥固形分として0.01〜10重量%、好ましくは0
.1〜5重量%である。
The blending amount of the loofah extract of the present invention is based on the weight of the bath additive.
0.01 to 10% by weight as dry solids, preferably 0
.. It is 1 to 5% by weight.

本発明の浴用剤原料としては、浴用剤をつくるために用
いられる原料をすべて用いることができる。例えば粉末
及び顆粒の場合には、硫酸ナトリウム、炭酸ナトリウム
、炭酸水素ナトリウム、セスキ炭酸ナトリウム、硼砂、
塩化ナトリウム、塩化カリウム等の無機塩、クエン酸、
リンゴ酸、酒石酸、コハク酸、フマル酸、アジピン酸等
の有機酸が、液体の場合には、精製水、エチルアルコー
ル、多価アルコール類を主剤とし、その他必要に応じて
油脂類、炭化水素類、脂肪酸類、高級アルコール類、エ
ステル類、界面活性剤類、植物の抽出物、殺菌防腐剤、
増粘剤、ビタミン類、香料、色素などがあげられ、これ
らの原料は、適当なものを選択し、組合わせて用いるこ
とができる。
All raw materials used for making bath agents can be used as the raw materials for bath agents of the present invention. For example, in the case of powders and granules, sodium sulfate, sodium carbonate, sodium bicarbonate, sodium sesquicarbonate, borax,
Inorganic salts such as sodium chloride and potassium chloride, citric acid,
When organic acids such as malic acid, tartaric acid, succinic acid, fumaric acid, and adipic acid are in liquid form, the main ingredients are purified water, ethyl alcohol, and polyhydric alcohols, and other oils and fats and hydrocarbons as necessary. , fatty acids, higher alcohols, esters, surfactants, plant extracts, bactericidal preservatives,
Examples include thickeners, vitamins, fragrances, pigments, etc. These raw materials can be appropriately selected and used in combination.

〔作用〕[Effect]

上記手段を施した結果、本発明の浴用剤は、保水作用に
優れ肌をしっとりとなめらかに保つ。
As a result of the above measures, the bath preparation of the present invention has excellent water-retaining properties and keeps the skin moist and smooth.

〔実施例〕〔Example〕

以下、実施例によって本発明の詳細な説明するが、これ
は本発明の技術的範囲を限定するものではない。
EXAMPLES Hereinafter, the present invention will be explained in detail with reference to Examples, but these are not intended to limit the technical scope of the present invention.

実施例−1 乾燥硫酸ナトリウム60部、炭酸水素ナトリウム37部
、ヘチマ軟エキス1部、香料1.2部、黄色202号−
(1) 0.3部、プロピレングリコール0.5部を順
次に加え混合し、均一として粉末浴用剤を得る。
Example-1 60 parts of dry sodium sulfate, 37 parts of sodium hydrogen carbonate, 1 part of loofah soft extract, 1.2 parts of fragrance, Yellow No. 202-
(1) 0.3 part and 0.5 part of propylene glycol were added and mixed in order to obtain a powdered bath agent.

実施例−2 アジピン酸45部、炭酸水素ナトリウム35部、炭酸ナ
トリウム10部、ヘチマ乾燥エキス1部、乾燥硫酸ナト
リウム8部、香料0.5部、リボフラビン0.1部、無
水ケイ酸0.4部を順次に加え混合し、均一としてロー
タリー打錠機にて直打し発泡錠剤浴用剤を得る。
Example-2 45 parts of adipic acid, 35 parts of sodium bicarbonate, 10 parts of sodium carbonate, 1 part of dried loofah extract, 8 parts of dry sodium sulfate, 0.5 part of fragrance, 0.1 part of riboflavin, 0.4 part of silicic anhydride The mixture was added one by one, mixed, homogenized, and directly pressed using a rotary tablet machine to obtain effervescent tablet bath preparations.

実施例−3 ポリオキシエチレンラノリンアルコール1部にエチルア
ルコール50部を加え溶解した液に、香料4部、グリセ
リン30部、ピロリドンカルボン酸ナトリウム(50%
水溶液)3部、ヘチマエキス5部、精製水7部を順次に
加え、攪拌混合し均一とした後、濾過して液体浴用剤を
得る。
Example 3 Add 50 parts of ethyl alcohol to 1 part of polyoxyethylene lanolin alcohol, add 4 parts of fragrance, 30 parts of glycerin, and sodium pyrrolidone carboxylate (50%
3 parts of aqueous solution), 5 parts of loofah extract, and 7 parts of purified water were sequentially added, stirred and mixed until the mixture was homogeneous, and then filtered to obtain a liquid bath agent.

次に、本発明の浴用剤と従来の浴用剤を用い、入浴惑判
定試験を行った結果について述べる。
Next, the results of a bathing sensation determination test using the bath additives of the present invention and conventional bath additives will be described.

