JPS62205317A - Degasing apparatus for liquid crystal - Google Patents

Degasing apparatus for liquid crystal

Info

Publication number
JPS62205317A
JPS62205317A JP4892486A JP4892486A JPS62205317A JP S62205317 A JPS62205317 A JP S62205317A JP 4892486 A JP4892486 A JP 4892486A JP 4892486 A JP4892486 A JP 4892486A JP S62205317 A JPS62205317 A JP S62205317A
Authority
JP
Japan
Prior art keywords
liquid crystal
tank
tube
pressure
reduced
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP4892486A
Other languages
Japanese (ja)
Inventor
Seiichi Kizaki
木崎 静一
Atsushi Motai
惇 馬渡
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Casio Computer Co Ltd
Original Assignee
Casio Computer Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Casio Computer Co Ltd filed Critical Casio Computer Co Ltd
Priority to JP4892486A priority Critical patent/JPS62205317A/en
Publication of JPS62205317A publication Critical patent/JPS62205317A/en
Pending legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G02OPTICS
    • G02FOPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
    • G02F1/00Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
    • G02F1/01Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour 
    • G02F1/13Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour  based on liquid crystals, e.g. single liquid crystal display cells
    • G02F1/133Constructional arrangements; Operation of liquid crystal cells; Circuit arrangements
    • G02F1/1333Constructional arrangements; Manufacturing methods
    • G02F1/1341Filling or closing of cells

Landscapes

  • Physics & Mathematics (AREA)
  • Nonlinear Science (AREA)
  • Mathematical Physics (AREA)
  • Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • General Physics & Mathematics (AREA)
  • Optics & Photonics (AREA)
  • Liquid Crystal (AREA)

Abstract

PURPOSE:To effectively enable to degas a gas contd. in the liquid crystal, omitting a troublesome hand working by supplying the liquid crystal to the reduced tank, after reducing the pressure of a reducing tank provided a degasing tube composed of a fine porous film made of a resin in the reduced tank. CONSTITUTION:The degasing tube 3 composed of the fine porous film made of polyolefin resin is provided in the reducing tank 1. The tube 3 is reduced the pressure by a vacuum pump 2, followed by supplying the liquid crystal to the tube 3 from a storage tank 5 by means of a supply pump 7. Accordingly, the gas dissolved in the liquid crystal is degased through a surrounding surface of the tube 3. And then, the pressure reduced tank 8 and the cell 10 are reduced by the vacuum pump 12, followed by opening a shut-off cock 14 and supplying the liquid crystal to the cell 10 through the liquid crystal receiver 11a, utilizing a pressure difference. Thus, the liquid crystal is degased and supplied to the cell efficiently, omitting the troublesome hand working.

Description

【発明の詳細な説明】 〔発明の技術分野〕 この発明は、液晶中に溶解した気体を分離して排除する
液晶の脱気装置に関する。
DETAILED DESCRIPTION OF THE INVENTION [Technical Field of the Invention] The present invention relates to a liquid crystal degassing device that separates and eliminates gas dissolved in liquid crystal.

〔発明の技術的背景とその問題点〕[Technical background of the invention and its problems]

近年、計測機器や家電機器などの分野において液晶表示
装置が広(普及し、活用されている。この種の液晶表示
装置は、それぞれ内面に電極を備える一対の透明基板を
枠状の封止材を間に挟んで結合することにより空のセル
を構成し、このセルの内部つまり封止材と各透明・基板
とで囲まれる空間内に液晶を注入して製造するものであ
る。
In recent years, liquid crystal display devices have become widespread and utilized in fields such as measuring instruments and home appliances.This type of liquid crystal display device consists of a pair of transparent substrates, each with electrodes on the inner surface, and a frame-shaped sealing material. These cells are bonded together to form an empty cell, and liquid crystal is injected into the inside of this cell, that is, into the space surrounded by the sealing material and each transparent substrate.

このような製造時において重要なことは、液晶中に溶解
した気体を充分に取除いて液晶をセルに注入することで
ある。気体が溶解したまま液晶を注入してしまうと、セ
ル内に気泡が発生し、画像等の表示の支障となり、また
注入不足などの不良を招いてしまう。
What is important during such manufacturing is to sufficiently remove the gas dissolved in the liquid crystal before injecting the liquid crystal into the cell. If the liquid crystal is injected while the gas is dissolved, bubbles will be generated within the cell, which will hinder the display of images and the like, and will also lead to defects such as insufficient injection.

