JPS6112931B2 - - Google Patents
Info
- Publication number
- JPS6112931B2 JPS6112931B2 JP58157539A JP15753983A JPS6112931B2 JP S6112931 B2 JPS6112931 B2 JP S6112931B2 JP 58157539 A JP58157539 A JP 58157539A JP 15753983 A JP15753983 A JP 15753983A JP S6112931 B2 JPS6112931 B2 JP S6112931B2
- Authority
- JP
- Japan
- Prior art keywords
- organopolysiloxane
- added
- reaction
- mol
- triorganohalosilane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229920001296 polysiloxane Polymers 0.000 claims description 23
- 239000003054 catalyst Substances 0.000 claims description 17
- 150000001339 alkali metal compounds Chemical class 0.000 claims description 5
- 125000005375 organosiloxane group Chemical group 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 239000003513 alkali Substances 0.000 description 11
- 238000006243 chemical reaction Methods 0.000 description 11
- 238000006386 neutralization reaction Methods 0.000 description 10
- 238000000034 method Methods 0.000 description 8
- 230000003472 neutralizing effect Effects 0.000 description 6
- -1 ammonium halide Chemical class 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 5
- 239000002904 solvent Substances 0.000 description 5
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 4
- 238000009835 boiling Methods 0.000 description 4
- 229910052801 chlorine Inorganic materials 0.000 description 4
- 239000000460 chlorine Substances 0.000 description 4
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 description 4
- 150000002430 hydrocarbons Chemical class 0.000 description 4
- 238000006116 polymerization reaction Methods 0.000 description 4
- 239000011347 resin Substances 0.000 description 4
- 229920005989 resin Polymers 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 239000004215 Carbon black (E152) Substances 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 229910052736 halogen Inorganic materials 0.000 description 3
- 150000002367 halogens Chemical class 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- FFUAGWLWBBFQJT-UHFFFAOYSA-N hexamethyldisilazane Chemical compound C[Si](C)(C)N[Si](C)(C)C FFUAGWLWBBFQJT-UHFFFAOYSA-N 0.000 description 3
- 229930195733 hydrocarbon Natural products 0.000 description 3
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 125000005843 halogen group Chemical group 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 229910052700 potassium Inorganic materials 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 230000000087 stabilizing effect Effects 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- SZIFAVKTNFCBPC-UHFFFAOYSA-N 2-chloroethanol Chemical compound OCCCl SZIFAVKTNFCBPC-UHFFFAOYSA-N 0.000 description 1
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 1
- 229910003691 SiBr Inorganic materials 0.000 description 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 125000003342 alkenyl group Chemical group 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 125000004218 chloromethyl group Chemical group [H]C([H])(Cl)* 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 229920001519 homopolymer Polymers 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 150000001282 organosilanes Chemical class 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 230000000379 polymerizing effect Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000003566 sealing material Substances 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910000077 silane Inorganic materials 0.000 description 1
- 150000004756 silanes Chemical class 0.000 description 1
- 125000003944 tolyl group Chemical group 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/32—Post-polymerisation treatment
- C08G77/34—Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Silicon Polymers (AREA)
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58157539A JPS6049033A (ja) | 1983-08-29 | 1983-08-29 | オルガノポリシロキサンの製造方法 |
| US06/641,454 US4563513A (en) | 1983-08-29 | 1984-08-16 | Method for the preparation of a low-impurity organopolysiloxane by the polymerization of an organopolysiloxane oligomer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58157539A JPS6049033A (ja) | 1983-08-29 | 1983-08-29 | オルガノポリシロキサンの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6049033A JPS6049033A (ja) | 1985-03-18 |
| JPS6112931B2 true JPS6112931B2 (US06373033-20020416-M00002.png) | 1986-04-10 |
Family
ID=15651886
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP58157539A Granted JPS6049033A (ja) | 1983-08-29 | 1983-08-29 | オルガノポリシロキサンの製造方法 |
Country Status (2)
| Country | Link |
|---|---|
| US (1) | US4563513A (US06373033-20020416-M00002.png) |
| JP (1) | JPS6049033A (US06373033-20020416-M00002.png) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3524484A1 (de) * | 1985-07-09 | 1987-01-15 | Wacker Chemie Gmbh | Verfahren zur herstellung von linearen organopolysiloxanen mit triorganosiloxygruppen als endstaendigen einheiten |
| FR2614028B1 (fr) * | 1987-04-16 | 1989-09-15 | Rhone Poulenc Chimie | Procede de preparation de polydiorganosiloxane a extremites silanol |
| JPH0660282B2 (ja) * | 1989-04-12 | 1994-08-10 | 信越化学工業株式会社 | 耐熱性シリコーンゲル組成物 |
| US4962221A (en) * | 1990-03-12 | 1990-10-09 | Dow Corning Corporation | Chloride reduction in polysiloxanes |
| JP3632736B2 (ja) | 1998-11-13 | 2005-03-23 | 信越化学工業株式会社 | オルガノポリシロキサンガムの製造方法 |
| JP3546727B2 (ja) | 1998-12-02 | 2004-07-28 | 信越化学工業株式会社 | オルガノポリシロキサンガムの製造方法 |
| JP5207627B2 (ja) * | 2006-12-27 | 2013-06-12 | 東レ・ダウコーニング株式会社 | オルガノポリシロキサンの熱安定性を改善する方法およびオルガノポリシロキサン混合物 |
| DE102011119341A1 (de) | 2011-11-25 | 2013-05-29 | Heraeus Quarzglas Gmbh & Co. Kg | Verfahren zur Herstellung von synthetischem Quarzglas nach der Sootmethode |
| DE102011119374A1 (de) | 2011-11-25 | 2013-05-29 | Heraeus Quarzglas Gmbh & Co. Kg | Verfahren zur Herstellung von synthetischem Quarzglas |
| DE102011119339A1 (de) | 2011-11-25 | 2013-05-29 | Heraeus Quarzglas Gmbh & Co. Kg | Zerstäubungsverfahren zur Herstellung von synthetischem Quarzglas |
| DE102011119373A1 (de) | 2011-11-25 | 2013-05-29 | Heraeus Quarzglas Gmbh & Co. Kg | Verfahren zur Herstellung von synthetischem Quarzglas |
| DE102016203192A1 (de) * | 2016-02-29 | 2017-08-31 | Wacker Chemie Ag | Verfahren zur Herstellung von Hydroxygruppen und Alkoxygruppen aufweisenden Siliconharzen |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3057821A (en) * | 1962-10-09 | Ammonium halide stabilized organo- | ||
| US3065203A (en) * | 1962-11-20 | Polybiloxane stabilization |
-
1983
- 1983-08-29 JP JP58157539A patent/JPS6049033A/ja active Granted
-
1984
- 1984-08-16 US US06/641,454 patent/US4563513A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6049033A (ja) | 1985-03-18 |
| US4563513A (en) | 1986-01-07 |
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