JPS62252301A - 高純度過酸化水素化チタン水溶液の製造法 - Google Patents
高純度過酸化水素化チタン水溶液の製造法Info
- Publication number
- JPS62252301A JPS62252301A JP9358386A JP9358386A JPS62252301A JP S62252301 A JPS62252301 A JP S62252301A JP 9358386 A JP9358386 A JP 9358386A JP 9358386 A JP9358386 A JP 9358386A JP S62252301 A JPS62252301 A JP S62252301A
- Authority
- JP
- Japan
- Prior art keywords
- titanium
- hydrogen peroxide
- aqueous solution
- high purity
- aqueous
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000007864 aqueous solution Substances 0.000 title claims abstract description 28
- DJGLQWCKPYQFJG-UHFFFAOYSA-N hydrogen peroxide;titanium Chemical compound [Ti].OO DJGLQWCKPYQFJG-UHFFFAOYSA-N 0.000 title claims description 16
- 238000004519 manufacturing process Methods 0.000 title claims description 8
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 38
- -1 titanium alkoxide Chemical class 0.000 claims abstract description 13
- 239000010936 titanium Substances 0.000 claims abstract description 12
- 229910052719 titanium Inorganic materials 0.000 claims abstract description 12
- 239000000243 solution Substances 0.000 claims description 11
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 abstract description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 7
- 239000000835 fiber Substances 0.000 abstract description 4
- 238000001816 cooling Methods 0.000 abstract description 3
- 239000005457 ice water Substances 0.000 abstract description 3
- 150000001299 aldehydes Chemical class 0.000 abstract description 2
- 150000002576 ketones Chemical class 0.000 abstract description 2
- 230000003647 oxidation Effects 0.000 abstract description 2
- 238000007254 oxidation reaction Methods 0.000 abstract description 2
- 239000000843 powder Substances 0.000 abstract description 2
- UYFXJSBYTIMJAH-UHFFFAOYSA-J [Ti+4].[O-]O.[O-]O.[O-]O.[O-]O Chemical compound [Ti+4].[O-]O.[O-]O.[O-]O.[O-]O UYFXJSBYTIMJAH-UHFFFAOYSA-J 0.000 abstract 2
- 150000004703 alkoxides Chemical class 0.000 abstract 1
- 125000003545 alkoxy group Chemical group 0.000 abstract 1
- HHFAWKCIHAUFRX-UHFFFAOYSA-N ethoxide Chemical compound CC[O-] HHFAWKCIHAUFRX-UHFFFAOYSA-N 0.000 abstract 1
- 239000010408 film Substances 0.000 abstract 1
- ZEIWWVGGEOHESL-UHFFFAOYSA-N methanol;titanium Chemical compound [Ti].OC.OC.OC.OC ZEIWWVGGEOHESL-UHFFFAOYSA-N 0.000 abstract 1
- 238000006467 substitution reaction Methods 0.000 abstract 1
- 239000004408 titanium dioxide Substances 0.000 abstract 1
- 238000005292 vacuum distillation Methods 0.000 abstract 1
- 239000012855 volatile organic compound Substances 0.000 abstract 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 12
- 239000002994 raw material Substances 0.000 description 11
- 239000007787 solid Substances 0.000 description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
- 239000000047 product Substances 0.000 description 8
- 239000001257 hydrogen Substances 0.000 description 6
- 229910052739 hydrogen Inorganic materials 0.000 description 6
- 239000012535 impurity Substances 0.000 description 6
- LLZRNZOLAXHGLL-UHFFFAOYSA-J titanic acid Chemical compound O[Ti](O)(O)O LLZRNZOLAXHGLL-UHFFFAOYSA-J 0.000 description 6
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 3
- 238000009833 condensation Methods 0.000 description 3
- 230000005494 condensation Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000000499 gel Substances 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- DCKVFVYPWDKYDN-UHFFFAOYSA-L oxygen(2-);titanium(4+);sulfate Chemical compound [O-2].[Ti+4].[O-]S([O-])(=O)=O DCKVFVYPWDKYDN-UHFFFAOYSA-L 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 229910000348 titanium sulfate Inorganic materials 0.000 description 2