そこで従来においては、液晶を皿やビー力などの容器に
収容し、これを減圧槽内に入れて減圧し、この減圧に基
づいて液晶中の気体を分離して排除し、つまり脱気し、
このように脱気した液晶をセルに注入している。
Therefore, in the past, liquid crystal was placed in a container such as a dish or a container, and the container was placed in a vacuum tank to reduce the pressure.Based on this pressure reduction, the gas in the liquid crystal was separated and eliminated, that is, it was degassed.
The degassed liquid crystal is injected into the cell.

しかしながらこのような手段においては、いちいち手作
業で液晶を容器に収容し、これを減圧槽内に挿入しなけ
ればならないから、作業能率が悪く、また容器に蓋をす
ると液晶に対する減圧の妨げとなるから蓋の装着を避け
なければならず、この結果、容器を減圧槽内に挿入する
際に液晶が容器から飛散しやすく、このため異種の液晶
を収容した複数の容器を同一の減圧槽内に挿入して脱気
を行なうことが困難となり、これによりさらに作業能率
が低下してしまう。そして、容器から液晶が飛散すると
、減圧槽の内部が液晶で汚染され、したがって減圧槽の
内部を頻繁に清掃する必要が生じてしまう。また、液晶
が開放状態の容器に収容される関係で、この内部に塵埃
等の異物が混入し、液晶の品質を低下させてしまう恐れ
があった。
However, with this method, the liquid crystal must be placed in a container by hand and then inserted into a vacuum tank, which is inefficient, and if the container is covered, it will interfere with the vacuum being applied to the liquid crystal. As a result, the liquid crystal tends to scatter from the container when the container is inserted into the vacuum tank, and for this reason, multiple containers containing different types of liquid crystals should not be placed in the same vacuum tank. It becomes difficult to insert and degas, which further reduces work efficiency. When the liquid crystal scatters from the container, the inside of the vacuum tank becomes contaminated with the liquid crystal, and therefore the inside of the vacuum tank needs to be cleaned frequently. Further, since the liquid crystal is housed in an open container, there is a risk that foreign matter such as dust may enter the container and deteriorate the quality of the liquid crystal.

(発明の目的〕 この発明はこのような点に着目してなされたもので、そ
の目的とするところは、煩しい手作業を何ら要すること
なく、また異種の液晶においても同時に、さらに減圧槽
の内部に対する汚染や、液晶に対する異物の混入を確実
に防止して、液晶中に溶解した気体を能率的に脱気する
ことができるようにした液晶の脱気装置を提供すること
にある。
(Objective of the Invention) This invention has been made with attention to the above points, and its purpose is to eliminate the need for any troublesome manual work, to simultaneously handle different types of liquid crystals, and to reduce pressure in a vacuum tank. An object of the present invention is to provide a liquid crystal degassing device that can efficiently degas the gas dissolved in the liquid crystal while reliably preventing contamination of the inside and mixing of foreign matter into the liquid crystal.

〔発明の概要〕[Summary of the invention]

すなわちこの発明は、減圧槽内に、ポリオレフィン系樹
脂からなる微多孔膜で形成した脱気チューブを設け、上
記減圧槽内を減圧した状態で、この脱気チューブ内に液
晶を導入し、この液晶中に溶解した気体を上記減圧に基
づいて脱気チューブの周壁面を通して排除するようにし
たものである。
That is, in this invention, a degassing tube formed of a microporous membrane made of polyolefin resin is provided in a vacuum tank, and a liquid crystal is introduced into the degassing tube while the pressure in the vacuum tank is reduced. The gas dissolved therein is removed through the peripheral wall surface of the degassing tube based on the reduced pressure.

〔発明の実施例〕[Embodiments of the invention]

以下、この発明の一実施例について図面を参照して説明
する。
An embodiment of the present invention will be described below with reference to the drawings.

