JPS6398369A - Cloud for drink - Google Patents

Cloud for drink

Info

Publication number
JPS6398369A
JPS6398369A JP61241986A JP24198686A JPS6398369A JP S6398369 A JPS6398369 A JP S6398369A JP 61241986 A JP61241986 A JP 61241986A JP 24198686 A JP24198686 A JP 24198686A JP S6398369 A JPS6398369 A JP S6398369A
Authority
JP
Japan
Prior art keywords
cloudy
saponin
quillaia
drink
cloud
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP61241986A
Other languages
Japanese (ja)
Inventor
Fumikazu Murakami
村上 文和
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Maruzen Kasei Co Ltd
Original Assignee
Maruzen Kasei Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Maruzen Kasei Co Ltd filed Critical Maruzen Kasei Co Ltd
Priority to JP61241986A priority Critical patent/JPS6398369A/en
Publication of JPS6398369A publication Critical patent/JPS6398369A/en
Pending legal-status Critical Current

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  • Non-Alcoholic Beverages (AREA)

Abstract

PURPOSE:To obtain cloud for drink, stable by itself, stable also in emulsion state formed when added to the drink and having excellent resistance to heating and change of pH, by using quillaia saponin as at least one part of emulsifier. CONSTITUTION:An oily flavor or vegetable oil or fat is emulsified using quillaia saponin, preferably purified quillaia saponin obtained by treating an extract containing quillaia saponin obtained from quillaia cortex with an active carbon as at least one part of emulsifier used in production of cloud and preferably using polyglycerin fatty acid ester, e.g. decaglycerinmonostearate as other surfactant and sugar or sugar alcohol as a stabilizer according to ordinary method.

Description

【発明の詳細な説明】 産栗上9−!り用分野 本発明は、飲料に濃厚感や果汁感を付快する目的で混入
されるクラウディーに関するものである。
[Detailed description of the invention] Chestnut 9-! TECHNICAL FIELD The present invention relates to cloudy mixed into beverages for the purpose of imparting a rich or fruity feel.

従来の技術 クラウディーは油性香料または植物油脂(必要に応じて
両者の混合物が使われることもある)の乳化物からなり
、飲料に添加すると安定な乳濁状態を生じて濃厚感と果
汁感を与えるもので、濁り剤とも呼ばれ、特にオレンジ
′ジュース等の果汁飲料にはよく使われている。飲料に
添加したときの乳濁状態を安定にするため、油相にはシ
ェークロースアセテートイソブチレート等の比重調整剤
を含有させて水相との間の比重差を少なくするのが普通
である。果汁飲料の多くが酸性のため、クラウディーに
使用可能な乳化剤はきわめて限定され、従来はほとんど
の場合アラビアガムが使われている。
Conventional technology Cloudy consists of an emulsion of oil flavoring or vegetable oil (sometimes a mixture of the two is used if necessary), and when added to a drink, it creates a stable emulsion, giving it a rich and fruity feel. It is also called a clouding agent, and is especially often used in fruit juice drinks such as orange juice. In order to stabilize the emulsion when added to beverages, the oil phase usually contains a specific gravity adjuster such as shakerose acetate isobutyrate to reduce the difference in specific gravity between it and the water phase. . Since most fruit juice drinks are acidic, the emulsifiers that can be used in Cloudy are extremely limited, and conventionally gum arabic has been used in most cases.

−発明が解決し主邊とする問題点 しかしながら、従来のクラウディーは、それ自体の安定
性が必ずしも充分でなく、長期間保存すると油層分離を
起こすことがあった。また、アラビアガムは近年原料不
足による慢性的な入手難が続いており、クラウディーの
製造に支障をきたすこともあった。したがって、アラビ
アガムを使わないで製造できしかも安定性のよいクラウ
ディーの出現が望まれていたが、この要望に答えうるも
のはまだ見当らない。
-Problems to be Solved by the Invention However, conventional Cloudy itself does not necessarily have sufficient stability, and oil layer separation may occur when stored for a long period of time. Additionally, gum arabic has been chronically difficult to obtain due to a shortage of raw materials in recent years, which has sometimes caused problems in the production of Cloudy. Therefore, there has been a desire for a cloudy product that can be produced without using gum arabic and has good stability, but nothing that can meet this demand has yet been found.

本発明は、クラウディーの製造と利用における上記問題
点を解決するため、アラビアガムを使わない高品質クラ
ウディーを提供しようとするものである。
The present invention aims to provide high-quality cloudy without using gum arabic in order to solve the above-mentioned problems in the production and use of cloudy.

