JPS61104431A - Production of vertical recording magnetic medium - Google Patents

Production of vertical recording magnetic medium

Info

Publication number
JPS61104431A
JPS61104431A JP22298084A JP22298084A JPS61104431A JP S61104431 A JPS61104431 A JP S61104431A JP 22298084 A JP22298084 A JP 22298084A JP 22298084 A JP22298084 A JP 22298084A JP S61104431 A JPS61104431 A JP S61104431A
Authority
JP
Japan
Prior art keywords
film
magnetic
permalloy
magnetization
medium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP22298084A
Other languages
Japanese (ja)
Inventor
Kyoji Noda
恭司 野田
Ryuji Sugita
龍二 杉田
Kazuyoshi Honda
和義 本田
Kiyokazu Touma
清和 東間
Taro Nanbu
太郎 南部
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Panasonic Holdings Corp
Original Assignee
Matsushita Electric Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Matsushita Electric Industrial Co Ltd filed Critical Matsushita Electric Industrial Co Ltd
Priority to JP22298084A priority Critical patent/JPS61104431A/en
Publication of JPS61104431A publication Critical patent/JPS61104431A/en
Pending legal-status Critical Current

Links

Abstract

PURPOSE:To obtain the intra-surface magnetization anisotropy of a 'Permal loy(R)' film by blanking a double layer film medium of lines of magnetic force into a circle by means of magnets arranged specially, a yoke and a mask when the 'Permalloy(R)' film is formed on a nonmagnetic substrate. CONSTITUTION:The steam supplied from an evaporation source 8 of a crucible 7 is vapor deposited onto a nonmagnetic substrate 9. A 'Permalloy(R)' film is continuously vapor-deposited on the substrate 9. Then the tangent direction of the line 12 of magnetic force is equal to the magnetization easy axis together with the normal line direction equal to the magnetization difficult axis respective ly for the 'Permalloy(R)' film. In other words, the magnetic anisotropy can be freely controlled with the vapor deposition of the 'Permalloy(R)' film using magnets 4. Thus a vertically magnetized film is formed on the substrate 9 containing a 'Permalloy(R)' film for production of a recording medium. This recording medium is blanked into a circle for production a disk medium 13. Thus it is possible to obtain a disk vertical recording magnetic medium having the anisotropy of the magnetization difficult axis to the circumferencial direction of the medium 13.

Description

【発明の詳細な説明】 (産業上の利用分野) 本発明は、高密度記録に優れた特性を有する、垂直記録
用磁気記録媒体の製造方法に関する。
DETAILED DESCRIPTION OF THE INVENTION (Industrial Field of Application) The present invention relates to a method of manufacturing a magnetic recording medium for perpendicular recording, which has excellent characteristics for high-density recording.

(従来例の構成とその問題点) 一般に、短波長記録特性に優れた効果のある記録方法と
して、垂直磁気記録方式がよく知られている。これは記
録媒体の膜面に垂直方向の残留磁化を利用するものであ
るから、記録媒体膜面にほぼ垂直方向に残留磁化が残る
膜、すなわち垂直磁化膜が必要となる。垂直磁化膜はC
o及びCrを主成分とする、Co −Cr垂直磁化膜が
優れた特性を有しており、それは、スノクッタリングや
真空蒸着(イオンプレティング法のような、蒸発原子の
一部を、イオン化して膜を堆積する方法も含む)などの
方法により製造されるが、特に後者の方法が極めて高い
膜堆積速度を有するので、量産に適している。
(Constitution of Conventional Example and its Problems) Generally, the perpendicular magnetic recording method is well known as a recording method that is effective in providing excellent short wavelength recording characteristics. Since this utilizes residual magnetization in a direction perpendicular to the film surface of the recording medium, a film in which residual magnetization remains in a direction substantially perpendicular to the film surface of the recording medium, that is, a perpendicular magnetization film is required. The perpendicular magnetization film is C
The Co-Cr perpendicularly magnetized film, whose main components are O and Cr, has excellent properties. The latter method has an extremely high film deposition rate and is therefore suitable for mass production.