図中1は脱気用の減圧槽で、この減圧槽1に真空ポンプ
2が接続し、この真空ポンプ2の作動で減圧槽1の内部
を減圧することができるようになっている。そしてこの
減圧槽1の内部に例えば二本の脱気チューブ3.3が設
けられ、これら脱気チューブ3.3の一端に導入管4a
、4aが、他端に導出管4b、4bがそれぞれ取付けら
れ、これら導入管4a 、4aおよび導出管4b、4b
が減圧槽1の壁面をそれぞれ気密的に貫通して外部に突
出している。脱気チューブ3.3は、気体のみを通し、
液体は通さない微多孔膜で形成されている。この微多孔
膜はポリオレフィン系高分子を材料とした厚さが50〜
2004m、平均孔径が0.15〜0.5um、空気孔
率が70〜90%の微多孔質膜であり、空気透過性はA
STM−D−726(ガーレ式)の試験で10〜230
8eC/ 100cc、枚 である。このような微多孔
質膜は、例えば旭化成工業株式会社製ハイボアー200
゜3000 (商品名)として提供されている。
In the figure, reference numeral 1 denotes a depressurizing tank for degassing, and a vacuum pump 2 is connected to this depressurizing tank 1, so that the inside of the decompressing tank 1 can be depressurized by the operation of this vacuum pump 2. For example, two deaeration tubes 3.3 are provided inside this decompression tank 1, and one end of these deaeration tubes 3.3 is connected to an introduction pipe 4a.
, 4a, and outlet pipes 4b, 4b are attached to the other end thereof, and these inlet pipes 4a, 4a and outlet pipes 4b, 4b
penetrate the wall surface of the decompression tank 1 in an airtight manner and protrude to the outside. The degassing tube 3.3 passes only gas,
It is made of a microporous membrane that does not allow liquid to pass through. This microporous membrane is made of polyolefin polymer and has a thickness of 50~
2004m, the average pore diameter is 0.15-0.5um, the air porosity is 70-90%, and the air permeability is A.
10-230 in STM-D-726 (Gurley method) test
8eC/100cc, sheet. Such a microporous membrane is, for example, HiBore 200 manufactured by Asahi Kasei Corporation.
It is provided as ゜3000 (product name).

5.5は液晶を収容した貯留槽で、これら貯留槽5.5
から供給管6.6が導出し、これら供給管6.6が上記
脱気チューブ3.3の導入管4a。
5.5 is a storage tank containing liquid crystal, and these storage tanks 5.5
Supply pipes 6.6 lead out from the inlet pipe 4a of the degassing tube 3.3.

4aに接続され、またこれら供給管6.6の途中に供給
ポンプ7.7が設けられている。
4a, and a supply pump 7.7 is provided in the middle of these supply pipes 6.6.

8.8は液晶注入用の減圧槽で、これら減圧槽8.8の
内部にそれぞれホルダ9.9を介して空のセル10.1
0が収納保持されている。そしてこれら減圧槽8.8か
ら注入管11.11が導出し、これら注入管11.11
の一端が脱気チューブ3.3の導出管4b、4bに、ま
た他端が減圧槽8.8の内部において液晶溜11a、1
1aにそれぞれ接続し、これら液晶溜’iia、1ia
に液晶にセル10.10の液晶注入口(図示せず)がそ
れぞれ対向している。なお、1’2.12は減圧槽8.
8内の空気を吸引する真空ポンプ、13゜13は減圧槽
8.8内を大気中に連通させる通気管、14.14はこ
れら通気管13.13の途中に設けられた開閉コックで
ある。
8.8 is a vacuum tank for liquid crystal injection, and empty cells 10.1 are placed inside each of these vacuum tanks 8.8 via a holder 9.9.
0 is stored and held. Injection pipes 11.11 are led out from these decompression tanks 8.8, and these injection pipes 11.11
One end is connected to the outlet pipe 4b, 4b of the degassing tube 3.3, and the other end is connected to the liquid crystal reservoir 11a, 1 inside the decompression tank 8.8.
1a, and these liquid crystal reservoirs 'iia, 1ia
The liquid crystal inlets (not shown) of the cells 10 and 10 respectively face the liquid crystal. In addition, 1'2.12 is the pressure reduction tank 8.
13. 13 is a ventilation pipe that communicates the inside of the decompression tank 8.8 with the atmosphere. 14.14 is an opening/closing cock provided in the middle of these ventilation pipes 13.13.

次に、動作について説明する。Next, the operation will be explained.

