JPS61266496A - Water soluble perfume - Google Patents

Water soluble perfume

Info

Publication number
JPS61266496A
JPS61266496A JP60108270A JP10827085A JPS61266496A JP S61266496 A JPS61266496 A JP S61266496A JP 60108270 A JP60108270 A JP 60108270A JP 10827085 A JP10827085 A JP 10827085A JP S61266496 A JPS61266496 A JP S61266496A
Authority
JP
Japan
Prior art keywords
water
saponin
oil
natural essential
natural
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP60108270A
Other languages
Japanese (ja)
Inventor
村上 文和
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Maruzen Kasei Co Ltd
Original Assignee
Maruzen Kasei Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Maruzen Kasei Co Ltd filed Critical Maruzen Kasei Co Ltd
Priority to JP60108270A priority Critical patent/JPS61266496A/en
Publication of JPS61266496A publication Critical patent/JPS61266496A/en
Pending legal-status Critical Current

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Landscapes

  • Seasonings (AREA)
  • Medicinal Preparation (AREA)
  • Fats And Perfumes (AREA)

Abstract

(57)【要約】本公報は電子出願前の出願データであるた
め要約のデータは記録されません。
(57) [Summary] This bulletin contains application data before electronic filing, so abstract data is not recorded.

Description

【発明の詳細な説明】 産呈上を男里分野 本発明は、天然精油を主要香料として含有する水溶性香
料に関するものである。
DETAILED DESCRIPTION OF THE INVENTION Field of the Invention The present invention relates to a water-soluble fragrance containing natural essential oil as a main fragrance.

従来の技術 天然精油は、フレーバーやエツセンスに比べ保留性がよ
く、また力強さを持った香料であって、各種飲料、デザ
ート類、菓子等、更には化粧品や医薬品にも添加されて
いる用途の広い香料である。
Conventional technology Natural essential oils have better retention properties than flavors and essences, and are strong fragrances, and are used as additives in various beverages, desserts, confectioneries, and even cosmetics and pharmaceuticals. It is a wide range of fragrances.

しかしながら、天然精油はいずれも冷水に溶は難く、そ
のため、添加対象物が油性のものである場合以外は、使
用に当り乳化剤や安定剤を添加し高圧乳化機を用いて乳
化・分散させるのが普通である。その場合、乳化安定剤
としては、安全性を考慮してアラビアガム、ショ糖脂肪
酸エステル、天然樹脂など天然物系のものが使わ枕るが
、これらの乳化安定剤により乳化された天然精油の安定
性は必ずしも充分でなく、長期間保存した場合、油層の
分離を起こすことがあった。
However, all natural essential oils are difficult to dissolve in cold water, so unless the substance to be added is oil-based, it is best to add an emulsifier or stabilizer and emulsify and disperse using a high-pressure emulsifier. It's normal. In this case, natural products such as gum arabic, sucrose fatty acid esters, and natural resins are used as emulsion stabilizers for safety reasons, but these emulsion stabilizers do not stabilize the emulsified natural essential oil. The properties were not always sufficient, and when stored for a long period of time, the oil layer sometimes separated.

発明が解決しようとする問題点 本発明は、従来の天然精油系水性香料が上述のような欠
点を持つものであったことに鑑み、長期にわたり油層分
離を生じないすぐれた安定性を有する水溶性香料を提供
しようとするものである。
Problems to be Solved by the Invention In view of the fact that conventional water-based fragrances based on natural essential oils had the above-mentioned drawbacks, the present invention provides a water-soluble fragrance that has excellent stability and does not cause oil phase separation over a long period of time. It is intended to provide fragrance.

問題点を解決するための手段 本発明は、サポニンを用いて天然精油を可溶化すること
により上記の課題を解決したものである。
Means for Solving the Problems The present invention solves the above problems by solubilizing natural essential oils using saponin.

サポニンは、植物界に広く存在するステロイドまたはテ
ルペンの配糖体の一種であって、糖成分はグルツース、
〃ラクトース、アラビ/−ス、ウロン酸等である。本発
明の水溶性香料が可溶化剤として含有するサポニンは、
サポニンを含有する植物組織、たとえばキラヤ(Qui
laja 5aponaria)の樹皮、ムクロジ(S
apinclus mukurossi)の果皮、サボ
ンソウ(Saponaria officinalis
 L、)の根、茶(Thea 5inensisL、)
の実などから得られたサポニン類含有エキスでもよいが
、これを活性炭、吸着樹脂等で処理することにより得ら
れた精製サポニンを用いるほうが、天然精油の香りに対
する影響が少なく、また着色も少ないので、有利である
Saponin is a type of steroid or terpene glycoside that widely exists in the plant kingdom, and its sugar components include gluten,
(Lactose, arabic acid, uronic acid, etc.) The saponin contained in the water-soluble fragrance of the present invention as a solubilizing agent is
Plant tissues containing saponins, such as Quillaya (Qui
The bark of Sapindium sapinata (S. 5aponaria),
apinclus mukurossi), saponaria officinalis
L, ) root, tea (Thea 5inensis L,)
A saponin-containing extract obtained from the fruit of a tree may be used, but it is better to use purified saponin obtained by treating it with activated carbon, adsorption resin, etc., since it has less effect on the aroma of natural essential oils and is less colored. , is advantageous.