上記のような単層膜のCo−Cr垂直磁化膜1は第1図
に断面を示すように、非磁性材料よりなる基板2との間
に、ツクーマロイ膜3を設けた、いわゆる2層膜媒体と
呼ばれる構造にすることにより、記録効率及び、再生出
力が向上することが知られており、特に公知の補助磁極
励磁型垂直磁気ヘッドを用いて記録再生を行なう際は、
記録効率、再生効率とも約20 dB向上する0 この上さらに特性を向上させるには上記2層膜媒体にお
ける、ツクーマロイ膜3の初透磁率を高くする必要があ
り、その方法として磁界中蒸着によって、面内磁化異方
性をつけることが考えられる。
As shown in the cross section of FIG. 1, the single-layer Co-Cr perpendicular magnetization film 1 as described above is a so-called two-layer film medium in which a Tsukuumalloy film 3 is provided between it and a substrate 2 made of a non-magnetic material. It is known that recording efficiency and reproduction output can be improved by adopting a structure called .
Both the recording efficiency and the reproduction efficiency are improved by about 20 dB.0 In order to further improve the characteristics, it is necessary to increase the initial permeability of the Tsukuumalloy film 3 in the above-mentioned two-layer film medium. It is possible to add in-plane magnetization anisotropy.

その面内磁化異方性の附与の方法は、長尺の非磁性基板
に・ぐ−マロイ膜を磁界中で、連続蒸着する際に、チー
ブ状垂直磁気記録媒体の製造にあっては、非磁性基板の
幅方向に単一磁界を印加すればよいが、′円板状の垂直
磁気記録媒体の製造の場合は、単一方向の磁界印加では
、出来上った円板状媒体の円周方向−周の記録再生出力
のエンベローブは、第2図に再生出力波形を示すように
モジュレーションが数十チにもなる。なお、モジュレー
ションとは、再生出力の最大値及び最小値をそれぞれA
、Bとするとき、(A−B)/(A+B)Xi OO(
%)で表わされ、一般的には10%以下の値が特性上要
求されている。
The method for imparting in-plane magnetization anisotropy is to continuously deposit a gummalloy film on a long non-magnetic substrate in a magnetic field. It is sufficient to apply a single magnetic field in the width direction of the non-magnetic substrate, but in the case of manufacturing a disk-shaped perpendicular magnetic recording medium, applying a magnetic field in a single direction will cause the circle of the finished disk-shaped medium to The envelope of the recording/reproduction output in the circumferential direction has a modulation of several tens of degrees, as shown in the reproduction output waveform in FIG. Note that modulation refers to the maximum and minimum values of the playback output, respectively.
, B, (A-B)/(A+B)Xi OO(
%), and generally a value of 10% or less is required for characteristics.

すなわち、円板状垂直記録媒体の製法にあっては、テー
プ状記録媒体と同様な面内磁化異方性附与の方法は適用
できず、新しい方法の開発が望まれていた。
That is, in the manufacturing method of disk-shaped perpendicular recording media, the method of imparting in-plane magnetization anisotropy similar to that for tape-shaped recording media cannot be applied, and the development of a new method has been desired.

(発明の目的) 本発明は上述の事情に鑑み、2層膜媒体構造の円板状垂
直磁気記録媒体において、その記録再生特性を一層向上
させるための、特に/IP−マロイ膜の面内磁化異方性
の附与を要点とする製造方法を提供するものである。
(Object of the Invention) In view of the above-mentioned circumstances, the present invention aims to improve the recording and reproducing characteristics of a disk-shaped perpendicular magnetic recording medium having a two-layer film structure, particularly by in-plane magnetization of an /IP-Malloy film. The present invention provides a manufacturing method that focuses on imparting anisotropy.