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 2
- RCZPHVPIOWNERS-UHFFFAOYSA-N CCCO[Ti] Chemical group CCCO[Ti] RCZPHVPIOWNERS-UHFFFAOYSA-N 0.000 description 1
- ZBZXIGONWYKEMZ-UHFFFAOYSA-N CCO[Ti] Chemical compound CCO[Ti] ZBZXIGONWYKEMZ-UHFFFAOYSA-N 0.000 description 1
- FLTYUJMFMHOICO-UHFFFAOYSA-N CO[Ti] Chemical compound CO[Ti] FLTYUJMFMHOICO-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000011362 coarse particle Substances 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- 229910001882 dioxygen Inorganic materials 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 230000020169 heat generation Effects 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 235000015110 jellies Nutrition 0.000 description 1
- 239000008274 jelly Substances 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000005502 peroxidation Methods 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 150000003608 titanium Chemical class 0.000 description 1
- 230000002747 voluntary effect Effects 0.000 description 1
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9358386A JPS62252301A (ja) | 1986-04-23 | 1986-04-23 | 高純度過酸化水素化チタン水溶液の製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9358386A JPS62252301A (ja) | 1986-04-23 | 1986-04-23 | 高純度過酸化水素化チタン水溶液の製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS62252301A true JPS62252301A (ja) | 1987-11-04 |
| JPH0369842B2 JPH0369842B2 (enrdf_load_stackoverflow) | 1991-11-05 |
Family
ID=14086297
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP9358386A Granted JPS62252301A (ja) | 1986-04-23 | 1986-04-23 | 高純度過酸化水素化チタン水溶液の製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS62252301A (enrdf_load_stackoverflow) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2350841A (en) * | 1999-06-08 | 2000-12-13 | Kansai Paint Co Ltd | Titanium oxide precursor coating composition |
| US6267944B1 (en) * | 1999-07-05 | 2001-07-31 | Morioki Sangyo Company Limited | Method of preparing a solution for titania film |
| US6733580B2 (en) * | 1999-06-08 | 2004-05-11 | Kansei Paint Co., Ltd | Inorganic film-forming coating composition, preparation method thereof and inorganic film-forming method |
| CN101831728A (zh) * | 2010-04-12 | 2010-09-15 | 南京理工大学 | 纳米晶光催化二氧化钛纤维的制备方法 |
-
1986
- 1986-04-23 JP JP9358386A patent/JPS62252301A/ja active Granted
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2350841A (en) * | 1999-06-08 | 2000-12-13 | Kansai Paint Co Ltd | Titanium oxide precursor coating composition |
| GB2350841B (en) * | 1999-06-08 | 2001-12-19 | Kansai Paint Co Ltd | Inorganic film-forming coating composition, preparation method therof and inorganic film-forming method |
| US6565641B1 (en) | 1999-06-08 | 2003-05-20 | Kansai Paint Co., Ltd. | Inorganic film-forming coating composition, preparation method thereof and inorganic film-forming method |
| US6733580B2 (en) * | 1999-06-08 | 2004-05-11 | Kansei Paint Co., Ltd | Inorganic film-forming coating composition, preparation method thereof and inorganic film-forming method |
| DE10028111B4 (de) * | 1999-06-08 | 2009-07-02 | Kansai Paint Co., Ltd., Amagasaki | Anorganische,filmbildende Überzugszusammensetzung, Herstellungsverfahren hierfür und Verfahren zur Ausbildung eines anorganischen Films |
| US6267944B1 (en) * | 1999-07-05 | 2001-07-31 | Morioki Sangyo Company Limited | Method of preparing a solution for titania film |
| CN101831728A (zh) * | 2010-04-12 | 2010-09-15 | 南京理工大学 | 纳米晶光催化二氧化钛纤维的制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0369842B2 (enrdf_load_stackoverflow) | 1991-11-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EXPY | Cancellation because of completion of term |