本発明の水溶性香料を製造するには、通常、可溶化しよ
うとする天然精油の0.5〜10倍量(好ましくは1〜
5倍量)のサポニン類を0.1〜40%水溶液(好まし
くは1〜30%水溶液)として用意し、撹拌しながら、
これに天然精油を滴下する。その場合、サポニン水溶液
には、その可溶化作用を妨げない範囲で、サポニン類以
外の界面活性剤、安定剤、糖類、アミノ酸類、その他香
料として必要な成分等を加えておくことがで終る。
To produce the water-soluble fragrance of the present invention, the amount of natural essential oil to be solubilized is usually 0.5 to 10 times (preferably 1 to 1 times) the amount of natural essential oil to be solubilized.
5 times the amount) of saponins as a 0.1 to 40% aqueous solution (preferably a 1 to 30% aqueous solution), and while stirring,
Add some natural essential oil to it. In that case, surfactants other than saponins, stabilizers, saccharides, amino acids, and other components necessary as flavoring agents may be added to the saponin aqueous solution within a range that does not interfere with the solubilization effect.

昨月二勺署 本発明の水溶性香料においては、前述のように天然精油
がサポニン類の可溶化作用によって可溶化されており、
これにより、水溶性香料全体が透明な水溶液状を呈して
いる。この可溶化液は、従来の天然物系界面活性物質に
よる天然精油乳化液よりも安定性においてはるかにすぐ
れており、また加熱、pH変化、希釈等に対する耐性も
すぐれている。
In the water-soluble fragrance of the present invention, natural essential oils are solubilized by the solubilizing action of saponins, as described above.
As a result, the entire water-soluble fragrance is in the form of a transparent aqueous solution. This solubilized liquid has much better stability than conventional natural essential oil emulsions using natural surfactants, and also has excellent resistance to heating, pH changes, dilution, etc.

したがって本発明の水溶性香料は、従来の乳化型天然精
油系香料よりも長期保存に耐え且つきわめて広範囲の飲
食品、医薬品等に容易に均一混合可能なすぐれた香料で
あり、これにより、従来は使用が困難であった分野にお
いても天然精油を香料として使用することが可能になっ
たのである。
Therefore, the water-soluble fragrance of the present invention is an excellent fragrance that can withstand longer storage than conventional emulsified natural essential oil-based fragrances and can be easily and uniformly mixed into a wide range of foods, drinks, medicines, etc. Natural essential oils can now be used as fragrances even in fields where it was difficult to use them.

加 以下実施例を示して本発明を説明する。Canada The present invention will be explained below with reference to Examples.

実施例 1 キラヤサポニン 20%を含有させた75%異性化液糖
90gに、天然シソオイル10gを攪拌しながら滴下し
、更に撹拌を続けることにより、シソオイルが可溶化し
た赤褐色の透明溶液を得た。
Example 1 10 g of natural perilla oil was added dropwise to 90 g of 75% high-fructose corn syrup containing 20% Quillaja saponin while stirring, and the stirring was continued to obtain a reddish-brown transparent solution in which perilla oil was solubilized.

この可溶化液は、水で500倍に希釈してもほぼ透明で
あり、香りも良好であった。
This solubilized liquid remained almost transparent even when diluted 500 times with water, and had a good aroma.

実施例 2 75%異性化液糖50g、キラヤサポニン25g1サン
ソ7)No、681C(コハク酸モノグリセライド:太
陽化学)5gを60℃に加温して均一に混合し、これに
天然レモンオイル25gを滴下しながら全体をホモミキ
サーで攪拌混合した。これにより、レモンオイルが可溶
化した黄褐色のほぼ透明な溶液を得た。
Example 2 50 g of 75% high-fructose corn syrup, 25 g of Quillaya saponin, 5 g of Sanso 7) No. 681C (succinic acid monoglyceride: Taiyo Kagaku) were heated to 60°C and mixed uniformly, and 25 g of natural lemon oil was added dropwise to this. While stirring, the whole mixture was stirred and mixed using a homomixer. This resulted in a yellow-brown, almost transparent solution in which the lemon oil was solubilized.