(発明の構成) 上記目的を達成するため本発明は、非磁性基板上にパー
マロイ膜を形成する際に、特別に配列した磁石、ヨーク
及びマスクによって、磁力線がマスクの中心部では基板
の進行方向に、端部では幅方向に加わるようにし、その
上に垂直磁化膜を形成することにより2層膜媒体とした
ものを円形に打抜いて、その円周方向をほぼ磁化困難方
向とするものである。
(Structure of the Invention) In order to achieve the above object, the present invention, when forming a permalloy film on a non-magnetic substrate, uses specially arranged magnets, a yoke, and a mask so that lines of magnetic force are directed in the direction of substrate movement at the center of the mask. A double-layered film medium is formed by forming a perpendicular magnetization film on the end portions in the width direction, and then punching out a circular shape so that the circumferential direction is almost the direction in which magnetization is difficult. be.

(実施例の説明) 以下、本発明を実施例を用いて説明する。(Explanation of Examples) The present invention will be explained below using examples.

第3図は連続真空蒸着装置の側面略図である。FIG. 3 is a schematic side view of the continuous vacuum evaporation apparatus.

4は磁石、5はヨーク、6はマスクであり、るつi!7
内の蒸発源8からの蒸気を、磁石4間を通して非磁性基
板9に蒸着する。なお、図中10はキャプスタン、11
は非磁性基板90巻枠である。
4 is a magnet, 5 is a yoke, 6 is a mask, and Rutsu i! 7
The vapor from the evaporation source 8 is passed between the magnets 4 and deposited on the nonmagnetic substrate 9. In addition, 10 in the figure is a capstan, 11
is a frame of 90 rolls of non-magnetic substrate.

本発明はこのような連続真空蒸着装置により、2層膜媒
体を形成するパーマロイ膜を蒸着する。
The present invention uses such a continuous vacuum deposition apparatus to deposit a permalloy film forming a two-layer film medium.

第4図(a) p (b)はそれぞれ本発明の実施に用
いる、第3図の磁石4、ヨーク5及びマスク6の部分の
配置を示す平面図であり、併記の矢印Aは非磁性基板9
の移動方向を示しており、6′はマスク孔である。(b
)図は(、)図の構成によるよりも効果を3倍にした配
置構成で、何れも磁石のN−8の磁極の向きを変えても
同一の効果が得られる。
4(a) and 4(b) are plan views showing the arrangement of the magnet 4, yoke 5, and mask 6 of FIG. 3, respectively, used for carrying out the present invention, and the arrow A shown therein indicates a non-magnetic substrate. 9
, and 6' is a mask hole. (b
) The figure shows an arrangement configuration that has three times the effect as the configuration shown in the figures (,), and in both cases, the same effect can be obtained even if the direction of the N-8 magnetic pole of the magnet is changed.

第5図は第4図(a)の構成の場合に発生する磁力線1
2、の全体図を示し、第6図はその磁力線12がマスク
孔6′の部分で示す状態を示しており、磁力線12はマ
スク孔6′の幅方向中央部分で、非磁性基板9の移動方
向を示す矢印Aにほぼ平行になり、両端部分ではほぼ垂
直になる。そこで、このような配置構成で第2図図示の
構成により、非磁性基板9上に・ぐ−マロイ膜を連続し
て真空蒸着すれば、磁力線12の接線方向が磁化容易軸
方向となり、また、法線方向が磁化困難軸方向になるi
4−マロイ膜を非磁性基板9上に形成できる。
Figure 5 shows magnetic field lines 1 generated in the configuration shown in Figure 4(a).
2, and FIG. 6 shows the state in which the lines of magnetic force 12 are at the mask hole 6', and the lines of magnetic force 12 are at the center of the mask hole 6' in the width direction, and the movement of the non-magnetic substrate 9 is shown in FIG. It is almost parallel to arrow A indicating the direction, and almost perpendicular at both ends. Therefore, if a gummalloy film is continuously vacuum-deposited on the non-magnetic substrate 9 using the arrangement shown in FIG. 2, the tangential direction of the magnetic lines of force 12 becomes the axis of easy magnetization, and The normal direction becomes the direction of the hard magnetization axis i
A 4-Malloy film can be formed on the nonmagnetic substrate 9.