問題点を解汲−iる一jqll!12p手我1ユ記目的
を達成することに成功した本発明のクラウディーは、乳
化剤の少なくとも一部にキラヤサポニンを用いて油性香
料または植物油脂を乳化したものである。
Solve the problem! The Cloudy of the present invention, which has successfully achieved the object of the present invention, is one in which an oily fragrance or vegetable oil is emulsified using Quillaja saponin as at least a part of the emulsifier.

本発明の飲料用クラウディーに乳化剤として使われるキ
ラヤサポニンは、南米大陸に産するキラヤ木の樹皮から
抽出されるトリテルペフイドサボニンを主成分とする天
然の界面活性物質であって、従来、洗剤や飲料の起泡剤
として使われているが、飲料用クラウディーに使われた
例はない。本発明のクラウディーに用いるキラヤサポニ
ンは、キラヤ樹皮から得られたキラヤサポニン含有エキ
スでもよいが、これを活性炭、吸着樹脂等で処理するこ
とによ1)得られた精製サポニンのほうか、飲料に加え
たとき、香り、色調等に及ぼす影響か少なく、また沈殿
生成のおそれもないので好ましい。
Quillaja saponin, which is used as an emulsifier in the Cloudy beverage of the present invention, is a natural surfactant whose main component is triterpefido saponin, which is extracted from the bark of the Quillaja tree grown in South America. It is used as a foaming agent in detergents and beverages, but it has never been used in Cloudy beverages. The Quillaja saponin used in Cloudy of the present invention may be Quillaya saponin-containing extract obtained from Quillaya bark, but by treating this with activated carbon, adsorption resin, etc. 1) The resulting purified saponin can be used as a beverage. When added to the water, it is preferable because it has little effect on aroma, color tone, etc., and there is no fear of precipitation formation.

本発明のクラウディーを製造するには、通常、用いる油
性香料または(および)植物油脂に適量の比重調整剤を
混合したものを用意し、別に、上記比重調整済油の約0
.01倍量〜等量(望ましくは0.1〜0.5倍量)の
キラヤサポニンを0.1〜40%水溶液(望ましくは1
〜30%溶液)として用意し、キラヤサポニン溶液に比
重調整済油を撹拌下に滴下する。その場合、キラヤサポ
ニン溶液にはその乳化作用を妨げない範囲で、キラヤサ
ポニン以外の界面活性物質、安定剤、保存料、着色料等
を加えておくことがで終る。特に、界面活性物質として
ポリグリセリン脂肪酸エステル(たとえばポリグリセリ
ン脂肪酸エステルがデカグリセリンモノステアレート)
、安定剤として糖もしくは糖アルコール(たとえば異性
化液糖、グルコース、ソルビット、キジリント、マンニ
ット)等の適量をキラヤサポニンと併用することは、ク
ラウディー自身およびそのクラウディーを添加したノユ
ースの安定性向−ににきわめて有効である。
In order to produce Cloudy of the present invention, a suitable amount of specific gravity adjuster is usually prepared by mixing the oil-based fragrance or (and) vegetable oil to be used, and separately, about 0% of the above-mentioned specific gravity adjusted oil is prepared.
.. A 0.1 to 40% aqueous solution (preferably 1 to 40%
~30% solution), and the specific gravity-adjusted oil is added dropwise to the Quillaja saponin solution while stirring. In that case, surfactants other than Quillaja saponin, stabilizers, preservatives, coloring agents, etc. may be added to the Quillaja saponin solution within a range that does not interfere with the emulsification effect of the Quillaja saponin solution. In particular, polyglycerol fatty acid ester (for example, polyglycerol fatty acid ester is decaglycerol monostearate) as a surfactant.
The use of an appropriate amount of sugar or sugar alcohol (e.g. high-fructose corn syrup, glucose, sorbitol, quijilint, mannitol) as a stabilizer with Quillaja saponin increases the stability of cloudy itself and the nouse to which cloudy is added. - Extremely effective.

作用・効果 本発明のクラウディーは、アラビアガムを用いた従来の
クラウディーと全く同様にして、オレンジノユース、レ
モンノユース、グレープフルーツジュース、ビーチジュ
ースなど、各種清涼飲料に添加することかでトる。そし
て、クラウディー自体が長期保存に耐える安定性を有す
るだけでなく、それを飲料に添加したとぎ形成される乳
濁状態は、従来のクラウディーによるものよりもはるか
に安定であり、加熱やpi(変化に対する耐性もすぐれ
ている。
Action/Effect The Cloudy of the present invention can be added to various soft drinks such as orange juice, lemon juice, grapefruit juice, and beach juice in exactly the same way as conventional cloudy using gum arabic. Ru. Not only is Cloudy itself stable enough to withstand long-term storage, but the emulsion that is formed when it is added to beverages is much more stable than that created by conventional Cloudy, and is even more stable when heated or heated. (It also has excellent resistance to change.

