JPS6133828B2 - - Google Patents
Info
- Publication number
- JPS6133828B2 JPS6133828B2 JP53080361A JP8036178A JPS6133828B2 JP S6133828 B2 JPS6133828 B2 JP S6133828B2 JP 53080361 A JP53080361 A JP 53080361A JP 8036178 A JP8036178 A JP 8036178A JP S6133828 B2 JPS6133828 B2 JP S6133828B2
- Authority
- JP
- Japan
- Prior art keywords
- perfluoro
- compound
- oxabicyclo
- octane
- electrolytic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 claims description 5
- 125000004432 carbon atom Chemical group C* 0.000 claims description 3
- 125000005010 perfluoroalkyl group Chemical group 0.000 claims description 3
- 150000001875 compounds Chemical class 0.000 description 20
- -1 perfluoro Chemical group 0.000 description 11
- 238000005868 electrolysis reaction Methods 0.000 description 7
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 6
- 229910000040 hydrogen fluoride Inorganic materials 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- 238000003682 fluorination reaction Methods 0.000 description 5
- 239000007789 gas Substances 0.000 description 5
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical compound FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 description 4
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 150000002170 ethers Chemical class 0.000 description 3
- 239000012442 inert solvent Substances 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- UJMWVICAENGCRF-UHFFFAOYSA-N oxygen difluoride Chemical compound FOF UJMWVICAENGCRF-UHFFFAOYSA-N 0.000 description 3
- SYNPRNNJJLRHTI-UHFFFAOYSA-N 2-(hydroxymethyl)butane-1,4-diol Chemical compound OCCC(CO)CO SYNPRNNJJLRHTI-UHFFFAOYSA-N 0.000 description 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 239000000969 carrier Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000004817 gas chromatography Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 229910000127 oxygen difluoride Inorganic materials 0.000 description 2
- 239000008188 pellet Substances 0.000 description 2
- 235000013024 sodium fluoride Nutrition 0.000 description 2
- 239000011775 sodium fluoride Substances 0.000 description 2
- KGXYNHNASARONK-UHFFFAOYSA-N 2,2,3,3,3a,4,4,5,5,6,6,6a-dodecafluorocyclopenta[b]furan Chemical compound FC1(F)C(F)(F)C(F)(F)C2(F)C(F)(F)C(F)(F)OC21F KGXYNHNASARONK-UHFFFAOYSA-N 0.000 description 1
- MQUDQJHJGDFQMH-UHFFFAOYSA-N 2,2,3,3,4,4,4a,5,5,6,6,7,7,8,8,8a-hexadecafluorochromene Chemical compound FC1(F)C(F)(F)C(F)(F)C(F)(F)C2(F)C(F)(F)C(F)(F)C(F)(F)OC21F MQUDQJHJGDFQMH-UHFFFAOYSA-N 0.000 description 1
- UEOZRAZSBQVQKG-UHFFFAOYSA-N 2,2,3,3,4,4,5,5-octafluorooxolane Chemical compound FC1(F)OC(F)(F)C(F)(F)C1(F)F UEOZRAZSBQVQKG-UHFFFAOYSA-N 0.000 description 1
- DPCLADKDWPQTOM-UHFFFAOYSA-N 2,2,3,3a,4,4,5,5,6,6,6a-undecafluoro-3-(1,1,2,2,2-pentafluoroethyl)cyclopenta[b]furan Chemical compound FC1(F)C(F)(F)C(F)(F)C2(F)C(C(F)(F)C(F)(F)F)(F)C(F)(F)OC21F DPCLADKDWPQTOM-UHFFFAOYSA-N 0.000 description 1
- QHINYJQPBCMLCJ-UHFFFAOYSA-N 3,3a,4,5,6,6a-hexahydro-2h-cyclopenta[b]furan Chemical compound C1COC2CCCC21 QHINYJQPBCMLCJ-UHFFFAOYSA-N 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- 229910000792 Monel Inorganic materials 0.000 description 1
- 238000000862 absorption spectrum Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 125000003545 alkoxy group Chemical group 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000002473 artificial blood Substances 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- IYRWEQXVUNLMAY-UHFFFAOYSA-N carbonyl fluoride Chemical compound FC(F)=O IYRWEQXVUNLMAY-UHFFFAOYSA-N 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 125000005843 halogen group Chemical group 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000006317 isomerization reaction Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000001819 mass spectrum Methods 0.000 description 1
- ZOBJJLMWIAHNIX-UHFFFAOYSA-N methyl 2-cyclopentylpropanoate Chemical compound COC(=O)C(C)C1CCCC1 ZOBJJLMWIAHNIX-UHFFFAOYSA-N 0.000 description 1
- 239000002808 molecular sieve Substances 0.000 description 1
- 125000002950 monocyclic group Chemical group 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 238000000655 nuclear magnetic resonance spectrum Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- BHZRJJOHZFYXTO-UHFFFAOYSA-L potassium sulfite Chemical compound [K+].[K+].[O-]S([O-])=O BHZRJJOHZFYXTO-UHFFFAOYSA-L 0.000 description 1
- 235000019252 potassium sulphite Nutrition 0.000 description 1
- 238000003822 preparative gas chromatography Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Furan Compounds (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP8036178A JPS558435A (en) | 1978-06-30 | 1978-06-30 | Production of perfluoro(4-alkyl-2-oxabicyclo 3 3 0 octane) |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP8036178A JPS558435A (en) | 1978-06-30 | 1978-06-30 | Production of perfluoro(4-alkyl-2-oxabicyclo 3 3 0 octane) |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS558435A JPS558435A (en) | 1980-01-22 |
| JPS6133828B2 true JPS6133828B2 (enrdf_load_stackoverflow) | 1986-08-04 |
Family
ID=13716107
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP8036178A Granted JPS558435A (en) | 1978-06-30 | 1978-06-30 | Production of perfluoro(4-alkyl-2-oxabicyclo 3 3 0 octane) |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS558435A (enrdf_load_stackoverflow) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2783137B2 (ja) * | 1993-12-03 | 1998-08-06 | 三菱電機株式会社 | 乗客コンベヤの乗降口装置 |
-
1978
- 1978-06-30 JP JP8036178A patent/JPS558435A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS558435A (en) | 1980-01-22 |
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