第7図は上述のようにして・ぐ−マロイ、膜を形成した
時のB−H曲線を示し、(■)図は比較のために示す磁
石4がない場合のもので、非磁性基板9の移動方向及び
幅方向に対して、はぼ特性は変りがない(なお図は非磁
性基板9の移動方向をB軸に、幅方向をH軸に画いてお
り、以下の説明においても同様である)。しかし、パー
マロイ膜のFe−Niの組成比によっては磁化異方性が
異なり多少違ってくるが、垂直記録用磁気記録媒体の製
造では、パーマロイ膜の面内磁化具・方性を自由に制御
できる必要があり、磁石のない場合はそれができない。
FIG. 7 shows the B-H curve when the Gumalloy film was formed as described above, and the (■) diagram shows the case without the magnet 4 shown for comparison, and the nonmagnetic substrate 9. The curve characteristics remain unchanged in the moving direction and the width direction. be). However, the magnetization anisotropy differs depending on the Fe-Ni composition ratio of the permalloy film, and the in-plane magnetization and orientation of the permalloy film can be freely controlled in the production of magnetic recording media for perpendicular recording. It is necessary and cannot be done without a magnet.

(n)図は磁石4を設けた場合を示し、磁石4を設けた
ときは非磁性基板の中央部分では、(a)のようにその
移動方向が磁化容易方向となり、両端では(b)に示す
ように幅方向が磁化容易方向となる。すなわち、上述の
ように磁石4を用いるパーマロイ膜の蒸着では磁化異方
性を自由に制御で゛きる。
(n) Figure shows the case where a magnet 4 is provided. When the magnet 4 is provided, the moving direction is the easy magnetization direction in the center part of the non-magnetic substrate as shown in (a), and the direction in which magnetization is easy at both ends (b). As shown, the width direction is the direction of easy magnetization. That is, in the vapor deposition of the permalloy film using the magnet 4 as described above, the magnetization anisotropy can be freely controlled.

以上のようにしてパーマロイ膜を形成した非磁性基板に
、Co −Cr垂直磁化膜を形成して製造した記録媒体
を、第8図のように円形に打抜き円板状媒体13とする
と、その円周方向に対して磁化困難軸の異方性を有する
、記録再生特性が従来の2層膜媒体よりも更に優れた円
板状の垂直記録用磁気記録媒体が得られる。なお、(a
) 、 (b)図は第4図の(a) 、 (b)の磁石
等の配置に対応しており、(b)図のように打抜くこと
により3枚の円形媒体を得ることができる。
If a recording medium manufactured by forming a Co--Cr perpendicularly magnetized film on a non-magnetic substrate on which a permalloy film is formed as described above is punched out into a circular shape as shown in FIG. A disk-shaped magnetic recording medium for perpendicular recording, which has anisotropy of the hard axis of magnetization in the circumferential direction and has recording and reproducing characteristics superior to conventional two-layer film media, can be obtained. In addition, (a
) and (b) correspond to the arrangement of magnets, etc. in (a) and (b) of Figure 4, and three circular media can be obtained by punching as shown in (b). .

次に具体例を示す。A specific example is shown below.