まず、真空ポンプ2を作動させ、脱気用の減圧槽1内の
空気を吸引して1Torr程度の圧力に減圧する。また
、貯留槽5.5内に貯留した液晶を供給ポンプ7.7を
作動させて供給管6,6から導入管4a、4aを通して
脱気チューブ3.3内に導入する。脱気チューブ3.3
は微多孔質性の高分子材料で形成され、また減圧槽1内
が減圧されているから、液晶が脱気チューブ3.3内に
導入するのに伴い、この液晶中に溶解した気体がその圧
力差で分離し、脱気チューブ3.3の周壁面を通して排
除される。
First, the vacuum pump 2 is operated to suck the air in the depressurizing tank 1 for degassing and reduce the pressure to about 1 Torr. Further, the liquid crystal stored in the storage tank 5.5 is introduced into the degassing tube 3.3 from the supply pipes 6, 6 through the introduction pipes 4a, 4a by operating the supply pump 7.7. Deaeration tube 3.3
is made of a microporous polymeric material, and since the pressure inside the vacuum tank 1 is reduced, as the liquid crystal is introduced into the degassing tube 3.3, the gas dissolved in the liquid crystal is It separates due to the pressure difference and is expelled through the circumferential wall of the degassing tube 3.3.

ついで、真空ポンプ12.12を作動させ、注入用の減
圧槽8.8内およびセル10.10内をQ、1Torr
程度の圧力に減圧し、またセル10.10の注入口を液
晶溜118.11a内の液晶に接触させ、こののち開閉
コック14.14を開放し、減圧槽8.8内を大気中に
連通させる。
Next, the vacuum pump 12.12 is operated to reduce the pressure inside the injection pressure tank 8.8 and the inside of the cell 10.10 to Q, 1 Torr.
Then, the injection port of the cell 10.10 is brought into contact with the liquid crystal in the liquid crystal reservoir 118.11a, and the opening/closing cock 14.14 is then opened to communicate the inside of the decompression tank 8.8 to the atmosphere. let

=6− これに伴い液晶が、セル10.10の内外の圧力差でセ
ル10.10内に吸入される。そしてこののちセル10
.10の注入口を封止材で封止する。
=6- Accordingly, the liquid crystal is sucked into the cell 10.10 due to the pressure difference between the inside and outside of the cell 10.10. And after this cell 10
.. 10 injection ports are sealed with a sealant.

このように、液晶を脱気デユープ3.3内に導入するだ
けで、その液晶中の気体を分離して排除でき、したがっ
て煩しい手作業が不要で、作業能率が大幅に向上する。
In this way, simply by introducing the liquid crystal into the degassing duplex 3.3, the gas in the liquid crystal can be separated and removed, thus eliminating the need for troublesome manual work and greatly improving work efficiency.

そして、液晶が密閉構造の流通経路を流通するのみであ
るから、液晶の飛散という問題が起り得す、このため同
一の減圧槽1内において異種の液晶を対象にして気体の
排除を行なうことができる。すなわち、貯留槽5.5に
異種の液晶を収容し、これらを同時に同一の減圧槽1内
の脱気チューブ3.3に導入して効率的に気体の排除を
図ることができるのである。また液晶が飛散するような
ことがないから、減圧槽1内を汚染することもなく、さ
らに液晶が密閉m造の流通経路を流通するのみであるか
ら、この液晶に異物が混入する恐れも全くなく、したが
って液晶の品質を常に良好に保ってセル10.10に注
入することができる。
Since the liquid crystal only flows through a closed distribution channel, the problem of liquid crystal scattering may occur.For this reason, it is difficult to remove gas from liquid crystals of different types in the same decompression tank 1. can. That is, different types of liquid crystals can be stored in the storage tank 5.5 and simultaneously introduced into the degassing tube 3.3 in the same decompression tank 1 to efficiently remove gas. Furthermore, since the liquid crystal does not scatter, there is no possibility of contaminating the inside of the decompression tank 1, and since the liquid crystal only flows through a closed distribution channel, there is no risk of foreign matter getting into the liquid crystal. Therefore, the liquid crystal can be injected into the cell 10.10 while maintaining good quality at all times.

なお、上記実施例においては、減圧槽1内に二本の脱気
チューブ3゜3を配設したが、これは一本でも、三本、
或いはそれ以上の本数を配設することも可能である。
In the above embodiment, two degassing tubes 3°3 were provided in the decompression tank 1, but this may be one, three, or three degassing tubes.
Alternatively, it is also possible to arrange a larger number.