入浴感判定試験例 乾燥硫酸ナトリウム60部、炭酸水素ナトリウム38部
、香料1.5部、黄色202号−(1) 0.5部を順
次に加え混合し、均一として浴用剤−A(従来品)を得
る。
Bathing sensation evaluation test example 60 parts of dry sodium sulfate, 38 parts of sodium bicarbonate, 1.5 parts of fragrance, and 0.5 part of Yellow No. 202-(1) were added in sequence and mixed until homogeneous. ).

乾燥硫酸ナトリウム60部、炭酸水素ナトリウム37.
9部、香料1.5部、黄色202号−fl) 0.5部
、ヘチマ乾燥エキス0.1部を順次に加え混合し、均一
として浴用剤−B(本発明品)を得る。
60 parts of dry sodium sulfate, 37 parts of sodium bicarbonate.
9 parts, 1.5 parts of perfume, 0.5 part of Yellow No. 202-fl), and 0.1 part of dried loofah extract were added and mixed to obtain a homogeneous bath agent-B (product of the present invention).

乾燥硫酸ナトリウム60部、炭酸水素ナトリウム37.
5部、香料1.5部、黄色202号−(110,5部、
ヘチマ乾燥エキス0.5部を順次に加え混合し、均一と
して浴用剤−〇(本発明品)を得る。
60 parts of dry sodium sulfate, 37 parts of sodium bicarbonate.
5 parts, fragrance 1.5 parts, yellow No. 202-(110.5 parts,
Add 0.5 part of dried loofah extract one by one and mix to obtain a homogeneous bath agent-0 (product of the present invention).

乾燥硫酸ナトリウム60部、炭酸水素ナトリウム37部
、香料1.5部、黄色202号−(1) 0.5部、ヘ
チマ乾燥エキス1部を順次に加え混合し、均一として浴
用剤=D(本発明品)を得る。
60 parts of dry sodium sulfate, 37 parts of sodium bicarbonate, 1.5 parts of fragrance, 0.5 part of Yellow No. 202-(1), and 1 part of dried loofah extract were added and mixed in order to make a homogeneous bath agent = D (this product). invention).

以上得られた浴用剤(15g入り)をパネラ−40名に
配付し、使用時、使用後の入浴惑の評価を依頼した。パ
ネラ−40名は■群〜■群に分け、パネラ−1群は浴用
剤A−B−C−Dの順に使用し、n群は浴用剤B−C4
D−Aの順に使用し、■群は浴用剤C−D−A→Bの順
に使用し、■群は浴用剤D−A−B−Cの順に使用する
。各浴用剤は、1週間で5包使用し、終了毎にアンケー
ト表を回収し、4週間後すべて終了し集計した。各項目
につき、肯定的評価を集計すると第1表に示すようにな
った。
The bath additives (containing 15 g) obtained above were distributed to 40 panelists and asked to evaluate their bathing sensations during and after use. The 40 panelists were divided into Groups ■ to Group ■, and Group 1 used bath additives A-B-C-D in that order, and Group N used bath additives B-C4.
Use the bath additives in the order of D-A, group (2) use the bath additives C-DA in the order B, and group (2) use the bath additives D-A-B-C in the order. Five packages of each bath preparation were used in one week, and questionnaires were collected after each use, and after 4 weeks, all tests were completed and tabulated. Table 1 shows the total number of positive evaluations for each item.

(以下余白) 表−1 〔発明の効果〕 本発明は、以上に述べたように構成されているので、入
浴時の肌になめらかさを付与し、かつ入浴後の肌をしっ
とりと保つなどの美容的効果を有すると共に、肌荒防止
、肌荒改善及び皮膚の細胞賦活等の優れた効果を有する
(Margin below) Table 1 [Effects of the Invention] Since the present invention is configured as described above, it can provide smoothness to the skin during bathing and keep the skin moist after bathing. In addition to having cosmetic effects, it also has excellent effects such as preventing rough skin, improving rough skin, and activating skin cells.

Claims (1)

【特許請求の範囲】[Claims] 1、ヘチマ(Luffa cyindrica M.R
oemen)の抽出物を配合してなることを特徴とする
浴用剤。
1. Luffa cyindrica M.R.
A bath agent characterized by containing an extract of ``Oemen''.
JP62065369A 1987-03-18 1987-03-18 Bath liquid Pending JPS63230625A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP62065369A JPS63230625A (en) 1987-03-18 1987-03-18 Bath liquid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP62065369A JPS63230625A (en) 1987-03-18 1987-03-18 Bath liquid

Publications (1)

Publication Number Publication Date
JPS63230625A true JPS63230625A (en) 1988-09-27

Family

ID=13284981

Family Applications (1)

Application Number Title Priority Date Filing Date
JP62065369A Pending JPS63230625A (en) 1987-03-18 1987-03-18 Bath liquid

Country Status (1)

Country Link
JP (1) JPS63230625A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0449226A (en) * 1990-06-15 1992-02-18 Masaichi Sakurashita Green tea bath medicine

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0449226A (en) * 1990-06-15 1992-02-18 Masaichi Sakurashita Green tea bath medicine

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