第4図(、)の構成で、マスク孔6′の寸法を40wX
140mとし、磁石4として10mX10mX20xの
Sn −Co磁石を長手方向に磁化したものを、また、
ヨーク5には40wX140襲X10m  の軟鉄を用
いて形成した。なお、磁石4の極性は第5図のとおりと
した。その時、磁石4によって生ずる磁界の強さは、1
00〜3000e程度であった。このような磁界部分を
構成し、非磁性基板′9として厚さ30μmのポリイミ
ド系耐熱性高分子フィルムを使用して、連続真空蒸着法
により膜厚1000〜5000にのパーマロイ膜を蒸着
した。その結果、前述の第7図の(10のよりなり−H
曲線が得られた。
With the configuration shown in Figure 4 (,), the dimensions of the mask hole 6' are 40wX.
140 m, and the magnet 4 was a 10 m x 10 m x 20 x Sn-Co magnet magnetized in the longitudinal direction.
The yoke 5 was formed using soft iron of 40w x 140w x 10m. Note that the polarity of the magnet 4 was as shown in FIG. At that time, the strength of the magnetic field generated by the magnet 4 is 1
It was about 00-3000e. A permalloy film having a thickness of 1,000 to 5,000 µm was deposited by continuous vacuum evaporation using a polyimide heat-resistant polymer film having a thickness of 30 µm as the nonmagnetic substrate '9, constituting such a magnetic field part. As a result, the above-mentioned figure 7 (10 twists - H
A curve was obtained.

さらに上記パーマロイ膜上に、Co −Crを連続真空
蒸着を行ない、第8図(、)のように円形に打ち抜いて
円板状媒体13に形成し、記録再生特性を測定したとこ
ろ、パーマロイ膜の磁化容易方向、磁化困難方向を考慮
しなかったり、その方向を制御できなかった従来の媒体
に比較して、3 dBB10特性向上を示した。また、
媒体の円周方向におけるモジュレーションは、従来数十
−であったものが、一般的に要求される10%以下の値
を十分満足した。
Furthermore, Co - Cr was continuously vacuum-deposited on the permalloy film, and a disk-shaped medium 13 was punched out as shown in FIG. Compared to conventional media in which the easy magnetization direction and the difficult magnetization direction were not taken into account or the directions could not be controlled, the characteristics were improved by 3 dBB10. Also,
The modulation in the circumferential direction of the medium, which was conventionally several tens of degrees, satisfies the generally required value of 10% or less.

(発明の効果) 以上詳細に説明して明らかなように、本発明は、非磁性
系基板上に・ぐ−マロイ膜を介して、垂直磁化膜が形成
される2層膜媒体において、そのパーマロイ膜の面内磁
化異方性を強制的に基板の幅方向に変化させて、従来の
2層膜構造で得られる特性よりも一層優れた特性を得る
ことができる垂直磁気記録媒体の製法であるから、高密
度記録のディジタル記録などに用いて大いに益するとこ
ろがある。
(Effects of the Invention) As is clear from the detailed explanation above, the present invention provides a two-layer film medium in which a perpendicularly magnetized film is formed on a non-magnetic substrate via a permalloy film. This is a method for manufacturing perpendicular magnetic recording media that forcibly changes the in-plane magnetization anisotropy of the film in the width direction of the substrate, thereby obtaining properties that are even better than those obtained with a conventional two-layer film structure. Therefore, it can be of great benefit when used in high-density digital recording.

【図面の簡単な説明】[Brief explanation of the drawing]