キラヤサポニンはアラビアガムよりもはるかに入手容易
であるから、本発明によれば従来よりも高品質のクラウ
ディー添加ジュースを安価に製造することが可能になる
Since Quillaja saponin is much easier to obtain than gum arabic, the present invention makes it possible to produce cloudy-added juice of higher quality at a lower cost than before.

犬簿倒 以下、実施例および比較例を示して本発明を説明する。Inu book fall The present invention will be described below with reference to Examples and Comparative Examples.

なお、以下の文中%とあるのは重量%を意味する。In addition, % in the following text means weight %.

実施例 1 次の配合で、飲料用クラウディーを製造した。Example 1 Beverage cloudy was manufactured using the following formulation.

オレンジオイル(比重0.84)   5%比重調整剤
×(比重1.146)  10%キラヤサポニン   
      5%75%異性化液糖        残
部× シュークロースアセテートイソブチレート製造す
る際は、ます液糖にキラヤサポニンを加えて加熱し、撹
拌してキラヤサポニンを溶解させたのち、これを撹拌し
ながら、あらかじめ混合しておいたオレンジオイルと比
重調整剤との混合物を滴下して乳化させた。
Orange oil (specific gravity 0.84) 5% specific gravity regulator x (specific gravity 1.146) 10% Quillaya saponin
5% 75% isomerized liquid sugar Remaining part A mixture of orange oil and specific gravity adjuster that had been mixed in advance was added dropwise to emulsify.

得られたクラウディーについて、乳化安定性(40°C
,2力月保存)および糖度11%、I)H3,Sのオレ
ンジジュースに添加したときの安定性(室温、60日保
存)を評価する試験を行なった。各評価基準は次のとお
りである。
Regarding the obtained Cloudy, emulsion stability (40°C
A test was conducted to evaluate the stability (storage at room temperature, 60 days) when added to orange juice with a sugar content of 11% and I)H3,S. The evaluation criteria are as follows.

=4− 乳化安定性 ○:問題なし ×:上層に油性成分、下層に水性成分が分離ジュース添
加時の安定性 ○:問題なし ×: リング形成あるいは沈殿生成あり実施例 2,3 キラヤサポニンとともにデカグリセリンモノステアレー
トを3%(実施例2)または5%(実施例3)併用した
ほかは実施例1と同様にしてクラウディーを製造し、実
施例1同様の評価試験を行なった。
= 4- Emulsion stability ○: No problem ×: Oil component in the upper layer and aqueous component in the lower layer Separated Stability when adding juice ○: No problem ×: Ring formation or precipitation formation Example 2, 3 Deka with Quillaya saponin Cloudy was produced in the same manner as in Example 1, except that 3% (Example 2) or 5% (Example 3) of glycerin monostearate was used, and the same evaluation test as in Example 1 was conducted.

比較例 1 従来の飲料用クラウディーの配合としては代表的なもの
である下記の配合で、クラウディーを製造した。
Comparative Example 1 Cloudy was manufactured using the following formulation, which is a typical formulation for conventional beverage Cloudy.

オレンジオイル(比重0.84>   5%比重調整剤
×(比重1.146)  10%アラビアガム    
     16.5%水              
 残部ゞ 実施例1で用いたものと同じ 製造する際はまずアラビアガムを水に加熱溶解し、14
0h/cm2のホモデナイザーを通して均質化した後、
オレンノオイルと比重調整剤との混合物を加え、10分
間撹拌して乳化させ、さらに圧力21.0 Kg/cm
2(−・次圧) −7Q Kg/cm2(二次圧)でホ
モゲナイザーを通して均質化した。得られたクラウディ
ーについて、実施例1同様の評価試験を行なった。
Orange oil (specific gravity 0.84> 5% specific gravity regulator x (specific gravity 1.146) 10% gum arabic
16.5% water
Remaining part: Same as that used in Example 1 When producing, first heat and dissolve gum arabic in water,
After homogenization through a homogenizer at 0 h/cm2,
Add a mixture of orenno oil and specific gravity adjuster, stir for 10 minutes to emulsify, and then apply a pressure of 21.0 Kg/cm.
The mixture was homogenized through a homogenizer at 2 (--secondary pressure) -7Q Kg/cm2 (secondary pressure). The obtained Cloudy was subjected to the same evaluation test as in Example 1.

比較例 2 キラヤサポニンを用いないほかは実施例3と同様1こし
てクラウディーを製造し、実施例1同様の評価試験を行
なった。
Comparative Example 2 Cloudy was produced by straining in the same manner as in Example 3, except that Quillaja saponin was not used, and the same evaluation test as in Example 1 was conducted.