この可溶化液は、水で500倍に希釈するとやや乳白色
になったが、油層の分離は認められなかった。またこの
希釈液は、そのpHをクエン酸で4まで低下させても全
く変化を示さず、更に、90°Cに30分間加熱したの
ち室温まで冷却しても安定であった。
When this solubilized liquid was diluted 500 times with water, it became slightly milky white, but no separation of the oil layer was observed. Further, this diluted solution showed no change at all even when its pH was lowered to 4 with citric acid, and was stable even when it was heated to 90° C. for 30 minutes and then cooled to room temperature.

実施例 3 75%水あめ50g1ムクロジサポニン 20g、サン
プ7)Q−18B(ポリグリセリン脂肪酸エステル;太
陽化学)5gを60℃に加温して均一に混合し、これに
天然オレンジ、 オイル25gを滴下しながら全体をホ
モミキサーで撹拌混合した。これにより、オレンジオイ
ルが可溶化した黄褐色のほぼ透明な溶液を得た。
Example 3 75% starch syrup 50g 1 Muclodisaponin 20g, sample 7) 5g of Q-18B (polyglycerin fatty acid ester; Taiyo Kagaku) were heated to 60°C and mixed uniformly, and 25g of natural orange oil was added dropwise to this. The whole mixture was stirred and mixed using a homomixer. This resulted in a yellow-brown, almost transparent solution in which the orange oil was solubilized.

この可溶化液は、水で500倍に希釈するとやや乳白色
になったが油層の分離は認められなかった。またこの希
釈液は、そのpHをクエン酸で4まで低下させても全く
変化を示さず、更に、90°Cに30分間加熱したのち
室温まで冷却しても安定であった。
When this solubilized liquid was diluted 500 times with water, it became slightly milky white, but no separation of the oil layer was observed. Further, this diluted solution showed no change at all even when its pH was lowered to 4 with citric acid, and was stable even when it was heated to 90° C. for 30 minutes and then cooled to room temperature.

手続補正書 昭和60年10月7日Procedural amendment October 7, 1985

Claims (3)

【特許請求の範囲】[Claims] (1)サポニン類により可溶化された天然精油を含有す
ることを特徴とする水溶性香料。
(1) A water-soluble fragrance characterized by containing natural essential oil solubilized by saponins.
(2)サポニン類がキラヤサポニンである特許請求の範
囲第1項記載の水溶性香料。
(2) The water-soluble fragrance according to claim 1, wherein the saponin is Quillaja saponin.
(3)サポニン類がムクロジサポニンである特許請求の
範囲第1項記載の水溶性香料。
(3) The water-soluble fragrance according to claim 1, wherein the saponin is Saponin saponin.
JP60108270A 1985-05-22 1985-05-22 Water soluble perfume Pending JPS61266496A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP60108270A JPS61266496A (en) 1985-05-22 1985-05-22 Water soluble perfume

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP60108270A JPS61266496A (en) 1985-05-22 1985-05-22 Water soluble perfume

Publications (1)

Publication Number Publication Date
JPS61266496A true JPS61266496A (en) 1986-11-26

Family

ID=14480386

Family Applications (1)

Application Number Title Priority Date Filing Date
JP60108270A Pending JPS61266496A (en) 1985-05-22 1985-05-22 Water soluble perfume

Country Status (1)

Country Link
JP (1) JPS61266496A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2847163A1 (en) * 2002-11-19 2004-05-21 Jean Claude Epiphani Preparing an aqueous solution of a perfume for application to the skin comprising mixing an aqueous saponoside solution with the perfume and water
JP2007143413A (en) * 2005-11-24 2007-06-14 Maruzen Pharmaceut Co Ltd Method for eliminating unfavorable smell-causing component and bitter taste component, method for producing quillai extract, and quillai extract

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2847163A1 (en) * 2002-11-19 2004-05-21 Jean Claude Epiphani Preparing an aqueous solution of a perfume for application to the skin comprising mixing an aqueous saponoside solution with the perfume and water
WO2004047787A3 (en) * 2002-11-19 2004-07-01 Jean-Claude Epiphani Method for hydrosolubilisation of a perfume and solution obtained by said method
CN100348165C (en) * 2002-11-19 2007-11-14 让-克劳德·埃皮法尼 Process for preparing an aqueous solution of a perfume and perfume solution
JP2007143413A (en) * 2005-11-24 2007-06-14 Maruzen Pharmaceut Co Ltd Method for eliminating unfavorable smell-causing component and bitter taste component, method for producing quillai extract, and quillai extract

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