第1図は2層膜構造の磁気記録媒体を説明する断面図、
第2図は磁気記録媒体の特性の1つであるモジュレーシ
ョンを説明する再生出力波形図、第3図は連続真空蒸着
装置の構成を示す側面図、第4図は本発明要部の磁石部
分の配置構成を示す平面図、第5図は前回における磁力
線を説明する平面図、第6図はマスク孔部分の磁力線を
説明する平面図、第7図はB−H,曲線図、第8図は円
板状媒体に形成する場合の打抜きを示す平面図である。 1・・・Co −Cr垂直磁化膜、2・・・基板、3・
・・パーマロイ膜、4・・・磁石、5・・・ヨーク、6
・・・マスク、6′・・・マスク孔1.7・・・るつぼ
、8・・・蒸発源、9・・・非磁性基板、10・・・キ
ャプスタン。 第1図 第4図 (a) (b) 第5図 第6図 第7図 第8図 (a)
FIG. 1 is a cross-sectional view illustrating a magnetic recording medium with a two-layer film structure.
Fig. 2 is a reproduction output waveform diagram explaining modulation, which is one of the characteristics of magnetic recording media, Fig. 3 is a side view showing the configuration of a continuous vacuum evaporation device, and Fig. 4 is a diagram of the magnet part, which is the main part of the present invention. A plan view showing the arrangement configuration, FIG. 5 is a plan view explaining the magnetic lines of force in the previous time, FIG. 6 is a plan view explaining the magnetic lines of force in the mask hole, FIG. 7 is a B-H, curve diagram, and FIG. FIG. 3 is a plan view showing punching when forming a disc-shaped medium. DESCRIPTION OF SYMBOLS 1... Co-Cr perpendicular magnetization film, 2... Substrate, 3...
...Permalloy film, 4...Magnet, 5...Yoke, 6
... Mask, 6'... Mask hole 1.7... Crucible, 8... Evaporation source, 9... Nonmagnetic substrate, 10... Capstan. Figure 1 Figure 4 (a) (b) Figure 5 Figure 6 Figure 7 Figure 8 (a)

Claims (2)

【特許請求の範囲】[Claims] (1)磁石、ヨーク及びマスクを配置した真空蒸着装置
によって磁界を印加しながら、非磁性基板上にパーマロ
イ膜を磁化容易軸方向が前記非磁性基板の幅方向になる
ように形成させ、さらにその表面に垂直異方性磁化膜を
蒸着して2層膜記録媒体を形成し、それを円板状に打抜
くことを特徴とする垂直記録用磁気記録媒体の製造方法
(1) While applying a magnetic field using a vacuum evaporation device equipped with a magnet, a yoke, and a mask, a permalloy film is formed on a non-magnetic substrate so that the axis of easy magnetization is in the width direction of the non-magnetic substrate; 1. A method for manufacturing a magnetic recording medium for perpendicular recording, which comprises forming a two-layer recording medium by depositing a perpendicularly anisotropic magnetized film on its surface, and punching it into a disk shape.
(2)打抜きされた円板状の記録媒体が記録再生時に磁
気ヘッドと相対的に移動する方向に、パーマロイ膜の磁
化困難軸が形成されるように、連続真空蒸着装置に設け
る磁石及びマスクを配置することを特徴とする、特許請
求の範囲第(1)項記載の垂直記録用磁気記録媒体の製
造方法。
(2) A magnet and a mask are installed in the continuous vacuum deposition apparatus so that the axis of difficult magnetization of the permalloy film is formed in the direction in which the punched disk-shaped recording medium moves relative to the magnetic head during recording and reproduction. A method of manufacturing a magnetic recording medium for perpendicular recording according to claim (1), characterized in that a magnetic recording medium for perpendicular recording is arranged.
JP22298084A 1984-10-25 1984-10-25 Production of vertical recording magnetic medium Pending JPS61104431A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP22298084A JPS61104431A (en) 1984-10-25 1984-10-25 Production of vertical recording magnetic medium

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP22298084A JPS61104431A (en) 1984-10-25 1984-10-25 Production of vertical recording magnetic medium

Publications (1)

Publication Number Publication Date
JPS61104431A true JPS61104431A (en) 1986-05-22

Family

ID=16790906

Family Applications (1)

Application Number Title Priority Date Filing Date
JP22298084A Pending JPS61104431A (en) 1984-10-25 1984-10-25 Production of vertical recording magnetic medium

Country Status (1)

Country Link
JP (1) JPS61104431A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH05114133A (en) * 1991-10-21 1993-05-07 Fujitsu Ltd Method and apparatus for production of magnetic disk

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH05114133A (en) * 1991-10-21 1993-05-07 Fujitsu Ltd Method and apparatus for production of magnetic disk

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