以上の各側の評価試験の結果をまとめて第1表に示す。The results of the above evaluation tests on each side are summarized in Table 1.

Claims (4)

【特許請求の範囲】[Claims] (1)乳化剤の少なくとも一部にキラヤサポニンを用い
て油性香料または植物油脂を乳化してなる飲料用クラウ
ディー。
(1) Cloudy for beverages is made by emulsifying an oily flavor or vegetable oil using Quillaja saponin as at least a part of the emulsifier.
(2)乳化剤がポリグリセリン脂肪酸エステルを含有す
るものである特許請求の範囲第1項記載の飲料用クラウ
ディー。
(2) Cloudy for beverages according to claim 1, wherein the emulsifier contains a polyglycerin fatty acid ester.
(3)乳化剤がポリグリセリン脂肪酸エステルおよび糖
もしくは糖アルコールを含有するものである特許請求の
範囲第1項記載の飲料用クラウディー。
(3) Cloudy for beverages according to claim 1, wherein the emulsifier contains a polyglycerol fatty acid ester and sugar or sugar alcohol.
(4)ポリグリセリン脂肪酸エステルがデカグリセリン
モノステアレートである特許請求の範囲第2項または第
3項記載の飲料用クラウディー。
(4) Cloudy for beverages according to claim 2 or 3, wherein the polyglycerin fatty acid ester is decaglycerin monostearate.
JP61241986A 1986-10-14 1986-10-14 Cloud for drink Pending JPS6398369A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP61241986A JPS6398369A (en) 1986-10-14 1986-10-14 Cloud for drink

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP61241986A JPS6398369A (en) 1986-10-14 1986-10-14 Cloud for drink

Publications (1)

Publication Number Publication Date
JPS6398369A true JPS6398369A (en) 1988-04-28

Family

ID=17082546

Family Applications (1)

Application Number Title Priority Date Filing Date
JP61241986A Pending JPS6398369A (en) 1986-10-14 1986-10-14 Cloud for drink

Country Status (1)

Country Link
JP (1) JPS6398369A (en)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003000195A (en) * 2001-06-21 2003-01-07 Maruzen Pharmaceut Co Ltd Water-dispersible or water-soluble extract composition of leaf of ginkgo
JP2009261258A (en) * 2008-04-22 2009-11-12 Asahi Breweries Ltd Method for producing flavored beverage without causing oil float
JP2010142205A (en) * 2008-12-22 2010-07-01 T Hasegawa Co Ltd O/w-type emulsified composition of liposoluble material
US8318233B2 (en) 2010-03-26 2012-11-27 Corn Products Development Inc Emulsions useful in beverages
JP2016015907A (en) * 2014-07-07 2016-02-01 キリンビバレッジ株式会社 Cloudy citrus fruit juice-containing container-packed beverage in which the precipitation of cloudy citrus fruit juice is masked
JP2018505912A (en) * 2014-12-12 2018-03-01 オーハイ エナジェティクス ピービーシー Microencapsulated cannabinoid composition
US11318096B2 (en) 2014-12-12 2022-05-03 Ojai Energetics Pbc Methods and systems for forming stable droplets
US11666079B2 (en) * 2012-03-13 2023-06-06 Givaudan S.A. Composition and method for manufacturing clear beverages comprising nanoemulsions with Quillaja saponins

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003000195A (en) * 2001-06-21 2003-01-07 Maruzen Pharmaceut Co Ltd Water-dispersible or water-soluble extract composition of leaf of ginkgo
JP4502549B2 (en) * 2001-06-21 2010-07-14 丸善製薬株式会社 Water-dispersible or water-soluble ginkgo biloba extract composition
JP2009261258A (en) * 2008-04-22 2009-11-12 Asahi Breweries Ltd Method for producing flavored beverage without causing oil float
JP2010142205A (en) * 2008-12-22 2010-07-01 T Hasegawa Co Ltd O/w-type emulsified composition of liposoluble material
US8318233B2 (en) 2010-03-26 2012-11-27 Corn Products Development Inc Emulsions useful in beverages
US11666079B2 (en) * 2012-03-13 2023-06-06 Givaudan S.A. Composition and method for manufacturing clear beverages comprising nanoemulsions with Quillaja saponins
JP2016015907A (en) * 2014-07-07 2016-02-01 キリンビバレッジ株式会社 Cloudy citrus fruit juice-containing container-packed beverage in which the precipitation of cloudy citrus fruit juice is masked
JP2018505912A (en) * 2014-12-12 2018-03-01 オーハイ エナジェティクス ピービーシー Microencapsulated cannabinoid composition
US11318096B2 (en) 2014-12-12 2022-05-03 Ojai Energetics Pbc Methods and systems for forming stable droplets

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