〔発明の効果〕〔Effect of the invention〕

以上説明したようにこの発明によれば、煩しい手作業を
何ら要することなく、単に減圧槽内の脱気チューブに液
晶を導入するのみでよく、したがって作業能率の大幅な
向上を図れ、また液晶の飛散の恐れがないから、異種の
液晶に対して同時に同一の減圧槽内で効率的に脱気を行
なうことが可能であるとともに、減圧槽の汚染を防止で
き、さらに液晶に対する異物の混入を防止して常に液晶
の品質を良好に保つことができるという効果を奏する。
As explained above, according to the present invention, it is sufficient to simply introduce the liquid crystal into the degassing tube in the decompression tank without any troublesome manual work. Since there is no fear of liquid crystals scattering, it is possible to efficiently degas different types of liquid crystals at the same time in the same vacuum tank, prevent contamination of the vacuum tank, and further prevent foreign matter from entering the liquid crystal. This has the effect that the quality of the liquid crystal can always be maintained at a good level.

【図面の簡単な説明】[Brief explanation of drawings]

図はこの発明の一実施例を示す構成図である。 1・・・減圧槽、3・・・脱気チューブ。 The figure is a configuration diagram showing an embodiment of the present invention. 1...Reducing pressure tank, 3...Degassing tube.

Claims (1)

【特許請求の範囲】[Claims] 減圧槽内に、ポリオレフィン系樹脂からなる微多孔膜で
形成した脱気チューブを設け、上記減圧槽内を減圧した
状態で、この脱気チューブ内に液晶を導入することを特
徴とした液晶の脱気装置。
A degassing tube made of a microporous membrane made of polyolefin resin is provided in a decompression tank, and the liquid crystal is introduced into the degassing tube while the pressure in the decompression tank is reduced. Air device.
JP4892486A 1986-03-06 1986-03-06 Degasing apparatus for liquid crystal Pending JPS62205317A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP4892486A JPS62205317A (en) 1986-03-06 1986-03-06 Degasing apparatus for liquid crystal

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP4892486A JPS62205317A (en) 1986-03-06 1986-03-06 Degasing apparatus for liquid crystal

Publications (1)

Publication Number Publication Date
JPS62205317A true JPS62205317A (en) 1987-09-09

Family

ID=12816801

Family Applications (1)

Application Number Title Priority Date Filing Date
JP4892486A Pending JPS62205317A (en) 1986-03-06 1986-03-06 Degasing apparatus for liquid crystal

Country Status (1)

Country Link
JP (1) JPS62205317A (en)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS55121806A (en) * 1979-03-13 1980-09-19 Jeol Ltd Deaerator
JPS60254118A (en) * 1984-05-31 1985-12-14 Fujitsu Ltd Liquid crystal injection device

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS55121806A (en) * 1979-03-13 1980-09-19 Jeol Ltd Deaerator
JPS60254118A (en) * 1984-05-31 1985-12-14 Fujitsu Ltd Liquid crystal injection device

Similar Documents

Publication Publication Date Title
EP1919622B1 (en) Systems, apparatus and methods for vacuum filtration
CN110186737B (en) Liquid-based sample slice-making and dyeing integrated machine
JPH04215992A (en) Device to draw ultra-pure liquid from container
JPS6356276A (en) Apparatus for performing biological test of cell
BR112018008386B1 (en) SAMPLE PREPARATION DEVICE AND SET
JPS62205317A (en) Degasing apparatus for liquid crystal
KR20160002365A (en) Hardware for the separation and degassing of dissolved gases in semiconductor precursor chemicals
JP3925762B2 (en) Wafer storage method and wafer case used therefor
JP3411422B2 (en) Liquid crystal injection device
CN112313009A (en) Liquid filtration system
CN106582289A (en) Filter system and filter method
JPH1082773A (en) Method for supplying eluent in chromatography and eluent container
CN220834251U (en) Reagent processing device and detection equipment
JPH076799Y2 (en) Culture bag
CN214809869U (en) Water sample filtering device
JPH0617074Y2 (en) Reagent supply device for analytical instruments
KR20000016634A (en) Method and device for filling an analysis card with a liquid medium
JPH076800Y2 (en) Culture bag
KR0130145Y1 (en) Bubble removal of liquid crystal
US4317797A (en) Resin purger
CN216170324U (en) Anti-pollution film filter for drug detection
CN215799514U (en) Biological sample save set and virus sampling pipe
JPH048348Y2 (en)
JP3769937B2 (en) Liquid crystal injection method and apparatus
US11075054B2 (en) Nanofluidic cell system